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Autore: Grafiati

Pubblicato: 4 giugno 2021

Ultima modifica: 1 febbraio 2022

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1

Ghavipanje, Navid, Mohammad Hasan Fathi Nasri, Seyyed Homayoun Farhangfar, Seyyed Ehsan Ghiasi e Einar Vargas-Bello-Pérez. "Regulation of Nutritional Metabolism in Transition Dairy Goats: Energy Balance, Liver Activity, and Insulin Resistance in Response to Berberine Supplementation". Animals 11, n. 8 (29 luglio 2021): 2236. http://dx.doi.org/10.3390/ani11082236.

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The objectives of this study were to evaluate the alleviating effects of the isoquinoline alkaloid berberine (BBR) on the energy balance (EB), glucose and insulin metabolism, and liver functionality in transition dairy goats, as reflected by blood metabolites and enzymes. Twenty-four primiparous Saanen goats were randomly allocated to four groups. Goats in each group received, ad libitum, the same basal diet during the pre- and post-partum periods of evaluation. Goats received daily0, 1, 2, or 4 g BBR (coded as CON, BBR1, BBR2, and BBR4, respectively). Dry matter intake (DMI) and milk yield were recorded daily. Blood samples were collected on days −21, −14, −7, 0, 7, 14, and 21 relative to kidding, and individual body condition scores (BCSs) were also recorded. Supplementation with either BBR2 or BBR4 increased (p < 0.05) pre- and post-partum DMI, increasing (p < 0.05) the intakes of net energy for lactating and metabolizable proteins. BBR2 and BBR4 increased (p < 0.05) post-partum milk production as well as fat-corrected milk (FCM), energy-corrected milk (ECM), and feed efficiency, indicating the alleviating effect of BBR on the negative energy balance (NEB) in transition goats. The daily ingestion of either 2 or 4 g BBR reduced (p < 0.05) plasma aspartate aminotransferase (AST), alanine aminotransferase (ALT), and alkaline phosphatase (ALP) and increased (p < 0.05) the dynamic change in the liver activity index (LAI) and liver functionality index (LFI), implying its hepatoprotective effect on transition goats. Overall, the results suggest that BBR supplementation of at least 2 g/d may help to ameliorate insulin resistance (IR) and fat metabolism disorders initiated by the NEB in transition dairy goats.

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2

Ziegler, Georg, Erwin Haug, Wolfgang Frey e Willi Kantlehner. "Orthoamide, LVII [1]. Lassen sich aromatische Aldehyde nach Fries aus Arylformiaten hersteilen? / Orthoamides, LVII [1]. Can Aromatic Aldehydes be Prepared from Aryl Formates via the Fries Rearrangement?" Zeitschrift für Naturforschung B 56, n. 11 (1 novembre 2001): 1178–87. http://dx.doi.org/10.1515/znb-2001-1113.

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The aromatic hydroxyaldehydes 3a-3g, 5a-5f, 8 , 10 can be prepared by the action of BCl3, BBr3 or trifluoromethanesulfonic acid, on the aryl formates 1a-1f, 4a-e, 7, 9 via Fries rearrangement. BBr3 is more effective than BCl3. The activating ability of BBr3 can be improved by addition of FeCl3. Rearrangements which are induced by trifluoromethanesulfonic acid can give rise to the formations of regioisomers, which might be different from the products formed when the reaction is performed with Lewis acids. The yields of the aldehydes are lowered by subsequent condensation reactions. This view was confirmed by the isolation of a condensation product, which was characterized as a dibenzo[a,j]xanthene derivative 6 by crystal structure analysis. For the Fries rearrangement of formyl groups a new mechanism is proposed. 2-Hydroxy-1-naphthaldehyde 5c can be obtained in good yield from formic acid, BBr3, and 2 -naphthol.

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3

Wrackmeyer, Bernd, e Alexandra Glöckle. "Synthesis of Pentaalkyl-6-bromo-2,3,4,5-tetracarba-nido-hexaboranes(6)". Zeitschrift für Naturforschung B 51, n. 6 (1 giugno 1996): 859–64. http://dx.doi.org/10.1515/znb-1996-0616.

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Abstract Peralkylated 2,3,4,5-tetracarba-mdo-hexaboranes(6) 1 react with boron tribromide, BBr3, via selective exchange of the alkyl substituent in 6-position to give the corresponding new 6- bromo derivatives 2 in quantitative yield. The 6-iodo derivatives 2(1) can be prepared in the same way using BI3. Treatment of the carbaboranes 2 with Li Et3BH leads to the 1,2,3,4,5- pentaalkyl-2,3,4,5-tetracarba-inido-hexaboranes(6) 3. 1,3,4,6-Tetraethyl-2,3,4,5-tetracarbaw do-hexaborane(6) 4 reacts with BBr3 via degradation of the carbaborane cage to give EtBBr2, and (Z)-1,4-bis [bis(dibromoboryl)]-3-hexene 5. A new bis(diethylboryl)-substituted dialkenyl(bromo)borane 8 was prepared, but attem pts failed to convert it into a 1-bromo- or 6-bromo-mdo-C4B2-carbaborane. Treatment of 1,1-dialkyl-3-diethylboryl-4-ethylstannoles 9 with a large excess of BBr3 also affords 5, whereas 6-bromo-l,3,4-triethyl-2,3,4.5-tetracarbamdo- hexaborane(6) 11 was isolated in low yield (<5%) from the reaction between 9 and BBr3 (slight excess)

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4

Wong, Edwin W. Y., Deepak Dange, Lea Fohlmeister, Terrance J. Hadlington e Cameron Jones. "Extremely Bulky Amido and Amidinato Complexes of Boron and Aluminium Halides: Synthesis and Reduction Studies". Australian Journal of Chemistry 66, n. 10 (2013): 1144. http://dx.doi.org/10.1071/ch13175.

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An extremely bulky secondary amine, HN(Ar†)(SiPr3i) HL† (Ar† = C6H2{C(H)Ph2}2Pri−2,6,4) has been synthesised and deprotonated with KH in toluene, to afford the potassium amide [KL†(η6-toluene)], which was structurally authenticated. Reaction of this with BBr3 and AlBr3, reproducibly gave the crystallographically characterised amido bromo-borane, [L†B(H)Br], and aluminacycle, [AlBr2{κ2-C,N-N(H)(SiPr3i){C6H2[CPh2][C(H)Ph2]Pri-2,6,4}}], respectively, via ligand C–H activation processes. The known secondary amines, HN(Dip)(Mes) (HLMes) and HN(Dip)(Trip) (HLTrip) (Dip =2,6-diisopropylphenyl, Mes = mesityl, Trip = 2,4,6-triisopropylphenyl), have been structurally characterised, and deprotonated to give the in situ generated lithium amides, [Li(LMes)] and [Li(LTrip)]. Reaction of these with BBr3 and AlBr3 has given the amido group 13 element halide complexes, [LMesBBr2] and [LAlBr2(THF)] (L = LMes or LTrip), the crystal structures of all of which have been determined. Synthetic routes to two new bulky amidine pro-ligands, ArN = C(But)-N(H)Ar, Ar = C6H2{C(H)Ph2}2Me-2,6,4 (Piso*H) or C6H2Pr2i(CPh3)-2,6,4 (Piso″H), have been developed, and the compounds crystallographically characterised. Deprotonation of Piso″H gave the potassium amidinate, [K(Piso″)], which was reacted with BBr3 to give [(Piso″)BBr2]. Reaction of Piso″H with AlMe3 afforded [(Piso″)AlMe2], which, when treated with I2 yielded [(Piso″)AlI2], the crystal structure of which was determined. Reductions of all of the prepared amido and amidinato group 13 element(iii) halide complexes were attempted using a variety of reducing reagents, with a view to prepare boron(i) or aluminium(i) complexes. While these were not successful, this study does offer synthetic inorganic chemists a variety of new very bulky anionic N-donor ligands, and boron/aluminium halide complexes thereof, for use in their own research.

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5

Nguyen, Ngoc Hoa, Charles Cougnon e Frédéric Gohier. "Deprotection of Arenediazonium Tetrafluoroborate Ethers with BBr3". Journal of Organic Chemistry 74, n. 10 (15 maggio 2009): 3955–57. http://dx.doi.org/10.1021/jo8027906.

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6

Haupfear, E. A., e L. D. Schmidt. "Kinetics of boron deposition from BBR3 + H2". Chemical Engineering Science 49, n. 15 (agosto 1994): 2467–81. http://dx.doi.org/10.1016/0009-2509(94)e0051-q.

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7

Kijewska, Monika, Miłosz Siczek e Miłosz Pawlicki. "Reductive Dimerization of Macrocycles Activated by BBr3". Organic Letters 23, n. 9 (15 aprile 2021): 3652–56. http://dx.doi.org/10.1021/acs.orglett.1c01047.

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8

Mamedov, E. G. "Asymmetric Diels-Alder reaction of 1,3-butadienes with (−)-dimenthyl fumarate in the presence of BBr3 and BBr3·OEt2". Russian Journal of Organic Chemistry 43, n. 2 (febbraio 2007): 184–87. http://dx.doi.org/10.1134/s1070428007020054.

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9

Sitaram, A. R., S. P. Murarka e T. T. Sheng. "Grain growth in boron doped LPCVD polysilicon films". Journal of Materials Research 5, n. 2 (febbraio 1990): 360–64. http://dx.doi.org/10.1557/jmr.1990.0360.

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Dopant induced grain growth in LPCVD polysilicon films has been investigated using BBr3 as the diffusion source at 900 and 950 °C. TEM and sheet resistance measurements indicate rapid growth under such doping conditions. Results are compared with the grain growth observed during (a) PBr3 doping of similar films, and (b) during anneals in ambients containing 1% oxygen in nitrogen, similar to that used during BBr3 or PBr3 doping. The results clearly demonstrate the rapid grain growth induced by both types of dopants, although phosphorus is more effective in inducing this grain growth.

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10

Uchikawa, Yuki, Kazuya Tazoe, Syogo Tanaka, Xing Feng, Taisuke Matsumoto, Junji Tanaka e Takehiko Yamato. "Synthesis and demethylation of 4,22-dimethoxy[2.10]metacyclophan-1-yne with BBr3 to afford a novel [10](2,9)-5a,11a-benzofuro-5a-bora-11-bromochromenophane". Canadian Journal of Chemistry 90, n. 5 (maggio 2012): 441–49. http://dx.doi.org/10.1139/v2012-014.

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4,22-Dimethoxy[2.10]metacyclophan-1-yne was prepared by bromination of [2.10]metacyclophan-1-ene followed by the dehydrobromination of the bromine adduct with KOBu-t. Treatment of 4,22-dimethoxy[2.10]metacyclophan-1-yne with BBr3 in CH2Cl2 at room temperature led to the demethylation and a successive intramolecular cyclization reaction to afford a novel [10](2,9)-5a,11a-benzofuro-5a-bora-11-bromochromenophane in good yield. Similar treatment of a mixture of the corresponding meso- and dl-1,2-dibromo-4,22-dimethoxy[2.10]metacyclophane with BBr3 in CH2Cl2 under the same conditions described above afforded cis-4b,9b-dihydro[10]benzofuro[3,2-b]benzofuranophane in 83% yield.

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11

Zhang, Ming, e Ai-Qin Zhang. "Synthesis of Functionalised Zirconium Complexes". Journal of Chemical Research 2007, n. 6 (giugno 2007): 356–57. http://dx.doi.org/10.3184/030823407x227110.

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12

Kim, Inja, Tae-Hyun Kim, Youngjin Kang e Yong-beom Lim. "BBr3-promoted cyclization to produce ladder-type conjugated polymer". Tetrahedron Letters 47, n. 49 (dicembre 2006): 8689–92. http://dx.doi.org/10.1016/j.tetlet.2006.10.020.

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13

Weller, F., M. Möhlen e Κ. Dehnicke. "Crystal structure of tribromo-(triphenylphosphane)boron, (C6H5)3P-BBr3". Zeitschrift für Kristallographie - New Crystal Structures 212, n. 1 (1 dicembre 1997): 159–60. http://dx.doi.org/10.1524/ncrs.1997.212.1.159.

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14

Pasquini, Chiara, Alessandra Coniglio e Mauro Bassetti. "Controlled dealkylation by BBr3: efficient synthesis of para-alkoxy-phenols". Tetrahedron Letters 53, n. 46 (novembre 2012): 6191–94. http://dx.doi.org/10.1016/j.tetlet.2012.08.132.

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15

Tanaka, Shinya, Yuki Saito, Takaya Yamamoto e Tetsutaro Hattori. "Electrophilic Borylation of Terminal Alkenes with BBr3/2,6-Disubstituted Pyridines". Organic Letters 20, n. 7 (12 marzo 2018): 1828–31. http://dx.doi.org/10.1021/acs.orglett.8b00335.

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16

Ponsold, Kurt, e Horst Wagner. "Spaltung von 3-Methoxy-östra-1,3,5 (10)-trienen mit BBr3". Zeitschrift für Chemie 17, n. 2 (1 settembre 2010): 61. http://dx.doi.org/10.1002/zfch.19770170209.

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17

Kimura, Yuki, Ryo Kato, Kin-ichi Oyama, Tadao Kondo e Kumi Yoshida. "Efficient Preparation of Various O-Methylquercetins by Selective Demethylation". Natural Product Communications 11, n. 7 (luglio 2016): 1934578X1601100. http://dx.doi.org/10.1177/1934578x1601100722.

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penta-O-Methylquercetin (2) was prepared by permethylation of quercetin (1). Selective demethylation of 2 using either BBr3 or BCl3/TBAI ( tetra-butylammonium iodide) gave five O-methylquercetins (3-6), with satisfactory yields. The reaction can be easily scaled-up. We established an efficient and large-scale preparation of O-methylquercetins.

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18

Doerk, Gregory S., Gabriella Lestari, Fang Liu, Carlo Carraro e Roya Maboudian. "Ex situ vapor phase boron doping of silicon nanowires using BBr3". Nanoscale 2, n. 7 (2010): 1165. http://dx.doi.org/10.1039/c0nr00127a.

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19

Selvakumar, Jayaraman, Alexandros Makriyannis e Chinnasamy Ramaraj Ramanathan. "An unusual reactivity of BBr3: Accessing tetrahydroisoquinoline units from N-phenethylimides". Organic & Biomolecular Chemistry 8, n. 18 (2010): 4056. http://dx.doi.org/10.1039/c0ob00269k.

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20

Cramer, Richard C., John English, Bastien Bonef e James S. Speck. "BBr3 as a boron source in plasma-assisted molecular beam epitaxy". Journal of Vacuum Science & Technology A 37, n. 6 (dicembre 2019): 061502. http://dx.doi.org/10.1116/1.5117240.

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21

Chen, Luyang, Yunle Gu, Liang Shi, Jianhua Ma, Zeheng Yang e Yitai Qian. "Low-Temperature Synthesis of Nanocrystalline ZrB2via Co-reduction of ZrCl4and BBr3". Bulletin of the Chemical Society of Japan 77, n. 7 (luglio 2004): 1423–24. http://dx.doi.org/10.1246/bcsj.77.1423.

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22

Ingleson, Michael J. "Metal-free acyl-directed electrophilic C-H borylation using just BBr3". Science China Chemistry 62, n. 12 (8 novembre 2019): 1547–48. http://dx.doi.org/10.1007/s11426-019-9642-0.

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23

Fritz, Susanne, Erkan Emre, Josh Engelhardt, Stefanie Ebert, Nicolas Nowak, Jonathan Booth e Giso Hahn. "Contacting BBr3-based Boron Emitters with Aluminium-free Screen-printing Paste". Energy Procedia 92 (agosto 2016): 925–31. http://dx.doi.org/10.1016/j.egypro.2016.07.103.

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24

Bayer, Michael J., Thomas Müller, Wolfgang Lößlein, Hans Pritzkow e Walter Siebert. "Synthesen und Strukturen von 1,3,5-Trihalogeno-1,3,5-triboracyclohexan-Derivaten / Syntheses and Structures of 1,3,5-Trihalogeno-1,3,5-triboracyclohexane Derivatives". Zeitschrift für Naturforschung B 59, n. 7 (1 luglio 2004): 782–88. http://dx.doi.org/10.1515/znb-2004-0706.

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On heating bis(diiodoboryl)methane (1c) and 1,1-bis(diiodoboryl)alkanes 1i, l (alkane = propane, butane) under reduced pressure elimination of BI3 takes place and the corresponding 1,3,5-triiodo- 1,3,5-triboracyclohexane derivatives 2c; 2i, i’; 2l, l’ are formed. Starting with bis(dichloroboryl)- and bis(dibromoboryl)methane (1a, 1b) only small amounts of the trimerization products (H2C-BCl)3 (2a) and (H2C-BBr)3 (2b) are detectable which can not be separated from 1a,b and by-products. Reaction of 1,3,5-trichloro-2,4,6-trimethyl-1,3,5-triboracyclohexane (2d) with BBr3 provides the corresponding bromo derivative 2e in high yield. An attempt to react 2,4-bis(dichloroboryl)-3-chloro- 3-borapentane (4d) with 1,1-bis(trimethylstannyl)-2,2-diphenylethene does not lead to the expected trichloro-triboracyclohexane, but the divinylchloroborane ClB(CH=CPh2)2 6a, is formed. The compositions of the products follow from analytical data and X-ray structure analyses of 2i, 2c, 2e, and 6a.

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25

Roy, Chandra D. "Regiocontrolled Opening of 2-Methyltetrahydrofuran with Various Boron Reagents". Australian Journal of Chemistry 59, n. 9 (2006): 657. http://dx.doi.org/10.1071/ch06272.

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Regiocontrolled halogenative cleavage of 2-methyltetrahydrofuran with various B-bromoboranes, by a predominantly SN2-type mechanism favouring the formation of primary bromide, is described. A comparative study of the relative reactivities of BH2Br·SMe2, BHBr2·SMe2, BBr3, (MeO)2BBr, and MeOBBr2 revealed that the newly synthesized (MeO)2BBr is a highly promising regioselective reagent, especially at lower temperatures.

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26

Tuzina, Pavel, Andreas Fischer e Peter Somfai. "N-Benzyl-1-(dimethylamino)-2-methyl-1-oxopropan-2-aminium bromide". Acta Crystallographica Section E Structure Reports Online 62, n. 7 (23 giugno 2006): o2971—o2972. http://dx.doi.org/10.1107/s1600536806023026.

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The title compound, C13H21N2O+·Br−, was crystallized from a CH2Cl2 solution of N 2,N 2-dibenzyl-N,N,2-trimethylalaninamide and BBr3. The geometry of the cation is unexceptional. Intermolecular N—H...O and N—H...Br hydrogen bonds link two cations and two anions into a hydrogen-bonded cluster. The crystal packing is further stabilized by van der Waals forces.

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27

Olander, J., e K. Larsson. "Cubic boron nitride growth from NH3 and BBr3 precursors: a theoretical study". Diamond and Related Materials 11, n. 3-6 (marzo 2002): 1286–89. http://dx.doi.org/10.1016/s0925-9635(01)00739-7.

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28

Bains, Satinder, James Green, Choo Tan Lay, Richard M. Pagni e George W. Kabalka. "The conversion of carboxylic acids into acid bromides on BBr3-modified alumina". Tetrahedron Letters 33, n. 49 (1992): 7475–76. http://dx.doi.org/10.1016/s0040-4039(00)60799-2.

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29

Wu, Gaorong, Xiaopan Fu, Yangyang Wang, Kezuan Deng, Lili Zhang, Tao Ma e Yafei Ji. "C–H Borylation of Diphenylamines through Adamantane-1-carbonyl Auxiliary by BBr3". Organic Letters 22, n. 17 (21 agosto 2020): 7003–7. http://dx.doi.org/10.1021/acs.orglett.0c02552.

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30

Santiso-Quiñones, G., e I. Krossing. "Reference Values for the B-X Bond Lengths of BI3 and BBr3". Zeitschrift für anorganische und allgemeine Chemie 634, n. 4 (aprile 2008): 704–7. http://dx.doi.org/10.1002/zaac.200700510.

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31

KELDER, E. M., P. J. VAN DER PUT, J. G. M. BECHT e J. SCHOONMAN. "DEPOSITION OF CUBIC BORON MONOPHOSPHIDE FROM BBr3 AND PBr3 : A REACTION MECHANISM". Le Journal de Physique IV 02, n. C2 (settembre 1991): C2–201—C2–208. http://dx.doi.org/10.1051/jp4:1991225.

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32

Gu, Yunle, Luyang Chen, Yitai Qian e Wanqun Zhang. "Synthesis of Nanocrystalline BP via Benzene-Thermal Co-reduction of PCl3and BBr3". Bulletin of the Chemical Society of Japan 76, n. 7 (luglio 2003): 1469–70. http://dx.doi.org/10.1246/bcsj.76.1469.

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33

Tertykh, V. A., A. M. Varvarin, A. V. Simurov e L. A. Belyakova. "Structure of surface compounds formed during chemisorption of BBr3 on dehydrated Aerosil". Theoretical and Experimental Chemistry 25, n. 3 (maggio 1989): 349–52. http://dx.doi.org/10.1007/bf01299020.

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34

Maeda, Takeshi, Hyun Cho, Jin Hong e S. J. Pearton. "New plasma chemistries for etching III–V compound semiconductors: Bl3 and BBr3". Journal of Electronic Materials 28, n. 2 (febbraio 1999): 118–23. http://dx.doi.org/10.1007/s11664-999-0229-1.

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35

Wu, Gaorong, Binghan Pang, Yangyang Wang, Li Yan, Lu Chen, Tao Ma e Yafei Ji. "Metal-Free ortho-Selective C–H Borylation of 2-Phenylthiopyridines Using BBr3". Journal of Organic Chemistry 86, n. 8 (8 aprile 2021): 5933–42. http://dx.doi.org/10.1021/acs.joc.1c00520.

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36

Lohmüller, Elmar, Sabrina Lohmüller (née Werner), Nico Wöhrle, Udo Belledin e Andreas Wolf. "BBr3 diffusion with second deposition for laser-doped selective emitters from borosilicate glass". Solar Energy Materials and Solar Cells 186 (novembre 2018): 291–99. http://dx.doi.org/10.1016/j.solmat.2018.06.042.

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37

Li, Xuan, Jianghua He e Yuetao Zhang. "BBr3-Assisted Preparation of Aromatic Alkyl Bromides from Lignin and Lignin Model Compounds". Journal of Organic Chemistry 83, n. 18 (8 agosto 2018): 11019–27. http://dx.doi.org/10.1021/acs.joc.8b01628.

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38

Lee, Woo-Jin, Gye-Choon Park, Chel-Jong Choi e O.-Bong Yang. "Optimization of BBr3-Based Co-Diffusion Processes for Bifacial N-Type Solar Cells". Journal of Nanoscience and Nanotechnology 17, n. 4 (1 aprile 2017): 2682–84. http://dx.doi.org/10.1166/jnn.2017.13365.

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39

Bell, H. B., H. M. Anderson e R. W. Light. "Reactive Ion Etching of Aluminum/Silicon in BBr3 / Cl2 and BCl3 / Cl2 Mixtures". Journal of The Electrochemical Society 135, n. 5 (1 maggio 1988): 1184–91. http://dx.doi.org/10.1149/1.2095919.

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40

Sousa, Carla, e Pedro J. Silva. "BBr3-Assisted Cleavage of Most Ethers Does Not Follow the Commonly Assumed Mechanism". European Journal of Organic Chemistry 2013, n. 23 (31 maggio 2013): 5195–99. http://dx.doi.org/10.1002/ejoc.201300337.

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41

Sousa, Carla, e Pedro J. Silva. "BBr3-Assisted Cleavage of Most Ethers Does Not Follow the Commonly Assumed Mechanism". European Journal of Organic Chemistry 2013, n. 35 (14 novembre 2013): 8048–49. http://dx.doi.org/10.1002/ejoc.201301647.

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42

Selvakumar, Jayaraman, Alexandros Makriyannis e Chinnasamy Ramaraj Ramanathan. "ChemInform Abstract: An Unusual Reactivity of BBr3: Accessing Tetrahydroisoquinoline Units from N-Phenethylimides." ChemInform 42, n. 4 (30 dicembre 2010): no. http://dx.doi.org/10.1002/chin.201104155.

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43

BIEHL, H. "Vacuum ultraviolet fluorescence excitation spectroscopy of BBr3 in the range 8-20 eV". Molecular Physics 87, n. 5 (1 aprile 1996): 1199–215. http://dx.doi.org/10.1080/00268979650027090.

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44

Nie, Yong, Hans Pritzkow e Walter Siebert. "Synthesis and Structure of Pyrrolidinobromodiboranes(4)". Zeitschrift für Naturforschung B 60, n. 9 (1 settembre 2005): 1016–19. http://dx.doi.org/10.1515/znb-2005-0918.

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Abstract (sommario):

The reaction of tetrapyrrolidinodiborane(4) (1) with BBr3 in a 1:1 molar ratio yields a mixture of 1,2-dibromo-1,2- dipyrrolidinodiborane(4) (2) and bromotripyrrolidino- diborane( 4) (3), while a 1:2 molar ratio leads in Et2O to compound 2 as the main product along with a small amount of [(C4H8N)2B2Br3(OEt)] (4). The new compounds have been characterized by NMR and MS data, as well as by X-ray structure analyses of 2 and 4, of which the former exhibits an interesting polymorphism phenomenon.

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45

Cho, Hyun, J. Hong, T. Maeda, S. M. Donovan, C. R. Abernathy, S. J. Pearton e R. J. Shul. "Novel plasma chemistries for highly selective dry etching of InxGaN1−x: BI3 and BBr3". Materials Science and Engineering: B 59, n. 1-3 (maggio 1999): 340–44. http://dx.doi.org/10.1016/s0921-5107(98)00379-1.

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46

BAINS, S., J. GREEN, TAN L. C. TAN L. C., R. M. PAGNI e G. W. KABALKA. "ChemInform Abstract: The Conversion of Carboxylic Acids into Acid Bromides on BBr3-Modified Alumina." ChemInform 24, n. 17 (20 agosto 2010): no. http://dx.doi.org/10.1002/chin.199317128.

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47

Tsuge, Akihiko, Tsuyoshi Sawada, Shuntaro Mataka, Nobuaki Nishiyama, Hirofumi Sakashita e Masashi Tashiro. "Isolation, characterization, and demethylation by BBr3 of two conformers of 8,15,23-trimethoxy[2,2.1]metacyclophane". Journal of the Chemical Society, Chemical Communications, n. 15 (1990): 1066. http://dx.doi.org/10.1039/c39900001066.

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48

Kosak, Talon M., Heidi A. Conrad, Andrew L. Korich e Richard L. Lord. "Ether Cleavage Re-Investigated: Elucidating the Mechanism of BBr3-Facilitated Demethylation of Aryl Methyl Ethers". European Journal of Organic Chemistry 2015, n. 34 (23 ottobre 2015): 7460–67. http://dx.doi.org/10.1002/ejoc.201501042.

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49

McNevin, S. C. "A thermochemical model for the plasma etching of aluminum in BCl3/Cl2 and BBr3/Br2". Journal of Vacuum Science & Technology B: Microelectronics and Nanometer Structures 8, n. 6 (novembre 1990): 1212. http://dx.doi.org/10.1116/1.584897.

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50

Cholet, V., R. Herbin e L. Vandenbulcke. "Chemical vapour deposition of boron carbide from BBr3CH4H2 mixtures in a microwave plasma". Thin Solid Films 188, n. 1 (luglio 1990): 143–55. http://dx.doi.org/10.1016/0040-6090(90)90200-w.

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