Bibliografías temáticas / High-pressure spectrophotometry

Literatura académica sobre el tema "High-pressure spectrophotometry"

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Publicado: 4 de mayo de 2024

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Artículos de revistas sobre el tema "High-pressure spectrophotometry"

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Arabas, J., P. Butz, C. Merkel, Z. Spolnicki, J. Szczepek y B. Tauscher. "Miniature optical cell for spectrophotometry under high pressure". High Pressure Research 19, n.º 1-6 (septiembre de 2000): 379–83. http://dx.doi.org/10.1080/08957950008202581.

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Duke, Stephen O., Mary V. Duke, Timothy D. Sherman y Ujjana B. Nandihalli. "Spectrophotometric and Spectrofluorometric Methods in Weed Science". Weed Science 39, n.º 3 (septiembre de 1991): 505–13. http://dx.doi.org/10.1017/s004317450007329x.

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The utility, advantages, and disadvantages of several spectrofluorometric and in vivo spectrophotometric methods in plant science are reviewed, with emphasis on their use in weed science. Examples of the use of in vivo, dual-wavelength spectrophotometry to probe the effects of herbicides on cytochromefoxidation/reduction, the P515 chromatic shift, phytochrome synthesis, and other processes are discussed. Use of in vivo spectrophotometry to examine effects of herbicides on phytylation of chlorophyllide, protochlorophyllide photoconversion, porphyrin accumulation, and other processes that result in spectral changes is discussed and examples are provided. Spectrofluorometric methods for pigment identification and quantification and for enzyme assays are illustrated with examples. Spectrofluorometric methods used in conjunction with high-pressure liquid chromatography (HPLC) and thin-layer chromatography (TLC) are discussed.
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Webb, D. J., B. K. Burnison, A. M. Trimbee y E. E. Prepas. "Comparison of Chlorophyll a Extractions with Ethanol and Dimethyl Sulfoxide/Acetone, and a Concern about Spectrophotometric Phaeopigment Correction". Canadian Journal of Fisheries and Aquatic Sciences 49, n.º 11 (1 de noviembre de 1992): 2331–36. http://dx.doi.org/10.1139/f92-256.

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Chlorophyll a (Chl a) in water samples from three mesotrophic to eutrophic lakes in north-central Alberta was extracted with one of three solvents (95% ethanol, 90% ethanol, or a 2:3 mixture of dimethyl sulfoxide and 90% acetone (DMSO/acetone)) and analyzed by two techniques (spectrophotometry and high pressure liquid chromatography (HPLC). The dominant phytoplankton were blue-green algae and diatoms. Total Chl a concentrations (i.e. no correction for phaeopigments (Pha)) were not significantly different among solvents (P > 0.5). Total Chl a concentrations from spectrophotometric analyses were significantly higher than those from HPLC analyses (4.2 ± 0.88 and 2.6 ± 0.50 μg∙L−1 respectively, P < 0.05). Pha concentrations derived by spectrophotometry were 64 times higher than those derived by HPLC (1.7 ± 0.52 and 0.025 ± 0.01 μg∙L−1 respectively, P < 0.005). Thus, spectrophotometry appears to dramatically overestimate Pha concentrations and may overestimate total Chl a (i.e. no correction for Pha). Therefore, ethanol and DMSO/acetone are equally suitable for Chl a extraction from natural populations dominated by blue-green algae and/or diatoms, but if information on Pha and/or accessory pigments is required, HPLC analyses are the appropriate route rather than spectrophotometry.
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Suleimenov, O. M. "Simple, compact, flow-through, high temperature high pressure cell for UV-Vis spectrophotometry". Review of Scientific Instruments 75, n.º 10 (24 de septiembre de 2004): 3363–64. http://dx.doi.org/10.1063/1.1791317.

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Hu†, Ye, Hao Liang†, Qipeng Yuan y Yuancheng Hong. "Determination of glucosinolates in 19 Chinese medicinal plants with spectrophotometry and high-pressure liquid chromatography". Natural Product Research 24, n.º 13 (15 de agosto de 2010): 1195–205. http://dx.doi.org/10.1080/14786410902975681.

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Afandy, Moh A., Wahyudi B. Sediawan, Muslikhin Hidayat, Devi Y. Susanti y Fikrah D. I. Sawali. "Bioactive Compound Contents and Antioxidant Activity of Purified Red Sorghum Pericarp Extract by Membrane Ultrafiltration Process". Jurnal Akademika Kimia 12, n.º 1 (28 de febrero de 2023): 13–19. http://dx.doi.org/10.22487/j24775185.2023.v12.i1.pp13-19.

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Sorghum plants contain bioactive compounds such as phenolic compounds and proanthocyanidins. The presence of these compounds is extremely valuable for use as antioxidants in health care. This study aims to determine the total phenolic content, total proanthocyanidin content, and antioxidant activity of purified red sorghum extract using the ultrafiltration membrane method with different transmembrane pressure. At pressures of 8, 9, and 10 Bar, an ultrafiltration process was carried out using a polyethersulfone (PES) membrane with a molecular weight cut-off size of 10 kDa. The total phenolic content was determined using the Follin-Ciocalteu method and identified using UV-Vis spectrophotometry at 760 nm. Total proanthocyanidin content was measured using the acid-butanol method and then analyzed using UV-Vis spectrophotometry at 550 nm. The DPPH (2,2-diphenyl-2-picrylhydrazyl) method will be used to determine the antioxidant activity of purified red sorghum extract. The results of the measurements show that the higher the transmembrane pressure, the higher the concentration of phenolic and proanthocyanidins content, and that the purified red sorghum extract has a high antioxidant value (IC 50 = 66.852 ppm).
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Pick, Frans E., Pieter R. De Beer, Susan M. Prinsloo y Louis P. Van Dyk. "Contaminant and formulation analysis of MSMA using high-pressure liquid chromatography - graphite furnace atomic absorption spectrophotometry". Pesticide Science 21, n.º 1 (1987): 45–49. http://dx.doi.org/10.1002/ps.2780210105.

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Von Fischern, T., S. Langefeld, L. Yuan, N. Völcker, M. Reim, B. Kirchhof y N. F. Schrage. "The “Aachen” keratoprosthesis: A New Approach towards Successful Keratoprosthesis-Surgery". International Journal of Artificial Organs 21, n.º 1 (enero de 1998): 52–57. http://dx.doi.org/10.1177/039139889802100111.

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Background None of the keratoprostheses available today is absolutely successful in the long term, neither the problems of extrusion, retroprosthetic membrane formation and intraocular pressure rise are yet solved. A new type of keratoprosthesis is required which can show improved ingrowth characteristics and allow intraocular pressure measurements. In order to possibly meet the above mentioned requirements we developed a flexible silicone keratoprosthesis with scleral fixation and chemical surface modification. Methods The one-piece keratoprosthesis is made of silicone rubber. Its optical zone has a diameter of 11 mm and is 0.3 mm thick. The surface-modified haptic consists of a scleral rim and eight branches for scleral fixation. A ridge at the back of the keratoprosthesis fitting into the trephination hole shall avoid leakage and retroprosthetic membrane formation. Optical and mechanical qualities are characterised by tensile tests, spectrophotometry and topography. Results A method for keratoprosthesis-production was established. The optical quality of the device was improved by submicron lathing of the mould. Spectrophotometry showed high visible and ultraviolet light transmission of the silicone. Mechanical tests with silicone samples revealed high tensile strength and elongation at break. The mechanical properties were not impaired by surface modification. Conclusions The production of a flexible silicone keratoprosthesis with high optical and mechanical properties was established. Its use both for the treatment of permanently opacified corneas and as temporary keratoprosthesis seems to be possible.
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Einhorn, Todd C., Cecil Stushnoff, Ann E. McSay, Phil L. Forsline, Sam Cox, Joel R. L. Ehrenkranz y Loretta Sandoval. "(18) Biodiversity of the Flavonoid Phlorizin in a Subset of the USDA Apple Germplasm Core Collection". HortScience 40, n.º 4 (julio de 2005): 1067D—1067. http://dx.doi.org/10.21273/hortsci.40.4.1067d.

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Phlorizin is known for its role in reducing glucotoxicity and has a long history of use in diabetes research. In addition, its contribution to the pool of total phenolics adds to the overall health benefits attributed to fruit. Phlorizin is limited to Rosaceae family plants, of which apple comprises its current commercial source; however, limited information exists regarding its biodiversity among apple taxa. A subset of 22 taxa from a core collection of apple accessions representative of the global genetic diversity of apple was used to investigate the biodiversity of phlorizin present in apple shoots and in fruit relative to total phenolic content and free radical scavenging capacity. Fruit and shoots were harvested from the USDA Plant Genetic Resources Unit in Geneva, N.Y. Validation and quantification of phlorizin was conducted using a rigorous high-pressure liquid chromatography (HPLC) procedure. Total phenolics in fruit, assayed using a Folin-Ciocalteu method and expressed as gallic acid equivalents, ranged from 227 to 7181 mg·L-1 and were strongly related to 2,2' azinobis (3-ethylbenzothiazoline-6-sulfonic acid) (ABTS) antioxidant capacity for the core collection (r= 0.778). On a molar basis, phlorizin had lower antioxidant capacity than other major phenolic compounds present in apple fruit, but was more effective than ascorbic acid. Phlorizin yield in dormant apple shoots, expressed as percent weight, ranged from 0.9% to 5.5%. A rapid, 96 well micro-plate spectrophotometric assay was also developed to aid in the screening of multiple samples for selection of high phlorizin yielding apple taxa. Spectrophotometry overestimated phlorizin content as expected, but the calibration curve between HPLC and spectrophotometry was acceptable, r2 = 0.88.
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Mao, Xiao Jing, Ye Hong Shi y Hua Chang Li. "Comments on Technical Progress in Pretreatment and Analysis Method of Inorganic Elements of Electroplating Sludge". Advanced Materials Research 1010-1012 (agosto de 2014): 413–16. http://dx.doi.org/10.4028/www.scientific.net/amr.1010-1012.413.

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The latest technical progress in pretreatment and analysis method of inorganic elements of electroplating sludge was briefly reviewed. Some pretreatment methods were summarized, including exposure system digestion, high-pressure tank digestion, microwave digestion and dry ash digestion as well as some analysis methods, such as spectrophotometry, atomic absorption spectrometry, inductively coupled plasma spectrometry and inductively coupled plasma mass spectrometry. Finally, the trend for future technical development in inorganic elements determination of electroplating sludge was prospected.
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Tesis sobre el tema "High-pressure spectrophotometry"

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Fabian, June. "Preformulation and formulation study of dexchlorphenniramine maleate for use in the development of a new sustained release dosage form". Thesis, 1994. https://hdl.handle.net/10539/25978.

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A Dissertation Submitted to the Faculty of Medicine, University of the Witwatersrand, Johannesburg, in Partial Fulfilment of the Requirements for the Degree of Master of Pharmacy Johannesburg, March 1994
Preformulation and formulation study of dexchlor- pheniramine maleate (DCPM) for it's inclusion into a gelforming sustained release dosage form was investigated. A modification of the USP apparatus 2 is proposed as an alternative to currently recommended USP dissolution apparatus for floating, gelforming drug delivery systems. In addition, the role of magnesium stearate and talc as dissolution retardants in controlled release matrix tablets is investigated, through application of a factorial design.
IT2018
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Dhumal, Ravindra S., Adrian L. Kelly, Peter York, Philip D. Coates y Anant R. Paradkar. "Cocrystalization and simultaneous agglomeration using hot melt extrusion". 2010. http://hdl.handle.net/10454/5955.

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PURPOSE: To explore hot melt extrusion (HME) as a scalable, solvent-free, continuous technology to design cocrystals in agglomerated form. METHODS: Cocrystal agglomerates of ibuprofen and nicotinamide in 1:1 ratio were produced using HME at different barrel temperature profiles, screw speeds, and screw configurations. Product was characterized for crystallinity by XRPD and DSC, while the morphology was determined by SEM. Dissolution rate and tabletting properties were compared with ibuprofen. RESULTS: Process parameters significantly affected the extent of cocrystallization which improved with temperature, applied shear and residence time. Processing above eutectic point was required for cocrystallization to occur, and it improved with mixing intensity by changing screw configuration. Product was in the form of spherical agglomerates, which showed directly compressible nature with enhanced dissolution rate compared to ibuprofen. This marks an important advantage over the conventional techniques, as it negates the need for further size modification steps. CONCLUSIONS: A single-step, scalable, solvent-free, continuous cocrystallization and agglomeration technology was developed using HME, offering flexibility for tailoring the cocrystal purity. HME being an established technology readily addresses the regulatory demand of quality by design (QbD) and process analytical technology (PAT), offering high potential for pharmaceuticals.
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Capítulos de libros sobre el tema "High-pressure spectrophotometry"

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Ikhiwili Oniha, Margaret, Eze Frank Ahuekwe y Sharon Oluwatobi Akinpelu. "Phytochemical Contents of Essential Oils from Cymbopogon Species: A Tropical Medicinal Plant". En Tropical Plant Species and Technological Interventions for Improvement. IntechOpen, 2023. http://dx.doi.org/10.5772/intechopen.105396.

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Natural resources especially medicinal plants possess the potentials to sustain all existence on earth. Cymbopogon, a globally cultivated herb, possesses high contents of diverse essential oils for medicinal and economic purposes including treatment of malaria and candidiasis. Notable species include Cymbopogon citratus and C. flexosus having citral as the main chemical compound. Numerous compounds of these species include limonene, citronella, geranyl acetic derivatives, elemol, among others. Phytochemical analysis of these essential oils is usually done by the gas chromatography-mass spectrometry (GC-MS) method sequel to obtaining them through solvent extraction, hydrodistillation, supercritical CO2 extraction, chromatography among others. Although the supercritical CO2 extraction method gives greater quality yields void of toxic wastes with preserved thermal stability compared with other methods, its high-working pressure generates issues of safety risks and costs. Quantitative determination is done using spectrophotometric, chromatographic, and Folin-Ciocalteu methods. In comparison with other chromatographic techniques employed, gas chromatography exhibits greater efficiency by quantifying and determining the presence of various components at low concentrations. This prominently economical plant with potent ethnobotanical benefits hinged on the essential oils phytochemicals is faced with diverse extraction challenges; thus, improvement in the extraction and quantification techniques is key to the harvest of pure yields of lemon grass essential oils.
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Epstein, Irving R. y John A. Pojman. "Apparatus". En An Introduction to Nonlinear Chemical Dynamics. Oxford University Press, 1998. http://dx.doi.org/10.1093/oso/9780195096705.003.0008.

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In the previous chapter, we developed a set of conceptual and mathematical tools for analyzing the models and experimental data that form the subject matter of nonlinear chemical dynamics. Here, we describe some of the key items of experimental apparatus used to obtain these data so that the reader can better appreciate the results discussed in the following chapters and can learn how to begin his or her own investigations. The first several sections are devoted to measurements of temporal behavior, with emphasis on the techniques used to monitor reactions in time and on the reactors in which these reactions are studied. The final section focuses on the study of spatial patterns and waves in chemical systems. It is possible, by methods that we shall discuss later, to reconstruct the qualitative dynamics of a system from the measurement of only a single variable. However, the more species whose concentrations can be measured, the easier it is to elucidate a mechanism and the more rigorously that mechanism can be tested. The most impressive study of multiple species in a chemical oscillator was carried out by Vidal et al. (1980), who were able, by a combination of techniques, to monitor the concentrations of Ce4 + , Ce3+ , Br2, Br-, bromomalonic acid, O2, and CO2 in the BZ reaction. In the following sections, we will look at the most widely employed techniques: spectroscopic and potentiometric methods. In principle, and occasionally in practice, essentially any technique that can be used to detect changes in concentration can be utilized to monitor the systems that we are interested in. Approaches that have been employed to date include polarography, high-pressure liquid chromatography, and calorimetry. If there are absorbing species, ultraviolet and/or visible (UV/vis) spectroscopy offers rapid response time and high sensitivity for monitoring concentrations, particularly if the species of interest have spectra with relatively little overlap. Measurements can be made in a cuvette placed in a standard UV/vis spectrophotometer, but this configuration has several limitations.
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Actas de conferencias sobre el tema "High-pressure spectrophotometry"

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Ahmad, Mohammad, Zuhair Khan, Mian Muneeb Ur Rehman, Asghar Ali y Shaheer Aslam. "A Study of Aluminum Doped ZnO Thin Films Developed via a Hybrid Method Involving Sputter Deposition and Wet Chemical Synthesis". En International Symposium on Advanced Materials. Switzerland: Trans Tech Publications Ltd, 2022. http://dx.doi.org/10.4028/p-s02qs7.

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Transparent conducting oxides (TCO) are semiconducting materials that are electrically conductive as well as optically transparent thus making them suitable for application in photovoltaics, transparent heat transfer windows, electrochromic windows, flexible display, and transparent electronics. One of the methods to enhance the conductivity of metal oxides is doping, however, it can adversely affect the optical transparency of metal oxide. Aluminum (Al) doped zinc (Zn) oxide (AZO) is an important TCO material whose optoelectronic properties heavily rely on the Al doping level. There are various methods to develop AZO thin films. However, since Al and Zn are high vapor pressure materials, and their precise content control isn’t that easy, that’s why we dedicated this study to devise a facile method of Al doping into the ZnO structure. We report a twostep synthesis route to develop AZO thin films over glass substrates. Sub stoichiometric zinc oxide (ZnOx) thin films were sputter deposited over glass employing RF magnetron sputtering at 70W and 9 x 10-3 Torr Ar pressure. To mitigate Zn losses during annealing at 450 °C, the films were first oxidized up to 200 °C in air so as to convert ZnOx into stoichiometric ZnO. To incorporate Al into the ZnO structure, Al was spin coated on top of ZnO from its stabilized sol of 0.07 molar aluminum nitrate nonahydrate in ethanol. The samples were subsequently annealed at 450 °C for 2h in air with a controlled heating ramp of 3 °C/min. The film morphology, microstructure, electronic, and optical characteristics were explored employing scanning electron microscopy, energy dispersive x-ray spectroscopy, Hall effect measurements, and UV-Vis-NIR spectrophotometry, respectively. We found that both the Al and oxygen (O) content affect the optoelectronic behavior of AZO. Even without Al doping, O deficient samples were found to be sufficiently conductive, however, the ZnOx is less transparent relative to O rich stoichiometric ZnO. Furthermore, if ZnOx is annealed at higher temperatures, it causes Zn losses, since Zn is a relatively high vapor pressure material. It degrades the film morphology as well. Once we have ZnO we can confidently treat it at 450 °C to allow Al diffusion into the interiors of the ZnO film. We found that AZO produced via this method is sufficiently conductive as well as transparent.
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Pandey, Rishabh, Ali Ousseini Tinni y Chandra Shekhar Rai. "Experimental Investigation of Amphoteric and Microbial Surfactants for Enhanced Oil Recovery in Shaly Sandstones". En SPE Oklahoma City Oil and Gas Symposium. SPE, 2023. http://dx.doi.org/10.2118/213102-ms.

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Abstract To meet the increasing demand for oil and gas, surfactants have been used to increase hydrocarbon recovery. Use of surfactants reduces the Interfacial Tension (IFT) at fluid/fluid interface and wettability at rock/fluid interface and mobilizes trapped oil out of the pores. However, there are two main limitations of the surfactant flooding process—first, high reservoir temperature & salinity, and second, adsorption of surfactants on the rock surface. Surfactant adsorption alters wettability of reservoir rock from oil-wet to water-wet. However, it may not increase oil recovery, especially in conventional reservoirs with high Total Dissolved Solids (TDS) and temperature due to excess surfactant adsorption. This study tested two synthetic amphoteric surfactants, one nonionic biosurfactant, and a base case with produced brine to understand wettability, IFT, surfactant adsorption, and their effect on oil recovery in shaly sandstone formation. Produced brine has a TDS of 238,000 ppm. First, surfactant stability tests were performed on the three surfactants. Then, IFT measurements were performed between crude oil and surfactant solutions along with produced brine. Next, wettability alteration was studied by measuring contact angle on oil saturated rock samples before and after being exposed with surfactants and produced brine. Then, surfactant adsorption experiments were performed using UV-Vis spectrophotometer to calculate the amount of surfactant adsorbed on the rock sample. Next, surfactants and produced brine imbibition experiments were performed on plug samples at 145°F and 500 psi pressure, and oil recovery was quantified using 12MHz Nuclear Magnetic Resonance (NMR) spectrometer. Results showed that all three surfactants reduced IFT and altered wettability, but biosurfactant showed most reduction of IFT, much lower surfactant adsorption, and made the sample most water wet as compared to amphoteric surfactants. Imbibition experiments showed that biosurfactant have the highest oil recovery, while amphoteric surfactants have oil recovery even lower than produced brine. This study shows that surfactant adsorption effects oil recovery, which can lead to loss of surfactants from solution to the rock surface. This study suggests that biosurfactants with glycolipids can be effectively used in shaly sandstone at high TDS and temperature.
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Fadlallah, Hadi, Mojtaba Jarrahi, Eric Herbert, Roselyne Ferrari, Annick Mejean y Hassan Peerhossaini. "Effects of Shear Stress on the Growth Rate of Micro-Organisms in Agitated Reactors". En ASME 2016 Fluids Engineering Division Summer Meeting collocated with the ASME 2016 Heat Transfer Summer Conference and the ASME 2016 14th International Conference on Nanochannels, Microchannels, and Minichannels. American Society of Mechanical Engineers, 2016. http://dx.doi.org/10.1115/fedsm2016-7590.

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The effects of hydrodynamic shear stress on the growth rate of cyanobacteria Synechocystis sp. and Chlamydomonas reinhardtii microalgae cells were studied in agitated photobioreactors, since they have different motility rates and sizes. An experimental setup was designed and constructed to monitor the growth rate of the micro-organisms versus the shear rate; experiments were carried out in a well controlled environment, under constant atmospheric pressure and 20 °C temperature. Digitally controlled magnetic agitator-photobioreactors were placed inside a closed chamber with air flow for 4 weeks, under a uniform full-time light intensity provided by two 6-watt white fluorescent light sources. To study the effects of shear stress produced by mechanical agitation on the growth rate of a micro-organism, different agitation frequencies were tested. All reactors were filled with 150 ml of culture medium and micro-organism suspension, with initial dilution factors (mlsuspenion/mltotal volume) of 1/30 and 1/300 for Synechocystis and C. reinhardtii respectively. The vessels were placed on different agitating systems at the desired agitator rotation speed, and were sealed with a cotton membrane from the top in order to permit air exchange with the external environment. The micro-organisms’ growth was monitored daily by measuring the optical density of the suspensions using a spectrophotometer and was then correlated with the cellular concentration, which was measured in turn using a microscopic cell counter. Throughout the experiments pH levels and temperature were measured regularly and adjusted to 7 and 20 °C respectively in order to maintain the photosynthetic activity of the species. In addition, to measure the shear stress inside the agitated reactors, a mathematical model was derived to determine the global shear stress magnitude. To determine the local shear stress distribution, the velocity field in the reactor was measured for different agitation frequencies using PIV. Different zones of high and low shear stress were identified. The results showed that the growth rate is independent of the shear stress magnitude for Synechocystis; Synechocystis showed strong resistance, unlike C. reinhardtii, which showed linear dependence of growth rate and shear stress.
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