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Artykuły w czasopismach na temat "Nuclear magnetic resonance spectroscopy"

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MATSUNAGA, Sho. "Nuclear Magnetic Resonance Spectroscopy". Journal of the Japan Society of Colour Material 64, nr 4 (1991): 247–54. http://dx.doi.org/10.4011/shikizai1937.64.247.

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FUJII, Naoyuki. "Nuclear Magnetic Resonance Spectroscopy". Journal of the Japan Society of Colour Material 78, nr 12 (2005): 572–82. http://dx.doi.org/10.4011/shikizai1937.78.572.

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Lehmann, Teresa. "Nuclear Magnetic Resonance Spectroscopy". Magnetochemistry 4, nr 2 (20.04.2018): 20. http://dx.doi.org/10.3390/magnetochemistry4020020.

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Jelinski, Lynn W. "Nuclear magnetic resonance spectroscopy". Analytical Chemistry 62, nr 12 (15.06.1990): 212–23. http://dx.doi.org/10.1021/ac00211a017.

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Rabenstein, Dallas L., i Wei Guo. "Nuclear magnetic resonance spectroscopy". Analytical Chemistry 60, nr 12 (15.06.1988): 1–28. http://dx.doi.org/10.1021/ac00163a001.

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Mc Cully, Kevin, Donna Mancini i Sanford Levine. "Nuclear Magnetic Resonance Spectroscopy". Chest 116, nr 5 (listopad 1999): 1434–41. http://dx.doi.org/10.1378/chest.116.5.1434.

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Balaban, Robert S. "Nuclear Magnetic Resonance Spectroscopy". Academic Radiology 2 (wrzesień 1995): S136—S137. http://dx.doi.org/10.1016/s1076-6332(12)80056-0.

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Haw, James F. "Nuclear magnetic resonance spectroscopy". Analytical Chemistry 64, nr 12 (15.06.1992): 243–54. http://dx.doi.org/10.1021/ac00036a014.

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Smith, Ian C. P., i Dorothea E. Blandford. "Nuclear magnetic resonance spectroscopy". Analytical Chemistry 67, nr 12 (15.06.1995): 509–18. http://dx.doi.org/10.1021/ac00108a037.

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Ettl, Armin, Christa Fischer-Klein, Andreas Chemelli, Albert Daxer i Stephan Felber. "Nuclear magnetic resonance spectroscopy". International Ophthalmology 18, nr 3 (1994): 171–81. http://dx.doi.org/10.1007/bf00915968.

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Rozprawy doktorskie na temat "Nuclear magnetic resonance spectroscopy"

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Patel, Sunil U. "Nuclear magnetic resonance spectroscopy and ultrasound". Thesis, Aston University, 1989. http://publications.aston.ac.uk/9708/.

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The work described in this thesis is directed to the examination of the hypothesis that ultrasound may be used to perturb molecular motion in the liquid phase. These changes can then be detected by nuclear magnetic resonance (NMR) in spin-lattice and spin-spin relaxation times. The objective being to develop a method capable of reducing the pulsed NMR acquisition times of slowly relaxing nuclei. The thesis describes the theoretical principles underlying both NMR spectroscopy and ultrasonics with particular attention being paid to factors that impinge on testing the above hypothesis. Apparatus has been constructed to enable ultrasound at frequencies between 1 and 10 mega-hertz with a variable power up to 100W/cm-2 to be introduced in the NMR sample. A broadband high frequency generator is used to drive PZT piezo-electric transducer via various transducer to liquid coupling arrangements. A commercial instrument of 20 kilo-hertz has also been employed to test the above hypothesis and also to demonstrate the usefulness of ultrasound in sonochemistry. The latter objective being, detection of radical formation in monomer and polymer ultrasonic degradation. The principle features of the results obtained are: Ultrasonic perturbation of T1 is far smaller for pure liquids than is for mixtures. The effects appear to be greater on protons (1H) than on carbon-13 nuclei (13C) relaxation times. The observed effect of ultrasonics is not due to temperature changes in the sample. As the power applied to the transducer is progressively increased T1 decreases to a minimum and then increases. The T1's of the same nuclei in different functional groups are influenced to different extents by ultrasound. Studies of the 14N resonances from an equimolar mixture of N, N-dimethylformamide and deuterated chloroform with ultrasonic frequencies at 1.115, 6, 6.42 and 10 MHz show that as the frequency is increased the NMR signal to noise ratio decreases to zero at the Larmor frequency of 6.42 MHz and then again rises. This reveals the surprising indication that an effect corresponding to nuclear acoustic saturation in the liquid may be observable. Ultrasonic irradiation of acidified ammonium chloride solution at and around 6.42 MHz appears to cause distinctive changes in the proton-nitrogen J coupling resonance at 89.56 MHz. Ultrasonic irradiation of N, N-dimethylacetamide at 2 KHz using the lowest stable power revealed the onset of coalescence in the proton spectrum. The corresponding effect achieved by direct heating required a temperature rise of approximately 30oC. The effects of low frequency (20 KHz) on relaxation times appear to be nil. Detection of radical formation proved difficult but is still regarded as the principle route for monomer and polymer degradation. The initial hypothesis is considered proven with the results showing significant changes in the mega-hertz region and none at 20 KHz.
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Norwood, Timothy John. "Nuclear magnetic resonance in inhomogeneous magnetic fields". Thesis, University of British Columbia, 1985. http://hdl.handle.net/2429/24875.

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The work described in this thesis was initiated in an attempt to overcome the limitations imposed upon NMR spectroscopy by magnetic field inhomogeneity in two specific areas: high resolution spectroscopy in isotropic liquids, and chemical shift resolved NMR imaging in isotropic liquids. In both cases magnetic field inhomogeneity may degrade the resolution of spectra to such an extent that no useful information can be obtained from them. In high resolution NMR spectroscopy it is necessary to be able to extract accurately the parameters present within the spectrum such as chemical shifts, coupling constants and peak areas. In chemical shift resolved imaging experiments the requirements are less stringent; and it is only necessary that the resonances of different chemical species be resolved. However, even the less stringent requirements of NMR imaging are often difficult to meet as the sample volumes required are often several orders of magnitude larger than those required in conventional high resolution NMR spectroscopy. The use of zero-quantum coherence has been investigated as a potential solution to the magnetic field inhomogeneity problem in both of these areas. Zero-quantum coherences are independent of magnetic field inhomogeneity and contain the parameters desired in both cases, though they are displayed in a way which differs from conventional NMR spectra. In this thesis, existing zero-quantum coherence experiments have been evaluated for use with inhomogeneous magnetic fields, and, where necessary, adapted for this purpose. Several completely new experiments have been developed for producing broad-band decoupled zero-quantum coherence spectra and also for presenting coupling constants and chemical shifts in a manner which is as close to conventional NMR spectra as possible, hence facilitating ease of use. Zero-quantum coherence has been evaluated as a tool for identifying unknown compounds and also for identifying the components of complex mixtures by "signature" recognition. Both decoupled and non-decoupled zero-quantum coherence experiments are adapted to provide imaging experiments which allow the separation of the images of different chemical species in inhomogeneous magnetic fields. The two-dimensional J-resolved experiment is also adapted for this purpose.
Science, Faculty of
Chemistry, Department of
Graduate
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Xu, Ping. "New methods in nuclear magnetic resonance spectroscopy". Thesis, University of Cambridge, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.239177.

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Cavanagh, John. "New techniques in nuclear magnetic resonance spectroscopy". Thesis, University of Cambridge, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.293707.

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Wu, Xi-Li. "New techniques in nuclear magnetic resonance spectroscopy". Thesis, University of Cambridge, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.385872.

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Claridge, Timothy David William. "Protein studies by nuclear magnetic resonance spectroscopy". Thesis, University of Oxford, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.303628.

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Wormald, Philip. "Nuclear magnetic resonance spectroscopy of vinylidenefluoride polymers". Thesis, Durham University, 2005. http://etheses.dur.ac.uk/2615/.

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High-resolution solid- and solution state NMR techniques have been applied in the study of a Semi crystalline fluoropolymer Poly(vinylidienfluoride) (PVDF) and a vinylidienfluoride telomer. The application of standard solution-state experiments with high power decoupling and two-dimensional techniques has provided a greater understanding of the structure of these two fluoropolymers. Specifically, Cosy and Tocsy experiments gave information on signals normally related to end groups and to previously unidentified structures, which suggest the presence of at least a second major structure. 19F solid-state Magic Angle spinning Nuclear Magnetic Resonance (MAs- NMR) using relaxation filters in pulse sequences, has revealed fundamental differences relating to morphology and structure. The location of reverse units in the amorphous and crystalline domains is investigated by fluorine Tip filtered Radio Frequency Driven Recoupling (RFDR) and spin-diffusion experiments. These experiments proved that the reverse units are dominant in the amorphous phase, yet could have association with rigid species. Furthermore, signals generally associated with crystalline domains are not homogenie in character. The presence of a highly mobile species was detected and investigated using the delayed acquisition technique and T2 measurements. This showed the possibility of end-group signal in the spectral region normally associated with reverse groups. Furthermore, proton Tip measurements of nascent and annealed PVDF, recorded at variable temperature are related to molecular motion and debated with respect to the effect of spin diffusion on populations. The relationship between thermal events and thermal history of PVDF and its effect on molecular motion is debated.
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Jones, David Nigel Mark. "Nuclear magnetic resonance spectroscopy of bacterial polysaccharides". Thesis, University of Cambridge, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.316713.

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Barker, P. B. "New techniques in nuclear magnetic resonance". Thesis, University of Oxford, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.375213.

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Clarke, William. "Human cardiac magnetic resonance spectroscopy". Thesis, University of Oxford, 2016. https://ora.ox.ac.uk/objects/uuid:b75351dc-e4eb-4856-b901-4ba486ffe175.

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The status of the myocardial 'high energy phosphate' metabolism is a sensitive marker of the occurrence and progression of heart failure. Magnetic resonance spectroscopy enables non-invasive, direct and potentially quantitative measurements of the phosphate containing metabolites present in the human myocardium. This thesis is primarily concerned with the creation of measurement techniques for cardiac phosphorus magnetic resonance spectroscopy (31P-MRS) at the 7 tesla field strength. Chapter 1 provides an overview of the physical basis of magnetic resonance spectroscopy, the myocardial high energy phosphate metabolism, and the clinical relevance of the technique. Chapter 2 describes the advantage of 7 tesla scanners over lower field strengths. The radio frequency coil hardware is characterised experimentally. The multivoxel spectroscopy methods used throughout the thesis are described. Chapter 3 details the implementation of an open source spectroscopy fitting program. It is validated against previous closed-source implementations. The program's use is demonstrated in several clinical studies of heart failure, and to improve a previously implemented 1H spectroscopy coil combination method. In Chapter 4 the measurement of inorganic phosphate in the presence of overlapping peaks is attempted. Suppression of overlapping peaks, originating from the blood, is tried using Bo gradients, then saturation transfer. The myocardial pH of hypertrophic cardiomyopathy patients is measured. Chapter 5 describes the effect of creatine kinase catalysed chemical exchange on the 31P-MRS spectrum. A survey of methods suitable for measuring creatine kinase kinetics at 7 tesla is made. Multi-parametric fitting of variable repetition time saturation transfer data is explored in simulation and experiment. Chapter 6 describes the re-implementation and extension, for dynamic measurements, of the triple repetition time saturation transfer method for two clinical studies at 3 tesla. The creatine kinase forward rate constant is measured in heart failure and healthy cohorts, at rest, and during cardiac stress. In Chapter 7 a Bloch-Siegert B1 mapping sequence is implemented for 31P-MRS. An optimal Bloch-Siegert method for X-nuclear spectroscopy is calculated. B1maps are validated in skeletal muscle and collected in 5 volunteer's hearts. Chapter 8 uses the Bloch-Siegert B1 mapping sequence and the four angle saturation transfer method to implement creatine kinase rate measurement at 7 tesla. The first 3D localised creatine kinase rate measurements in the human myocardium are achieved in 10 volunteers.
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Książki na temat "Nuclear magnetic resonance spectroscopy"

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Bovey, Frank Alden. Nuclear magnetic resonance spectroscopy. Wyd. 2. San Diego: Academic Press, 1988.

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Dutta, Mala. Nuclear magnetic resonance spectroscopy. Delhi: Ivy Publishig House, 2000.

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Bovey, F. A. Nuclear magnetic resonance spectroscopy. Wyd. 2. London: Academic Press, 1988.

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J, Mowthorpe David, i ACOL (Project), red. Nuclear magnetic resonance spectroscopy. Chichester [West Sussex]: Published on behalf of ACOL, London, by J. Wiley, 1986.

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Bovey, Frank A. Nuclear magnetic resonance spectroscopy. Wyd. 2. San Diego: Academic Press, 1988.

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Hore, P. J. Nuclear magnetic resonance. Oxford: Oxford University Press, 1995.

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J, Oppenheimer Norman, i James Thomas L, red. Nuclear magnetic resonance. San Diego: Academic Press, 1989.

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Saul, Schaefer, i Balaban Robert Stephen 1953-, red. Cardiovascular magnetic resonance spectroscopy. Boston: Kluwer Academic Publishers, 1993.

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1955-, Brown Mark A., red. Clinical MR spectroscopy: First principles. New York: Wiley-Liss, 1998.

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1953-, Rudin M., i Beer R. de, red. In-vivo magnetic resonance spectroscopy. Berlin: Springer-Verlag, 1992.

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Części książek na temat "Nuclear magnetic resonance spectroscopy"

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Gupta, Preeti, S. S. Das i N. B. Singh. "Nuclear Magnetic Resonance Spectroscopy". W Spectroscopy, 23–92. New York: Jenny Stanford Publishing, 2023. http://dx.doi.org/10.1201/9781003412588-2.

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Aliev, Abil E. "Solid state NMR spectroscopy". W Nuclear Magnetic Resonance, 120–80. Cambridge: Royal Society of Chemistry, 2022. http://dx.doi.org/10.1039/9781839167690-00120.

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Aliev, A. E., i R. V. Law. "Solid state NMR spectroscopy". W Nuclear Magnetic Resonance, 294–347. Cambridge: Royal Society of Chemistry, 2015. http://dx.doi.org/10.1039/9781782622758-00294.

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Aliev, Abil E. "Solid state NMR spectroscopy". W Nuclear Magnetic Resonance, 139–87. Cambridge: Royal Society of Chemistry, 2020. http://dx.doi.org/10.1039/9781788010665-00139.

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Aliev, Abil E. "Solid state NMR spectroscopy". W Nuclear Magnetic Resonance, 98–150. Cambridge: Royal Society of Chemistry, 2021. http://dx.doi.org/10.1039/9781839164965-00098.

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Atta-ur-Rahman. "Experimental Procedures in NMR Spectroscopy". W Nuclear Magnetic Resonance, 87–139. New York, NY: Springer US, 1986. http://dx.doi.org/10.1007/978-1-4612-4894-1_3.

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Kemp, William. "Nuclear Magnetic Resonance Spectroscopy". W Organic Spectroscopy, 101–241. London: Macmillan Education UK, 1991. http://dx.doi.org/10.1007/978-1-349-15203-2_3.

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Atta-ur-Rahman. "Chemical Shift in 1H-NMR Spectroscopy". W Nuclear Magnetic Resonance, 1–33. New York, NY: Springer US, 1986. http://dx.doi.org/10.1007/978-1-4612-4894-1_1.

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Atta-ur-Rahman. "Spin—Spin Coupling in 1-NMR Spectroscopy". W Nuclear Magnetic Resonance, 34–86. New York, NY: Springer US, 1986. http://dx.doi.org/10.1007/978-1-4612-4894-1_2.

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Ashbrook, Sharon E., i Daniel M. Dawson. "NMR spectroscopy of minerals and allied materials". W Nuclear Magnetic Resonance, 1–52. Cambridge: Royal Society of Chemistry, 2016. http://dx.doi.org/10.1039/9781782624103-00001.

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Streszczenia konferencji na temat "Nuclear magnetic resonance spectroscopy"

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Ernst, R. R. "Nuclear magnetic resonance Fourier transform spectroscopy". W Optical 3D Measurement Techniques II: Applications in Inspection, Quality Control, and Robotics, redaktorzy Armin Gruen i Heribert Kahmen. SPIE, 1994. http://dx.doi.org/10.1117/12.169824.

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Verkhoglazova, E. V., D. A. Kupriyanov, Carlos Granja, Claude Leroy i Ivan Stekl. "Spectroscopy in Magnetic Resonance Tomography". W Nuclear Physics Medthods and Accelerators in Biology and Medicine. AIP, 2007. http://dx.doi.org/10.1063/1.2825818.

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"Structural Analysis of Nuclear Magnetic Resonance Spectroscopy Data". W International Conference on Bioinformatics Models, Methods and Algorithms. SciTePress - Science and and Technology Publications, 2013. http://dx.doi.org/10.5220/0004321902120222.

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Peters, T. M. "Magnetic resonance imaging and spectroscopy in medicine". W OSA Annual Meeting. Washington, D.C.: Optica Publishing Group, 1987. http://dx.doi.org/10.1364/oam.1987.thg3.

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Magnetic resonance techniques were developed in the mid-1940s to analyze the structures of chemical compounds. In the last 10 years, however, the same principles have been evolved, along with advances in magnet, computer, and display technology into one of the most exciting imaging methods available in the medical field today. Magnetic resonance imaging utilizes the property that certain nuclei when placed in a magnetic field can be stimulated into a resonance condition by external radio-frequency radiation. In recovering from this disturbance, the nuclei in turn emit rf signals (whose frequencies depend on the magnetic field strength in which the nuclei are located). To image the human body, the patient is placed in a large solenoidal magnet (field strength typically 0.5-1.5 T), and the magnetic field Is coded in various ways by the application of gradient fields, causing the protons within the volume to resonate with a range of frequencies. Relating these frequencies to positions within this volume is performed by a Fourier analysis of the signal. Reconstructed images are displayed to the user as slices of the 3-D volume being imaged.
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Pinilla, Samuel, Kareth León, Daniel Molina, Ariolfo Camacho i Henry Arguello. "Subsampling Schemes for the 2D Nuclear Magnetic Resonance Spectroscopy". W Computational Optical Sensing and Imaging. Washington, D.C.: OSA, 2018. http://dx.doi.org/10.1364/cosi.2018.ctu5d.3.

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Bilgic, A. M., J. W. Kunze, V. Stegemann, M. Zoeteweij i J. Hogendoorn. "B6.2 - Multiphase flow metering with nuclear magnetic resonance spectroscopy". W AMA Conferences 2015. AMA Service GmbH, Von-Münchhausen-Str. 49, 31515 Wunstorf, Germany, 2015. http://dx.doi.org/10.5162/sensor2015/b6.2.

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Meireles, L. T. P., C. Ravnås, M. J. Welch i I. L. Fabricius. "Failure characterization in geomechanical testing using nuclear magnetic resonance spectroscopy". W Chalk 2018 Engineering in Chalk. ICE Publishing, 2018. http://dx.doi.org/10.1680/eiccf.64072.541.

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Scott, Katherine N., David C. Wilson, Angela P. Bruner, Teresa A. Lyles, Brandon Underhill, Edward A. Geiser, J. Ray Ballinger, James D. Scott i Christine B. Stopka. "Automatic analysis of nuclear-magnetic-resonance-spectroscopy clinical research data". W 26th AIPR Workshop: Exploiting New Image Sources and Sensors, redaktor J. Michael Selander. SPIE, 1998. http://dx.doi.org/10.1117/12.300074.

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Gottstein, Eva, Dirk Lachenmeier i Thomas Kuballa. "Applications of Nuclear Magnetic Resonance Spectroscopy for Food Authenticity Control". W Virtual 2021 AOCS Annual Meeting & Expo. American Oil Chemists’ Society (AOCS), 2021. http://dx.doi.org/10.21748/am21.444.

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Fricke, Florian, Safdar Mahmood, Javier Hoffmann, Marcelo Brandalero, Sascha Liehr, Simon Kern, Klas Meyer i in. "Artificial Intelligence for Mass Spectrometry and Nuclear Magnetic Resonance Spectroscopy". W 2021 Design, Automation & Test in Europe Conference & Exhibition (DATE). IEEE, 2021. http://dx.doi.org/10.23919/date51398.2021.9473958.

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Raporty organizacyjne na temat "Nuclear magnetic resonance spectroscopy"

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Axelson, D. E. Carbon-13 solid state nuclear magnetic resonance spectroscopy of pitch. Natural Resources Canada/ESS/Scientific and Technical Publishing Services, 1986. http://dx.doi.org/10.4095/304931.

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Colvin, M., i V. V. Krishnan. New Approaches to Quantum Computing using Nuclear Magnetic Resonance Spectroscopy. Office of Scientific and Technical Information (OSTI), luty 2003. http://dx.doi.org/10.2172/15007477.

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TonThat, Dinh M. DC SQUID Spectrometers for Nuclear Quadrupole and Low-Field Nuclear Magnetic Resonance Spectroscopy. Office of Scientific and Technical Information (OSTI), kwiecień 1998. http://dx.doi.org/10.2172/760336.

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Pease, J. Structures of peptide families by nuclear magnetic resonance spectroscopy and distance geometry. Office of Scientific and Technical Information (OSTI), grudzień 1989. http://dx.doi.org/10.2172/7003404.

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Barrufet, M. A., F. W. Flumerfelt, M. P. Walsh i A. T. Watson. Development of Nuclear Magnetic Resonance Imaging/spectroscopy for improved petroleum recovery. Final report. Office of Scientific and Technical Information (OSTI), kwiecień 1994. http://dx.doi.org/10.2172/10141643.

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Bradbury, E. M., P. Catasti, X. Chen, G. Gupta, B. Imai, R. Moyzis, R. Ratliff i S. Velupillai. Neutron scattering and nuclear magnetic resonance spectroscopy structural studies of protein-DNA complexes. Office of Scientific and Technical Information (OSTI), marzec 1996. http://dx.doi.org/10.2172/206538.

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Klein, Joshua, Peter Irwin i Susan Lurie. Use of Nuclear Magnetic Resonance Spectroscopy to Determine Cell Wall Changes in Apple Fruit. United States Department of Agriculture, czerwiec 1993. http://dx.doi.org/10.32747/1993.7603841.bard.

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Verkade, J. Functional group analysis in coal and on coal surfaces by NMR (nuclear magnetic resonance) spectroscopy. Office of Scientific and Technical Information (OSTI), czerwiec 1989. http://dx.doi.org/10.2172/6918499.

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Cho, Herman M. Preliminary Feasibility Study of Using Solid-State Nuclear Magnetic Resonance Spectroscopy to Characterize Hanford Tank Waste Solids. Office of Scientific and Technical Information (OSTI), październik 2001. http://dx.doi.org/10.2172/789275.

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Cho, Herman M., i Gregg J. Lumetta. Preliminary Feasibility Study of Using Solid-State Nuclear Magnetic Resonance Spectroscopy to Characterize Hanford Tank Waste Solids. Office of Scientific and Technical Information (OSTI), październik 2001. http://dx.doi.org/10.2172/15001299.

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