Добірка наукової літератури з теми "Hydro-thermal Synthesis"

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Статті в журналах з теми "Hydro-thermal Synthesis"

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Das, Birinchi K. "Solvo(hydro)thermal synthesis of metal-carbonyl tellurido clusters." Proceedings / Indian Academy of Sciences 108, no. 3 (June 1996): 323. http://dx.doi.org/10.1007/bf02870090.

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Yang, Xianfeng, Hiromi Konishi, Huifang Xu, and Mingmei Wu. "Comparative Sol–Hydro(Solvo)thermal Synthesis of TiO2 Nanocrystals." European Journal of Inorganic Chemistry 2006, no. 11 (June 2006): 2229–35. http://dx.doi.org/10.1002/ejic.200500855.

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Zhao, Wei, Zhengping Hao, and Chun Hu. "Synthesis of MCM-48 with a high thermal and hydro-thermal stability." Materials Research Bulletin 40, no. 10 (October 2005): 1775–80. http://dx.doi.org/10.1016/j.materresbull.2005.05.012.

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Zhang, Wenchao, Bin Jiang, Xiaohang Ma, Jiaxin Wang, Jiaqi Liu, Runhui Wu, Zilong Zheng, Jingping Liu, and Kefeng Ma. "Controllable synthesis of multi-shelled NiCo2O4 hollow spheres catalytically for the thermal decomposition of ammonium perchlorate." RSC Advances 9, no. 41 (2019): 23888–93. http://dx.doi.org/10.1039/c9ra03865e.

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LI, Yan, and Chuan-sheng LIU. "Hydro/solvo-thermal synthesis of ZnO crystallite with particular morphology." Transactions of Nonferrous Metals Society of China 19, no. 2 (April 2009): 399–403. http://dx.doi.org/10.1016/s1003-6326(08)60285-x.

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Wu, Jing-Yun, Sheng-Ming Huang, and Ming-Hsi Chiang. "Hydro(solvo)thermal synthesis of homochiral metal–camphorate coordination polymers." CrystEngComm 12, no. 11 (2010): 3909. http://dx.doi.org/10.1039/c000872a.

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Sano, Saburo, Takeshi Fukuda, and Yasuo Shibasaki. "Development of Platy Alumina and its Application." Advances in Science and Technology 45 (October 2006): 2204–11. http://dx.doi.org/10.4028/www.scientific.net/ast.45.2204.

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It has been required to change the industrial production processes to low waste emission ones from a view point of environmental issue. In the production of aluminum building materials, large amount of sludge is emitted as industrial waste. If we can change the waste to valuable products, we can respond to the request. Synthesis technology of kaolinitic particles from various starting raw materials had been established at National Industrial Research Institute of Nagoya (NIRIN, present: AIST Chubu). Hydro-thermal treatment is applied to the technology and obtained particles show various shapes such as plate, shell and so on. Collaborative research work between NIRIN and YKK corporation to develop high performance alumina powder form aluminum sludge, a by-product from surface treatment process in the manufacturing of aluminum building materials, had been done by using the fruits from the research project on kaolinite synthesis at NIRIN. As the result, high performance platy alumina powder was developed by using hydro-thermal synthesis technology.
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Moon, S. M., Chongmu Lee, and N. H. Cho. "Structural features of nanoscale BaTiO3 powders prepared by hydro-thermal synthesis." Journal of Electroceramics 17, no. 2-4 (December 2006): 841–45. http://dx.doi.org/10.1007/s10832-006-0458-0.

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QASIM, A. K., L. A. JAMIL, and A. F. ABDULRAHMAN. "SYNTHESIS OF RUTILE-TiO2 NANOROD ARRAYS FOR EFFICIENT SOLAR WATER SPLITTING VIA MICROWAVE-ASSISTED HYDROTHERMAL METHOD." Digest Journal of Nanomaterials and Biostructures 15, no. 1 (January 2020): 157–65. http://dx.doi.org/10.15251/djnb.2020.151.157.

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Using a microwave-assisted hydro thermal method (MWAHM) a single crystalline of vertically aligned TiO2 nanorod (NR) arrays has been achieved via the novel ultra-rapid synthetic method for the production. High-quality NR arrays with controlled film thickness were achieved with fine control of the growth conditions as well. The effect of the different reaction conditions of MWAHM such as reaction time and growth temperature on the morphology, crystal orientation, and photo catalytic activity have been systematically investigated. In a typical condition of the MWAHM using 0.4 cm3 of titanium(IV) n-butoxide (TBO) at 180 °C for 40 minutes, a small diameter of 124 nm and short length 2.93 µm of TiO2 nanorods, are grown on fluorine-doped tin oxide (FTO) substrate. However, the photo current density produced TiO2 NRs of 2.90 mA cm-2 with a maximum photo conversion efficiency of about 2.7% which confers excellent photoelectrochemical performance. In comparison with the typical hydro thermal method (HM) synthesized NRs, the ultra-fast MWAHM synthesized NRs offers five times more efficiency photoelectrochemical (PEC) water splitting than the hydro thermal method (HM). The results suggest that these dense and aligned one-dimensional TiO2 nanorods are promising for hydrogen generation from water splitting based on PEC cells.
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Gheorghievici, Gavril Lucian, Corneliu Trisca Rusu, Elena Voicila, Ion Marius Nafliu, Anca Maria Cimbru, and Szidonia Katalin Tanczos. "Titanium Dioxide for Biomedical Uses I. The controlled production of nanoparticles by hidrothermal synthesis moderated by dimedone." Revista de Chimie 68, no. 1 (February 15, 2017): 11–15. http://dx.doi.org/10.37358/rc.17.1.5378.

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The controlled the solvo-hydro-thermal titanium dioxide synthesis moderated by dimedone from organometallic precursors is approached in order to obtain nanoparticles compatible with the polymeric systems used in the dental technique. The experiments carried out with relation to the production of titanium dioxide nanoparticles using the solvo-hydro-thermal synthesis allowed the production of three types of materials by means of varying the nature of the used solvent: methanol, ethanol and propanol (TiO2-M, TiO2-E and TiO2-P).The characterisation using electron microscopy (SEM and HRTEM), X-ray analysis, FTIR and UV-Vis spectrometry show that the diameter of the produced nanoparticles is less than 15 nm and decreases in the order: dpMethanol ] dpEthanol ] dpPropanol. The nanoparticles contain trace organic substances which the smaller they are, the bigger the alcohol chain used as a solvent is. The adsorption of a target dye showed increasing values with the increasing number of atoms in the hydrocarbon alcohol chain. The highlighted characteristics suggest the possibility of using the synthesised nanoparticles in the production of hard implants for dental reconstruction.
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Дисертації з теми "Hydro-thermal Synthesis"

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Campos, Viviane de Oliveira. "S?ntese e caracteriza??o de redes metalorg?nicas baseadas em zinco e ?cidos benzenodicarbox?licos." Universidade Federal do Rio Grande do Norte, 2014. http://repositorio.ufrn.br:8080/jspui/handle/123456789/17771.

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Анотація:
Made available in DSpace on 2014-12-17T15:42:25Z (GMT). No. of bitstreams: 1 VivianeOC_DISSERT.pdf: 3402531 bytes, checksum: e2e7a469bf001a9ef16d573773ea7bda (MD5) Previous issue date: 2014-01-24
Conselho Nacional de Desenvolvimento Cient?fico e Tecnol?gico
Metal Organic Frameworks (MOFs) are supramolecular structures consisted of ions or metal clusters coordinated to organic ligands which are repeated in two or three dimensions. These structures have atracted much attention due to their properties such as low density, high specific surface area and large volume of pores. In this work, MOFs consisted of zinc clusters connected by ditopic ligands, terephthalic acid (1,4- H2BDC) or isophthalic acid (1,3-H2BDC) were synthesized. To obtain the proposed materials, different routes and synthetic parameters were tested, such as the molar ratio of the precursors, the addition of template molecules, the type of solvente, the addition of organic base or the type of a counter-ion of Zn salt. It was found that the variation of these parameters led to the formation of different metalorganic structures. The solids obtained were characterized by XRD, SEM and IR. For the samples identified as MOF- 5, it was verified that the structure was composed of both interpenetrated and non interpenetrated structures. These samples showed a low stability, becoming totally transformed into another structure within less than 72 hours. The addition of the nickel and/or cobalt was found to be a promissing method for increasing the stability of MOF- 5, which in this case, still remained unconverted to another structure even after 15 days of exposure to air. The samples prepared from 1,3-H2BDC were probably new, still unknown Metal Organic Frameworks
Redes Metalorg?nicas (MOFs) s?o estruturas supramoleculares constitu?das de ?ons ou clusters met?licos coordenados com ligantes org?nicos que se repetem em duas (2D) ou tr?s (3D) dimens?es. Essas estruturas t?m atra?do muita aten??o devido ?s suas propriedades, como por exemplo, baixa densidade, elevada ?rea superficial espec?fica e elevado volume de poro livre. Neste trabalho foram sintetizadas MOFs formadas por clusters met?licos de zinco conectados por ligantes dit?picos, ?cido tereft?lico (1,4- H2BDC) ou isoft?lico (1,3-H2BDC). Para a obten??o dos materiais propostos foram testadas diferentes rotas e par?metros de s?ntese, tais como, raz?o molar dos precursores, adi??o de mol?culas de molde, tipo de solvente, adi??o de base org?nica ou do contra-?on do sal de Zn. Constatou-se que a varia??o destes par?metros pode conduzir a forma??o de diferentes estruturas metalorg?nicas. Os s?lidos obtidos foram caracterizados por DRX, MEV e IV e TG. Para as amostras onde foi identificada a rede metalorg?nica MOF-5 verificou-se a exist?ncia de por??es de estrutura interpenetrada, assim como de estrutura n?o interpenetrada. Estas amostras apresentaram baixa estabilidade, convertendo-se totalmente em outra estrutura num per?odo de tempo inferior a 72 h. A adi??o de n?quel e/ou cobalto mostrou-se promissora para o aumento de estabilidade da MOF-5, a qual foi identificada mesmo ap?s 15 dias de exposi??o ao ar. Dentre as amostras preparadas com 1,3-H2BDC apenas uma estrutura foi identificada, com base nos bancos de dados de estruturas conhecidas, levando a crer que tr?s redes metalorg?nicas obtidas apresentam estruturas in?ditas
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"Structural and bonding studies on polynuclear metal complexes: Part I, transition metal polychalcogenides from hydro(solvo)thermal synthesis : Part II, double salts of silver acetylide/pseudohalide with soluble silver salt." 1999. http://library.cuhk.edu.hk/record=b6073171.

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Анотація:
Guo-cong Guo.
"June 1999."
Thesis (Ph.D.)--Chinese University of Hong Kong, 1999.
Includes bibliographical references.
Electronic reproduction. Hong Kong : Chinese University of Hong Kong, [2012] System requirements: Adobe Acrobat Reader. Available via World Wide Web.
Mode of access: World Wide Web.
Abstracts in English and Chinese.
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Частини книг з теми "Hydro-thermal Synthesis"

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H. El-Moayed, Mohamed, Justin Kühn, Sea-Hyun Lee, Mahmoud Farag, and Sherif Mehanny. "Potential of Lignin Valorization with Emphasis on Bioepoxy Production." In Lignin - Chemistry, Structure, and Application [Working Title]. IntechOpen, 2022. http://dx.doi.org/10.5772/intechopen.108263.

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Анотація:
Lignin is the second most abundant natural polymer after cellulose. It has high molecular weight and poor dispersity, which lowers its compatibility with other polymeric materials. Accordingly, it is hard to integrate lignin into polymer-based applications in its native form. Recently, lignin valorization, which aims to boost lignin value and reactivity with other materials, has captured the interest of many researchers. The volatility of oil and gas prices is one strong incentive for them to consider lignin as a potential replacement for many petroleum-based materials. In this chapter, lignin valorization processes, namely hydrogenolysis, pyrolysis, hydro-thermal liquefaction, and hydro-thermal carbonization, are discussed in brief. The chapter also discusses the synthesis of lignin-based epoxy resin as an already existing example of a lignin-based product.
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Тези доповідей конференцій з теми "Hydro-thermal Synthesis"

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Hu, Lili, Junlan Wang, Zijian Li, Shuang Li, and Yushan Yan. "Interfacial Adhesion of Nanoporous Zeolite Thin Films." In ASME 2004 International Mechanical Engineering Congress and Exposition. ASMEDC, 2004. http://dx.doi.org/10.1115/imece2004-62022.

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Nanoporous zeolite thin films are promising candidates as future low-k materials. During the integration with other semiconducting materials, the high stresses resulted from the synthesis process can cause the film to fracture or delaminate from the substrates. Evaluating the interfacial adhesion of zeolite thin films is very important in achieving high performance low-k materials. In this work, laser spallation technique is utilized to investigate the interfacial strength of zeolite thin films from three different synthesis processes. The preliminary results show that the fully crystalline zeolite thin films from hydro-thermal in-situ and seeded growth methods have a stronger interface than that from the spin-on process. Effort is also being made to compare the interfacial strength of the zeolite films between the two hydro-thermal methods. This is the first time that the interfacial strength of zeolite thin films is quantitatively evaluated. The results have great significance in the future applications of low-k zeolite thin films.
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R., Anil Kumar M., Hendry Izaac Elim, Mohd Sobri Idris, Akhmad Herman Yuwono, Brian Yuliarto, P. T. D. Rompas, Azeez Abdullah Barzinjy, et al. "Hydro thermal synthesis and electrochemical characterization of (V1/2Sb1/2Sn)O4 and (Fe1/2Sb1/2Sn)O4 as energy storage materials." In INTERNATIONAL CONFERENCE ON ENERGY AND ENVIRONMENT (ICEE 2021). AIP Publishing, 2021. http://dx.doi.org/10.1063/5.0061746.

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Balster, Lori M., Walter J. Balster, and E. Grant Jones. "Extended Liquid-Phase Oxidation of Aviation Fuels." In ASME 1999 International Gas Turbine and Aeroengine Congress and Exhibition. American Society of Mechanical Engineers, 1999. http://dx.doi.org/10.1115/99-gt-055.

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Liquid-phase oxidation of two jet fuels classified as hydro-treated and straight-run (without dissolved metals) is studied at 185°C by measuring the depletion of dissolved oxygen in an isothermal, high-pressure flowing system. The goal is to simulate some of the effects of fuel recirculation by studying changes in oxidation that occur during the course of reaction. Recirculation of fuel is used in modem aircraft to optimize the ability of the fuel to dissipate heat from component systems. Following extended oxidation (prestressing), hydrotreated fuel oxidizes more rapidly than in its neat form resulting, in part, from formation of catalytic oxidation products such as hydroperoxides and depletion of synthetic primary antioxidants. In contrast, the straight-run fuel oxidizes more slowly following prestressing; this effect is ascribed to the formation of efficient secondary antioxidants and to depletion of radical initiators. Results are discussed in terms of changes in the distribution of primary and secondary antioxidants and their effect on subsequent oxidation and the thermal stability of recirculated fuel.
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