Literatura académica sobre el tema "353(.25)"
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Artículos de revistas sobre el tema "353(.25)"
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Villegas, Victor M., Aaron Gold y Timothy G. Murray. "Fine-Needle Aspiration Biopsy for Molecular Genomic Classification: Evaluation of Transscleral vs Transvitreal Biopsy". Journal of VitreoRetinal Diseases 2, n.º 4 (22 de junio de 2018): 208–12. http://dx.doi.org/10.1177/2474126418782069.
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Purpose: To evaluate the transvitreal and transscleral fine-needle aspiration biopsy (FNAB) approach for molecular classification with gene-expression profiling (GEP) of uveal melanoma. Methods: Institutional review board–approved single-surgeon retrospective analysis of a consecutive case series of all patients undergoing FNAB using a 25-gauge-needle multipass approach for GEP analysis of uveal melanoma between 2012 and 2016. All FNAB specimens were processed for uveal melanoma diagnostic testing using a standard processing approach, and all testing was completed at a single laboratory (Castle Biosciences, Inc.). Results: Three hundred fifty-three eyes (353 patients) were included. Transvitreal biopsies were performed in 216 eyes (216/353, 61.2%), whereas transscleral biopsies were performed in 137 eyes (137/353, 38.8%). Twenty biopsies exhibited multiple gene failure (20/353, 5.6%). Excessive fluid biopsy volume was the primary association with reported multiple gene failure, occurring in 10 of 20 eyes (50%). FNAB performed via the transvitreal approach was significantly more likely to have an excessive volume report compared with transscleral biopsy (18/216, 8.3% vs 1/137, 0.7%; P < .001). Conclusions: FNAB performed via a transscleral or transvitreal multipass approach utilizing a 25-gauge needle achieves molecular classification in 95% of all patients undergoing treatment for presumed uveal melanoma independent of tumor size. Complications related to FNAB using these techniques are rare and may be associated with the presentation of the uveal melanoma.
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Bhardwaj, Vinay, Ashwani Kumar, Sanjeev Sharma, Baljeet Singh, Poonam, Salej Sood, Bhawna Dipta et al. "Analysis of Genetic Diversity, Population Structure and Association Mapping for Late Blight Resistance in Potato (Solanum tuberosum L.) Accessions Using SSR Markers". Agronomy 13, n.º 2 (18 de enero de 2023): 294. http://dx.doi.org/10.3390/agronomy13020294.
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The allelic variations in a diversity panel of 353 potato accessions, including 256 accessions belonging to Solanum tuberosum sub spp. tuberosum, 49 accessions belonging to Solanum tuberosum sub spp. andigena, and 48 Indian potato varieties were analysed using 25 simple sequence repeat (SSR) markers. The SSR allelic profiles revealed high levels of polymorphism and distinctness among the accessions studied. A total of 343 alleles of 25 SSR markers were observed in the diversity panel of 353 highly diverse tetraploid potato accessions. The number of alleles produced per SSR varied from 8 for the marker STM1053 to 25 for the marker STIKA. The polymorphic information content (PIC) ranged from 0.66 (STG0010) to 0.93 (STM1106) with an average of 0.82. The cluster analysis using the SSR allelic profiles of 353 accessions divided the population into five major groups. The association mapping for late blight resistance identified six markers with the general linear model (GLM), and out of these six markers significance of three markers was reconfirmed with the mixed linear model (MLM). The findings of this study suggest that SSRs are the appropriate markers for evaluating genetic diversity and population structure within different potato germplasm collections. A significant diversity across the tetraploid potato accessions was observed. Moreover, the markers identified in this study could be useful in marker-assisted selection (MAS) breeding in potato for late blight resistance (LBR).
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Qiao, Qiao, Hua-Jiang Wang, Cui-Ping Li, Xiao-Zu Wang y Xiao-Ming Ren. "Improving proton conduction of the Prussian blue analogue Cu3[Co(CN)6]2·nH2O at low humidity by forming hydrogel composites". Inorganic Chemistry Frontiers 8, n.º 9 (2021): 2305–14. http://dx.doi.org/10.1039/d1qi00070e.
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Composites of Prussian blue analogue (PBA) adsorbed imidazole-acetic acid with polyvinyl alcohol hydrogel show excellent water-retention capacity and fast proton conduction at 25% RH in 298–353 K, herein X is the mass ratio of PBA to hydrogel.
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Rogerson, A. "Irradiation growth in annealed and 25% cold-worked Zircaloy-2 between 353–673 K". Journal of Nuclear Materials 154, n.º 2-3 (julio de 1988): 276–85. http://dx.doi.org/10.1016/0022-3115(88)90364-9.
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Perrod, Guillaume, Elia Samaha, Gabriel Rahmi, Sherine Khater, Leila Abbes, Camille Savale, Geraldine Perkins et al. "Impact of an optimized colonoscopic screening program for patients with Lynch syndrome: 6-year results of a specialized French network". Therapeutic Advances in Gastroenterology 11 (1 de enero de 2018): 175628481877505. http://dx.doi.org/10.1177/1756284818775058.
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Background: Despite colonoscopic screening, colorectal cancer (CRC) remains frequent in patients with Lynch syndrome (LS). The objective of this study was to evaluate the impact of an optimized colorectal screening program within a French dedicated network. Methods: All LS patients followed at our institution were consecutively included in the Prédisposition au Cancer Colorectal-Ile de France (PRED-IdF) network. Patients were offered an optimized screening program allowing an adjustment of the interval between colonoscopies, depending on bowel preparation, chromoendoscopy achievement and adenoma detection. Colonoscopies were defined as optimal when all the screening criteria were respected. We compared colonoscopy quality and colonoscopy detection rate before and after PRED-IdF inclusion, including polyp detection rate (PDR), adenoma detection rate (ADR) and cancer detection rate (CDR). Results: Between January 2010 and January 2016, 144 LS patients were consecutively included (male/female = 50/94, mean age = 51 ± 13 years and mutations: MLH1 = 39%, MSH2 = 44%, MSH6 = 15%, PMS2 = 1%). A total of 564 colonoscopies were analyzed, 353 after inclusion and 211 before. After PRED-IdF inclusion, 98/144 (68%) patients had optimal screening colonoscopies versus 33/132 (25%) before ( p < 0.0005). The optimal colonoscopy rate was 304/353 (86%) after inclusion versus 87/211 (41%) before, ( p < 0.0001). PRED-IdF inclusion was associated with a reduction of CRC occurrence with a CDR of 1/353 (0.3%) after inclusion versus 6/211 (2.8%) before ( p = 0.012). ADR and PDR were 99/353 (28%) versus 60/211 (28.8%) ( p > 0.05) and 167/353 (48.1%) versus 90/211 (42.2%) ( p > 0.05), respectively after and before inclusion. Conclusions: An optimized colonoscopic surveillance program in LS patients seems to improve colonoscopic screening quality and might possibly decrease colorectal interval cancer occurrence. Long-term cohort studies are needed to confirm these results.
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Dolbeault, Joël. "Sébastien Balibar & Edouard Brézin , Demain, la physique , Odile Jacob, 2009, 353 pages, 25 €". Études Tome 412, n.º 3 (1 de marzo de 2010): XVI. http://dx.doi.org/10.3917/etu.4123.0405p.
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Smirnov, E. "New in Financial Legislation". Auditor 8, n.º 9 (7 de noviembre de 2022): 3–9. http://dx.doi.org/10.12737/1998-0701-2022-8-9-3-9.
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In the course of improving fi nancial legislation based on an analysis of market practice, the Parliament of Russia this year adopted, in particular, Federal Laws No. 61-FZ dated March 25, 2022, No. 97-FZ dated April 16, 2022 and No. 353-FZ dated increasing the level of protection of the fi nancial interests of the state and the individual.
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Al-Maali, G. A., N. A. Bisko y A. M. Ostapchuk. "The effect of citrate and sulfate of different metals on carbohydrates composition of medicinal mushroom Trametes versicolor (Polyporales, Polyporaceae)". Visnyk of Dnipropetrovsk University. Biology, medicine 7, n.º 1 (9 de marzo de 2016): 32–36. http://dx.doi.org/10.15421/021606.
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The aim of our research was to study the influence of citrate and sulfate of copper, manganese and zinc on the carbohydrates composition of biomass of the medicinal mushroom Trametes versicolor (L.) Lloyd. cultivated in a liquid medium. The studied strain of Trametes versicolor 353 was obtained from the Culture Collection of Mushrooms (IBK) from the M. G. Kholodny Institute of Botany, National Academy of Sciences of Ukraine. Citrates of copper, manganese and zinc were obtained from the Institute of Nanobiotechnologies and Resource Conservation of Ukraine, Kyiv. In this study we used glucose-peptone-yeast extract medium (GPY) with the following composition of (g/L): glucose – 25, peptone – 3, yeast extract – 3, K2HPO4 – 1, KH2PO4 – 1, MgSO4 ∙ 7H2O – 0.25, distilled water – 1,000 ml; pH 6,5 (control medium). Cu2+ (sulfate form or citrate form) were added to control medium in concentration 4 mg/L, Zn2+ and Mn2+ (sulfate form or citrate form) were added to control medium in concentration 1 mg/L. Mycelium was grown in a submerged culture on a rotary shaker (120 rpm) at 26 °C in 250 ml Erlenmeyer flasks, containing 50 ml of liquid medium. The biomass was harvested after 9 days of cultivation in the liquid medium. Monosaccharides and sugar alcohols was analyzed by high-performance liquid chromatography Agilent 1200 (Agilent technologies, USA). The results of our research demonstrated that the fraction of total carbohydrates from T. versicolor 353, which were cultivated on the control medium, consists of glucose (91.5%), galactose (1.9%), mannose (5.4%), fucose (0.6%) and xylose (0.7%). The adding of sulfate of zinc or copper to the liquid medium didn’t change the content of monosaccharides of T. versicolor 353 biomass relative to the control medium. At the same time, in the medium with citrate of zinc the amount of glucose increased and the amount of mannose decreased relative to the control medium. Xylose and fucose were not detected in this case. In mycelium of T. versicolor 353 that was cultivated in the medium with manganese sulfate or manganese citrate we detected a small amount of ribose. But the content of other monosaccharides didn’t change in the medium with sulfate of manganese. At the same time, the addition of citrate of manganese to the medium raised the amount of mannose and reduced the amount of glucose in the biomass of T. versicolor 353 relative to the control medium. Also copper citrate reduced the content of glucose in mycelium of T. versicolor 353 relative to the control medium. But in this case we detected mannitol and sorbitol in the biomass. This data indicates that synthesis of sugur alcohols in T. versicolor 353 depend on copper ions in bioactive forms of citrate.
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John, Elenjickal Elias, Athul Thomas, Jeethu Joseph Eapen, Sabina Yusuf, Sanjeet Roy, Anna T. Valson, Vinoi George David, Santosh Varughese y Suceena Alexander. "Latency, Anti-Bacterial Resistance Pattern, and Bacterial Infection–Related Glomerulonephritis". Clinical Journal of the American Society of Nephrology 16, n.º 8 (7 de junio de 2021): 1210–20. http://dx.doi.org/10.2215/cjn.18631120.
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Background and objectivesBacterial infection–related GN occurs concurrent to or after known or unknown infections. It is important to understand the clinical implications of the bacterial isolates, antimicrobial resistance patterns, and effect of latency-based classification on kidney and patient outcomes.Design, setting, participants, & measurementsIn total, 501 consecutive adults diagnosed with bacterial infection–related GN between 2005 and 2017 were included from a biopsy registry of 15,545 patients at a single center in South India, and follow-up data were collected from electronic medical records until December 2019. Latency was defined as time between resolution of infection and onset of GN, which was classified as parainfectious, peri-infectious, or postinfectious GN. Longitudinal kidney and patient outcomes were studied.ResultsThe mean age of the cohort was 40 (± 15) years, 6% were above 65 years, and 330 (66%) were men. Diabetes was present in 93 (19%) patients. Seventy percent (353 of 501) of patients had known infections, with the median latent period for parainfectious (115 of 353, 33%), peri-infectious (97 of 353, 27%), and postinfectious (141 of 353, 40%) GN being 0, 5 (4–7), and 15 (10–31) days, respectively. The most common predisposing organism was Streptococcus pyogenes (137 of 353, 39%). Drug-resistant nonstreptococcal bacteria were methicillin-resistant Staphylococcus aureus (25%, four of 16), extended-spectrum β-lactamases (20%, 12 of 59), and carbapenem-resistant organisms (10%, six of 59). Twenty of 22 (91%) of the drug-resistant organisms were isolated from the parainfectious group. The most common site of infection was skin in peri- (23 of 97, 24%) and postinfectious GN (61 of 141, 43%), and urinary tract in parainfectious GN (35 of 115, 30%). Of 321 patients with >3 months of follow-up, 48 (15%) developed kidney failure over a median period of 10 (2–37) months and 14 (4%) died. Parainfectious GN, eGFR<30 ml/min per 1.73 m2, moderate-to-severe interstitial fibrosis and tubular atrophy, and nontreatment with renin-angiotensin system blockers were significant risk factors for progression to kidney failure by a Cox proportional-hazards model.ConclusionsAlong with clinical and histologic predictors, parainfectious GN caused predominantly by nonstreptococcal and drug-resistant bacterial infections was associated with poor kidney prognosis.
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Paiz, Laís Moraes, Rodrigo Costa da Silva, Benedito Donizete Menozzi y Helio Langoni. "Antibodies to Neospora caninum in sheep from slaughterhouses in the state of São Paulo, Brazil". Revista Brasileira de Parasitologia Veterinária 24, n.º 1 (marzo de 2015): 95–100. http://dx.doi.org/10.1590/s1984-29612015009.
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Neosporosis is an emergent disease responsible for considerable economic impact due to reproductive losses. Its zoonotic potential remains unknown. This study involved a survey of antibodies to Neospora caninum in slaughtered sheep and their association with epidemiological variables. Serum samples from 596 sheep from the states of São Paulo and Rio Grande do Sul, Brazil, were collected in two slaughterhouses located in São Paulo and evaluated by indirect fluorescence antibody test (IFAT), using cut-off titers of 25. Among these samples, 353/596 (59.23%; 95%CI 55.23-63.10) were positive and 263/353 (74.50%; 95%CI 69.71-78.77%) were from Rio Grande do Sul. Statistical associations were determined in the univariate analysis between the serological results and sex, breed and municipality of origin. Sheep that came from extensive breeding system showed higher chance (OR=2.09) of presenting antibodies to N. caninum in relation to those from semi-intensive system. Higher chance was also observed for the different studied breeds, except Bergamácia, in relation to Hampshire Down. The results revealed the presence of infection by N. caninum in sheep from slaughterhouses.
Tesis sobre el tema "353(.25)"
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Le, Bot Pierre. "La première marine de Louis XV : une expérience fondatrice (1715-1745)". Electronic Thesis or Diss., Sorbonne université, 2021. http://www.theses.fr/2021SORUL054.
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Après avoir été la première d’Europe, la marine de Louis XIV a commencé à s’effondrer à partir de 1707, et elle n’était déjà plus que l’ombre d’elle-même lorsque Louis XV a succédé à son arrière-grand-père en 1715. Secrétaire d’État de la Marine de 1723 à 1749, le comte de Maurepas est traditionnellement considéré comme le bâtisseur d’une nouvelle marine, qui aurait fait ses preuves au cours de la guerre de Succession d’Autriche, après une longue période de paix avec la Grande-Bretagne. Les archives du Conseil de Marine révèlent pourtant que c’est dès 1719, que cette reconstruction a été entreprise. Avec le soutien du Régent, les membres de ce conseil dirigé par le comte de Toulouse, Amiral de France, ont alors entrepris de se doter d’un instrument naval puissant, qu’ils destinaient à la guerre d’escadre. Pendant quelques années, d’importants efforts ont été faits pour mettre en chantier un grand nombre de nouveaux vaisseaux, avant que ce projet ne soit abandonné en 1725, suite à une forte réduction des dépenses. Il s’avère donc que le rôle de Maurepas a surtout consisté à entretenir, tant bien que mal, une marine restée inachevée. Il s’est également efforcé, il est vrai, de la préparer à la guerre de course qu’il entendait mener en cas de nouveau conflit contre la Grande-Bretagne. Le fait est cependant que les opérations qui ont suivi l’entrée en guerre de la France en 1744 ont très vite révélé, non seulement les limites de cette stratégie, mais aussi l’impuissance et les fragilités de la première marine de Louis XV, dont Maurepas prononcera lui-même l’acte de décès dans ses « Réflexions sur le commerce et sur la marine » de 1745After being the first in Europe, Louis XIV’s navy began to collapse from 1707, and it was already half-ruined when Louis XV succeeded its great grandfather in 1715. Having been Secretary of State for the Navy from 1723 to 1749, the Comte de Maurepas is traditionally regarded as the founder of a new navy, which would have proved its worth during the War of the Austrian Succession, after a long period of peace with Great Britain. However, the archives of the Navy Council reveal that it was as early as 1719 that this reconstruction was undertaken. With the support of the Regent, the members of this board headed by the Comte de Toulouse, Admiral of France, planned to create the naval instrument they needed for a guerre d’escadre. For a few years, great efforts were made to build a large number of new ships, before this program was abandoned in 1725, following a drastic budget reduction. It turns out, therefore, that Maurepas’s role was mainly to maintain, as best he could, a navy that remained unfinished. Admittedly, he also tried to prepare it for the guerre de course he intended to fight in the event of a new war with Great Britain. The fact is, however, that the naval operations which followed the outbreak of war in 1744 quickly revealed not only the limits of this strategy, but also the inability and the weaknesses of Louis XV's first navy, of which Maurepas himself performs the autopsy in his « Reflec- tions on Trade and Navy » of 1745
Libros sobre el tema "353(.25)"
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United States. Congress. Senate. Committee on Energy and Natural Resources. Subcommittee on Public Lands, Forests, and Mining. Current public lands, forests, and mining bills: Hearing before the Subcommittee on Public Lands, Forests, and Mining of the Committee on Energy and Natural Resources, United States Senate, One Hundred Thirteenth Congress, first session, on S. 27, S. 28, S. 159, S. 241, S. 255, S. 256, S. 258, S. 312, S. 327, S. 340, S. 341, S. 342, S. 353, S. 360, S. 366, S. 368, S. 447, S. 609, S. 736, S. 757, April 25, 2013. Washington: U.S. Government Printing Office, 2013.
Buscar texto completoCapítulos de libros sobre el tema "353(.25)"
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Cui, Shiliang, Zhongbin Wang y Luyi Yang. "Distance-Based Service Priority". En Innovative Priority Mechanisms in Service Operations, 99–118. Cham: Springer International Publishing, 2023. http://dx.doi.org/10.1007/978-3-031-30841-3_6.
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AbstractObtaining a service usually comes with both rewards and costs. For example, dining at a popular restaurant provides customers with a pleasant dining experience, but also incurs costs to them. The costs include the direct service charge that customers have to pay to receive the service (the meal cost) and indirect hassle costs such as going to the restaurant and waiting in line for the service. When the service reward is too low or the service fee is too high, customers will be less likely interested in the service. The same happens when the hassle cost of seeking service is too high, which is especially true when customers must travel a long distance to obtain a service that tends to have cumbersome wait times. It is without question that increasing the number of customers being served (i.e. system throughput) is critical for service providers, as it translates directly into service revenue in the case of a for-profit company and service provision in the case of a non-profit organization. Therefore, how may service providers incentivize customers located far away from the service location to seek service? In this chapter, we introduce an innovative but natural distance-based service priority mechanism to help service providers increase their system throughput. The idea is to assign higher service priority to customers who have to travel farther for the service, thus giving them with new incentives to consider using the service. We shall demonstrate, among other results, that such a mechanism can significantly increase system throughput by attracting more customers to use the service, and the increase can be up to 50% compared to the ordinary first-come-first-served service discipline. This chapter is primarily based on Wang et al. (Manuf Serv Oper Manag, 25(1), 353–369, 2023) where interested readers can find proofs of the findings shown in this chapter.
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Taber, Douglass F. "C–N Ring Construction: The Harrity Synthesis of Quinolizidine (–)-217A". En Organic Synthesis. Oxford University Press, 2015. http://dx.doi.org/10.1093/oso/9780190200794.003.0054.
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David M. Jenkins of the University of Tennessee devised (J. Am. Chem. Soc. 2011, 133, 19342) an iron catalyst for the aziridination of an alkene 1 with an aryl azide 2. Yoshiji Takemoto of Kyoto University cyclized (Org. Lett. 2011, 13, 6374) the prochiral oxime derivative 4 to the azirine 5 in high ee. Organometallics added to 5 syn to the pendant ester. Hyeung-geun Park of Seoul National University used (Adv. Synth. Catal. 2011, 353, 3313) a chiral phase transfer catalyst to effect the enantioselective alkylation of 6 to 7. Yian Shi of Colorado State University showed (Org. Lett. 2011, 13, 6350) that a chiral Brønsted acid mediated the enantioselective cyclization of 8 to 9. Mattie S.M. Timmer of Victoria University of Wellington and Bridget L. Stocker of Malaghan Institute of Medical Research effected (J. Org. Chem. 2011, 76, 9611) the oxidative cyclization of 10 to 11. They also showed (Tetrahedron Lett. 2011, 52, 4803, not illustrated) that the same cyclization worked well to construct piperidine derivatives. Jose L. Vicario of the Universidad del País Vasco extended (Adv. Synth. Catal. 2011, 353, 3307) organocatalysis to the condensation of 12 with 13 to give the pyrrolidine 14. Jinxing Ye of the East China University of Science and Technology used (Adv. Synth. Catal. 2011, 353, 343) the same Hayashi catalyst to condense 15 with 16 to give 17. André B. Charette of the Université de Montreal expanded (Org. Lett. 2011, 13, 3830) 18, prepared by Petasis-Mannich coupling followed by ring-closing metathesis, to the piperidine 20. Marco Bella of the “Sapienza” University of Roma effected (Org. Lett. 2011, 13, 4546) enantioselective addition of 22 to the prochiral 21 to give 23. Ying-Chun Chen of Sichuan University and Chun-An Fan of Lanzhou University cyclized (Adv. Synth. Catal. 2011, 353, 2721) 24 to 25 in high ee. Andreas Schmid of TU Dortmund showed (Adv. Synth. Catal. 2011, 353, 2501) that ω-laurolactam hydrolases could be used to cyclize the ester 26, but not the free acid, to the macrolactam 27.
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Taber, Douglass F. "Functional Group Transformations". En Organic Synthesis. Oxford University Press, 2015. http://dx.doi.org/10.1093/oso/9780190200794.003.0003.
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Mark Gandelman of the Technion–Israel Institute of Technology devised (Adv. Synth. Catal. 2011, 353, 1438) a protocol for the decarboxylative conversion of an acid 1 to the iodide 3. Doug E. Frantz of the University of Texas, San Antonio effected (Angew. Chem. Int. Ed. 2011, 50, 6128) conversion of a β-keto ester 4 to the diene 5 by way of the vinyl triflate. Pei Nian Liu of the East China University of Science and Technology and Chak Po Lau of the Hong Kong Polytechnic University (Adv. Synth. Catal. 2011, 353, 275) and Robert G. Bergman and Kenneth N. Raymond of the University of California, Berkeley (J. Am. Chem. Soc. 2011, 133, 11964) described new Ru catalysts for the isomerization of an allylic alcohol 6 to the ketone 7. Xiaodong Shi of West Virginia University optimized (Adv. Synth. Catal. 2011, 353, 2584) a gold catalyst for the rearrangement of a propargylic ester 8 to the enone 9. Xue-Yuan Liu of Lanzhou University used (Adv. Synth. Catal. 2011, 353, 3157) a Cu catalyst to add the chloramine 11 to the alkyne 10 to give 12. Kasi Pitchumani of Madurai Kamaraj University converted (Org. Lett. 2011, 13, 5728) the alkyne 13 into the α-amino amide 15 by reaction with the nitrone 14. Katsuhiko Tomooka of Kyushu University effected (J. Am. Chem. Soc. 2011, 133, 20712) hydrosilylation of the propargylic ether 16 to the alcohol 17. Matthew J. Cook of Queen’s University Belfast (Chem. Commun. 2011, 47, 11104) and Anna M. Costa and Jaume Vilarrasa of the Universitat de Barcelona (Org. Lett. 2011, 13, 4934) improved the conversion of an alkenyl silane 18 to the iodide 19. Vinay Girijavallabhan of Merck/Kenilworth developed (J. Org. Chem. 2011, 76, 6442) a Co catalyst for the Markovnikov addition of sulfide to an alkene 20. Hojat Veisi of Payame Noor University oxidized (Synlett 2011, 2315) the thiol 22 directly to the sulfonyl chloride 23. Nicholas M. Leonard of Abbott Laboratories prepared (J. Org. Chem. 2011, 76, 9169) the chromatography-stable O-Su ester 25 from the corresponding acid 24.
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Taber, Douglass F. "Arrays of Stereogenic Centers: The Barker Synthesis of (+)-Galbelgin". En Organic Synthesis. Oxford University Press, 2015. http://dx.doi.org/10.1093/oso/9780190200794.003.0043.
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Gang Zhao of the Shanghai Institute of Organic Chemistry and Gang Zou of the East China University of Science and Technology devised (Adv. Synth. Catal. 2011, 353, 3129) an elegant catalyst for the direct enantioselective epoxidation of a simple acyclic enone 1. Ismail Ibrahem and Armando Córdova of Mid Sweden University and Stockholm University prepared (Adv. Synth. Catal. 2011, 353, 3114) 6 by combining three catalysts to effect the enantioselective addition of 5 to 4. Giovanni Casiraghi and Franca Zanardi of the Università degli Studi di Parma used (J. Org. Chem. 2011, 76, 10291) a silver catalyst to mediate the addition of 8 to 7 to give 9. Keiji Maruoka of Kyoto University condensed (Nature Chem. 2011, 3, 642) the diazo ester 10 with an aldehyde 4, leading, after reduction of the initial adduct and protection, to the diamine 11. Christoph Schneider of the Universität Leipzig effected (Synthesis 2011, 4050) the vinylogous addition of 13 to an imine 12, setting both stereogenic centers of 14. In the course of the coupling of 16 with the diol 15, Michael J. Krische of the University of Texas established (J. Am. Chem. Soc. 2011, 133, 12795) four new stereogenic centers. By adding (Chem. Commun. 2011, 47, 10557) an α-nitro ester 18 to the maleimide 19, Professor Maruoka established both the alkylated secondary center and the N-substituted quaternary center of 20. Srinivas Hotha of the Indian Institute of Science Education & Research and Torsten Linker of the University of Potsdam showed (Chem. Commun. 2011, 47, 10434) that the readily prepared lactone 21 could be opened to 23 without disturbing the stereogenic center adjacent to the carbonyls. Allan D. Headley and Bukuo Ni of Texas A&M University-Commerce devised (Synthesis 2011, 1993) a recyclable catalyst for the addition of an aldehyde 7 to a nitroalkene 24 in water to give 25. Alexandre Alexakis of the University of Geneva effected (Chem. Commun. 2011, 47, 7212) the triply convergent coupling of 26, 27, and 28 to give 29 as a single dominant diastereomer.
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Kraggerud, Egil. "Ars 353. An ignored question mark *". En Critica, 153–56. Routledge, 2020. http://dx.doi.org/10.4324/9781003016847-25.
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Taber, Douglass F. "Metal-Mediated Carbocyclic Construction: The Chen Synthesis of Ageliferin". En Organic Synthesis. Oxford University Press, 2015. http://dx.doi.org/10.1093/oso/9780190200794.003.0074.
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Djamaladdin G. Musaev and Huw M.L. Davies of Emory University designed (J. Am. Chem. Soc. 2011, 133, 19198) a Rh catalyst that added 2 to 1 to give 3 with high dr and ee. Shunichi Hashimoto of Hokkaido University reported (Angew. Chem. Int. Ed. 2011, 50, 6803) a Rh catalyst that would add the α-diazo ester 5 to a terminal alkyne 4 to give the cyclopropene 6 in high ee. Gaëlle Blond and Jean Suffert of the Université de Strasbourg cyclized (Adv. Synth. Catal. 2011, 353, 3151) the alkyne 7, then coupled the Pd intermediate with a terminal alkyne 8 to give the cyclobutane 9. Nuno Maulide of the Max-Planck-Institute Mülheim ionized (Angew. Chem. Int. Ed. 2011, 50, 12631) the lactone 10 to a prochiral intermediate, which could then be coupled with 11 to give either diastereomer of 12 in high ee. Martin Hiersemann of the Technische Universität Dortmund devised (Org. Lett. 2011, 13, 4438) a Pd catalyst for the selective cyclization of 13 to 14. Naoya Kumagai and Masakatsu Shibasaki of the Institute of Microbial Chemistry, Tokyo effected (Angew. Chem. Int. Ed. 2011, 50, 7616) the enantioselective Conia ene cyclization of 15 to 16. Barry M. Trost of Stanford University developed (J. Am. Chem. Soc. 2011, 133, 19483) an enantioselective variant of the trimethylenemethane cycloaddition of 18 to 17 to give 19. In the course of a synthesis of (–)-oseltamivir phosphate, Masahiko Hayashi of Kobe University found (J. Org. Chem. 2011, 76, 5477) conditions for the enantioselective oxidation of 20 to 21. Quanrui Wang of Fudan University and Andreas Goeke of Givaudan Fragrances (Shanghai) cyclized (J. Org. Chem. 2011, 76, 5825) the propargylic acetate 22 to the cyclohexenone 23. Chuang-chuang Li, Tuoping Luo, and Zhen Yang of Peking University cyclized (J. Am. Chem. Soc. 2011, 133, 14944) the diyne 24 to the lactone 25. Hiromitsu Takayama of Chiba University used (Angew. Chem. Int. Ed. 2011, 50, 8025) the silyl tether of 26 to constrain the diastereomeric outcome of the cyclization to 27.
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Taber, Douglass F. "Enantioselective Synthesis of Alcohols and Amines: The Fujii/Ohno Synthesis of (+)-Lysergic Acid". En Organic Synthesis. Oxford University Press, 2015. http://dx.doi.org/10.1093/oso/9780190200794.003.0035.
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Ramón Gómez Arrayás and Juan C. Carretero of the Universidad Autónoma de Madrid effected (Chem. Commun. 2011, 47, 6701) enantioselective conjugate borylation of an unsaturated sulfone 1, leading to the alcohol 2. Robert E. Gawley of the University of Arkansas found (J. Am. Chem. Soc. 2011, 133, 19680) conditions for enantioselective ketone reduction that were selective enough to distinguish between the ethyl and propyl groups of 3 to give 4. Vicente Gotor of the Universidad de Oviedo used (Angew. Chem. Int. Ed. 2011, 50, 8387) an overexpressed Baeyer-Villiger monoxygenase to prepare 6 by dynamic kinetic resolution of 5. Li Deng of Brandeis University prepared (J. Am. Chem. Soc. 2011, 133, 12458) 8 in high ee by kinetic enantioselective migration of the alkene of racemic 7. Bernhard Breit of the Freiburg Institute for Advanced Studies established (J. Am. Chem. Soc. 2011, 133, 20746) the oxygenated quaternary center of 10 by the addition of benzoic acid to the allene 9. Keith R. Fandrick of Boehringer Ingelheim constructed (J. Am. Chem. Soc. 2011, 133, 10332) the oxygenated quaternary center of 13 by enantioselective addition of the propargylic nucleophile 12 to 11. Yian Shi of Colorado State University devised (J. Am. Chem. Soc. 2011, 133, 12914) conditions for the enantioselective transamination of the α-keto ester 14 to the amine 15. Professor Deng added (Adv. Synth. Catal. 2011, 353, 3123) 18 to an enone 17 to give the protected amine 19. Song Ye of the Institute of Chemistry, Beijing effected (J. Am. Chem. Soc. 2011, 133, 15894) elimination/addition of an unsaturated acid chloride 20 to give the γ-amino acid derivative 22. Frank Glorius of the Universität Münster added (Angew. Chem. Int. Ed. 2011, 50, 1410) an aldehyde 23 to 24 to give the amide 25. Sentaro Okamoto of Kanagawa University designed (J. Org. Chem. 2011, 76, 6678) an organocatalyst for the enantioselective Steglich rearrangement of 26, creating the aminated quaternary center of 27. Most impressive of all was the report (Org. Lett. 2011, 13, 5460) by Hélène Lebel of the Université de Montréal of the direct enantioselective C–H amination of 28 to give 29.
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Taber, Douglass F. "Heteroaromatic Construction: The Sperry Synthesis of (+)-Terreusinone". En Organic Synthesis. Oxford University Press, 2015. http://dx.doi.org/10.1093/oso/9780190200794.003.0066.
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Akio Saito and Yuji Hanzawa of Showa Pharmaceutical University found (Tetrahedron Lett. 2011, 52, 4658) that an alkynyl keto ester 1 could be oxidatively cyclized to the furan 2. Eric M. Ferreira of Colorado State University showed (Org. Lett. 2011, 13, 5924) that depending on the conditions, a Pt catalyst could cyclize 3 to either 4 or 5. Shunsuke Chiba of Nanyang Technological University used (J. Am. Chem. Soc. 2011, 133, 13942) Cu catalysis for the oxidation of 6 to the pyrrole 7. Vladimir Gevorgyan of the University of Illinois at Chicago devised (Org. Lett. 2011, 13, 3746) a convergent assembly of the pyrrole 10 from the alkyne 8 and the alkyne 9. Dale L. Boger of Scripps La Jolla extended (J. Am. Chem. Soc. 2011, 133, 12285) the scope of the Diels-Alder addition of the triazine 11 to an alkyne 12 to give the pyridine 13. Tomislav Rovis, also of Colorado State University, used (Chem. Commun. 2011, 47, 11846) a Rh catalyst to add an alkyne 15 to the oxime 14 to give the pyridine 16. Sensuke Ogoshi of Osaka University, under Ni catalysis, added (J. Am. Chem. Soc. 2011, 133, 18018) a nitrile 18 to the diene 17 to give the pyridine 19. Alexander Deiters of North Carolina State University showed (Org. Lett. 2011, 13, 4352) that the complex tethered diyne 20 combined with 21 with high regiocontrol to give 22. Yong-Min Liang of Lanzhou University prepared (J. Org. Chem. 2011, 76, 8329) the indole 24 by cyclizing the alkyne 23. Xiuxiang Qi and Kang Zhao of Tianjin University found (J. Org. Chem. 2011, 76, 8690) that the enamine 25 could be oxidatively cyclized to the indole 26. Kazuhiro Yoshida and Akira Yanagisawa of Chiba University established (Org. Lett. 2011, 13, 4762) that ring-closing metathesis converted the keto ester 27 to the indole 28. Alessandro Palmieri and Roberto Ballini of the Università di Camerino observed (Adv. Synth. Catal. 2011, 353, 1425) that the pyrrole 30 spontaneously added to the nitro acrylate 29 to give an adduct that cyclized to 31 on exposure to acid.
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Taber, Douglass F. "Organocatalytic Carbocyclic Construction: The You Synthesis of (–)-Mesembrine". En Organic Synthesis. Oxford University Press, 2015. http://dx.doi.org/10.1093/oso/9780190200794.003.0070.
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Frank Glorius of the Universität Münster devised (Angew. Chem. Int. Ed. 2011, 50, 12626) a catalyst for the enantioselective acylation of a cyclopropene 1 to the ketone 3. Geum-Sook Hwang of Chungnam National University and Do Hyun Ryu of Sungkyunkwan University effected (J. Am. Chem. Soc. 2011, 133, 20708) the enantioselective addition of the diazo ester 5 to an α,β-unsaturated aldehyde 4 to give the cyclopropane 6. We showed (J. Org. Chem. 2011, 76, 7614) that face-selective allylation of an α-iodo enone 7 followed by Suzuki coupling and oxy-Cope rearrangement delivered the cyclopentanone 9. Karl Anker Jørgensen of Aarhus University combined (Org. Lett. 2011, 13, 4790) two organocatalysts to effect the addition of 11 to an α,β-unsaturated aldehyde 10, leading to the cyclopentenone 12. Tomislav Rovis of Colorado State University also used (Chem. Sci. 2011, 2, 1835) two organocatalysts to condense 13 with 14 to give the cyclopentanone 15. Gregory C. Fu, now at CalTech, found (J. Am. Chem. Soc. 2011, 133, 12293) that both enantiomers of the racemic allene 16 combined with 17 to give the cyclopentene 18 in high ee. Piotr Kwiatkowski of the University of Warsaw found (Org. Lett. 2011, 13, 3624) that under elevated pressure (8–10 kbar), enantioselective conjugate addition of nitromethane proceeded well even with a β-substituted cyclohexenone 19. Marco Bella of the Università di Roma observed (Adv. Synth. Catal. 2011, 353, 2648) remarkable diastereoselectivity in the addition of the aldehyde 22 to an activated acceptor 21. Following the procedure of List, Jiong Yang of Texas A&M University cyclized (Org. Lett. 2011, 13, 5696) 24 to 25 in high ee. Bor-Cherng Hong of the National Chung Cheng University described (Synthesis 2011, 1887) the double Michael combination of 26 with 27 to give 28 in high ee. Observing a secondary 13C isotope effect only at the β-carbon of 30, Li Deng of Brandeis University concluded (Chem. Sci. 2011, 2, 1940) that the addition to 29 was stepwise, not concerted. In contrast, the cyclization of 32 to 33 reported (Org. Lett. 2011, 13, 3932) by Tadeusz F. Molinski of the University of California San Diego likely was concerted.
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Taber, Douglass. "Functionalization of C-H Bonds: The Baran Synthesis of Dihydroxyeudesmane". En Organic Synthesis. Oxford University Press, 2011. http://dx.doi.org/10.1093/oso/9780199764549.003.0016.
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Arumugam Sudalai of the National Chemical Laboratory, Pune reported (Tetrahedron Lett. 2008, 49, 6401) a procedure for hydrocarbon iodination. With straight chain hydrocarbons, only secondary iodination was observed. Chao-Jun Li of McGill University uncovered (Adv. Synth. Cat. 2009, 351, 353) a procedure for direct hydrocarbon amination, converting cyclohexane 1 into the amine 3. Justin Du Bois of Stanford University established (Angew. Chem. Int. Ed. 2009, 48, 4513) a procedure for alkane hydroxylation, converting 4 selectively into the alcohol 6. The oxirane 8 usually also preferentially ozidizes methines, hydroxylating steroids at the C-14 position. Ruggero Curci of the University of Bari found (Tetrahedron Lett. 2008, 49, 5614) that the substrate 7 showed some C-14 hydroxylation, but also a useful yield of the ketone 9. The authors suggested that the C-7 acetoxy group may be deactivating the C-14 C-H. C-H bonds can also be converted directly to carbon-carbon bonds. Mark E. Wood of the University of Exeter found (Tetrahedron Lett. 2009, 50, 3400) that free-radical removal of iodine from 10 followed by intramolecular H-atom abstraction in the presence of the trapping agent 11 delivered 12 with good diastereo control. Professor Li observed (Angew. Chem. Int. Ed. 2008, 47, 6278) that under Ru catalysis, hydrocarbons such as 13 could be directly arylated. He also established (Tetrahedron Lett. 2008, 49, 5601) conditions for the direct aminoalkylation of hydrocarbons such as 13, to give 17. Huw M. L. Davies of Emory University converted (Synlett 2009, 151) the ester 4 to the homologated diester 19 in preparatively useful yield using the diazo ester 18, the precursor to a selective, push-pull stabilized carbene. Intramolecular bond formation to an unactivated C-H can be even more selective. Guoshen Liu of the Shanghai Institute of Organic Chemistry developed (Organic Lett. 2009, 11, 2707) an oxidative Pd system that cyclized 20 to the seven-membered ring lactam 21 . Professor Du Bois devised (J. Am. Chem. Soc. 2008 , 130, 9220) a Rh catalyst that effected allylic amination of 22, to give 23 with substantial enantiocontrol. Dalibor Sames of Columbia University designed (J. Am. Chem. Soc. 2009, 131, 402) a remarkable cascade approach to C-H functionalization. Exposure of 24 to Lewis acid led to intramolecular hydride abstraction. Cyclization of the resulting stabilized carbocation delivered the tetrahydropyan 25 with remarkable diastereocontrol.
Actas de conferencias sobre el tema "353(.25)"
1
Nuruddin, Md, Mahesh Hosur, Eldon Triggs y Shaik Jeelani. "Comparative Study of Properties of Cellulose Nanofibers From Wheat Straw Obtained by Chemical and Chemi-Mechanical Treatments". En ASME 2014 International Mechanical Engineering Congress and Exposition. American Society of Mechanical Engineers, 2014. http://dx.doi.org/10.1115/imece2014-36174.
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Objective of this work was to compare morphology, crystalline and thermal properties of cellulose nano fibers derived from wheat straw by two different processes (ball milling and acid hydrolysis treatment). The characterization of extracted CNFs was done by Scanning electron micrograph (SEM), Transmission electron microscopy (TEM), X-ray diffraction (XRD) and Thermogravimetric analysis (TGA). It was found from morphological, crystalline and thermal analyses that isolated cellulose nanofibers have diameter of nano meter ranges (10–25 nm), 68–80 % crystallinity and decomposition temperature of around 284–353° C, depending upon isolation techniques.
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Гергіль, І. В. "Психологічні чинники реалізації життєвих планів особистості у зрілому віці". En ПСИХОЛОГІЯ СВІДОМОСТІ: ТЕОРІЯ І ПРАКТИКА НАУКОВИХ ДОСЛІДЖЕНЬ. Liha-Pres, 2023. http://dx.doi.org/10.36059/978-966-397-353-1-25.
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ONOFREI, Cornelia. "Perspectives on skills building strategies musical-creative". En Ştiință și educație: noi abordări și perspective. "Ion Creanga" State Pedagogical University, 2023. http://dx.doi.org/10.46727/c.v2.24-25-03-2023.p349-353.
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This article refers to the strategies adopted for the formation and development of musicalcreative skills of students with special educational needs. In recent years, Romanian schools have promoted a legal framework aligned with European educational policies, ensuring equal opportunities for all students, ensuring the maximum development possibilities for each student, depending on his skills and interests. Students have different learning rates, and some of them encounter difficulties in assimilating knowledge or in forming skills and attitudes. In this case, it is necessary to adopt different learning methods, use different materials and didactic means to motivate the students to participate in the educational process according to the possibilities of each one. Through various strategies, carefully selected, focused on age-specific songs, musical games and toys, children can form and develop musical skills and abilities. Even if mainstream school focuses on the development of writing, reading, arithmetic skills because these are the ones evaluated in tests and exams, through music students develop their self-confidence, improve their linguistic and creative skills. The personality of the future adult stands to gain as long as the child is granted the fundamental rights, his possibilities and limits are recognized and accepted, and he is offered equal learning opportunities.
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Liu, Chung Y., Per Wallen, Dean Handley y Jena Smith. "FIERIN POTENTIATING THE ACTIVATION OF FIBRINOLYTIC SYSTEM ON THE ENDOTHELIAL CELL SURFACE: FORMATION OF THE SURFACE-BOUND TRIMOLECULAR COMPLEX OF FIBRIN, PLASMINOGEN, AND PLASMINOGEN ACTIVATOR". En XIth International Congress on Thrombosis and Haemostasis. Schattauer GmbH, 1987. http://dx.doi.org/10.1055/s-0038-1643318.
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Previous reports have shown that f ibrin (Fn), plasminogen (Pig), and tissue plasminogen activator (tPA) can bind to bovine aortic endothelial cell (BAEC) respectively. The present studies are to examine the formation of the trimolecular complex of Fn, Pig, and tPA on the BAEC surface. BAEC monolayers were first incubated with one of the three components in buffer (pH 7.5, 25 C) and washed, and then incubated with the second component and washed. Finally, the BAEC monolayers after the first and second incubations were incubated with the third component in the presence of plasmin substrate S-2251. Plasminogen activation rates (PAR)(pM/min) were measured. The results (TABLE) show that Pig and tPA retain their respective activities after their binding to BAEC surface, either Pig or tPA as the first bound component. These results suggest that the formation of Plg-tPA complex can occur after their binding to the BAEC surface. With Fn as the second binding component, BAEC monolayers show higher PAR values (138 & 187, pM/imin) than those without Fn (34.5 & 59.1 pM/min), suggesting Fn potentiation of tPA-induced Pig activation on the BAEC surface. Since the reaction of Fn with the Plg-tPA complex is required for the expression of fibrin potentiation, the present results suggest that the formation of trimolecular complex can occur on the BAEC surface. Further, when Fn was the first bound component and Pig or tPA was the second or third bound component, the BAEC rmonolayers show the highest PAR values (353 & 331 nVrmin), suqqestinq that both Plq and tPA can bind not only to BAEC surface but also to Fn which was already first bound to BAEC surface. Thus, trimolecular complex may have multiple binding sites on BAEC surface and anyone of the three binding sites (Fn, Pig, and tPA) may act as the binding site for the trimolecular couplex on the BAEC surface.
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Homes, W. E., H. R. Lijnen, L. Nelles, C. Kluft y D. Collen. "AN ALANINE INSERTION IN α2-ANTIPLASMIN ‘ENSCHEDE’ ABOLISHES ITS PLASM IN INHIBITORY ACTIVITY". En XIth International Congress on Thrombosis and Haemostasis. Schattauer GmbH, 1987. http://dx.doi.org/10.1055/s-0038-1642897.
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Congenital deficiencies of the fibrinolytic inhibitor α2antiplasmin (α2AP) may result in bleeding disorders. An abnormal a AP (α2AP‘Enschede’) is known. 2 siblings with 3% functional activity and normal antigen level have parents with 50% activity and normal antigen. The protein interacts normally with the lysine-binding site(s) of plasmin(ogen) but does not inhibit plasmin irreversibly. α2AP Enschede is a plasmin substrate that like the normal protein releases a M 8,000 peptide upon reaction with plasmin. In the present study, Southern blot analysis, using an α2AP cDNA probe showed a restriction fragment length polymorphism within a small genomic DNA fragment of the Enschede family members. Cloning and sequencing of these fragments revealed a GCG inframe insertion that results in an alanine addition between amino acids 353 and 357, 7-10 positions NH -terminal to the reactive site PI residue, Arg364. This area is homologous to the A4 B-sheet of reactive site cleaved a -antitrypsin. Clones from each individual confirm the parents as true heterozygotes and the children as true homozygotes. A cloned genomic DNA sequence containing the insertion (V ) was exchanged for the normal sequence in a eukaryotic a AP expression plasmid. Recombinant α2AP‘Enschede’ (ra AfVAla) purified from the conditioned media of transfected Chinese Hamster Ovary Cells is analogous to plasma a α2AP‘Enschede’ with respect to interactions with plasmin and plasminogen. Preliminary analysis of the released Mr 8,000 recombinant peptide shows that its NH -terminus is the same as the peptide cleaved from normal a AP. Although ra α2APVAla does not inhibit plasmin irreversibly it does, however, act as a competitive inhibitor of hydrolysis of the chromogenic substrate S-2251 by plasmin.The K for this interaction is 25 nM. Thus, α2APAla retains a high affinity for the active center of plasmin. In conclusion, an Ala insertion near the reactive site of α2AP must have resulted in a structural perturbation that has abolished the plasmin inhibitory activity of a α2AP‘Enschede’. This variant may provide a model for further investigation of structure-function relationships in the serpins which determine the relative inhibitor vs. substrate properties.
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Harb, H. y S. Armstrong. "B279 An obstetric anaesthetists’ association (OAA) survey of the use of ultrasound scanning to assist with central neuraxial blocks in obstetric anaesthesia". En ESRA Abstracts, 39th Annual ESRA Congress, 22–25 June 2022. BMJ Publishing Group Ltd, 2022. http://dx.doi.org/10.1136/rapm-2022-esra.353.
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Parpinel, G., M. Buffa, JDI Muzio, A. Peruzzo Cornetto, C. Palladino, ME Laudani, M. Barboni et al. "353 Dose-dense NACT followed by CCRT in locally advanced cervical cancer: feasibility and safety". En ESGO 2021 Congress. BMJ Publishing Group Ltd, 2021. http://dx.doi.org/10.1136/ijgc-2021-esgo.25.
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Tesař, O., J. Malý, K. Malá-Ladová, M. Doseděl y J. Vlček. "5PSQ-158 Food and drink management as part of medication administration safety". En 26th EAHP Congress, Hospital pharmacists – changing roles in a changing world, 23–25 March 2022. British Medical Journal Publishing Group, 2022. http://dx.doi.org/10.1136/ejhpharm-2022-eahp.353.
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Lee, Hannah, Harriet Corbett, Joanne Blair, Sara Webster y Cara Williams. "418 Risk of adrenal insufficiency in pre-pubertal girls treated with ultra-potent steroids for lichen sclerosus". En Royal College of Paediatrics and Child Health, Abstracts of the RCPCH Conference, Glasgow, 23–25 May 2023. BMJ Publishing Group Ltd and Royal College of Paediatrics and Child Health, 2023. http://dx.doi.org/10.1136/archdischild-2023-rcpch.353.
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Ramakrishnan, A., M. Kambalimath y D. Jayachandran. "G411 Audit on the diagnosis and management of congenital hypothyroidism (CHT)". En Royal College of Paediatrics and Child Health, Abstracts of the RCPCH Conference–Online, 25 September 2020–13 November 2020. BMJ Publishing Group Ltd and Royal College of Paediatrics and Child Health, 2020. http://dx.doi.org/10.1136/archdischild-2020-rcpch.353.
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