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Artigos de revistas sobre o assunto "302.3/5"

1

Zhang, Hualei, Xinlei Wang, Jie Zhou e Weihua Tang. "Azo-Linkage Redox Metal–Organic Framework Incorporating Carbon Nanotubes for High-Performance Aqueous Energy Storage". Molecules 28, n.º 22 (8 de novembro de 2023): 7479. http://dx.doi.org/10.3390/molecules28227479.

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The design of well-defined hierarchical free-standing electrodes for robust high-performance energy storage is challenging. We report herein that azo-linkage redox metal–organic frameworks (MOFs) incorporate single-walled carbon nanotubes (CNTs) as flexible electrodes. The in situ-guided growth, crystallinity and morphology of UiO-66-NO2 MOFs were finely controlled in the presence of CNTs. The MOFs’ covalent anchoring to CNTs and solvothermal grafting anthraquinone (AQ) pendants endow the hybrid (denoted as CNT@UiO-66-AQ) with greatly improved conductivity, charge storage pathways and electrochemical dynamics. The flexible CNT@UiO-66-AQ displays a highest areal specific capacitance of 302.3 mF cm−2 (at 1 mA cm−2) in −0.4~0.9 V potential window, together with 100% capacitance retention over 5000 cycles at 5 mA cm−2. Its assembled symmetrical supercapacitor (SSC) achieves a maximum energy density of 0.037 mWh cm−2 and a maximum power density of 10.4 mW cm−2, outperforming many MOFs-hybrids-based SSCs in the literature. Our work may open a new avenue for preparing azo-coupled redox MOFs hybrids with carbaneous substrates for high-performance robust aqueous energy storage.
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2

Ongas, Martin O., Elizabeth Juma, Caroline G. Kirimi, Florence Oloo, Gilbert Kokwaro, Rashid Aman e Bernhards R. Ogutu. "A selective LC-MS/MS method for simultaneous quantification of Artemether, Lumefantrine and their principle metabolites in human plasma". ABC Research Alert 6, n.º 3 (31 de dezembro de 2018): Kenya. http://dx.doi.org/10.18034/ra.v6i3.335.

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We have developed and validated a sensitive, selective and reproducible reversed-phase high-performance liquid chromatography method coupled with electrospray ionization mass spectrometry (HPLC–ESI-MS/MS) for the simultaneous quantitation of artemether (ART), dihydroartemisinin (DHA), lumefantrine (LUM) and desbutyl-lumefantrine (DBL) in human plasma. Mefloquine was used as an internal standard (IS). The analytes were extracted by protein precipitation procedure and separated on a reversed-phase Zorbax SB-Ciano column with a mobile phase composed of acetonitrile and 20mM aqueous ammonium formate containing 0.5% (v/v) formic acid. Multiple reaction monitoring was performed in the positive ion mode using the transitions m/z 316.3→m/z 163.1 (ART), m/z 302.3→m/z 163.1 (DHA), m/z 530.3→m/z 512.2. (LUM), m/z 472.2→m/z 454.1 (DBL) and m/z 379.1→m/z 361.1(MQ) to quantify the drugs. Calibration curves in spiked plasma were linear (r2 ≥ 0.9992) over the range of 5–1500 ng/mL for ART/ DHA and 5–5,000 ng/mL for LUM/DBL. The lower limit of quantitation (LLOQ) was 10 ng/mL ART/ DHA and 5 ng/mL for LUM/ DBL. The mean R.S.D. values for the intra-run precision were 2.2% , 3.8%, 1.9% and 4.7% and for the inter-run precision were 3.2%, 3.6% , 4.4% and 3.5% for ART, DHA, LUM and DBL, respectively. The mean percentage recovery values were 93.2%, 98.5%, 97.1% and 99.4% for ART, DHA, LUM and DBL, respectively. No matrix effect was detected for all the analytes and the IS. The validated method was successfully applied to determine the plasma concentrations of ART, DHA, LUM and DBL in pregnant and non-pregnant women volunteers in a multiple-dose pharmacokinetics study over the course of 336 hours.
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3

Tor, Yu N., R. Shapich e N. A. Rusina. "Psychodynamic psychotherapy in the diagnosis and treatment of gender dysphoria". Patient-Oriented Medicine and Pharmacy 1, n.º 2 (6 de junho de 2023): 31–35. http://dx.doi.org/10.37489/2949-1924-0011.

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Relevance. In this article, we consider the possibilities of a psychodynamic psychotherapeutic approach in the diagnosis and treatment of gender dysphoria on the example of a clinical case. Gender dysphoria refers to the distress that may accompany a mismatch with the patient's biological sex and assigned gender. In the past few years, there has been an increase in the number of patients requesting the restoration of congenital anatomical sex characteristics due to regret after genderaffirmation surgery (GAS). Recent studies have shown that one of the key regrets after GAS is inadequate psychological and psychiatric evaluation in determining whether GAS is an indication.Case study. In this article, we explored how psychodynamic psychotherapy can be used to diagnose and treat disorders associated with gender dysphoria in the case of a 21-year-old man who presented with symptoms that met the diagnostic criteria for two conditions: unspecified gender dysphoria 302.85 (F64.1) and transvestic disorder with autogynephy 302.3 (F65.1) according to DSM-5. The main symptom appeared when the patient was at pre-school age and has been a constant concern ever since. The symptoms disappeared after psychodynamic psychotherapy, which lasted 11 months. Evaluation of psychotherapeutic effects 2 years after the completion of psychotherapy showed the stability of the results achieved.Conclusion. Based on our analysis, we concluded that the use of psychodynamic psychotherapy for patients with gender dysphoria helps recognize neurotic conflicts that may underlie transgender symptoms, and thereby reduce the likelihood of a diagnostic error in determining the presence of indications for GAS. Looking at cases of gender dysphoria in Balint groups can also be of great help in understanding the etiology of gender dysphoria symptoms.
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4

Mahmood, Yadgar, Halgurd Nasraden Hassan e Masood Saber Mohammed. "Yield Performance of Barley Hybrids (Hordeum vulgare L.) under Drought stress and non-stressed Conditions". Passer Journal of Basic and Applied Sciences 3, n.º 1 (2019): 107–13. http://dx.doi.org/10.24271/psr.20.

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This study was carried out at the experiment field, Kalar Technical Institute, Garmian Region in two growing seasons of 2016-2017 and 2017-2018 in order to evaluate the growth and yield potentials of barley under water stressed using hybrids as a source of wide range of genotypic variations. Therefore, five F2 barley hybrids (Hordeum vulgare L.) were screened for grain yield, biomass dry matter, plant height and harvest index under irrigated and drought conditions. Results showed that there was no effect of drought on grain yield (P>0.05) in 2017, while significantly reduced yield in 2018 and across-year mean (P-2 (3//14) under irrigated condition, and 267.8 (3//5) to 302.3 g m-2 (3//4) under unirrigated condition (P=0.001), biomass dry matter was ranged from 1099.1 (3//1) to 1370.5 g m-2 (3//14) under irrigated condition, and 892.6 (3//1) to 1153.9 g m-2 (3//14) under unirrigated condition (P=0.05), and harvest index were from 25.1 (3//14) to 28.0 (3//1) under irrigated conditions, and 25.9 (3//14) to 31.2 (3//1) under unirrigated conditions (P=0.04). Regression analysis, averaging over years, showed a positive relationship between grain yield and biomass under irrigated (R2=0.76; P=0.05), despite that, any positive relation was not found under unirrigated conditions (R2=0.43; P=0.23) due to post-anthesis drought stress. A strong relationship was also found between plant height and biomass dry matter under both irrigated (R2=0.89; P=0.02) and unirrigated (R2=0.97; P=0.003) conditions due to the high contribution of plant height in increasing plant biomass. It is concluded that genotypes had different response to drought due to their genetic diversity, and relatively low impact of water stress was appeared on growth and grain yield of barley in this semi-arid region compared to worldwide expected range of yield reduction.
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Musikhin, A. E., M. A. Bespyatov, T. M. Kuzin, V. D. Grigorieva e V. N. Shlegel. "The low temperature heat capacity of Li2Mo0.05W0.95O4". Journal of Physics: Conference Series 2119, n.º 1 (1 de dezembro de 2021): 012137. http://dx.doi.org/10.1088/1742-6596/2119/1/012137.

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Abstract The heat capacity of a lithium tungstate single crystal doped by 5% molybdenum Li2Mo0.05W0.95O4 in the range of 78.5–302.8 K was measured by the adiabatic method. No anomalous behavior of heat capacity was found. The heat capacity function was obtained in the range of 0–303 K by extrapolating to zero temperature and fitting experimental points. Thermodynamic functions of entropy, enthalpy increment and Gibbs free energy at 298.15 K were calculated using the obtained data.
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Malashkevich, V. N., P. Burkhard, P. Dominici, P. S. Moore, C. Borri Voltattorni e J. N. Jansonius. "Preliminary X-ray analysis of a new crystal form of recombinant pig kidney DOPA decarboxylase". Acta Crystallographica Section D Biological Crystallography 55, n.º 2 (1 de fevereiro de 1999): 568–70. http://dx.doi.org/10.1107/s0907444998006283.

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DOPA decarboxylase is responsible for the synthesis of the key neurotransmitters dopamine and serotonin via decarboxylation of L-3,4-dihydroxyphenylalanine (L-DOPA) and L-5-hydroxytryptophan, respectively. The crystals of recombinant DOPA decarboxylase differ from those previously reported for the enzyme purified from pig kidney. They belong to space group P622 with unit-cell dimensions a = b = 302.6, c = 178.1 Å. Both the self-rotation function and the good diffraction quality of these crystals (2.5 Å on a synchrotron source) suggest that there should be at least three protein dimers in the asymmetric unit. Diffraction data sets have been collected for the native enzyme and a heavy-atom derivative.
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7

Ghassemzadeh, Mitra, Klaus Harms e Kurt Dehnicke. "Kristallstruktur von [PMePh3] [Cl - 1 - C≡C - Ph]/Crystal Structure of [PMePh3] [Cl - I - C≡C - Ph]". Zeitschrift für Naturforschung B 52, n.º 6 (1 de junho de 1997): 772. http://dx.doi.org/10.1515/znb-1997-0618.

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Abstract The donor-acceptor complex [Cl-I-C≡C-Ph]- has been prepared as the methyl-triphenyl-phosphonium salt from 1-iodo-2-phenylacetylene and [PMePh3]N3 in CH2Cl2 solution. It forms co­lourless single crystals which were characterized by a crystal structure determination. Space group Pbca, Z = 8, lattice dimensions at -80 °C: a = 1047.1(1), b = 1700.3(1), c = 2793.2(1) pm, R = 0.035. The chloride ion is coordinated at the io­dine atom of the 1-iodo-2-phenylacetylene molecule in a nearly linear arrangement [CI-I-C≡C-Ph]- with bond lengths I-Cl of 302.4 pm and I-C of 203.1(5) pm.
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8

Shields, E. J., e P. S. Taylor. "Potato Leafhopper Control in Alfalfa, 1991". Insecticide and Acaricide Tests 17, n.º 1 (1 de janeiro de 1992): 183. http://dx.doi.org/10.1093/iat/17.1.183.

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Abstract Experimental plots measuring 7.3 × 7.3 m (24 × 24 ft) were established in a 5-yr-old field of ‘Oneida VR’ alfalfa in Ithaca, NY. Soils were silt loam. The trial was performed on water stressed regrowth 27 days after the first cutting. Some hopperburn was evident. Nine treatments and 1 untreated check were replicated 4 times in a randomized complete block design. Treatments were applied on 3 Jul with a C02 pressurized ATV-mounted, 8 nozzle spray boom which spanned 3.66 m (12 ft). The sprayer delivered 302.8 liters/ha (32 gal/acre) at 40 psi and an ATV speed of 5.6 km/hr (3.5 mi/hr). Rain showers occurred in the afternoon and evening both 1 and 2 DAT. PLH density was evaluated 1 d pretreatment and 4, 7, 14 and 20 DAT by taking 10 sweeps per plot with a 40 cm diam sweep net. Data for all plot samplings were expressed as the number of PLH/10 sweeps.
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9

Shields, E. J., e P. S. Taylor. "Alfalfa Weevil Control in Alfalfa, 1991". Insecticide and Acaricide Tests 17, n.º 1 (1 de janeiro de 1992): 182–83. http://dx.doi.org/10.1093/iat/17.1.182.

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Abstract Experimental plots measuring 7.3 × 7.3 m (24 × 24 ft) were established in a 5-yr-old field of ‘Oneida VR’ alfalfa in the early bud stage located in Ithaca, NY. Soils were silt loam. Eleven treatments and 2 untreated checks were replicated 4 times in a randomized complete block design. Treatments were applied on 21 May with a C02 pressurized ATV-mounted 8 nozzle spray boom which spanned 3.66 m (12 ft). The sprayer delivered 302.8 liters/ha (32 gal/acre) at 40 psi and an ATV speed of 5.6 km/h (3.5 mph). AW density was evaluated 1 day pre-treatment and 4 DAT by collecting 25 stems per plot and counting total number of larvae collected per plot. AW density was evaluated 7 and 14 DAT by collecting 10 stems per plot and counting total number of larvae collected per plot. Data for all plot samplings were expressed as mean AW/stem.
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10

Oliveira, Risalvo F., Alexandre F. Perazzo, Douglas dos S. Pina, Henry D. R. Alba, Vagner M. Leite, Manoel M. dos Santos, Edson M. Santos et al. "Productive and Qualitative Traits of Sorghum Genotypes Used for Silage under Tropical Conditions". Crops 4, n.º 2 (18 de junho de 2024): 256–69. http://dx.doi.org/10.3390/crops4020019.

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The aim of this study was to evaluate the productive potential, chemical composition, and fermentation profile of 24 genotypes of forage sorghum after ensiling. For this agronomic evaluation, a completely randomized block design with six replicates and twenty-four treatments was employed. Genotype 5 had the highest dry matter (DM) yield of 22.24 t/ha. The plant DM content ranged (p < 0.001) from 271.8 g/kg of fresh matter (FM) in genotype 9 to 330.0 g/kg FM in genotype 3, averaging 302.9 g/kg FM. The crude protein and non-fibrous carbohydrates differed significantly (p < 0.001) in the evaluated silages, with mean values of 61.0 and 275.3 g/kg DM, respectively. The pH of the sorghum silages also differed (p < 0.001), despite having an average of 3.94, with values ranging from 3.68 to 4.27. No changes were observed (p > 0.05) for the dry matter recovery of the sorghum genotype silages, which averaged at 853.9 g/kg FM. In the present study, genotype 5 resulted in being the most recommended genotype because it demonstrated a higher yield and higher nutritional value in both its fresh form and its ensiled form; had the lowest losses; and showed an ideal dry matter recovery after ensiling of 880 g/kg.
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Livros sobre o assunto "302.3/5"

1

J, Frost Peter, ed. Organizational culture. Beverly Hills: Sage Publications, 1985.

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2

Leenders, Roger Th. A. J. e Gabbay Shaul M, eds. Corporate social capital and liability. Boston: Kluwer Academic, 1999.

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3

1970-, Kelly Gavin, Kelly Dominic 1965- e Gamble Andrew, eds. Stakeholder capitalism. Houndmills, Basingstoke [England]: Macmillan Press, 1997.

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4

Richard, Whitley, e Kristensen Peer Hull, eds. The Changing European firm: Limits to convergence. London: Routledge, 1995.

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5

1947-, Ward Anthony, ed. The changing face of Chinese management. London: Routledge, 2003.

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6

McGuire, Gibson, Biggs Robert D, University of Chicago. Oriental Institute. e University of Chicago. Dept. of Near Eastern Languages and Civilizations., eds. The Organization of power: Aspects of bureaucracy in the ancient Near East. 2a ed. Chicago, Ill: Oriental Institute of the University of Chicago, 1991.

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7

John, Hickson David, ed. Great writers on organizations. 2a ed. Aldershot: Brookfield, USA, 2000.

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8

M, Beyer Janice, ed. The cultures of work organizations. Englewood Cliffs, N.J: Prentice Hall, 1993.

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9

Organizational Behviour: An Introductory Text with Organizational Behviour Premium CWS Pin Card. Pearson Education, Limited, 2006.

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10

Extreme Facilitation: Guiding Groups Through Controversy and Complexity. Jossey-Bass, 2005.

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