Artículos de revistas: "Liquid chromatography"

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Zhang, Jing y Hongye Zhang. "Research progress on the detection of water-soluble vitamins in food using liquid chromatography". Theoretical and Natural Science 37, n.º 1 (4 de junio de 2024): 158–69. http://dx.doi.org/10.54254/2753-8818/37/20240183.

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Currently, liquid chromatography is widely used for the analysis and determination of water-soluble vitamins (WSVs) in functional foods. However, due to the diversity of sample characteristics and the requirement for purification accuracy, the chromatographic conditions and specific methods used vary. This paper reviews the chromatographic conditions of liquid chromatography techniques for detecting WSVs in food, as well as the selection of liquid chromatography methods in different application fields. The chromatographic conditions include chromatographic columns, column temperature, mobile phase, flow rate, and elution gradient, and the application scope of different chromatographic conditions is compared. Liquid chromatography methods include high-performance liquid chromatography and liquid chromatography-tandem mass spectrometry, and discussions are made on the applications and prospects of these two methods under different chromatographic conditions. Therefore, this review provides research insights into different chromatographic conditions and methods for food quality inspection and biochemical analysis research.

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Adel, E. Ibrahim, Elhenawee Magda, Saleh Hanaa y M. Sebaiy Mahmoud. "Overview on liquid chromatography and its greener chemistry application". Annals of Advances in Chemistry 5, n.º 1 (7 de abril de 2021): 004–12. http://dx.doi.org/10.29328/journal.aac.1001023.

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This literature review is concerning with liquid chromatography specifically high performance liquid chromatography (HPLC), Ultra high performance liquid chromatography (UHPLC), chromatography theory, chromatographic parameters, monolithic columns, principles of green chemistry and its application ingreen chromatography.

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Yatsenko, Larisa Anatolyevna, Maria Yurevna Printseva, Ilya Danilovich Cheshko y Artur Alexandrovich Tumanovsky. "Detection of residues and determination of the composition of combustible components in case of explosions of vapor-gas-air mixtures". Technology of technosphere safety 97 (2022): 51–60. http://dx.doi.org/10.25257/tts.2022.3.97.51-60.

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Introduction. Liquefied hydrocarbon gases (LHG) are widely used in various fields. The main components of LHG are: propane, isobutane and n-butane, which are not only combustible, but also explosive gases capable of detonation combustion. The detection of LHG in the air is a very urgent task in expert studies. To determine the component composition of various flammable liquids, for the purpose of their identification, chromatographs equipped with a capillary quartz column with a phase that allows detecting saturated hydrocarbons of the homologous series from pentane to pentatetracontane inclusive are used in the Forensic Expertise Institutions of Federal Fire Service of EMERCOM of Russia. However, it is not possible to analyze the component composition of lighter hydrocarbons according to the previously proposed and used in expert practice method for detecting and studying flammable liquids/high liquids under these conditions. To solve the problem of unification of the use of the instrumental base for the detection of residues of flammable liquids, liquid liquids and light hydrocarbons, new chromatography conditions were selected using the existing equipment set. Goals and objectives. The aim of the study is to select the analysis conditions for detecting the remains of liquefied hydrocarbon gases after explosions of steam-air mixtures on the basis of the instrumental gas chromatographic complex in service with the Forensic Expertise Institutions of Federal Fire Service of EMERCOM of Russia. Research methods. To detect and determine the composition of residues of combustible components during explosions of vapor-gas-air mixtures, a hardware-software instrumental complex based on a gas-liquid chromatograph equipped with a flame ionization detector, a ZB-50 capillary column, and an attachment from a two-stage thermal desorber was used. Results and its discussion. In the course of the study, the optimal conditions for conducting gas chromatographic analysis were defined and selected in order to detect liquefied hydrocarbon gases. Recommended pressures are given for various carrier gases. It is shown that, by varying the pressure and inlet temperature, light hydrocarbons propane, butane, isobutane is fairly well separated on a gas-liquid chromatograph with a flame ionization detector and on a ZB-50 capillary column 30 meters long. Conclusion. The research shows that the problem of combining a hardware-software instrumental complex based on a gas chromatograph with an attachment from a two-stage thermal desorber used for the analysis of two groups of substances (liquefied hydrocarbons and flammable liquids, gas liquids) is solved by varying the pressure and temperature of the input. Keywords: gas-liquid chromatography, thermal desorption, liquefied petroleum gases, light hydrocarbons, air-fuel mixtures, vapor-gas-air mixtures, explosion, fire examination.

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Kazantseva, I. L., V. V. Egorova y D. M. Osokin. "Application of Chromatographic Methods in Forensic Examination of Wine Products". Theory and Practice of Forensic Science 19, n.º 2 (26 de julio de 2024): 40–48. http://dx.doi.org/10.30764/1819-2785-2024-2-40-48.

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. The article overviews the changes in the Russian legislation regarding the terminology and classification of wine products, which should be considered when solving diagnostic and classification problems within the framework of complex examinations (commodity expertise of food products and forensic examination of materials, substances and products of alcoholcontaining liquids). The authors stress the importance and relevance of chromatographic methods in wine products examination. They also present the results of testing a method for organic acids determination in wine using JetChrom liquid chromatograph. Some examples are given from expert practice regarding the use of the gas chromatographic methods for analyzing the composition of toxic micro-impurities of base alcohol liquids and the high-performance liquid chromatography method for analyzing the composition of organic acids of the objects under research.

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Meng, Xin Xin y Shu Lin Yang. "Comparison of Gas Chromatography and Liquid Chromatogram Detecting Pesticide Residue". Applied Mechanics and Materials 539 (julio de 2014): 113–16. http://dx.doi.org/10.4028/www.scientific.net/amm.539.113.

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The existing methods of detecting pesticide residue include gas chromatography, high performance liquid chromatography, gas chromatograph-mass, liquid chromatograph-mass, capillary electrophoresis, radioimmunoassay, biosensor and rapid detection on the spot. The paper analyzes the comparison of gas chromatography and liquid chromatogram detecting pesticide residue, for achieving the development tendency and the future goal of analyzing pesticide residue.

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Durai Ananda Kumar T, Sai Charan, Venkateswarlu A y Supriya Reddy K. "Evolution of liquid chromatography: Technologies and applications". International Journal of Research in Pharmaceutical Sciences 11, n.º 3 (8 de julio de 2020): 3204–11. http://dx.doi.org/10.26452/ijrps.v11i3.2449.

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Liquid chromatographic offers efficient analyte separation employing high pressure pumps. The reversed phase high performance liquid chromatography (RP-HPLC) is widely utilized in the purity testing and quantitative determination of pharmaceuticals and neutraceuticals. The limitations of traditional liquid chromatography such as particle size, resolution and selectivity demanded for the developments and Waters Corporation developed ultraperformance liquid chromatography (UPLC). Ultrafast liquid chromatography (UFLC) is another milestone, which offers faster and efficient separation. Multidimensional UHPLC provides separation of complex molecules. The particle size decrease enhances the resolution of LC separation. Ethylene bridged hybrid (BEH), Charged surface hybrid (CSH) and Peptide separation technology (PST) offer better performance in. The amalgamation of chromatographic and spectroscopic detectors namely fluorescence detector (FD) and mass spectrometry (MS) provides efficient separation. Liquid chromatography (LC) offers the analysis of pharmaceuticals, biological, food materials, and natural products. This review covers technologies and recent pharmaceutical and biomedical applications of liquid chromatography technologies

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Custodio-Mendoza, Jorge Antonio, Patryk Pokorski, Havva Aktaş, Alicja Napiórkowska y Marcin Andrzej Kurek. "Advances in Chromatographic Analysis of Phenolic Phytochemicals in Foods: Bridging Gaps and Exploring New Horizons". Foods 13, n.º 14 (18 de julio de 2024): 2268. http://dx.doi.org/10.3390/foods13142268.

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Chromatographic analysis of phenolic phytochemicals in foods has significantly advanced over the past decade (2014–2024), meeting increasing demands for precision and efficiency. This review covers both conventional and advanced chromatographic techniques used for detecting phenolic phytochemicals in foods. Conventional methods like High-Performance Liquid Chromatography, Ultra High-Performance Liquid Chromatography, Thin-Layer Chromatography, and Gas Chromatography are discussed, along with their benefits and limitations. Advanced techniques, including Hydrophilic Interaction Liquid Chromatography, Nano-LC, Multidimensional Liquid Chromatography, and Capillary Electrophoresis, are highlighted for their innovations and improved capabilities. The review addresses challenges in current chromatographic methods, emphasizing the need for standardized and validated procedures according to the Food and Drug Administration, European Cooperation for Accreditation of Laboratories, and The International Organization for Standardization guidelines to ensure reliable and reproducible results. It also considers novel strategies for reducing the environmental impact of chromatographic methods, advocating for sustainable practices in analytical chemistry.

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8

Peterson, Robert E., Gail M. Shannon y Odette L. Shotwell. "Purification of Cyclopiazonic Acid by Liquid Chromatography". Journal of AOAC INTERNATIONAL 72, n.º 2 (1 de marzo de 1989): 332–35. http://dx.doi.org/10.1093/jaoac/72.2.332.

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Abstract A purification procedure for cyclopiazonic acid has been developed, using sequential preparative and semi-preparative liquid chromatography. Crude cyclopiazonic acid (324 mg) was extracted from a 1 L fermentation medium with chloroform-methanol (80 + 20), dried, dissolved in chloroform, and chromatographed on an oxalic acid/ silica preparative column with chloroform-methanol (99 + 1) as the eluant. A semi-preparative oxalic acid/silica column and chloroform- methanol (99.5 + 0.5) were then used for rechromatography of the partially purified cyclopiazonic acid. This second chromatographic treatment yielded fractions from which cyclopiazonic acid was readily crystallized (106.7 mg; 33% recovery). Analytical chromatography was developed using an amino column in an ion-exchange mode, with a methanol-phosphate buffer eluant. Response was linear from 10 to 800 μg/injection of standard solutions. Cyclopiazonic acid chemically binds sodium from soda-lime vials.

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9

Tong, Daixin, Keith D. Bartle, Anthony A. Clifford y Robert E. Robinson. "Unified chromatograph for gas chromatography, supercritical fluid chromatography and micro-liquid chromatography". Analyst 120, n.º 10 (1995): 2461. http://dx.doi.org/10.1039/an9952002461.

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Hammack, Walter, Mary C. Carson, Barbara K. Neuhaus, Jeffrey A. Hurlbut, Cristina Nochetto, James S. Stuart, Amy Brown et al. "Multilaboratory Validation of a Method To Confirm Chloramphenicol in Shrimp and Crabmeat by Liquid Chromatography-Tandem Mass Spectrometry". Journal of AOAC INTERNATIONAL 86, n.º 6 (1 de noviembre de 2003): 1135–43. http://dx.doi.org/10.1093/jaoac/86.6.1135.

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Abstract An existing method for chloramphenicol (CAP) determination in shrimp using a gas chromatograph with electron capture detector was adapted for confirmation of CAP with a liquid chromatograph interfaced to a triple quadrupole mass spectrometer. CAP residues are extracted from tissue with ethyl acetate, isolated via liquid–liquid extraction, and concentrated by evaporation. Extracts are chromatographed by using a reversed-phased column and analyzed by electrospray negative mode tandem mass spectrometry. Four product ions (m/z 152, 176, 194, and 257) of precursor m/z 321 were monitored. Moving from gas chromatography to liquid chromatography–tandem mass spectrometry improved the sensitivity of the method greatly, enabling reliable confirmation of CAP residues at 0.3 μg/kg (ppb). The method meets confirmation criteria recommended by the U.S. Food and Drug Administration and 4-point identification criteria established by the European Union. With slight modifications to accommodate different equipment, the method was validated in 3 laboratories.

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11

Christopoulou, C. N. y E. G. Perkins. "Chromatographic studies on fatty acid dinners: Gas-liquid chromatography, high performance liquid chromatography and thin-layer chromatography". Journal of the American Oil Chemists' Society 66, n.º 9 (septiembre de 1989): 1353–59. http://dx.doi.org/10.1007/bf03022761.

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El Deeb, Sami. "Enhancing Sustainable Analytical Chemistry in Liquid Chromatography: Guideline for Transferring Classical High-Performance Liquid Chromatography and Ultra-High-Pressure Liquid Chromatography Methods into Greener, Bluer, and Whiter Methods". Molecules 29, n.º 13 (5 de julio de 2024): 3205. http://dx.doi.org/10.3390/molecules29133205.

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This review is dedicated to sustainable practices in liquid chromatography. HPLC and UHPLC methods contribute significantly to routine analytical techniques. Therefore, the transfer of classical liquid chromatographic methods into sustainable ones is of utmost importance in moving toward sustainable development goals. Among other principles to render a liquid chromatographic method green, the substitution of the organic solvent component in the mobile phase with a greener one received great attention. This review concentrates on choosing the best alternative green organic solvent to replace the classical solvent in the mobile phase for easy, rapid transfer to a more sustainable normal phase or reversed-phase liquid chromatography. The main focus of this review will be on describing the transfer of non-green to green and white chromatographic methods in an effort to elevate sustainability best practices in analytical chemistry. The greenness properties and greenness ranking, in addition to the chromatographic suitability of seventeen organic solvents for liquid chromatography, are mentioned to have a clear insight into the issue of rapidly choosing the appropriate solvent to transfer a classical HPLC or UHPLC method into a more sustainable one. A simple guide is proposed for making the liquid chromatographic method more sustainable.

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Noga, Sylwia, Attila Felinger y Bogusław Buszewski. "Hydrophilic Interaction Liquid Chromatography and Per Aqueous Liquid Chromatography in Fungicides Analysis". Journal of AOAC INTERNATIONAL 95, n.º 5 (1 de septiembre de 2012): 1362–70. http://dx.doi.org/10.5740/jaoacint.sge_noga.

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Abstract The goal of the study was to investigate the retention mechanism of selected fungicides in hydrophilic interaction liquid chromatography (HILIC) and per aqueous liquid chromatography (PALC). Chromatographic measurements were made on four physicochemically diversified HILIC columns, which were evaluated for the analysis of nine biologically active compounds, such as strobilurins and triazoles. The effects of the operating conditions on separations were investigated, including the concentration of the organic solvent in the aqueous-organic (acetonitrile) mobile phase. The results were compared, and it was shown that two different retention mechanisms dominate in PALC at low acetonitrile concentrations and in HILIC at high acetonitrile concentrations.

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Kostanyan, Artak E., Vera V. Belova, Yulia V. Tsareva y Maria M. Petyaeva. "Separation of Rare Earth Elements in Multistage Extraction Columns in Chromatography Mode: Experimental Study and Mathematical Simulation". Processes 11, n.º 6 (9 de junio de 2023): 1757. http://dx.doi.org/10.3390/pr11061757.

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The application of liquid–liquid chromatography principles to solvent extraction processes in hydrometallurgy can greatly simplify rare earth metal separation technologies by separating multicomponent mixtures in one technological operation. In this study, the chromatographic separation of rare earth elements (REEs) in multistage extraction columns was experimentally studied under conditions of impulse sample injection—single and multiple loading of large volumes of metal salt solution into the installation. The results obtained showed the feasibility of operating sieve plate extraction columns in the liquid–liquid chromatography mode. A closed-loop recycling technology is proposed for the separation of rare earth elements in multistage extraction columns operating in the liquid–liquid chromatography mode. For further development and industrial implementation of this technology, experimental studies should be conducted on intensified multistage extraction columns, such as sectioned columns with agitators and vibrating plate columns. Computer simulation of the chromatographic separation of rare earth elements by closed-loop recycling liquid–liquid chromatography was carried out.

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Vanitha Madhuri T, Manasa Krishna Pandreka, Geetha Gayatri B, Yamini M, Abhishek G, Edward Raju Gope, Raghava D y Nageswara Rao K. "Advances in High-Performance Liquid Chromatography (HPLC) and Ultra-Performance Liquid Chromatography (UPLC)". Journal of Pharma Insights and Research 2, n.º 6 (5 de diciembre de 2024): 039–46. https://doi.org/10.69613/t4nhz921.

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High-Performance Liquid Chromatography (HPLC) and Ultra-Performance Liquid Chromatography (UPLC) are fundamental analytical techniques that have revolutionized chemical analysis across various fields. These chromatographic methods offer exceptional separation capabilities, high resolution, and precise quantification of complex mixtures. HPLC has evolved significantly since its inception, with improvements in column technology, detection systems, and automation. UPLC, introduced as an advancement to conventional HPLC, operates at significantly higher pressures using sub-2-μm particle sizes, resulting in enhanced resolution, speed, and sensitivity. Both techniques have found extensive applications in pharmaceutical analysis, environmental monitoring, food safety, clinical diagnostics, and biomedical research. The implementation of various detection methods, including UV-visible, fluorescence, mass spectrometry, and electrochemical detection, has expanded their analytical capabilities. Recent developments in column technology, such as core-shell particles and monolithic columns, have further improved separation efficiency. The integration of artificial intelligence and machine learning has enhanced method development and data analysis. This review discusses the fundamental principles, technological advancements, and diverse applications of HPLC and UPLC. Additionally, it discusses current challenges, emerging trends, and future prospects in chromatographic science, including green chromatography initiatives and miniaturization efforts. The continuous evolution of these techniques contributes significantly to analytical chemistry's advancement, promising even more sophisticated applications in various scientific disciplines.

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KITAGAWA, Shinya. "Liquid Chromatography". Analytical Sciences 35, n.º 9 (10 de septiembre de 2019): 949–50. http://dx.doi.org/10.2116/analsci.highlights1909.

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KAGAWA, Nobuyuki. "Liquid Chromatography". Journal of the Japan Society of Colour Material 93, n.º 6 (20 de junio de 2020): 189–93. http://dx.doi.org/10.4011/shikizai.93.189.

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Hanai, Toshihiko. "Quantitative Explanation of Retention Mechanisms in Reversed-phase Mode Liquid Chromatography, and Utilization of Typical Reversed-phase Liquid Chromatography for Drug Discovery". Current Chromatography 6, n.º 1 (18 de septiembre de 2019): 52–64. http://dx.doi.org/10.2174/2213240606666190619120733.

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The retention mechanism in reversed-phase liquid chromatography was quantitatively described using log P (octanol-water partition coefficient). The hydrophobic (lipophilic) interaction liquid chromatography was then used to measure the hydrophobicity of a variety of compounds. Furthermore, the technique has been used as an analytical method to determine molecular properties during the drug discovery process. However, log P values cannot be applied to other chromatographic techniques. Therefore, the direct calculation of molecular interactions was proposed to describe the general retention mechanisms in chromatography. The retention mechanisms in reversed-phase liquid chromatography were quantitatively described in silico by using simple model compounds and phases. The competitive interactions between a bonded-phase and a solvent phase clearly demonstrated the retention mechanisms in reversed-phase liquid chromatography. Chromatographic behavior of acidic drugs on a pentyl-, an octyl-, and a hexenyl-phase was quantitatively described in the in silico analysis. Their retention was based on their hydrophobicity, and hydrogen bonding and electrostatic interaction were selectivity of the hexenyl-phase. This review focuses on the quantitative explanation of the retention mechanisms in reversed-phase liquid chromatography and the practical applications in drug discovery.

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Naida, O. O., B. A. Rudenko, R. Kh Khamizov y M. A. Kumakhov. "Polycapillary (multichannel) chromatographic columns in liquid chromatography". Journal of Analytical Chemistry 64, n.º 7 (30 de junio de 2009): 721–24. http://dx.doi.org/10.1134/s1061934809070107.

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Grob, Konrad y Zhangwan Li. "Damage to gas chromatographic columns caused by peroxides in liquid chromatographic eluents for coupled liquid chromatography-gas chromatography". Journal of Chromatography A 455 (enero de 1988): 297–300. http://dx.doi.org/10.1016/s0021-9673(01)82128-2.

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Memon, Najma, Tahira Qureshi, Muhammad Iqbal Bhanger y Muhammad Imran Malik. "Recent Trends in Fast Liquid Chromatography for Pharmaceutical Analysis". Current Analytical Chemistry 15, n.º 4 (3 de julio de 2019): 349–72. http://dx.doi.org/10.2174/1573411014666180912125155.

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Background: Liquid chromatography is the workhorse of analytical laboratories of pharmaceutical companies for analysis of bulk drug materials, intermediates, drug products, impurities and degradation products. This efficient technique is impeded by its long and tedious analysis procedures. Continuous efforts of scientists to reduce the analysis time resulted in the development of three different approaches namely, HTLC, chromatography using monolithic columns and UHPLC. Methods: Modern column technology and advances in chromatographic stationary phase including silica-based monolithic columns and reduction in particle and column size (UHPLC) have not only revolutionized the separation power of chromatographic analysis but also have remarkably reduced the analysis time. Automated ultra high-performance chromatographic systems equipped with state-ofthe- art software and detection systems have now spawned a new field of analysis, termed as Fast Liquid Chromatography (FLC). The chromatographic approaches that can be included in FLC are hightemperature liquid chromatography, chromatography using monolithic column, and ultrahigh performance liquid chromatography. Results: This review summarizes the progress of FLC in pharmaceutical analysis during the period from year 2008 to 2017 focusing on detecting pharmaceutical drugs in various matrices, characterizing active compounds of natural products, and drug metabolites. High temperature, change in the mobile phase, use of monolithic columns, new non-porous, semi-porous and fully porous reduced particle size of/less than 3μm packed columns technology with high-pressure pumps have been extensively studied and successively applied to real samples. These factors revolutionized the fast high-performance separations. Conclusion: Taking into account the recent development in fast liquid chromatography approaches, future trends can be clearly predicated. UHPLC must be the most popular approach followed by the use of monolithic columns. Use of high temperatures during analysis is not a feasible approach especially for pharmaceutical analysis due to thermosensitive nature of analytes.

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Saad Rasheed, Ashraf, Bashaer A. Al-Phalahy y Mustafa J. Mohammed. "Modern Chromatographic Methods for Determination Flavonoids". Al-Nahrain Journal of Science 27, n.º 2 (1 de junio de 2024): 28–49. http://dx.doi.org/10.22401/anjs.27.2.00.

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Flavonoids are a prominent group of plant phenolics (polyphenol group)extensively present in the human diet and associated with health promotion. Flavonoids are essential in various pharmaceutical, nutraceutical, and cosmetic applications. To collect and categorize these compounds, we comprehensively assessedHigh-performance liquid chromatography (HPLC) techniques published to analyze flavonoids in various matrices. Mostdocumented methods employed liquid chromatography with ultraviolet detection (HPLC-UV) and tandem mass spectrometry (LC-MS/MS) methods. Among chromatographic techniques, reversed-phaseliquidchromatographyremains the predominant and efficient method for separating various analytes. This review explores the primary chromatographic methods used to separate and quantify flavonoids in herbs, fruits, and biological samples. This article exam inesrecent literature on applying liquid chromatography with different detection methods for analyzing flavonoids. To examine recent literature on applying liquid chromatography with different detection methods for analyzing flavonoids. It offers valuable insights to researchers as they prepare to develop quantification methods.

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Kataev, S. S., O. N. Dvorskaya, M. A. Gofenberg, A. V. Labutin y A. B. Melentyev. "ANALYTICAL FEATURES OF SYNTHETIC MDMB(N)-073F CANNABIMIMETICS AND ITS MARKERS IN BIOLOGICAL MATERIAL". Pharmacy & Pharmacology 7, n.º 4 (10 de septiembre de 2019): 184–97. http://dx.doi.org/10.19163/2307-9266-2019-7-4-184-197.

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The aim of the research is to study both analytical features of synthetic MDMB(N)-073F cannabimimetics of indazole carboxamides group by gas chromatography methods combined with tandem mass spectrometry (GC-MS) and high performance liquid chromatography with high-resolution mass spectrometry (HPLC-HRMS) as well as characteristics of the major MDMB(N)-073F metabolite, its glucuronide and derivatives, using gas chromatography with mass-spectrometric (GC-MS) detection and high-performance liquid chromatography (HPLC) with MS/MS mass spectrometry (HPLC-MS/MS) in urine samples to be applied in expert practice, chemical-toxicological and forensic and chemical analyses.Materials and methods. To carry out the study, the following materials were used: plant-based objects with narcotic drugs withdrawn from illegal trafficking and applied to them;. urine samples to be studied under chemical-toxicological and forensic and chemical analyses. For solid-phase epitaxy, SampliQ EVIDEX TFE cartridges – 200 mg – 3 ml (Agilent, USA) were used for sample preparation; β-glucuronidase, Type HP-2, From Helix Pomatia, 100000 UA/ml (Sigma-ALDRICH CHEMI, Germany) was used for enzymatic hydrolysis. GC-MS/MS analysis was made using Agilent 7890 gas chromatograph with a tandem quadrupolar mass-spectrometer Agilent 7000 (Agilent, США); GC-MS analysis was carrid out using gas chromatograph Agilent 7820 with mass-selective detector Agilent 5975 (Agilent, USA); HPLC-HRMS research was made on liquid chromatograph Agilent 1260 with tandem hybrid high-resolution quadrupole-time-of-flight detector Agilent 6540 (Agilent, США); liquid chromatograph Agilent 1260 with Agilent 6460 (Agilent, USA) with tandem mass-spectrometer were used for making HPLC-MS/MS research.Results. The structure of MDMB(N)-073F compound has been confirmed and an exact mass of the protonated molecule corresponding to the chemical formula C19H27FN3O3 fixed by GC-MS/MS and HPLC-HRMS methods. Spectral characteristics of MDMB(N)-073F have been given. One of the branches in MDMB(N)-073F biotransformation in the human body found out by GC-MS and HPLC-MS/MS methods, is the ester decomposition with further conjugation of the resulting acid. The product interacting with glucuronic acid, is found to be the conjugate of major MDMB(N)-073F metabolite of the Ist phase in biotransformation. Metabolites appearing due to the ester decomposition and its conjugate with glucuronic acid, are recommended to be used as markers for synthetic MDMB(N)-073F cannabimimetics in the analysis by chromatographic methods; they can be used for regular screening of biological samples.Conclusion. The research results presented here, are the following: the analytical features characteristic for synthetic MDMB(N)-073F cannabimimetics found out by gas chromatography methods combined with tandem mass spectrometry (GC-MS/ MS) and liquid chromatography of hybrid high-resolution quadrupole-time-of-flight mass spectrometry (HPLC-HRMS), as well as characteristics of major MDMB(N)-073F metabolite, its glucuronide and derivatives with the use of gas chromatography with mass-spectrometric detection (GC-MS) and liquid chromatography combined with tandem mass spectrometry (HPLC-MS/MS) in urine samples to be applied in expert practice, chemical-toxicological, forensic and chemical analyses.

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Rawle, N. W., R. G. Willis y J. D. Baty. "Identification of triacylglycerols by high-performance liquid chromatography-gas-liquid chromatography and liquid chromatography-mass spectrometry". Analyst 115, n.º 5 (1990): 521. http://dx.doi.org/10.1039/an9901500521.

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Kostanyan, A. E. y A. A. Voshkin. "Pulsation cyclic liquid-liquid chromatography". Theoretical Foundations of Chemical Engineering 43, n.º 5 (octubre de 2009): 729–33. http://dx.doi.org/10.1134/s0040579509050194.

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Tong, Shengqiang. "Liquid-liquid chromatography in enantioseparations". Journal of Chromatography A 1626 (agosto de 2020): 461345. http://dx.doi.org/10.1016/j.chroma.2020.461345.

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Cong, Jing Xiang, Shao Yan Wang y Hong Gao. "Separation of Liquiritin by Two-Dimensional Liquid Chromatography". Advanced Materials Research 455-456 (enero de 2012): 1232–38. http://dx.doi.org/10.4028/www.scientific.net/amr.455-456.1232.

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Two-dimensional liquid chromatography (2DLC) is an important technology for the separation and analysis of complex samples. Liquiritin, an important active component in licorice, was chosen as the target compound and it was separated by three kinds of off-line 2DLC, i.e. size exclusion chromatography × reversed phase chromatography, normal phase × reversed phase chromatography and reversed phase chromatography × reversed phase chromatography (SEC×RP, NP×RP and RP×RP). The chromatographic conditions were selected and the 2D systems were combined. The results show that it is feasible to separate Liquiritin from licorice extract using 2DLC. Among the 2D modes mentioned above, the highest purity of Liquiritin was obtained in the RP×RP mode, and the concentration of Liquiritin was increased most significantly in the NP×RP mode.

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Xu, Sihua, Robert A. Norton, Ferrast G. Crumley y W. David Nes. "Comparison of the chromatographic properties of sterols, select additional steroids and triterpenoids: gravity-flow column liquid chromatography, thin-layer chromatography, gas—liquid chromatography and high-performance liquid chromatography". Journal of Chromatography A 452 (octubre de 1988): 377–98. http://dx.doi.org/10.1016/s0021-9673(01)81462-x.

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Schiff, Paul L. "Chromatography of Alkaloids, Part B: Gas–Liquid Chromatography and High-Performance Liquid Chromatography". Journal of Pharmaceutical Sciences 74, n.º 10 (julio de 1985): 1139–40. http://dx.doi.org/10.1002/jps.2600741038.

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Tsecheev, Arthur T. y Yurii N. Karpenko. "Application of UV spectrophotometry and reversed-phase HPLC to determine the ionization constant of a new biologically active compound". Aspirantskiy Vestnik Povolzhiya 23, n.º 2 (16 de junio de 2023): 60–65. http://dx.doi.org/10.55531/2072-2354.2023.23.2.60-65.

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Aim to determine the ionization constant (pKa) of the biologically active compound 2-ABPPC by UV spectrophotometry and high performance liquid chromatography (HPLC). Material and methods. The object of the study was the substance 2-ABPPC (2-amino-1-(4-bromophenyl)-5-(3,3-dimethyl-2-oxobutylidene)-4-oxo-4,5-dihydro-1H-pyrrole-3- carboxamide). The methods of UV spectrophotometry and high performance liquid chromatography were used to determine the ionization constant. The spectrophotometric analysis was carried out on a Shimadzu UV-1800 spectrophotometer. The chromatographic determination of the pKa value was carried out on an LC-20 Prominence liquid chromatograph (Shimadzu) using a Zorbax Extend-C18 reversed-phase column. Results. In the course of study, it was found that 2-ABPPC has one pKa value. When using two different methods to estimate the ionization constant, the comparable results were obtained: 7.64 (UV spectrophotometry method) and 7.40 (reversed phase HPLC method).

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31

Eliashvili, Levan. "Quantification of Glucose and Fructose in Georgian Semi-sweet Wines". Works of Georgian Technical University, n.º 2(532) (10 de junio de 2024): 11–14. http://dx.doi.org/10.36073/1512-0996-2024-2-11-14.

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One of the important parameters for wine certification is the quantitative determination of glucose and fructose, for which the highly efficient liquid chromatographic method is tested and is accurate. The quantitative determination of glucose and fructose in semi-sweet wines using high performance liquid chromatography is discussed in the article. A high-performance liquid chromatograph (HPLC) with a refractive index detector (RID) and a reversed-phase alkali amine chromatography column was used during the analysis. The method showed a high correlation coefficient during calibration (R2 = 0.99). With the given method, the concentration of glucose and fructose in semi-sweet wines of some denominations of Georgian production was measured. Quantification of these sugars is of particular importance in assessing the sweetness profile of wine and ensuring compliance with quality standards. For analysis, semi-sweet wines of Georgian production were used, in which the total amount of glucose and fructose is within the norm according to the Georgian Government Resolution #524.

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32

Dondelinger, Robert M. "Liquid Chromatography Systems". Biomedical Instrumentation & Technology 46, n.º 4 (1 de julio de 2012): 299–306. http://dx.doi.org/10.2345/0899-8205-46.4.299.

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33

"A Concise Review on High-Performance Liquid Chromatography". Journal of Pharmaceutical Research 8, n.º 2 (18 de julio de 2023). http://dx.doi.org/10.33140/jpr.08.02.13.

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A review of High-Performance Liquid Chromatography included an introduction, chromatographic terms, different classes, and types of HPLC techniques. Also included a brief introduction to HPLC principle and instrumentation. Columns, pumps, and detectors used in HPLC are also included in detail with their efficiency. Applications of the HPLC and overall new advantage cues are included in this review article.: High performance liquid chromatography (HPLC) is an important qualitative and quantitative technique, generally used for the estimation of pharmaceutical and biological samples. The chromatography term is derived from the Greek words namely chroma (colour) and graphein (to write). Chromatography is defined as a set of techniques that are used for the separation of constituents in a mixture. This technique involves 2 phases stationary phase and a mobile phase. The separation of constituents is based on the difference between partition coefficients of the two phases. chromatography is a very popular technique and it is mostly used analytically. There are different types of chromatographic techniques namely Paper Chromatography, Thin Layer Chromatography (TLC), Gas Chromatography, Liquid Chromatography, Ion exchange Chromatography, and lastly Liquid Chromatography (HPLC). This review is mainly based on the HPLC technique its principle, types, instrumentation, and applications. The mixture is separated using the basic principle of column chromatography and then identified and quantified by spectroscopy. In the 1960s, the column chromatography LC with its low-pressure suitable glass columns was further developed to the HPLC with its high- pressure adapted metal columns.

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34

Ingale, Arvind, Dr Shailesh J. Wadher, Srushti Bagul, Priyanka Gujrati y Anjali Govande. "High Performance Liquid Chromatography: An Overview". International Journal of Pharmaceutical Sciences Review and Research 82, n.º 2 (octubre de 2023). http://dx.doi.org/10.47583/ijpsrr.2023.v82i02.003.

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35

Lohoyda, L. S. "Validation of assay method of nifedipine in tablets by liquid chromatography". Medical and Clinical Chemistry, n.º 4 (17 de febrero de 2017). http://dx.doi.org/10.11603/mcch.2410-681x.2016.v0.i4.7267.

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The aim of this study was the validation of methods of quantitative determination of nifedipine in tablets by liquid chromatography. The chromatographic analysis was performed on nifedipine liquid chromatograph Agilent 1290 Infinity II LC System. A validation of methods of quantitative determination of nifedipine by high performance liquid chromatography tablets was performed. It was established that the method proves the requirements of the State Pharmacopoeia of Ukraine for the main validation parameters: specificity, accuracy, linearity, robasnist. The results obtained in this study clearly indicate that the developed HPLC method is fast, economical, simple, accurate and suitable for determination of nifedipine in medicines.

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36

"Liquid chromatography". Choice Reviews Online 39, n.º 01 (1 de septiembre de 2001): 39–0321. http://dx.doi.org/10.5860/choice.39-0321.

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37

"Liquid chromatography". Smart Materials Bulletin 2002, n.º 9 (septiembre de 2002): 6. http://dx.doi.org/10.1016/s1471-3918(02)00918-8.

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38

Berek, D. y A. Russ. "Limited sample recovery in coupled methods of high-performance liquid chromatography of synthetic polymers". Chemical Papers 60, n.º 3 (1 de enero de 2006). http://dx.doi.org/10.2478/s11696-006-0044-6.

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AbstractComplex polymer systems, which exhibit multiple distributions in their molecular parameters can be characterized by coupled liquid chromatographic methods. The latter combine entropic (exclusion) and enthalpic (interaction) retention mechanisms. However, recent experimental results suggest that some coupled liquid chromatographic methods may suffer from incomplete sample recovery. This refers, for example, to liquid chromatography under critical conditions of enthalpic interactions and to eluent gradient liquid chromatography. Sample recovery in both latter methods was investigated for selected model systems applying adsorption retention mechanism. Reduced sample recovery was confirmed for both methods. It was revealed that even very high final strength of mobile phase may be insufficient for complete elution of polymer samples in eluent gradient polymer liquid chromatography.

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39

Kaur, Gagandeep, Sonali Garg, Pratima Sharma y Dhiraj Sud. "A Review on High Performance Liquid Chromatographic Methods for determination of Metformin". Current Analytical Chemistry 16 (10 de marzo de 2020). http://dx.doi.org/10.2174/1573411016666200310141939.

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Background: The presence of pharmaceuticals (PACs) drugs in the environment and their detection and quantification have emerged as one of the challenging issues for the scientific community. Introduction: The gold standard, an anti-diabetic drug, Metformin has a strong potential to contaminate the aquatic bodies, being a highly polar drug. Different analytical methods based on spectroscopic evaluation or chromatographic techniques have been developed to find out the concentration of drug/ their metabolites. Methods: This review article discussed the chromatographic techniques for analysis of Metformin (in ng/L to μg/L) in aqueous samples, pharmaceutical drugs and biological fluids such as urine and human plasma are High-Performance Liquid Chromatography (HPLC), Reverse-Phase High-Performance Liquid Chromatography (RP-HPLC), High-Performance Thin-layer Chromatography (HPTLC), Hydrophilic Interaction Liquid Chromatography HILIC–MS/MS, Liquid Chromatographic–tandem mass spectrometric (LC-MS-MS), Ultra-High Performance Liquid Chromatography (UPLC). Result: The relevance modifications of traditional HPLC methods for separation of the mixture of drugs with a focus on the lesser time, better resolution, sensitivity, symmetry of peaks, the limit of detection and accuracy of the results has been envisaged through research findings. Hydrophilic interaction liquid chromatography (HILIC) – tandem mass spectrometry method offered the possible solution for highly polar drugs detection and quantification in effluent and surface water samples. Conclusion: HPLC based analytical techniques offer the advantages viz. less time requirement, minimum usage of organic solvents and better separation and quantification of Metformin. The futuristic research approach lies in the development of newer extraction strategies, mobile phases and adsorbent materials for the HPLC based separations.

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40

Bhattacharya, Kunal, Nongmaithem Randhoni Chanu, Atanu Bhattacharjee, Bhargab Jyoti Sahariah, Chanam Melody Devi y Ripunjoy Bordoloi. "Ultra-Performance Liquid Chromatography - An Updated Review". Research Journal of Pharmacy and Technology, 24 de diciembre de 2022, 5849–53. http://dx.doi.org/10.52711/0974-360x.2022.00987.

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Ultra-performance liquid chromatography (UPLC) has an advantage over conventional High-performance liquid chromatography (HPLC) as UPLC offers substantial resolution, speed, and sensitivity during analysis. This advanced chromatographic technique uses sub-2μm particles for the stationary phase. As a result, it saves time and reduces solvent consumption, which allows it to take less run time and makes it highly efficient.

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41

Sotnikova, Larisa, Larisa Sotnikova, Polina Goryunova, Polina Goryunova, Sergey Sozinov, Sergey Sozinov, Natal’ya Ivanova y Natal’ya Ivanova. "CHROMATOGRAPHIC BEHAVIOR OF BORNYL ACETATE DIASTEREOMERS UNDER THE CONDITIONS OF REVERSED-PHASE HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)". Science Evolution, 30 de diciembre de 2017, 44–48. http://dx.doi.org/10.21603/2500-1418-2017-2-2-44-48.

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The present paper illustrates the results of the study on chromatographic behavior and optimization of some parameters of the method of quantitative determination of bornyl acetate and isobornyl acetate diastereomers under the conditions of reversed-phase high- performance liquid chromatography. Chromatography was performed with HPLC platform Agilent 1200 with diode-matrix detector and a column Agilent Zorbax XDB, Extend-C18. Detection of the studied analytes was performed at a wavelength of 210 nm. Determinationof the concentration of bornyl acetate isomers was carried out in mixture with other components of the Abiessibirica essential oil in chromatographic systems with mobile phases of acetonitrile-water or isopropyl alcohol-water. The range of analyte concentrations in a sample was varied from 2 to 430 mg/ml for bornyl acetate and from 2 to 950 mg/ml for isobornyl acetate. It is stated that in a chromatographic system with a mobile phase, based on acetonitrile, the peaks of the studied components have an asymmetric shape, and the retention times of analytes increase with the decrease of their concentrations in a sample. In a chromatographic system with isopropyl alcohol the asymmetry of the bornyl acetate peak disappears, the width decreases and the retention time stabilizes. For isobornyl acetate a peak width also decreases, its asymmetry is preserved, but at the same time, the asymmetry coefficient takes on permitted values (less than 2). Calibration charts for the mentioned compounds in the used eluents are linear throughout the studiedconcentration range with correlation coefficients of R2>0.998. Thus, the conducted researches allow to recommend the reversed-phaseHPLC variant for the separate quantitative determination of bornyl acetate and isobornyl acetate in the pine oil samples.

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42

Chavda, Nirma y Suresh Kumar. "A Review article on Analytical Method Development for the combination of Azelnidipine and Telmisartan". Asian Journal of Pharmaceutical Analysis, 16 de agosto de 2021, 227–34. http://dx.doi.org/10.52711/2231-5675.2021.00040.

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The literature survey explains that there is not any stability indicating method reportedly for combination of Azelnidipine and Telmisartan till date. Validation and development of stability indicating analytical methods is possible as per ICH Guidelines. There are several of Spectroscopic methods such as Ultraviolet Spectroscopy, Mass spectroscopy, infrared spectroscopy, Nuclear magnetic resonance spectroscopy and Chromatographic methods such as High performance liquid chromatography, Thin layer Chromatography, High Performance thin layer chromatography, Gas chromatography and Ultra performance liquid chromatography etc. used for stability indicating method development and validation.

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43

Boltia, Shereen A., Shrouk E. Algmaal, Nadia M. Mostafa y Yasser S. El Saharty. "Validated Smart Different Chromatographic Methods for Selective Quantification of Acefylline Piperazine, Phenobarbital Sodium and Methylparaben Additive in Bulk and Pharmaceutical Dosage Form". Journal of Chromatographic Science, 29 de enero de 2022. http://dx.doi.org/10.1093/chromsci/bmac003.

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Abstract Two chromatographic methods have been proposed for the simultaneous determination of acefylline piperazine (ACEF) and phenobarbital (PHENO) in presence of methylparaben as additive in pharmaceutical dosage form. The first method was thin-layer chromatography. The separation was achieved using silica gel as stationary phase and chloroform: methanol: glacial acetic acid (2.0, 8.0 and 0.1, by volume) as a developing system at 254 nm. Accurate determination of both drugs was attained over the concentration range of 0.5–25 μg/band. The second method was based on the use of reversed phase liquid chromatography with diode array detection, by which the proposed components were separated on a reversed phase C18 analytical column using methanol: water (60: 40, by volume) as a mobile phase with flow rate of 0.8 mL/min at 214 nm in a concentration range of 0.5–100 μg/mL. The proposed chromatographic methods were practiced successfully for the determination of ACEF and PHENO in pharmaceutical dosage form. Both methods were validated according to the International Conference on Harmonization guidelines and statistically compared with a reported high-performance liquid chromatograph method. Planar chromatography has never been proposed in the literature for ACEF and PHENO determination besides the proposed columnar chromatographic method using an isocratic eco-friendly mobile phase.

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44

Nimra Sohail, Bushra Naureen, Mehmood Asghar, Aziza Sarwar y Aisha Altaf. "RECENT ADVANCES IN GAS, LIQUID AND SUPERCRITICAL FLUID CHROMATOGRAPHY IN THE CONTEXT OF SUSTAINABLE/ GREEN CHEMISTRY". International Journal of Pharmacy & Integrated Health Sciences 6, n.º 1 (7 de octubre de 2024). http://dx.doi.org/10.56536/ijpihs.v6i1.203.

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Background: Chromatographic techniques such as gas chromatography (GC), liquid chromatography (LC) and supercritical fluid chromatography (SFC) have long been employed in analytical chemistry. However, using or producing certain organic solvents and non-renewable gases is hazardous to the environment. Green chemistry is essential for addressing the environmental hazards associated with traditional procedures. Objectives: This review focuses on recent updates and profound insights into new, greener techniques introduced in GC, LC and SFC. Methodology: To compile this review, several electronic databases were searched, preferably from January 2019-December 2023. Results: This review highlights advancements in miniaturization, rapid methods, and eco-friendly solvents in chromatographic techniques. Integrating micro-electro-mechanical systems (MEMS) and nano-electro-mechanical systems (NEMS) in GC enhances sensitivity and resolution while reducing solvent consumption. Innovations like monolithic micro-GC chips and the Quick, Easy, Cheap, Effective, Rugged, and Safe (QuEChERS) method further streamline analysis times. In LC, supercritical fluids are utilized as green mobile phases, optimizing techniques like electrochemical flow liquid chromatography (EFLC), high-performance liquid chromatography (HPLC), and ultra-high-performance liquid chromatography UHPLC. In contrast, SFC employs rapid methods, such as ultra-high-performance supercritical fluid chromatography-mass spectrometry (UHPSFC-MS). These developments collectively promote sustainability and efficiency in chromatographic practices. Conclusion: Green chromatography has become an essential tool in pharmaceutical analysis because it safeguards the operator’s health and the environment. It opens new horizons and generates new ideas for further experimentation while focusing on recent cutting-edge green technologies incorporated in GC, LC and SFC. These advancements significantly enhance safety and sustainability in analytical practices.

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45

Kavya, R., K. Bhavya Sri, D. Anil y Mogili Sumakanth. "Qualification and Calibration of Hyphenated Techniques Liquid Chromatography: Mass Spectroscopy and Gas Chromatography - Mass Spectroscopy". International Journal of Pharmaceutical Sciences Review and Research 84, n.º 3 (marzo de 2024). http://dx.doi.org/10.47583/ijpsrr.2024.v84i03.027.

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46

A. Gavit, Harish, Amol R. Pawar, Vikas V. Patil, Pankaj S. Patil y Pushpendra H. Sisodiya. "Advancement in High-Performance Liquid Chromatography Techniques: A Comprehensive Review". Asian Journal of Pharmaceutical Analysis, 28 de mayo de 2024, 95–103. http://dx.doi.org/10.52711/2231-5675.2024.00017.

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Today, chromatography is the backbone of separation science and is being used in all research laboratories and pharmaceutical industries of the world. In these chromatography techniques, HPLC is one of the chromatographic techniques, which is mostly used analytical technique. Recent developments in chromatographic supports and instrumentation for liquid chromatography (LC) are enabling rapid and highly efficient separations. This article represents a brief review of HPLC along with its principle and instrumentation. It describes about new trends in HPLC such as RRLC, UPLC, UFLC and Nano LC. In this article mainly focus on detailed comparison of new developments of HPLC in terms of instrumental operating conditions, applications and advantages over HPLC of each technique. Keywords: Liquid chromatography, HPLC, RRLC, UPLC, UFLC, Nano LC.

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47

Kaur, Jashanpreet, Naresh Kumar Rangra y Pooja A. Chawla. "A comprehensive review on recent trends in amino acids detection through analytical techniques". SEPARATION SCIENCE PLUS, 15 de agosto de 2023. http://dx.doi.org/10.1002/sscp.202300040.

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AbstractThe process of growth, development, and reproduction cannot take place in a live body without the presence of amino acids (AAs) since they are necessary for appropriate functioning. Detection of AAs in pharmaceutical and food samples is required to ensure quality, quantity, and efficacy. The AAs generally do not contain chromophores; hence their chromatographic analysis requires derivatization. The research papers published in the last few years were used to compile this manuscript. This manuscript covers various analytical, bioanalytical, and electrochemical approaches used in the identification of AAs. The analytical techniques like high‐performance liquid chromatography, ultra‐performance liquid chromatography, etc., and the hyphenated analytical techniques like liquid chromatography‐mass spectrometry, ultra‐performance liquid chromatography‐electrospray tandem mass spectrometry, and hydrophilic interaction ultra‐performance liquid chromatography are also discussed. This manuscript also briefly outlines the electrochemical analytical techniques including sensors and biosensors. This review article will be useful to the researcher working in the area of the development of analytical techniques for the detection of AAs.

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48

"Basic liquid chromatography". Choice Reviews Online 37, n.º 12 (1 de agosto de 2000): 37Sup—280–37Sup—280. http://dx.doi.org/10.5860/choice.37sup-280.

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49

"Liquid Chromatography Calendar". Journal of Liquid Chromatography & Related Technologies 32, n.º 11-12 (19 de mayo de 2009): 1828–30. http://dx.doi.org/10.1080/10826070902959687.

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50

"Liquid Chromatography Calendar". Journal of Liquid Chromatography & Related Technologies 32, n.º 16 (4 de septiembre de 2009): 2462–64. http://dx.doi.org/10.1080/10826070903209629.

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