Дисертації з теми "Surface strain measurement"

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1

Friedlander, Jeffrey B. "Wireless Strain Measurement with Surface Acoustic Wave Sensors." The Ohio State University, 2011. http://rave.ohiolink.edu/etdc/view?acc_num=osu1306874020.

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2

Groves, Roger M. "Development of shearography for surface strain measurement of non-planar objects." Thesis, Cranfield University, 2001. http://hdl.handle.net/1826/4053.

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Анотація:
The subject of this thesis is the development of optical instrumentation for surface strain measurement of non-planar objects. The speckle interferometry technique of shearography is used to perform quantitative measurements of surface strain on nonplanar objects and to compensate these measurements for the errors that are due to the shape and slope of the object. Shearography is an optical technique that is usually used for defect location and for qualitative strain characterisation. In this thesis a multi-component shearography system is described that can measure the six components of displacement gradient. From these measurements the surface strain can be fully characterised. For non-planar objects an error is introduced into the displacement gradient measurement due to the variation of the sensitivity vector across the field of view and the variation in the magnitude of applied shear due to the curvature of the object surface. To correct for these errors requires a knowledge of the slope and shape of the object. Shearography may also be used to measure object slope and shape by a source displacement technique. Therefore slope, shape and surface strain may be measured using the same optical system. The thesis describes a method of multiplexing the shear direction using polarisation switching, a method of measuring the source position using shadow Moire and the shearography source displacement technique for measuring the surface slope and shape of objects. The multi-component shearography system is used to perform measurements of the six components of surface strain, on an industrial component, with a correction applied for errors due to the shape and slope of the object.
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3

Drew, Richard John. "An investigation into sub-surface strain measurement using X-ray radioscopy." Thesis, Loughborough University, 1999. https://dspace.lboro.ac.uk/2134/33075.

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Анотація:
There are numerous techniques used to measure strain. Most are only capable of taking surface measurements. The penetrating nature of X-rays has been used to measure deformation, and thus strain, but only with radiographic images. Radioscopic techniques are faster and do not require film processing, but produce less detailed results than digitised radiographic images. The research covered by this thesis tested radioscopic images and showed them to be suitable for strain measurement. The thesis includes details of the design and capabilities of the radioscopic equipment. Pin cushion distortion is a common feature of radioscopic images, and an automatic method of identifying, and correcting for the distortion was implemented.
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4

Francis, Daniel. "Surface strain measurement using pulsed laser shearography with fibre-optic imaging bundles." Thesis, Cranfield University, 2008. http://hdl.handle.net/1826/2999.

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Анотація:
This thesis describes the development of a shearography instrument for the quantitative measurement of surface strain on dynamic test objects. Shearography is a non-contact, full-field interferometric speckle technique used for the measurement of displacement gradient. It is often used in industry for qualitative inspection of industrial components. To fully characterize the surface strain, a total of six components of displacement gradient are required. These can be measured using shearography instrumentation with at least three measurement channels. Phase measurements from each measurement channel are combined using a matrix transformation to produce the orthogonal displacement gradient measurements. The instrument presented in this thesis possesses four measurement channels consisting of four views of the object under investigation. Images from the four views are transported to the shearing interferometer using coherent fibre-optic imaging bundles. The signals from the four views are then spatially multiplexed onto the four quadrants of a CCD camera. The optical source is a frequency doubled, pulsed Nd:YAG laser which is used to effectively ‘freeze’ the motion of the dynamic object for the duration of the laser pulse. The optical phase difference between images recorded from two laser pulses is determined using the spatial carrier technique. This method involves introducing a carrier frequency into the recorded speckle pattern using a Mach-Zehnder interferometer. A Fourier transform is used to access the phase dependent spectral features, from which the phase distribution is calculated. The instrument is first validated through the measurement of two static test objects. The results of these measurements are compared with modelled data and with results from a multiple-illumination-direction shearography system using a continuous-wave laser. The instrument is then used to investigate two dynamic objects; a plate rotating at 610 rpm and a speaker cone vibrating at frequencies in the range of 1 – 5 kHz.
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5

Tuncay, Orbay. "Wireless Strain Gauge System in a Multipath Environment." The Ohio State University, 2008. http://rave.ohiolink.edu/etdc/view?acc_num=osu1222089977.

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6

vechalapu, uday bhaskar. "Real-Time 2D Digital Image Correlation to Measure Surface Deformation on Graphics Processing Unit using CUDA C." University of Akron / OhioLINK, 2018. http://rave.ohiolink.edu/etdc/view?acc_num=akron1522108261138081.

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7

Nguyen, Tran. "Optical measurement of shape and deformation fields on challenging surfaces." Thesis, Loughborough University, 2012. https://dspace.lboro.ac.uk/2134/10551.

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Анотація:
A multiple-sensor optical shape measurement system (SMS) based on the principle of white-light fringe projection has been developed and commercialised by Loughborough University and Phase Vision Ltd for over 10 years. The use of the temporal phase unwrapping technique allows precise and dense shape measurements of complex surfaces; and the photogrammetry-based calibration technique offers the ability to calibrate multiple sensors simultaneously in order to achieve 360° measurement coverage. Nevertheless, to enhance the applicability of the SMS in industrial environments, further developments are needed (i) to improve the calibration speed for quicker deployment, (ii) to broaden the application range from shape measurement to deformation field measurement, and (iii) to tackle practically-challenging surfaces of which specular components may disrupt the acquired data and result in spurious measurements. The calibration process typically requires manual positioning of an artefact (i.e., reference object) at many locations within the view of the sensors. This is not only timeconsuming but also complicated for an operator with average knowledge of metrology. This thesis introduces an automated artefact positioning system which enables automatic and optimised distribution of the artefacts, automatic prediction of their whereabouts to increase the artefact detection speed and robustness, and thereby greater overall calibration performance. This thesis also describes a novel technique that integrates the digital image correlation (DIC) technique into the present fringe projection SMS for the purpose of simultaneous shape and deformation field measurement. This combined technique offers three key advantages: (a) the ability to deal with geometrical discontinuities which are commonly present on mechanical surfaces and currently challenging to most deformation measurement methods, (b) the ability to measure 3D displacement fields with a basic single-camera single-projector SMS with no additional hardware components, and (c) the simple implementation on a multiple-sensor hardware platform to achieve complete coverage of large-scale and complex samples, with the resulting displacement fields automatically lying in a single global coordinate system. A displacement measurement accuracy of ≃ 1/12,000 of the measurement volume, which is comparable to that of an industry-standard DIC system, has been achieved. The applications of this novel technique to several structural tests of aircraft wing panels on-site at the research centre of Airbus UK in Filton are also presented. Mechanical components with shiny surface finish and complex geometry may introduce another challenge to present fringe projection techniques. In certain circumstances, multiple reflections of the projected fringes on an object surface may cause ambiguity in the phase estimation process and result in incorrect coordinate measurements. This thesis presents a new technique which adopts a Fourier domain ranging (FDR) method to correctly identifying multiple phase signals and enables unambiguous triangulation for a measured coordinate. Experiments of the new FDR technique on various types of surfaces have shown promising results as compared to the traditional phase unwrapping techniques.
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8

Junge, Michael Dominic Alexander. "Measurement of applied stresses using the polarization of Rayleigh surface waves." Thesis, Available online, Georgia Institute of Technology, 2004:, 2003. http://etd.gatech.edu/theses/available/etd-04062004-164653/unrestricted/junge%5Fmichael%5Fd%5Fa%5F200312%5Fms.pdf.

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Анотація:
Thesis (M.S. in E.S.M.)--School of Civil and Environmental Engineering, Georgia Institute of Technology, 2004. Directed by Laurence Jacobs and Jianmin Qu.
Includes bibliographical references (leaves 113-117).
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9

Pereira, Pedro André Marques. "Measuring the strain of metallic surfaces in real time through vision systems." Master's thesis, Universidade de Aveiro, 2015. http://hdl.handle.net/10773/16447.

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Анотація:
Mestrado em Engenharia Mecânica
Vision systems have already proven to be a useful tool in various elds. The ease of their implementation, allied to their low cost mean that their growth potential is immense. In this dissertation it is proposed a approach to measure strains in metallic surfaces, using stereo vision. This approach is based on the 3D DIC. This method measures the strain of the surface by dividing this surface in small sections, called subsets, and iteratively nding the equation that describes its shape variation through time. However, calculating the transformation of this subset is very timeconsuming. The proposed approach tries to optimize this calculation by rst determine the displacement eld, and then the strain eld by derivation. The dissertation also presents some experimental data and practical considerations relatively to the camera setup and image equalization algorithms in order to obtain better disparity maps. The results were veri ed experimentally and compared with the results obtained from other softwares.
Os sistemas de vis~ao j a provaram ser uma ferramenta util em v arios campos. A facilidade da sua implementa c~ao, aliada ao seu baixo custo signi cam que o seu potencial de crescimento e enorme. Nesta disserta c~ao e proposta uma abordagem para medir deforma c~oes em superf cies met alicas usando vis~ao stereo. Esta abordagem e baseada na t ecnica 3D DIC. Este m etodo mede as deforma c~oes da superf cie dividindo-a em pequenas se c~oes, designadas por sub- sets, tentando iterativamente encontrar a equa c~ao que de ne as varia c~oes das suas formas ao longo do tempo. No entanto, o c alculo das transforma c~oes destes subsets e demorado. A abordagem proposta pretende pretende otimizar este c alculo determinando primeiro o campo de deslocamentos e depois o campo das deforma c~oes atrav es da deriva c~ao. A disserta c~ao apresenta tamb em dados experimentais e considera c~oes pr aticas relativamente a con gura c~ao (setup) das c^amaras e algoritmos de equaliza c~ao de imagens de forma a se obterem melhores mapas de disparidade. Os resultados foram veri cados experimentalmente e comparados com os resultados obtidos por outros softwares.
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10

Cuthbert, Douglas Lee. "Experimental determination of the surface displacement of a small flexural disk sonar transducer from surface strain measurements." Thesis, Monterey, Calif. : Springfield, Va. : Naval Postgraduate School ; Available from National Technical Information Service, 1993. http://handle.dtic.mil/100.2/ADA271165.

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Анотація:
Thesis (M.S. in Engineering Acoustics and M.S. in Systems Technology (Antisubmarine Warfare)) Naval Postgraduate School, June 1993.
Thesis advisor(s): Steven R. Baker. "June 1993." Includes bibliographical references. Also available online.
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11

Benia, Hadj Mohamed. "Spatially resolved optical measurements on supported metal particles and oxide surfaces with the STM." Doctoral thesis, Humboldt-Universität zu Berlin, Mathematisch-Naturwissenschaftliche Fakultät I, 2008. http://dx.doi.org/10.18452/15862.

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Анотація:
In der vorliegenden Arbeit wurde mit Hilfe eines Photon-STM die Korrelation zwischen optischen Eigenschaften und der lokalen Morphologie an zwei unterschiedlichen Systemen untersucht. Hierfür wurden zum einem oxidgetragene Ensemble von Silber-Partikeln präpariert, wobei sowohl die Partikelform (Kuppel- und Scheibenform) als auch die deponierte Partikeldichte variiert werden konnte. Neben der Präparation solcher Partikel auf Al10O13/NiAl, konnten sphärische Silber-Kolloide geordnet, als auch ungeordnet auf HOPG aufgebracht und untersucht werden. Dabei zeigte sich, dass das Verhältnis von Höhen zu Breiten nicht nur einen signifikanten Einfluss auf die Mie-Resonanz des einzelnen Partikels hat, sondern auch die elektromagnetische Kopplung der Partikel in einem Ensemble stark kontrolliert. Die energetische Lage der Mie-Resonanz zeigt im Fall der kuppelförmigen Ag-Partikel eine starke Abhängigkeit vom Intepartikel-Abstand, was sich in einer Verschiebung zu höheren Energien für eine steigende Partikeldichte äußert. Eine solche Abhängigkeit konnte bei den Ensembles der scheibenförmigen Partikel nicht beobachtet werden. Des weiteren zeigte sich, dass, verglichen mit den ungeordneten Ensembles, die selbstorganisierte langreichweitige Ordnung der Silber-Kolloide auf HOPG nur einen schwachen Einfluss auf die energetische Position der Mie Resonanz hat.Das zweite hier untersuchte System sind dünne MgO Filme unterschiedlicher Dicken auf einem Mo(001) Substrat. Diese zeigen ein reichhaltiges Wachstumsverhalten, welches durch eine Differenz in den Gitterkonstanten von 5.3% begründet ist und erst ab etwa 25 ML zu einem flachen und defektarmen Film führt. Die so induzierte Spannung relaxiert bis zu einer Dicke von etwa 7 ML in einer periodischen Überstruktur die aus abwechselnd flachen und verkippten Ebenen an der MgO-Mo Grenzschicht hervorgeht. Für MgO Filme mit einer Dicke von etwa 12 ML werden dann Schraubenversetzungen, ausgedehnte verkippte Ebenen und Stufenkanten mit einer Orientierung entlang der Richtung beobachtet. Die optische Charakterisierung durch Feldemission von Elektronen aus der STM-Spitze in den MgO-Film wird dominiert von zwei Emissionsmaxima bei Energien von 3.1 eV und 4.4 eV. Die kontrollierte Nukleation von Gold Partikeln und die Erzeugung von Farbzentren im MgO Film erlaubten eine Zuordnung dieser Emissionen zu strahlenden Zerfällen von Exitonen an Ecken, Kinken bzw. Stufen des Magnesiumoxids. Solche Emissionsprozesse konnten allerdings nur unter Einstellungen beobachtet werden, bei denen ein gleichzeitiges Rastern der Oberfläche unmöglich ist. Bei moderaten Einstellungen war auch eine ortsaufgelösten Spektroskopie möglich, wobei dann neue Emissionsmechanismen beobachtet wurden. Dabei sind zwei Prozesse wesentlich; zum einen die Ausbildung von sog. Spitzen-induzierten Plasmonen im Bereich zwischen Spitze und dem Mo-Substrat, zum anderen strahlende Elektronenübergänge zwischen sog. Feldemissionsresonanzen, die sich im Spitze/MgO-Film System ausbilden.
In this thesis, the correlation between the optical properties and the local morphology of supported silver nanoparticle ensembles and MgO thin films deposited on Mo(001) systems is explored by means of Photon-STM. In the first section, dome and disk shaped Ag nanoparticle ensembles with increasing density on an alumina film on NiAl(110) were analyzed as well as ordered and disordered ensembles of Ag nanocolloids on HOPG. The aspect ratio of the Ag nanoparticles was found to have a significant influence not only on the Mie plasmon resonance of a single particle, but also on the electromagnetic coupling within the nanoparticle ensembles. The Mie resonance in the ensemble of dome shaped Ag nanoparticles shows a strong dependence on the interparticle distance, where it shifts to higher energies with increasing particle density, due to destructive interference effects. In the disk-like Ag ensembles, however, the plasmon energy is independent of particle-particle separation. The long-range lateral ordering of size-selected Ag nanocolloids is found to induce a high dipole-dipole coupling within the ensemble. This is mainly reflected by the enhancement of the spectral intensity of the in-plane Mie mode, due to constructive coupling. However, ensembles with either well-ordered or disordered arrangements reveal no important difference in their optical properties, reflecting the weak influence of the long-range order in the particle ensemble. Thin MgO films with different thicknesses were grown on a Mo(001) surface. The stress resulting from the 5.3% lattice mismatch between the MgO(001) and the Mo(001) lattice parameters is found to control the surface morphology of the MgO film until thicknesses of around 25ML at which flat and defect-poor films are obtained. The relaxation of the stress induces a periodic network in the first 7ML of the MgO film, consisting of alternated flat and tilted mosaics. The presence of screw dislocations, steps oriented along the MgO directions, and tilted planes is observed when the MgO films are approximately 12ML thick. In addition, an increase of the MgO work function around these new surface features is revealed from STM spectroscopy. The photon emission induced by field-emitted electron injection from the STM tip into the MgO films is dominated by two emission bands located at 3.1eV and 4.4eV. To check the origin of these bands, further experiments, namely, nucleation of Au particles and creation of F-centers on the MgO surface, have been performed. The nucleation of Au particles at the low coordinated sites is found to quench the MgO optical signal, while the creation or annihilation of F-centers does not alter the MgO emission bands. The 3.1eV and the 4.4eV bands are therefore assigned to the radiative decay of MgO excitons at corner and kink sites, and step sites, respectively. Besides, spatially resolved optical measurements in the tunneling mode of the STM revealed different light emission mechanisms. These radiative processes are mainly related to tip-induced plasmons that form between the tip and the Mo support and to electron transitions between field-emission-resonance states in the STM tip-MgO film junction. The signal from exciton decays at corners and kinks of the MgO surface is however only observed at excitation conditions where the spatial resolution is already strongly reduced.
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12

Tsai, Yuan-Chuan, and 蔡源泉. "Surface Strain Measurement and Analysis ofthe ThoracoLumbar Vertebrae Body." Thesis, 2004. http://ndltd.ncl.edu.tw/handle/41339797123050683784.

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Анотація:
碩士
國立臺灣大學
醫學工程學研究所
92
Abstract Background Study. The mechanisms of vertebral injuries depend on the external loading condition. It is hence important to find the relationship of bony strain of vertebral body with respect to the corresponding external loading condition. Objectives. To investigate the micro mechanical response of thoracolumbar vertebral body during the eccentric impact and creep loading. Methods. Ten thoracolumbar porcine two-motion segment specimens were subjected to 1.2 J compressive eccentric impact loading and 14 specimens were tested at cyclic loading at 5 Hz for 5 hours. Surface strain of vertebral body was measured with three-axis strain gauges rosette attached to the base of the pedicles and anterior wall of vertebral body. Results. Three major phenomena were observed in the current study: First, compressive strain was measured when the impact force was applied on the top of anterior vertebral bodies. Second, the strain of vertebral body was minimal when the impact force was applied on the center of motion segments. Third, the tensile strain occurred and directed towards spinal cannel when the impact force applied on top of posterior process. The first phenomenon may explain the mechanism of compressive fracture, while the third may explain the burst fracture.
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13

Han, Yougun. "Development of Methodologies for Strain Measurement and Surface Energy Characterization." Thesis, 2011. http://hdl.handle.net/10012/6097.

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Development of new scientific disciplines such as bioengineering and micro-nano engineering adopting nonconventional materials requests innovative methodologies that can accurately measure the mechanical properties of soft biological materials and characterize surface energy and adhesion properties of them, independent of measurement conditions. One of emerging methods to measure the deformation of materials under stress is digital image correlation (DIC) technique. As a noncontact strain measurement method, DIC has the advantages of prevention of experimental errors caused by the use of contact type sensors and of flexibility in its application to soft materials that are hard to be tested by conventional method. In the first part of the thesis, 2 dimensional and 3 dimensional DIC codes were developed and optimized, and then applied to two critical applications: 1) determining the stress-strain behaviour of polydimethylsiloxane (PDMS) sample, as a model soft material, using the optical images across large deformation region, and 2) detecting the stiffness variation within the gel mimicking the breast tumour using ultrasound images. The results of this study showed the capability of DIC as a strain sensor and suggested its potential as a diagnosing tool for the malignant lesion causing local stiffness variation. In the characterization of surface energy and adhesion properties of materials, two most common methods are contact angle measurement and JKR-type indentation test. In the second part of the thesis, the experimental set-up for these methods were developed and verified by using the PDMS in static (quasi equilibrium) state. From the dynamic tests, it showed its possible usage in studying adhesion hysteresis with respect to speed. The adhesion hysteresis was observed at high speed condition in both contact angle measurement and JKR-type indentation tests.
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14

Wildy, Stuart James. "Scanning laser doppler vibrometry for strain measurement and damage detection." Thesis, 2012. http://hdl.handle.net/2440/93519.

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Анотація:
Numerous strain measurement and damage detection techniques have been developed over the last century. These techniques include strain gauges, digital image correlation, radiography and ultrasonic inspections. All have various advantages, as well as disadvantages, which make each suited to specific applications. With the development of laser Doppler vibrometry, a number of techniques have been established for non-destructive evaluation, such as the measurement of bending strain, as well as damage detection using kinematic parameters, including displacement and curvature. With recent advancements in laser Doppler vibrometry technology (such as 3D scanning laser Doppler vibrometry for three-dimensional displacement measurements, improved velocity decoders and increased spatial resolution) the door has been opened to develop techniques for measuring surface strain from in-plane displacements, as well as the development of new damage detection techniques based on the fundamental principle of deformation:- the governing differential equation of displacement. The extensive literature review contained in this thesis identified a number of gaps in the field, including the evaluation of the accuracy of quasi-static bending strain measurements using current 1D SLDV technology, the precision of full-field surface strain measurement techniques utilising 3D SLDV, and new detection techniques based on the violation of the governing differential equations of displacement. Thus, the research contained in this thesis focussed on these areas. The first part of this thesis presents an investigation into the use of 1D and 3D scanning laser Doppler vibrometry for non-contact measurement of quasi-static bending strain in beams and surface strain in plates, respectively. The second part presents a new damage detection technique based on the governing differential equations of displacement in beam and plate structures. Two algorithms are developed to determine a violation in the governing differential equations created by either a delamination in a composite beam with out-of-plane displacements, or by a crack in a plate with in-plane displacements.
Thesis (Ph.D.) -- University of Adelaide, School of Mechanical Engineering, 2012
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15

Kazemi-Moridani, Amir. "Thermal Radiation Measurement and Development of Tunable Plasmonic Thermal Emitter Using Strain-induced Buckling in Metallic Layers." 2018. https://scholarworks.umass.edu/masters_theses_2/719.

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Анотація:
An infrared radiometry setup has been developed based on a commercially available FTIR spectrometer for measuring mid-infrared thermal radiation. The setup was calibrated with a lab-built blackbody source. The setup was tested with a grating structure with 4-micron periodicity. Periodic microstructures using nickel and gold are fabricated on elastomeric substrates by use of strain-induced buckling of the nickel layer. The intrinsically low emissivity of gold in the mid-infrared regime is selectively enhanced by the surface plasmonic resonance at three different mid-infrared wavelengths, 4.5 µm, 6.3 µm, and 9.4 µm. As the thermal emission enhancement effect exists only for the polarization perpendicular to the orientation of the microstructures, substantially polarized thermal emission with an extinction ratio of close to 3 is demonstrated. Moreover, the elastically deformed plasmonic thermal emitters demonstrate strain-dependent emission peaks, which can be applied for future mechano-thermal sensing and dynamic thermal signature modulation.
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16

Huang, Chao-Chin, and 黃朝琴. "Evaluation of Interlaminar Shear Stress by Strain Measurements on Laminate Surface." Thesis, 1996. http://ndltd.ncl.edu.tw/handle/14344647530685208774.

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Анотація:
碩士
大葉工學院
機械工程研究所
84
The interlaminar shear stresses of composite laminate have been the keys to the delamination of laminated structures. In most cases, because of the uncertainty in the loading on a structure, it is not possible to predict precisely the stresses during design stage. Therefore, monitoring the structural responses during service becomes crucial for structure with concerns, e.g. the composite panels on an airplane, etc.. However, the strain on a preformed structure can only be measured on surfaces by strain gages or other experimental techniques. In this study, the strains on surfaces of the laminate, along with the classical lamination theory and the higher order shear deformation theory, were used to predict the interlaminar shear stresses in the laminate. Several numerical examples using the simulated surface strains were employed to assess the accuracy of proposed models. It is found that the model using higher order shear deformation theory has improved accuracy for the analysis of thick symmetric laminate(S>4) over the model using the classical lamination theory. However, the simplicity and good accuracy of the model using classical lamination theory for thin laminates(S>20)still makes it an attractive technique.
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17

An, JinWoo. "Estimation of beam prestress by deflection and strain measurements." Thesis, 2012. http://hdl.handle.net/2152/ETD-UT-2012-08-6267.

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Анотація:
Laboratory test of reinforced and prestressed concrete structures have been used widely to explore the behavior of reinforced and prestressed concrete components and structures; Such tests are often time-consuming and costly. However, numerical models have been shown to compare favorably with experiments. Thus, computations are viewed nowadays as efficient alternatives to tests, time-wise and cost-wise. In the research reported in this thesis, finite-element model were used in a study of pretressed structural components in order to correlate levels of pretension with deflection and strain measurements. The two main objectives were to develop a suitable finite element model of prestressed concrete beams and to forecast beam prestension on the basis of deformations resulting from specified simple load, e.g., a uniformly distributed transverse load. A commercial finite-element analysis package (ANSYS 12) was used to set up, use and evaluate the computational model. Furthermore, a finite-difference model was employed in order to ascertain the validity of ANSYS results by comparison with engineering beam theory taking into account the applied pretension. This study demonstrates the potential usefulness of deflection and strain measurements as indicators of the pretension applied or remaining in prestressed concrete beams.
text
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18

"Stress and Structure Evolution during Cu/Au(111) -(22 X√3) Heteroepitaxy: An In-Situ Study with UHV-STM." Doctoral diss., 2012. http://hdl.handle.net/2286/R.I.14505.

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Анотація:
abstract: This research focuses on the stress and structure evolution observed in-situ during the earliest stages of thin film growth in Cu on Au(111)-reconstruction. For the research, an ultra high vacuum-scanning tunneling microscopy (UHV-STM) system was modified to have the additional capabilities of in-situ deposition and in-situ stress evolution monitoring. The design and fabrication processes for the modifications are explained in detail. The deposition source enabled imaging during the deposition of Cu thin films, while also being columnar enough to avoid negatively impacting the function of the microscope. It was found that the stress-induced changes in piezo voltage occurred over a substantially longer time scale and larger piezo scale than used during imaging, allowing for the deconvolution of the two sources of piezo voltage change. The intrinsic stress evolution observed at the onset of Cu growth was tensile in character and reached a maximum of 0.19 N/m at approximately 0.8ML, with an average tensile slope of 1.0GPa. As the film thickness increased beyond 0.8 ML, the stress became less tensile as the observation of disordered stripe and trigon patterns of misfit dislocations began to appear. The transport of atoms from the surface of enlarged Cu islands into the strained layer played an important role in this stage, because they effectively reduce the activation barrier for the formation of the observed surface structures. A rich array of structures were observed in the work presented here including stripe, disordered stripe and trigon patterns co-existing in a single Cu layer. Heteroepitaxial systems in existing literature showed a uniform structure in the single layer. The non-uniform structures in the single layer of this work may be attributed to the room temperature Cu growth, which can kinetically limit uniform pattern formation. The development of the UHV-STM system with additional capabilities for this work is expected to contribute to research for the stress and structure relationships of many other heteroepitaxial systems.
Dissertation/Thesis
Ph.D. Materials Science and Engineering 2012
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Lübbe, Jannis Ralph Ulrich. "Cantilever properties and noise figures in high-resolution non-contact atomic force microscopy." Doctoral thesis, 2013. https://repositorium.ub.uni-osnabrueck.de/handle/urn:nbn:de:gbv:700-2013040310741.

Повний текст джерела
Анотація:
Different methods for the determination of cantilever properties in non-contact atomic force microscopy (NC-AFM) are under investigation. A key aspect is the determination of the cantilever stiffness being essential for a quantitative NC-AFM data analysis including the extraction of the tip-surface interaction force and potential. Furthermore, a systematic analysis of the displacement noise in the cantilever oscillation detection is performed with a special focus on the thermally excited cantilever oscillation. The propagation from displacement noise to frequency shift noise is studied under consideration of the frequency response of the PLL demodulator. The effective Q-factor of cantilevers depends on the internal damping of the cantilever as well as external influences like the ambient pressure and the quality of the cantilever fixation. While the Q-factor has a strong dependence on the ambient pressure between vacuum and ambient pressure yielding a decrease by several orders of magnitude, the pressure dependence of the resonance frequency is smaller than 1% for the same pressure range. On the other hand, the resonance frequency highly depends on the mass of the tip at the end of the cantilever making its reliable prediction from known cantilever dimensions difficult. The cantilever stiffness is determined with a high-precision static measurement method and compared to dimensional and dynamic methods. Dimensional methods suffer from the uncertainty of the measured cantilever dimensions and require a precise knowledge its material properties. A dynamic method utilising the measurement of the thermally excited cantilever displacement noise to obtain cantilever properties allows to characterise unknown cantilevers but requires an elaborative measurement equipment for spectral displacement noise analysis. Having the noise propagation in the NC-AFM system fully characterised, a proposed method allows for spring constant determination from the frequency shift noise at the output of the PLL demodulator with equipment already being available in most NC-AFM setups.
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