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Littérature scientifique sur le sujet « Thermal and fire resistance of aeronautic resins »
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Articles de revues sur le sujet "Thermal and fire resistance of aeronautic resins"
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Raimondo, M., S. Russo, L. Guadagno, P. Longo, S. Chirico, A. Mariconda, L. Bonnaud, O. Murariu et Ph Dubois. « Effect of incorporation of POSS compounds and phosphorous hardeners on thermal and fire resistance of nanofilled aeronautic resins ». RSC Advances 5, no 15 (2015) : 10974–86. http://dx.doi.org/10.1039/c4ra11537f.
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Barra, Giuseppina, Liberata Guadagno, Luigi Vertuccio, Bartolome Simonet, Bricio Santos, Mauro Zarrelli, Maurizio Arena et Massimo Viscardi. « Different Methods of Dispersing Carbon Nanotubes in Epoxy Resin and Initial Evaluation of the Obtained Nanocomposite as a Matrix of Carbon Fiber Reinforced Laminate in Terms of Vibroacoustic Performance and Flammability ». Materials 12, no 18 (16 septembre 2019) : 2998. http://dx.doi.org/10.3390/ma12182998.
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Different industrial mixing methods and some of their combinations ((1) ultrasound; (2) mechanical stirring; (3) by roller machine; (4) by gears machine; and (5) ultrasound radiation + high stirring) were investigated for incorporating multi-walled carbon nanotubes (MWCNT) into a resin based on an aeronautical epoxy precursor cured with diaminodiphenylsulfone (DDS). The effect of different parameters, ultrasound intensity, number of cycles, type of blade, and gear speed on the nanofiller dispersion were analyzed. The inclusion of the nanofiller in the resin causes a drastic increase in the viscosity, preventing the homogenization of the resin and a drastic increase in temperature in the zones closest to the ultrasound probe. To face these challenges, the application of high-speed agitation simultaneously with the application of ultrasonic radiation was applied. This allowed, on the one hand, a homogeneous dispersion, and on the other hand, an improvement of the dissipation of heat generated by ultrasonic radiation. The most efficient method was a combination of ultrasound radiation assisted by a high stirring method with the calendar, which was used for the preparation of a carbon fiber reinforced panel (CFRP). The manufactured panel was subjected to dynamic and vibroacoustic tests in order to characterize structural damping and sound transmission loss properties. Under both points of view, the new formulation demonstrated an improved efficiency with reference to a standard CFRP equivalent panel. In fact, for this panel, the estimated damping value was well above the average of the typical values representative of the carbon fiber laminates (generally less than 1%), and also a good vibroacoustic performance was detected as the nanotube based panel exhibited a higher sound transmission loss (STL) at low frequencies, in correspondence with the normal mode participation region. The manufactured panel was also characterized in terms of fire performance using a cone calorimeter and the results were compared to those obtained using a commercially available monocomponent RTM6 (Hexcel composites) epoxy aeronautic resin with the same process and the same fabric and lamination. Compared to the traditional RTM6 resin, the panel with the epoxy nanofilled resin exhibits a significant improvement in fire resistance properties both in terms of a delay in the ignition time and in terms of an increase in the thermal resistance of the material. Compared to the traditional panel, made in the same conditions as the RTM6 resin, the time of ignition of the nanotube-based panel increased by 31 seconds while for the same panel, the heat release rate at peak, the average heat release rate, and the total heat release decreased by 21.4%, 48.5%, and 15%, respectively. The improvement of the fire performance was attributed to the formation of a non-intumescent char due to the simultaneous presence of GPOSS and carbon nanotubes.
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FAINLEIB, A. M. « BIO-BASED CYANATE ESTER RESINS AND THERMOSTABLE POLYMER NETWORKS DERIVED THEREOF. MINI REVIEW ». Polymer journal 44, no 2 (20 juin 2022) : 93–100. http://dx.doi.org/10.15407/polymerj.44.02.093.
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This article is devoted to a review of the literature on a very promising direction in the chemistry of macromolecular compounds: the synthesis and study of polymers, more specifically, high performance polycyanurates based on bis(poly)phenols) of natural origin. Cyanate Ester Resins (CER) are characterized by a very regular structure of the polymer networks, namely polycyanurates (PCNs), obtained by their polycyclotrimerization. They have received much attention because of their unique combination of physical properties, including high thermal stability (> 400 °C), high glass transition temperature (> 270 °C), high fire-, radiation and chemical resistance, low water absorption and low outgassing, high adhesion to different substrates and excellent dielectric properties (ε=2,64−3,11). As a result, CER are currently used as structural or functional materials in aeronautics, space (composite strakes, fins, nose radomes, heat shields), printed circuit boards, adhesives etc. It has to be noted here that CER thermosetting resins, expanding the high-temperature operations regimes, are produced from synthetic petroleum-derived bisphenols, such as bisphenol A, which are toxic and dangerous for environment. In the past decade, naturally occurring phenolic derivatives have arisen as attractive precursors for developing new materials from renewable bio-sources for use in eco-friendly processes. Resins have been prepared utilizing either the whole liquid product or a phenolic-enriched fraction obtained after fractional condensation or further processing, such as solvent extraction or use of greener extraction methods. However, to date, none of the phenolic production and fractionation techniques has been utilized to allow for substitution of 100% of the phenol content of the resin without impacting its effectiveness compared to commercial formulations based on petroleum-derived phenol. The variable nature of the percentage of phenolic compounds in terms of purity from different batches of crops from one season to another and geographical influence does not allow from the reproducibility of phenolic compounds, and hence the resulting polymers. However, the direction that needs to be explored should be oriented towards complete replacement of petro-based phenolics with bio-based ones in the face of an urgent petroleum crisis. In addition, there is a necessity for materials showing enhanced applicability and improved performance. It is a beginning of the era of such a step, which requires further exploration of natural phenolic sources aimed at their enhanced utilization.
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Grange, Nathan, Pietro Tadini, Khaled Chetehouna, Nicolas Gascoin, Guillaume Bouchez, Samuel Senave et Isabelle Reynaud. « Experimental determination of fire degradation kinetic for an aeronautical polymer composite material ». International Journal of Structural Integrity 9, no 1 (5 février 2018) : 76–92. http://dx.doi.org/10.1108/ijsi-03-2017-0021.
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Purpose The purpose of this paper is to evaluate the fire resistance of an innovative carbon-reinforced PEKK composite for aeronautical applications. To this end, thermal degradation analysis under inert and oxidative atmosphere is carried out. Moreover, a linear model fitting approach is compared to a generally used isoconversional method to validate its reliability for kinetic triplet estimation. Design/methodology/approach Thermogravimetric analysis carried out under inert and oxidative atmospheres, between 25 and 1000°C for three different heating rates (5, 15, 25°C/min), followed by a qualitative SEM observation of the samples before and after thermal treatment. After the reaction identification by TG/DTG curves, an isoconversional analysis is carried out to estimate the activation energy as a function of the reaction conversion rate. For the identified reactions, the kinetic triplet is estimated by different methods and the results are compared to evaluate their reliability. Findings In inert case, one global reaction, observed between 500-700°C, seems able to describe the degradation of carbon-PEKK resin. Under oxidative atmosphere, three main reactions are identified, besides the resin degradation, the other two are attributed to char and fiber oxidation. Good agreement achieved between isoconversional and linear model fitting methods in activation energy calculation. The achieved results demonstrate the high thermal resistance of PEKK associated with the ether and ketone bonds between the three aromatic groups of its monomer. Originality/value This paper provides a possible degradation model useful for numerical implementation in CFD calculations for aircraft components design, when exposed to high temperatures and fire conditions.
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Chtourou, Halim, Abdelatif Atarsia et Bo Fisa. « Prediction of Thermal and Fire Resistance of Phenolic Resins by Dynamic TG Analysis ». Journal of Reinforced Plastics and Composites 18, no 4 (mars 1999) : 339–45. http://dx.doi.org/10.1177/073168449901800404.
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De Aloysio, Giulia, Mattia Morganti, Luca Laghi, Matteo Scafè, Enrico Leoni, Claudio Mingazzini et Stefano Bassi. « Characterization in expected working environments of recyclable fire-resistant materials ». MATEC Web of Conferences 349 (2021) : 01009. http://dx.doi.org/10.1051/matecconf/202134901009.
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This study focuses on the development of multi-material solutions for fire-resistant structural materials for transport and thermal insulation in the construction field. Special attention was paid to combining recyclable and bio-mass derived raw materials without interfering with an easy end-of-life separation, recycling and reuse. Fire-resistant biomass derived resins were associated with basalt derived Mineral Fibres (BDMF) in the form of prepregs, which were studied as semi-finished materials. Fire-resistance was obtained by associating these prepregs with thin gres tiles in the case of fire-resistant thermal insulating facades and with aluminum layers (giving origin to Fibre Metal Laminates-FML) in the case of structural components for transport applications. Thermophysical characterization of the solutions was carried out to assess both thermal conductivity and thermal diffusivity. Fire resistance tests were performed on FML to determine the number of Al layers needed to ensure fire resistance. Results suggest that fire resistance depends primarily on the number of Al layers, rather than on their thickness. Accelerated ageing tests (salty mist and freeze-thaw) were executed to predict durability in the expected working conditions. Results suggest a durability issue in FML with preceramic interface in salty environments.
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Zielecka, Maria, Anna Rabajczyk, Krzysztof Cygańczuk, Łukasz Pastuszka et Leszek Jurecki. « Silicone Resin-Based Intumescent Paints ». Materials 13, no 21 (27 octobre 2020) : 4785. http://dx.doi.org/10.3390/ma13214785.
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Silicone resins are widely applied as coating materials due to their unique properties, especially those related to very good heat resistance. The most important effect on the long-term heat resistance of the coating is connected with the type of resin. Moreover, this structure is stabilized by a chemical reaction between the hydroxyl groups from the organoclay and the silicone resin. The novel trends in application of silicone resins in intumescent paints used mostly for protection of steel structures against fire will be presented based on literature review. Some examples of innovative applications for fire protection of other materials will be also presented. The effect of silicone resin structure and the type of filler used in these paints on the properties of the char formed during the thermal decomposition of the intumescent paint will be discussed in detail. The most frequently used additives are expanded graphite and organoclay. It has been demonstrated that silicate platelets are intercalated in the silicone matrix, significantly increasing its mechanical strength and resulting in high protection against fire.
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Nguyen, Tuan Anh, et Thi Thu Trang Bui. « Study the Effects of Carbon Nanotubes and Graphene Oxide Combinations on the Mechanical Properties and Flame Retardance of Epoxy Nanocomposites ». Journal of Nanomaterials 2021 (27 décembre 2021) : 1–9. http://dx.doi.org/10.1155/2021/1437929.
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Carbon-based fillers have attracted a lot of interest in polymer composites because of their ability to alter beneficial properties at low filler concentrations, good surface bonding with polymers, availability in different forms, etc. Carbon-based materials (such as fullerene, CNTs, graphene, and graphite) have been studied as fillers with enhanced fire resistance to epoxy resins. In order to reduce the flammability and improve the thermal stability of epoxy resin-based nanocomposite materials, which can be achieved by a simultaneous combination of graphene oxide and multiwall carbon nanotubes, the graphite oxide (GO) epoxy nanomaterial was developed by 1% wt.% GO combined with 0.02 wand 0.04 wt.% MWCNT. The homogeneous dispersion of GO and MWCNTs in epoxy resins is supported by ultrasonic vibrations. The results showed that when nanocomposite materials were present at the same time MWCNTs and GO, their mechanical properties and fire resistance were significantly improved. Nanomaterials are characterized by FT-IR spectroscopy and SEM imaging, mechanical strength, and flame retardant properties (LOI, UL94).
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Dowbysz, Adriana, Mariola Samsonowicz et Bożena Kukfisz. « Recent Advances in Bio-Based Additive Flame Retardants for Thermosetting Resins ». International Journal of Environmental Research and Public Health 19, no 8 (15 avril 2022) : 4828. http://dx.doi.org/10.3390/ijerph19084828.
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Thermosetting resins are used in many applications due to their great mechanical properties, chemical resistance, and dimensional stability. However, the flammability of thermosets needs to be improved to minimize fire risk and meet fire safety regulations. Some commercially available flame retardants have an adverse effect on people’s health and the environment. Thus, the development of novel, more sustainable flame retardants obtained or derived from biomass has become an objective of contemporary research. The objective of this study is to summarize recent progress on bio-based flame retardants for thermosetting resins so as to promote their prompt development. Groups of biomass compounds with a potential for flame retardant industrial applications were introduced, and their thermal degradation was investigated. The authors focused mostly on the thermal degradation of composites containing bio-based flame retardants determined by thermogravimetric analysis, their tendency to sustain a flame determined by a limiting oxygen index, and fire behavior determined by a cone calorimeter test. The results showed that the mode of action is mostly based on the forming of the char layer. However, in many cases, there is still a necessity to input a high amount of additive to achieve significant flame retardancy effects, which may adversely impact mechanical properties.
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Sayin, Baris, et Erdem Damcı. « A Numerical Evaluation of Insulated CFRP-Strengthened RC Beams Exposed to Fire ». Advanced Materials Research 742 (août 2013) : 62–69. http://dx.doi.org/10.4028/www.scientific.net/amr.742.62.
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There are mainly two approaches to improve the fire resistance of FRP systems. While the most common way is to protect or insulate the FRP systems, the other way is to use fibers and resins with better fire-performance. In this paper a numerical investigation for evaluating the fire behavior of insulated CFRP-strengthened RC beams is presented.The effects of external loading and thermal expansion of materials in both the structural and the thermal behavior of composite elements due to loading and elevated temperatures are taken into consideration in a finite element model. The validity of the numerical model isdemonstrated withthe results from an existing experimental study on insulated CFRP-strengthened RC beam. The conclusions of this investigation have been employed to predict the structural behavior of concrete structures successfully.
Thèses sur le sujet "Thermal and fire resistance of aeronautic resins"
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Raimondo, Marialuigia. « Improving the aircraft safety by advanced structures and protecting nanofillers ». Doctoral thesis, Universita degli studi di Salerno, 2014. http://hdl.handle.net/10556/1480.
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2012 - 2013Inspection and Maintenance are important aspects when considering the availability of aircraft for revenue flights. Modern airframe design is exploiting new exciting developments in materials and structures to construct ever more efficient air vehicle able to enable efficient maintenance. The improvement in the aircraft safety by advanced structures and protecting nanofillers is a revolutionary approach that should lead to the creation of novel generation of multifunctional aircraft materials with strongly desired properties and design flexibilities. In recent years, the development of new nanostructured materials has enabled an evolving shift from single purpose materials to multifunctional systems that can provide greater value than the base materials alone; these materials possess attributes beyond the basic strength and stiffness that typically drive the science and engineering of the material for structural systems. Structural materials can be designed to have integrated electrical, electromagnetic, flame resistance, and possibly other functionalities that work in synergy to provide advantages that reach beyond that of the sum of the individual capabilities. Materials of this kind have tremendous potential to impact future structural performance by reducing size, weight, cost, power consumption and complexity while improving efficiency, safety and versatility. It is a well-known fact that, actually, also a very advanced design of an aircraft has to take required inspection intervals into account. An aircraft with inherent protective abilities could help to significantly extend the inspection intervals, thereby increasing aircraft availability. The challenge in this research is to develop and apply a multifunctional composite for structural applications. The aim of this project is the formulation, preparation and characterization of structural thermosetting composites containing dispersed protective nanofillers. This project specifically targets composites tailored for multifunctional applications such as lightning strike protection, and flame resistance. These composites were designed to enable their application on next generation aircrafts. With regard to the objectives of this PhD project the multifunctional composite systems were developed with the aim of overcoming the following drawbacks of the composite materials: • reduced electrical conductivity; • poor flame resistance. The thermosetting material was projected considering compatibility criteria so that to integrate different functions into a material that is capable of bearing mechanical loads and serves as a structural material element. [edited by author]
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Actes de conférences sur le sujet "Thermal and fire resistance of aeronautic resins"
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Živković, Andreja, Nataša Tomić, Marija Vuksanović et Aleksandar Marinković. « Synthesis and characterization of epoxy resin coating with improved fire resistance by the addition of modified tannic acid ». Dans 8th International Conference on Renewable Electrical Power Sources. SMEITS, 2020. http://dx.doi.org/10.24094/mkoiee.020.8.1.35.
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The paper presents a new process for obtaining eco-epoxide materials with reduced combustibility or completely non-combustible, which are synthesized from bio-renewable raw materials, whose production process consists of two stages. A particular aspect of multiple environmental significance is the use of bio-renewable resources and the reduction of the share of the toxic epoxy component in the production of epoxy materials. The first stage considers the synthesis epoxy resin components: epoxy functionalized tannic acid (TA) – ETA, and synthesis of phosphate derivatives of TA - glycidyl ester of TA modified by phosphoric acid (PGET). The second stage considers the synthesis of bio-epoxy resins using ETA and PGET that are used as a replacement of the epoxy resin component (A) – bisphenol A based epoxy in a ratio 25-100% as a reactive diluent to obtain products that can be used in the construction and other industrial fields and have reduced combustibility or completely non-combustible. The second part presents the results of thermal and mechanical tests for some of the obtained derivatives. The addition of 25% of TA derivate improved the toughness as well as the tensile strength of epoxy material. Thermogravimetry showed that samples containing tannin epoxide showed more residue left. Partial or full replacement of the epoxy component with a tannin component produces eco-friendly material with while significantly increased fire resistance (V-2 to V-0).