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Tesi sul tema "Crystallization"

Autore: Grafiati

Pubblicato: 4 giugno 2021

Ultima modifica: 25 luglio 2025

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1

Sweed, Muhamed. "Co-crystallization in polyolefin blends studied by various crystallization analysis techniques." Thesis, Link to the online version, 2006. http://hdl.handle.net/10019.1/2733.

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2

Patki, Rahul P. "Quench Crystallization of Linear Polyethylene: Crystallization Kinetics, Morphology and Structure Investigation." Cincinnati, Ohio : University of Cincinnati, 2008. http://rave.ohiolink.edu/etdc/view.cgi?acc_num=ucin1227282696.

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3

Núñez, Eugenia. "Crystallization in Constrained Polymer Structures : Approaching the Unsolved Problems in Polymer Crystallization." Doctoral thesis, KTH, Fiber- och polymerteknik, 2006. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-4041.

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Abstract (sommario):

The knowledge regarding certain issues in polymer crystallization e.g. the possible existence of short–lived mesophases remains inconclusive due to experimental limitations. Polymers undergo chain folding upon crystallization, which introduces some complications that are not found in crystallization of low molar mass materials. Chain–folded crystals are far from their equilibrium shape and they rearrange rapidly at the crystallization temperature. This, together with the slow experimental techniques traditionally used, impedes the observation of the originally formed structures. To approach th

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4

Suzuki, Yasuhito [Verfasser]. "How different is water crystallization from polymer crystallization under confinement? / Yasuhito Suzuki." Mainz : Universitätsbibliothek Mainz, 2015. http://d-nb.info/1078386684/34.

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5

Robertson, Divann. "Studying crystallization kinetics using solution crystallization analysis by laser light scattering (Scalls)." Thesis, Stellenbosch : Stellenbosch University, 2012. http://hdl.handle.net/10019.1/20112.

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Thesis (MSc)--Stellenbosch University, 2012.<br>ENGLISH ABSTRACT: This study involved the analysis of crystallization kinetics by means of a unique and newly developed Solution crystallization analysis by laser light scattering (Scalls) technique. In the main study we compared two commercial linear low-density polyethylene (LLDPE) polymers (PE-1- octene and PE-1-hexene) and studied the effect of short-chain branching on the solution crystallization of these complex polymer systems. Characterization of the polymers was done by nuclear magnetic resonance spectroscopy (NMR) and high-tempera

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6

Walter, Thomas S. "Methodology for macromolecular crystallization." Thesis, University of Oxford, 2010. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.542989.

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7

Pridmore, Derik A. (Derik Arnold) 1978. "Online polymer crystallization experiment." Thesis, Massachusetts Institute of Technology, 2005. http://hdl.handle.net/1721.1/33335.

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Thesis (M. Eng.)--Massachusetts Institute of Technology, Dept. of Electrical Engineering and Computer Science, 2005.<br>Includes bibliographical references (leaves 119-120).<br>An architecture for online remote operation of a polymer crystallization experiment was refined, beta tested in actual use conditions, and extended based on feedback from those tests. In addition, an application for graphically simulating macroscopic crystal spherulite growth was developed for use as an educational tool. Finally, the experiment was used in the design process for modifying the generic iLab framework to i

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8

Yang, Li-yin 1952. "Crystallization kinetics of diphenylhydantoin." Thesis, The University of Arizona, 1989. http://hdl.handle.net/10150/277190.

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The crystallization kinetics of diphenylhydantoin (DPH) has been studied at constant conditions in a small mixed suspension mixed product removal (MSMPR) crystallizer. Supersaturation is created by changing the pH of a DPH solution in the crystallization vessel. Crystal size distributions (CSD's) are measured by an in situ zone sensing method. Effects of pH and supersaturation on crystallization kinetics and CSD are summarized. The effect of an additive on the crystal growth of DPH has been studied in a batch system. Avoidance of nucleation in the early stages of crystallization is essential t

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9

Jana, Sarbojeet. "Crystallization behavior of waxes." Thesis, Utah State University, 2016. http://pqdtopen.proquest.com/#viewpdf?dispub=10239292.

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<p> Crystallization behavior of different waxes such as beeswax (BW), paraffin wax (PW), ricebran wax (RBW), sunflower wax (SFW) was studied individually and in different oil solutions. Binary mixture at various proportions of the individual waxes was also explored in this study. Soybean oil is used in most of the study but olive, corn, sunflower, safflower, and canola oils were also explored. Lipid crystalline networks were characterized by several physical properties such as melting profile, solid fat content, viscoelastic parameters, cooling rate, phase behavior, crystal morphology. High in

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10

Taffs, Jade. "Local structure in crystallization." Thesis, University of Bristol, 2015. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.685975.

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In the work presented here, we use simulations of hard and nearly-hard spheres to examine the role of local structures in crystallisation. We are motivated by the work of Sir Charles Frank, who suggested that locally favoured structures, if incommensurate with crystalline ordering, could potentially suppress nucleation [1). Structural analysis is carried out using the topological cluster classification [2], which identifies those local arrangements of 5 < n < 13 particles which are structurally equivalent to the ground state structure for 11 particles considered in isolation. Initial work comp

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11

Núñez, Eugenia. "Crystallization in molecularly constrained polymer structures : approaching the unsolved problems in polymer crystallization /." Stockholm, 2006. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-4041.

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12

Sohn, Seungman. "Crystallization Behavior of Bisphenol-A Polycarbonate: Effects of Crystallization Time, Temperature, and Molar Mass." Diss., Virginia Tech, 2000. http://hdl.handle.net/10919/26980.

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Crystallization and multiple melting behavior of bisphenol-A polycarbonate (PC) was investigated using differential scanning calorimetry (DSC) for the monitoring of thermal behavior and atomic force microscopy (AFM) for the morphology study. The exceedingly slow crystallization kinetics of PC and the feasibility of obtaining near monodisperse fractions provide distinct advantages for the elucidation of the effects of crystallization time, temperature, and molar mass on crystallization kinetics. The effects of molar mass on the glass transition temperature (Tg) and heat capacity change at Tg

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13

Thati, Jyothi. "Spherical Crystallization of Benzoic Acid." Licentiate thesis, Stockholm : Skolan för kemivetenskap, Kungliga Tekniska högskolan, 2007. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-4602.

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14

Sura, Ravi Kishore. "Oriented crystallization of syndiotactic polypropylene." Diss., Georgia Institute of Technology, 2000. http://hdl.handle.net/1853/8293.

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15

Kimble, Walter Lee. "Mineral induce crystallization of lysozyme." Thesis, Georgia Institute of Technology, 1993. http://hdl.handle.net/1853/11266.

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16

Gambrel, Timothy Wayne. "Batch crystallization and crystal purity." Thesis, Georgia Institute of Technology, 1989. http://hdl.handle.net/1853/11831.

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17

Ronca, Gladys. "Heterogeneous nucleation in polymer crystallization." Thesis, Brunel University, 1985. http://bura.brunel.ac.uk/handle/2438/7285.

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The effect of talc, sodium benzoate, boron nitride, saccharin and sorbitol on the nucleation and crystallisation of PP, PE, PB, POM, PHB, PET and Nylon 66 has been investigated by DSC, light microscopy and electron microscopy. The effectiveness of the nucleating agent has been evaluated by the study of the interfacial layer between the polymer and the substrate of densely packed particles using light microscopy and by quantitative analysis of the DSC cooling exotherms, obtained from polymers with homogeneously dispersed nucleating agent. It has been found that the crystallisation temperature o

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18

Barker, Phil. "Crystallization of hydroxybutyrate/hydroxyvalerate copolymers." Thesis, University of Bristol, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.317156.

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19

Goldbeck-Wood, E. Gerhard. "Computer simulation of polymer crystallization." Thesis, University of Bristol, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.317157.

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20

Hillmann, William C. (William Carmen). "Crystallization studies of Pictet-Spenglerases." Thesis, Massachusetts Institute of Technology, 2008. http://hdl.handle.net/1721.1/43812.

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Thesis (S.M.)--Massachusetts Institute of Technology, Dept. of Chemistry, 2008.<br>Vita.<br>Includes bibliographical references.<br>Natural products are a rich source of medicinally important molecules. Monoterpene indole alkaloids from plants are an especially important source of therapeutic molecules. Due to the complexity of these molecules, biosynthesis of derivatives is an attractive way of obtaining molecules with potentially new or improved functionality. The rational design of mutants with altered/expanded substrate scope is an important step in engineering organisms to produce such co

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21

Silver, Barry R. "New approaches to protein crystallization." Thesis, University of Warwick, 2013. http://wrap.warwick.ac.uk/55616/.

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This thesis was focussed toward providing new approaches to protein crystallization. Herein, we describe three new such approaches. Firstly, we describe proof-of-concept studies which demonstrate that simple DC electrochemical systems may be used to enhance and/or control the growth of lysozyme protein crystals on the surface of platinum disc electrodes. Secondly, we demonstrate how various oil/water interfaces provide both novel and unique environments for the study and enhancement of protein crystallization studies. In particular, we show how some oil/water interfaces greatly enhance the ext

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22

Ogbuoji, Ebuka. "Protein Crystallization Methods and Apparatus." University of Toledo / OhioLINK, 2019. http://rave.ohiolink.edu/etdc/view?acc_num=toledo1556924307276754.

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23

Kesani, Sheshanka. "Crystallization studies of epigallocatechin gallate." [Tampa, Fla.] : University of South Florida, 2007. http://purl.fcla.edu/usf/dc/et/SFE0002100.

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24

Waechter, David F. (David Francis) Carleton University Dissertation Engineering Electrical. "Crystallization processes in amorphous silicon." Ottawa, 1987.

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25

Shek, Lai Yung. "Hydrothermal crystallization of organic compounds /." View abstract or full-text, 2004. http://library.ust.hk/cgi/db/thesis.pl?CHEM%202004%20SHEK.

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26

Konishi, Takashi. "Polymer crystallization through intermediate state." 京都大学 (Kyoto University), 2006. http://hdl.handle.net/2433/144031.

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Kyoto University (京都大学)<br>0048<br>新制・課程博士<br>博士(工学)<br>甲第12346号<br>工博第2675号<br>新制||工||1378(附属図書館)<br>24182<br>UT51-2006-J338<br>京都大学大学院工学研究科高分子化学専攻<br>(主査)教授金谷利治, 教授麹谷信三, 教授堀井文敬<br>学位規則第4条第1項該当

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27

Guo, Z. "Ultrasonic effects of crystallization processes." Thesis, University College London (University of London), 2007. http://discovery.ucl.ac.uk/1445538/.

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This thesis reports a study of the effects of ultrasound on crystal nuclcation from solution and particle breakage. Firstly, the effect of ultrasound on reactive crystallization when nuclcation is consistent with a predominantly homogeneous model is studied by measuring the induction time. Barium sulphate is used as the working substance precipitated by mixing aqueous BaCl2 and Na:S04 solutions. The relationship between amplitude of ultrasonic processor and power input was determined. The experiments were carried with various ultrasonic power inputs. It is observed that increasing ultrasound h

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28

Fleming, Sean D. "Computer modelling of gibbsite crystallization." Thesis, Curtin University, 1999. http://hdl.handle.net/20.500.11937/1274.

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Abstract (sommario):

This thesis documents the development and application of a computer model for gibbsite, an aluminium tri-hydroxide polymorph. In particular, the work has emphasized the idea of computer modelling techniques combining with ex- observations to provide greater insight than either could separately. Chapter One provides an overview and introduction to the fields of solid state chemistry, crystallization and computer modelling. These ideas are extended in Chapter Two to include a more detailed discussion of the theoretical principles behind the modelling in this project. The development of transfera

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29

Fleming, Sean D. "Computer modelling of gibbsite crystallization." Curtin University of Technology, School of Applied Chemistry, 1999. http://espace.library.curtin.edu.au:80/R/?func=dbin-jump-full&object_id=10273.

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Abstract (sommario):

This thesis documents the development and application of a computer model for gibbsite, an aluminium tri-hydroxide polymorph. In particular, the work has emphasized the idea of computer modelling techniques combining with ex- observations to provide greater insight than either could separately. Chapter One provides an overview and introduction to the fields of solid state chemistry, crystallization and computer modelling. These ideas are extended in Chapter Two to include a more detailed discussion of the theoretical principles behind the modelling in this project. The development of transfera

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30

FORTUNATI, Andrea. "Crystallization kinetics in Stromboli magma." Doctoral thesis, Università degli Studi di Camerino, 2011. http://hdl.handle.net/11581/401852.

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Shoshonitic basalt composition (PST9) has been studied to investigate the kinetics of crystallisation and implications for magma dynamics at Stromboli volcano. A series of decompression experiments over a range of pressure (100 - 5 MPa) at constant temperature (1075Â°C) show that plagioclase is stable at 50 MPa or less under water saturated conditions. Moreover, these experiments show that plagioclase An content decreases with decreasing P(H2O) reaching the same composition, as the natural plagioclase in Sromboli scoria and that the bulk crystal fraction increases as the experimental condition

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31

Chang, Li-Ching. "Cloning, purification and crystallization of selenophosphate synthetase cloning, purification and crystallization of ERp44 from Mus musculus /." [S.l.] : [s.n.], 2006. http://deposit.ddb.de/cgi-bin/dokserv?idn=980297311.

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32

Encarnacion-Gomez, Luis G. "Design and operation of enzymatic reactive crystallization: Applications in chiral purity and kinetically controlled synthesis." Diss., Georgia Institute of Technology, 2015. http://hdl.handle.net/1853/54322.

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The work presented in this thesis is aimed to design efficient reactive crystallization operations that could potentially be implemented in the manufacture of enantiomerically pure compounds and β-lactam antibiotics. Multiple aspects of solution thermodynamics, reaction engineering and crystallization from complex solutions are involved and will be discussed in detail through the following chapters. The first piece of this work utilizes reactive crystallization for the manufacture of enantiomerically pure amino acids. Chemo-enzymatic stereoiversion reactions are used to enrich saturated or s

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33

Lam, Wai Hung. "Chiral resolution by diastereomeric salt crystallization /." View abstract or full-text, 2005. http://library.ust.hk/cgi/db/thesis.pl?BIEN%202005%20LAM.

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34

Jibbouri, Sattar al. "Effects of additives in solution crystallization." [S.l. : s.n.], 2002. http://deposit.ddb.de/cgi-bin/dokserv?idn=967410673.

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35

Jiang, Yuan. "Precursor phases in non-classical crystallization." Phd thesis, Universität Potsdam, 2011. http://opus.kobv.de/ubp/volltexte/2011/5246/.

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The main objective of this thesis is to understand molecular crystallization as a multistep process with or without polymeric additives, including transient liquid-liquid phase separation, nanocrystal nucleation within the dense phase, and subsequent nanocrystal self-assembly or self-organization in sequence. The thesis starts with a quaternary model system, containing DL-Glutamic acid (Glu), polyethyleneimine (PEI), water, and EtOH, for the understanding of multistep precipitation of Glu with PEI as an additive. The experiments were performed by mixing Glu-PEI aqueous solution with a non-solv

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36

Yang, Huaiyu. "Investigations intothe crystallization of butyl paraben." Licentiate thesis, KTH, Teknisk strömningslära, 2011. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-34051.

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In thisproject, solubility of butyl paraben in 7 puresolvents and 5 ethanol aqueous solvents has been determined at from 1 ℃to 50 ℃. Thermodynamic properties of butyl paraben have been measured by DifferentialScanning Calorimetey. Relationship between molar solubility of butyl paraben in6 pure solvents and thermodynamic properties has been analyzed. Thisrelationship suggests a method of estimating activity of solute at equilibrium fromcombining solubility data with DSC measurements. Then, activity coefficient accordingto the solubility at different temperatures can be estimated. Duringthe solu

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37

Derakhshandeh, Maziar. "Crystallization of polypropylene : experiments and modeling." Thesis, University of British Columbia, 2015. http://hdl.handle.net/2429/55605.

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In this study, the quiescent crystallization of several polypropylenes (PPs) with different molecular characteristics was first examined using Differential Scanning Calorimetry (DSC) and Polarized Optical Microscopy (POM). The Avrami/Nakamura equation was employed to fit and predict crystallization kinetics under isothermal and non-isothermal conditions. The Avrami/Nakamura model was found to predict the non-isothermal crystallization data of the various PPs very well over a range of cooling rates. POM was used in line with a rotational rheometer to further examine the behaviour under quiescen

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38

Shore, Mark. "Cooling and crystallization of komatiite flows." Thesis, University of Ottawa (Canada), 1996. http://hdl.handle.net/10393/10267.

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Despite their $\sim$2710 Ma age, thin komatiite lava flows in Munro township, NE Ontario have sufficiently well-preserved primary structures, textures, mineralogy, and whole-rock geochemistry to constrain the physical processes of cooling and crystal growth. Seawater convection drove a cooling and fracturing front through the upper surface and was the dominant mechanism of heat loss, leading to pronounced textural asymmetry within flows. Large plate-like crystals of olivine in the upper layers of flows grew by constrained crystallization arising from strong thermal pradients and the high latti

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39

Ståhl, Marie. "Process modeling of semibatch reaction crystallization /." Stockholm : Kemiteknik, 2005. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-538.

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40

Lee, Chung-Kook. "Crystallization of Nano-sized barium ferrite." Diss., Georgia Institute of Technology, 1994. http://hdl.handle.net/1853/19920.

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41

Beard, Collen Alana. "Rubredoxin cobalt substitution and crystallization attempts." Thesis, Georgia Institute of Technology, 1989. http://hdl.handle.net/1853/29863.

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42

Lungu, Cristian 1968. "Crystallization behavior and kinetics of polyolefins." Thesis, McGill University, 2000. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=31061.

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In order to understand crystallization behavior and to predict polymer resin properties, crystallization kinetics and morphology studies are performed. Thermal analysis of sixteen polyethylene and polypropylene resins was carried out, using Differential Scanning Calorimetry (DSC) to study the crystallization kinetics and mechanism of crystallization. Attention is given to different polyethylene grades, particularly linear low-density polyethylenes (LLDPE) manufactured with Ziegler-Natta and metallocene catalysts. The polymers are obtained with different monomers (1-butene, 1-hexene or 1-octene

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43

Tiang, Jen. "Shear-induced crystallization of nucleated polymers." Thesis, McGill University, 2010. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=92255.

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Crystallization that occurs during or after a strong shear is important in polymer processing due to its strong effect on product properties and production rate. This study addresses several major gaps in our knowledge of this phenomenon by investigating shear-induced crystallization of nucleated isotactic polypropylenes by simultaneous measurement of light intensity and rheology using a sliding plate rheometer at high, uniform shear rates. An optical fiber probe was devised for the light intensity measurement. For the conditions studied, both measurements were found equally able to detect nas

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44

Keats, Clare J. "Crystallization and polymorphism of putative drugs." Thesis, University of Oxford, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.404167.

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45

Pratola, Federica. "Micro-mechanics of agglomerative crystallization processes." Thesis, University College London (University of London), 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.483559.

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46

Leukel, Sebastian [Verfasser]. "Crystallization via Amorphous Intermediates / Sebastian Leukel." Mainz : Universitätsbibliothek Mainz, 2018. http://d-nb.info/1172380783/34.

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47

Kulkarni, Chandrashekhar V. "In-Cubo Crystallization of Membrane Proteins." Thesis, Imperial College London, 2009. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.508495.

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48

Sinclair, D. M. "Crystallization of high silica molecular sieves." Thesis, University of Edinburgh, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.384262.

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49

Lai, Tsai-Ta Christopher. "Control of polymorphism in continuous crystallization." Thesis, Massachusetts Institute of Technology, 2016. http://hdl.handle.net/1721.1/104203.

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Thesis: Ph. D., Massachusetts Institute of Technology, Department of Chemical Engineering, 2016.<br>Cataloged from PDF version of thesis.<br>Includes bibliographical references.<br>Continuous manufacturing has gained significant interest in recent years as the ultra-lean mode of pharmaceutical production. Albeit the increasing number of studies on the process dynamics in continuous crystallization, in particular in yield improvement and impurity separation, the research community lacks the systematic understanding of the control of polymorphism in continuous crystallization. Variations in the

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50

Nasser, Paola B. (Paola Beatriz) 1979. "Remote microscope for Polymer Crystallization WebLab." Thesis, Massachusetts Institute of Technology, 2002. http://hdl.handle.net/1721.1/87281.

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Thesis (M.Eng.)--Massachusetts Institute of Technology, Dept. of Electrical Engineering and Computer Science, 2002.<br>Includes bibliographical references (leaves 65-66).<br>by Paola B. Nasser.<br>M.Eng.

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