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Artículos de revistas sobre el tema "Cp2TiCl"

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Publicado: 6 de septiembre de 2023

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1

Cozak, Daniel, Abdelhakim Mardhy y André Morneau. "Titanocene derivatives of purine and adenine. Synthesis and characterization of reaction products with (η5-C5H5)2Ti(CO)2, (η5-C5H5)2TiCl, and (η5-C5H5)2TiCl2". Canadian Journal of Chemistry 64, n.º 4 (1 de abril de 1986): 751–59. http://dx.doi.org/10.1139/v86-121.

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The reaction of CpTi(CO)2 (1), Cp2TiCl (2), and Cp2TiCl2 (3) (Cp = η5-C5H5) with purine (PuH) and adenine (AdH) in organic solvents is described. The compound 1 reacts with both molecules in an oxidative fashion giving Cp2Ti(C5H3N4)(C5H4N4) (4) and (Cp2Ti)2(C5H3N5) (5) with concomitant liberation of molecular carbon monoxide and hydrogen (4:1) following a first order rate law in metal complex. The compound 2 forms an adduct compound Cp2TiCl(C5H4N4) (6) with PuH. Monosubstituted derivatives Cp2TiCl(C5H3N4) (7) and Cp2TiCl(C5H4N5) (8) are formed from the reaction of the deprotonated bases with 3. In addition to the usual elemental analysis, the characteristic ir, 1H nmr, epr, and ms results are given for the new compounds.
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2

Maué, Paul G. y Dieter Fenske. "Zur Reaktion von [Cp2TiCl2] und [CpTiCl3] mit E(SiMe3)2 (E = S, Se) Die Kristallstrukturen von [Cp3Ti2S2Cl], [Cp4Ti2S2Cl2], [Cp3Ti2Se2Cl] und [Cp4Ti4Se7O] / Reaction of [Cp2TiCl2] and [CpTiCl3 ] with E(SiMe 3)2 (E = S. Se) The Crystal Structures of [Cp3Ti2S2Cl], [Cp3Ti2S2Cl2], [Cp3Ti2Se2Cl] and [Cp4Ti4Se7O]". Zeitschrift für Naturforschung B 43, n.º 10 (1 de octubre de 1988): 1213–18. http://dx.doi.org/10.1515/znb-1988-1001.

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Abstract The reaction of [Cp2TiCl2 ] with E(SiMe3)2 leads to dinuclear Ti complexes. In [Cp3Ti2S2Cl] (1) and [Cp3Ti2Se2Cl] (3) two μ2 -S(Se) ligands bridge the Cp2Ti and CpTiCl units, respectively in contrast to these, [Cp4Ti2S2Cl2] (2) contains a μ2η1-S2 bridge connecting two Cp2TiCl fragments. A similar reaction of [CpTiCl3] with Se(SiMe3)2 leads to the tetranuclear cluster [Cp4Ti4Se7O] (4). 4 consists of a Ti4 -tetrahedron which encloses an oxygen atom.
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3

Thewalt, Ulf y Reinhard Friedrich. "Cp2TiIV-Komplexe mit Oximatoliganden / Cp2TiIV Complexes with Oximato Ligands". Zeitschrift für Naturforschung B 46, n.º 4 (1 de abril de 1991): 475–82. http://dx.doi.org/10.1515/znb-1991-0409.

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The reaction of Cp2TiCl2 with oximes in the two phase system (CHCl3, Cp2TiCl2)/(H2O, NaOH, oxime) leads to ionic complexes of the type [Cp2TiIV(H2O)(oximato)]+X-. Several complexes of this type were prepared. They are surprisingly stable against air and water. The following compounds are described in detail: [Cp2Ti(H2O)(ONC6H10)]NO3 (8) containing a cyclohexanoneoximato ligand, and two complexes with 1,4-cyclohexanedionedioximato ligands, namely the mononuclear complex [Cp2Ti(H2O)(ONC6H8NOH)]Cl · H2O (9) and the dinuclear complex [Cp2Ti(H2O)(ONC6H8NO)(H2O)TiCp2](NO3)2 · 4H2O (10). X-ray structure determinations show, that the ON fragment of the oximato ligand acts as side-on bonded three-electron donating ligand. The Ti atom thus has an 18-electron configuration.
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4

Breunig, H. J., O. Moldovan, M. Nema, U. Rosenthal, C. I. Rat y R. A. Varga. "Formation of [Cp2TiSbMe2]2, [Cp2TiSb(SiMe3)2]2 and [Cp2TiCl]2·2Mes4Sb2". Journal of Organometallic Chemistry 696, n.º 2 (enero de 2011): 523–26. http://dx.doi.org/10.1016/j.jorganchem.2010.09.007.

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5

Srivastava, A. K., O. P. Pandey y S. K. Sengupta. "Synthesis, Spectral and Antimicrobial Studies of Bis(cyclopentadienyl)titanium(IV) Derivatives with Schiff Bases Derived from 2-Amino-5-phenyl-1,3,4-thiadiazole". Bioinorganic Chemistry and Applications 3, n.º 3-4 (2005): 289–97. http://dx.doi.org/10.1155/bca.2005.289.

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The reactions of bis(cyclopentadienyl)titanium(IV) dichloride with Schiff bases derived by condensing 2- amino-5-phenyl-1,3,4-thiadiazole with benzaldehyde (SPT), 4-nitrobenzaldehyde (SNT), 4-methoxybenzaldehyde (SMT), 2-hydroxybenzaldehyde (SSTH) or 2-hydroxyacetophenone (SATH) have been studied in refluxing tetrahydrofuran and complexes of types [Cp2TiCl(SB)]Cl (SB= SPT, SNT or SMT) and [Cp2Ti(SB')]Cl (SB'H= SSTH or SATH) have been isolated. Tentative structural conclusions are drawn for these reaction products based upon elemental analyses, electrical conductance, magnetic moment and spectral (UV-vis, IR and1H NMR) data. Studies were conducted to assess the growth-inhibiting potential of the complexes synthesized, and the ligands, against various fungal and bacterial strains.
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6

Rosales, Jennifer, Gustavo Cabrera y José Justicia. "Exploring Short and Efficient Synthetic Routes Using Titanocene(III)-Catalyzed Reactions: Total Synthesis of Natural Meroterpenes with Trisubstituted Unsaturations". Molecules 27, n.º 8 (8 de abril de 2022): 2400. http://dx.doi.org/10.3390/molecules27082400.

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The stereo- and regioselective total syntheses of OMe derivatives of the scarce bioactive meroterpenoids makassaric acid (1) and fascioquinol B (2) have been accomplished. The synthetic sequences are based on the following three efficient and selective catalytic reactions: Cu-catalyzed addition of Grignard compounds to an epoxide; a regioselective Barbier-type reaction, catalyzed by Cp2TiCl; and regio- and stereoselective bioinspired cyclization, also catalyzed by Cp2TiCl. These three key processes allow us to obtain the main skeletons of 1 and 2 in a few steps. The valuable synthetic proposal shown in this work provides fast access to scarce, structurally complex meroterpenes with promising biological activities, which are a sustainable source for later studies and applications in medicine.
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7

Song, Li-Cheng, Cong Han, Qing-Mei Hu y Zhi-Pan Zhang. "Synthesis of new organotitanium (IV) complexes Cp2Ti(SeR)2 and Cp2TiCl(SeR) via tandem reactions involving `Cp2Ti' intermediate. Crystal structures of Cp2TiCl(SeR) (R=p-ClC6H4, p-BrC6H4)". Inorganica Chimica Acta 357, n.º 8 (junio de 2004): 2199–204. http://dx.doi.org/10.1016/j.ica.2003.06.011.

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8

Rosales Martínez, Antonio, Juan F. García-Martín y Ignacio Rodríguez-García. "Cp2TiCl/H2O as a Sustainable System for the Reduction of Organic Functional Groups: Potential Application of Cp2TiCl/D2O to the Analysis of Bioactive Phenols in Olive Oil". Processes 11, n.º 4 (23 de marzo de 2023): 979. http://dx.doi.org/10.3390/pr11040979.

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Significant efforts have been made toward developing sustainable reduction reactions of organic and bioorganic compounds. In these studies, the selection of reagents and solvents has played a very important role in the development of environment-friendly methodologies. In this context, the reducing agent Cp2TiCl/H2O has been introduced as a safe, efficient, selective, and low-cost reagent, and thus as a sustainable alternative for the reduction of organic compounds. To facilitate understanding of the reductions mediated by this system, in this study we focus on describing the intermediates, mechanisms, and representative examples. Finally, a reflection is made on the future perspectives of this reducing agent, including its analog Cp2TiCl/D2O as a powerful tool for the preparation of deuterated phenols, which can be successfully used as an internal standard for analyzing bioactive phenols in olive oil.
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9

Rosales, Antonio y Ignacio Rodríguez-García. "Cp2TiCl/D2O/Mn, a formidable reagent for the deuteration of organic compounds". Beilstein Journal of Organic Chemistry 12 (25 de julio de 2016): 1585–89. http://dx.doi.org/10.3762/bjoc.12.154.

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Cp2TiCl/D2O/Mn is an efficient combination, sustainable and cheap reagent that mediates the D-atom transfer from D2O to different functional groups and can contribute to the synthesis of new deuterated organic compounds under friendly experimental conditions and with great economic advantages.
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10

Castro Rodríguez, María, Ignacio Rodríguez García, Roman Nicolay Rodríguez Maecker, Laura Pozo Morales, J. Enrique Oltra y Antonio Rosales Martínez. "Cp2TiCl: An Ideal Reagent for Green Chemistry?" Organic Process Research & Development 21, n.º 7 (22 de junio de 2017): 911–23. http://dx.doi.org/10.1021/acs.oprd.7b00098.

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11

Gordon, Jonathan, Sven Hildebrandt, Kendra R. Dewese, Sven Klare, Andreas Gansäuer, T. V. RajanBabu y William A. Nugent. "Demystifying Cp2Ti(H)Cl and Its Enigmatic Role in the Reactions of Epoxides with Cp2TiCl". Organometallics 37, n.º 24 (30 de noviembre de 2018): 4801–9. http://dx.doi.org/10.1021/acs.organomet.8b00793.

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12

Morcillo, Sara P., Delia Miguel, Araceli G. Campaña, Luis Álvarez de Cienfuegos, José Justicia y Juan M. Cuerva. "Recent applications of Cp2TiCl in natural product synthesis". Org. Chem. Front. 1, n.º 1 (2014): 15–33. http://dx.doi.org/10.1039/c3qo00024a.

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13

Kool, Lawrence B., Marvin D. Rausch, Helmut G. Alt, Max Herberhold, Brigitte Wolf y Ulf Thewalt. "Structural and spectroscopic comparison of the complexes Cp2M(PMe3)(CO) (M = Ti, Zr, Hf), (C9H7)2Ti(PMe3)(CO) and Cp2TiCl(PMe3); X-ray structures of Cp2Ti(PMe3)(CO) and Cp2TiCl(PMe3)". Journal of Organometallic Chemistry 297, n.º 2 (diciembre de 1985): 159–69. http://dx.doi.org/10.1016/0022-328x(85)80414-9.

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14

Rosales Martínez, Antonio. "Cp2TiCl is a useful reagent to teach multidisciplinary chemistry". Educación Química 32, n.º 5 (4 de octubre de 2021): 191. http://dx.doi.org/10.22201/fq.18708404e.2021.5.77418.

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15

Hardouin, Christophe, Floris Chevallier, Bernard Rousseau y Eric Doris. "Cp2TiCl-Mediated Selective Reduction of α,β-Epoxy Ketones". Journal of Organic Chemistry 66, n.º 3 (febrero de 2001): 1046–48. http://dx.doi.org/10.1021/jo001358g.

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16

Monleón, Laura M., Manuel Grande y Josefa Anaya. "Radical cyclisation of epoxynitrile-2-azetidinones mediated by Cp2TiCl". Tetrahedron 63, n.º 14 (abril de 2007): 3017–25. http://dx.doi.org/10.1016/j.tet.2007.01.049.

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17

Moisan, Lionel, Christophe Hardouin, Bernard Rousseau y Eric Doris. "Cp2TiCl-mediated selective reduction of α,β-unsaturated ketones". Tetrahedron Letters 43, n.º 11 (marzo de 2002): 2013–15. http://dx.doi.org/10.1016/s0040-4039(02)00170-3.

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18

Hansen, Thomas, Sussie L. Krintel, Kim Daasbjerg y Troels Skrydstrup. "A convenient synthesis of glycals employing in-situ generated Cp2TiCl". Tetrahedron Letters 40, n.º 33 (agosto de 1999): 6087–90. http://dx.doi.org/10.1016/s0040-4039(99)01266-6.

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19

Márquez, Irene R., Alba Millán, Araceli G. Campaña y Juan M. Cuerva. "Cp2TiCl-catalyzed highly stereoselective intramolecular epoxide allylation using allyl carbonates". Org. Chem. Front. 1, n.º 4 (2014): 373–81. http://dx.doi.org/10.1039/c4qo00012a.

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20

Rosales Martínez, Antonio, Laura Pozo Morales y Emilio Díaz Ojeda. "Cp2TiCl-catalyzed, concise synthetic approach to marine natural product (±)-cyclozonarone". Synthetic Communications 49, n.º 19 (9 de julio de 2019): 2554–60. http://dx.doi.org/10.1080/00397911.2019.1633671.

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21

Morcillo, Sara P., Delia Miguel, Araceli G. Campana, Luis Alvarez de Cienfuegos, Jose Justicia y Juan M. Cuerva. "ChemInform Abstract: Recent Applications of Cp2TiCl in Natural Product Synthesis". ChemInform 45, n.º 25 (5 de junio de 2014): no. http://dx.doi.org/10.1002/chin.201425250.

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22

Asandei, Alexandru D. y Gobinda Saha. "Cp2TiCl-catalyzed living radical polymerization of styrene initiated from peroxides". Journal of Polymer Science Part A: Polymer Chemistry 44, n.º 3 (2005): 1106–16. http://dx.doi.org/10.1002/pola.21206.

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23

Grande, Manuel, Laura Monleón y Josefa Anaya. "Acyl Radicals from Nitriles Promoted by Cp2TiCl in β-Lactam Chemistry". Synlett 2010, n.º 08 (15 de abril de 2010): 1227–30. http://dx.doi.org/10.1055/s-0029-1219830.

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24

Grande, Manuel, Laura Monleón y Josefa Anaya. "Approach to Substituted Methylcarbapenems and Benzocarbacephems by Radical Cyclization Using Cp2TiCl". Synlett 2007, n.º 08 (8 de mayo de 2007): 1243–46. http://dx.doi.org/10.1055/s-2007-980336.

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25

Moisan, Lionel, Christophe Hardouin, Bernard Rousseau y Eric Doris. "ChemInform Abstract: Cp2TiCl-Mediated Selective Reduction of α,β-Unsaturated Ketones." ChemInform 33, n.º 26 (21 de mayo de 2010): no. http://dx.doi.org/10.1002/chin.200226051.

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26

Hardouin, Christophe, Floris Chevallier, Bernard Rousseau y Eric Doris. "ChemInform Abstract: Cp2TiCl-Mediated Selective Reduction of α,β-Epoxy Ketones." ChemInform 32, n.º 27 (25 de mayo de 2010): no. http://dx.doi.org/10.1002/chin.200127105.

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27

Paradas, Miguel, Araceli G. Campaña, Maria Luisa Marcos, Jose Justicia, Ali Haidour, Rafael Robles, Diego J. Cárdenas, J. Enrique Oltra y Juan M. Cuerva. "Unprecedented H-atom transfer from water to ketyl radicals mediated by Cp2TiCl". Dalton Transactions 39, n.º 37 (2010): 8796. http://dx.doi.org/10.1039/c001689f.

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28

Hansen, Thomas, Sussie L. Krintel, Kim Daasbjerg y Troels Skrydstrup. "ChemInform Abstract: A Convenient Synthesis of Glycals Employing in situ Generated Cp2TiCl." ChemInform 30, n.º 44 (13 de junio de 2010): no. http://dx.doi.org/10.1002/chin.199944233.

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29

Spencer, Roxanne P. y Jeffrey Schwartz. "Variously substituted glycals are readily prepared from glycosyl bromides using (Cp2TiCl)2". Tetrahedron Letters 37, n.º 25 (junio de 1996): 4357–60. http://dx.doi.org/10.1016/0040-4039(96)00865-9.

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30

Bermejo, Francisco y Celso Sandoval. "Cp2TiCl-Promoted Isomerization of Trisubstituted Epoxides toexo-Methylene Allylic Alcohols on Carvone Derivatives". Journal of Organic Chemistry 69, n.º 16 (agosto de 2004): 5275–80. http://dx.doi.org/10.1021/jo049358u.

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31

Asandei, Alexandru D., Yanhui Chen, Gobinda Saha y Isaac W. Moran. "Cp2TiCl-catalyzed radical chemistry: living styrene polymerizations from epoxides, aldehydes, halides, and peroxides". Tetrahedron 64, n.º 52 (diciembre de 2008): 11831–38. http://dx.doi.org/10.1016/j.tet.2008.08.106.

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32

Begum, Sabnam y Tushar Kanti Chakraborty. "Cp2TiCl-Mediated Reductive Cyclization: Total Synthesis of Pestalotiolactone A, Myrotheciumone A, and Scabrol A". Journal of Organic Chemistry 86, n.º 17 (2 de agosto de 2021): 11812–21. http://dx.doi.org/10.1021/acs.joc.1c01243.

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33

Khan, Hina P. A. y Tushar Kanti Chakraborty. "Application of Cp2TiCl-Promoted Radical-Induced Cyclization: An Expeditious Access to [a]-Annelated Indoles". Journal of Organic Chemistry 85, n.º 12 (29 de mayo de 2020): 8000–8012. http://dx.doi.org/10.1021/acs.joc.0c00817.

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34

Asandei, Alexandru D. y Yanhui Chen. "Cp2TiCl-Catalyzed SET Reduction of Aldehydes: A New Initiating Protocol for Living Radical Polymerization". Macromolecules 39, n.º 22 (octubre de 2006): 7549–54. http://dx.doi.org/10.1021/ma0604791.

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35

Asandei, Alexandru D. y Gobinda Saha. "Cp2TiCl-Catalyzed Epoxide Radical Ring Opening: A New Initiating Methodology for Graft Copolymer Synthesis". Macromolecules 39, n.º 26 (diciembre de 2006): 8999–9009. http://dx.doi.org/10.1021/ma0618833.

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36

SPENCER, R. P. y J. SCHWARTZ. "ChemInform Abstract: Variously Substituted Glycals Are Readily Prepared from Glycosyl Bromides Using (Cp2TiCl)2." ChemInform 27, n.º 41 (4 de agosto de 2010): no. http://dx.doi.org/10.1002/chin.199641205.

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37

von Gudenberg, Dorothea Wolff, Hak-Chul Kang, Werner Massa, Kurt Dehnicke, C�cilia Maichle-M�ssmer y Joachim Str�hle. "Silanolato-Komplexe von Titan und Zirconium. Die Kristallstrukturen von Cp2TiCl(OSiPh3) und Cp2ZrCl(OSiPh3)". Zeitschrift f�r anorganische und allgemeine Chemie 620, n.º 10 (octubre de 1994): 1719–24. http://dx.doi.org/10.1002/zaac.19946201010.

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38

Fenske, D., A. Grissinger, E. M. Hey-Hawkins y J. Magull. "Zur Reaktion von [Cp2TiCl]2 und TiCl4 mit LiE(SiMe3)2 (E = P, As) und P(SiMe3)3 Die Kristallstrukturen von [Cp2TiP(SiMe3)2], [(Cp2Ti)2ClAs(SiMe3)2] und [TiCl3 {P(SiMe3)3}2]". Zeitschrift f�r anorganische und allgemeine Chemie 595, n.º 1 (abril de 1991): 57–66. http://dx.doi.org/10.1002/zaac.19915950109.

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39

Kunkely, Horst y Arnd Vogler. "Photoreactivity of Titanocene Pentasulfide". Zeitschrift für Naturforschung B 53, n.º 2 (1 de febrero de 1998): 224–26. http://dx.doi.org/10.1515/znb-1998-0214.

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Abstract The electronic spectrum of Cp2TiS5 shows a long-wavelength absorption at λ max = 492 nm which is assigned to the lowest-energy S52- → TiIV ligand-to-metal charge transfer (LMCT) transition. The photolysis of the complex in CH2CI2 leads to the formation of Cp2TiCl2 and elemental sulfur. It is suggested that LMCT excitation initiates a reductive elimination with the extrusion of S5 while the reduced titanocene is reoxidized by the solvent.
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40

Khan, Hina P. A., Dipendu Das y Tushar Kanti Chakraborty. "Application of Cp2TiCl-Promoted Radical Cyclization: A Unified Strategy for the Syntheses of Iridoid Monoterpenes". Journal of Organic Chemistry 83, n.º 11 (16 de mayo de 2018): 6086–92. http://dx.doi.org/10.1021/acs.joc.8b00752.

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41

Chakraborty, Tushar Kanti, Rajarshi Samanta y Sanjib Das. "Radical-Mediated Opening of 2,3-Epoxy Alcohols Using Cp2TiCl: Stereoselective Construction of Quaternary Chiral Centers†". Journal of Organic Chemistry 71, n.º 8 (abril de 2006): 3321–24. http://dx.doi.org/10.1021/jo0600961.

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42

Avdeev, A. V., L. I. Gvinter y V. Z. Sharf. "Hydrogenation and isomerization of allylbenzene in the presence of the (Cp2TiCl)2-LiAlH4 catalytic system". Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 38, n.º 3 (marzo de 1989): 655–57. http://dx.doi.org/10.1007/bf00958075.

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43

Monlen, Laura M., Manuel Grande y Josefa Anaya. "Synthesis of polycyclic ?-lactams. Evolution of tertiary radicals generated by Cp2TiCl from 1,5- and 1,6-epoxynitriles". Tetrahedron 68, n.º 52 (diciembre de 2012): 10794–805. http://dx.doi.org/10.1016/j.tet.2011.11.015.

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44

Asandei, Alexandru D., Yanhui Chen, Isaac W. Moran y Gobinda Saha. "Similarities and differences of epoxide, aldehyde and peroxide initiators for Cp2TiCl-catalyzed styrene living radical polymerizations". Journal of Organometallic Chemistry 692, n.º 15 (julio de 2007): 3174–82. http://dx.doi.org/10.1016/j.jorganchem.2007.01.042.

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45

Chakraborty, Tushar Kanti, Rajarshi Samanta y Krishnan Ravikumar. "Studies on radical cyclization of 2,3-epoxy alcohols containing a β-(alkoxy)acrylate moiety using Cp2TiCl". Tetrahedron Letters 48, n.º 36 (septiembre de 2007): 6389–92. http://dx.doi.org/10.1016/j.tetlet.2007.06.139.

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46

Chakraborty, Tushar K. y Sanjib Das. "Synthesis of chiral 1,3-diols by radical-mediated regioselective opening of 2,3-epoxy alcohols using cp2TiCl". Tetrahedron Letters 43, n.º 12 (marzo de 2002): 2313–15. http://dx.doi.org/10.1016/s0040-4039(02)00241-1.

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47

Barrero, Alejandro F., M. Mar Herrador, José F. Quílez del Moral, Pilar Arteaga, Jesús F. Arteaga, María Piedra y Elena M. Sánchez. "Reductive Coupling of Terpenic Allylic Halides Catalyzed by Cp2TiCl: A Short and Efficient Asymmetric Synthesis of Onocerane Triterpenes". Organic Letters 7, n.º 12 (junio de 2005): 2301–4. http://dx.doi.org/10.1021/ol050335r.

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Liu, Xiao-hui, Zhong-min Dong, Xiu-lan Tang y Yue-sheng Li. "Synthesis and characterization of hyperbranched polymers via Cp2TiCl-catalyzed self-condensing vinyl polymerization using glycidyl methacrylate as inimer". Polymer 51, n.º 4 (febrero de 2010): 854–59. http://dx.doi.org/10.1016/j.polymer.2009.12.042.

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Chakraborty, Tushar K. y Sanjib Das. "ChemInform Abstract: Synthesis of Chiral 1,3-Diols by Radical-Mediated Regioselective Opening of 2,3-Epoxy Alcohols Using Cp2TiCl." ChemInform 33, n.º 26 (21 de mayo de 2010): no. http://dx.doi.org/10.1002/chin.200226088.

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Anaya, Josefa, Manuel Grande, Laura M. Monleón y Ramón M. Sánchez. "Synthesis and reactivity against Cp2TiCl of 4-isoprenyl-β-lactams. Trapping of N-titanoimidoyl radicals from cyanoformyl-2-azetidinones". Tetrahedron 74, n.º 38 (septiembre de 2018): 5415–26. http://dx.doi.org/10.1016/j.tet.2018.01.003.

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