Journal articles on the topic 'U/Pb zircon age'

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1

Huang, Yong-Shu, Qiu-Li Li, Yu Liu, Ping-Ping Liu, Sun-Lin Chung, and Xian-Hua Li. "238U–206Pb dating of U-series disequilibrium zircons by secondary ion mass spectrometry." Journal of Analytical Atomic Spectrometry 36, no. 5 (2021): 999–1006. http://dx.doi.org/10.1039/d0ja00510j.

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Theoretical and analytical methods for 238U–206Pb dating of U-series disequilibrium zircons by secondary ion mass spectrometry are developed. U–Pb dates improve age precision 3 times better than U–Th dating for zircon >150 ka.
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2

SHUMLYANSKYY, L. V., V. KAMENETSKY, and B. V. BORODYNYA. "Age and Composition of Zircons From the Devonian Petrivske Kimberlite Pipe of the Azov Domain, the Ukrainian Shield." Mineralogical Journal 43, no. 4 (2021): 50–55. http://dx.doi.org/10.15407/mineraljournal.43.04.050.

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Results of a study of U-Pb and Hf isotope systematics and trace element concentrations in five zircon crystals separated from the Devonian Petrivske kimberlite are reported in the paper. Four zircons have yielded Paleoproterozoic and Archean ages, while one zircon grain gave a Devonian age of 383.6±4.4 Ma (weighted mean 206Pb/238U age). The Precambrian zircons have been derived from terrigenous rocks of the Mykolaivka Suite that is cut by kimberlite, or directly from the Precambrian rock complexes that constitute continental crust in the East Azov. The Devonian zircon crystal has the U-Pb age that corresponds to the age of kimberlite emplacement. It is 14 m.y. younger than zircon megacrysts found in the Novolaspa kimberlite pipe in the same area. In addition, Petrivske zircon is richer in trace elements than its counterparts from the Novolaspa pipe. Petrivske and Novolaspa zircons crystallized from two different proto-kimberlite melts, whereas the process of kimberlite formation was very complex and possibly included several episodes of formation of proto-kimberlite melts, separated by extended (over 10 M.y.) periods of time.
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3

Jackson, William T., Matthew P. McKay, Donald A. Beebe, Carolyn Mullins, Adelie Ionescu, Barry Shaulis, and David L. Barbeau. "Late Cretaceous sediment provenance in the eastern Gulf Coastal Plain (U.S.A.) based on detrital-zircon U-Pb ages and Th/U values." Journal of Sedimentary Research 91, no. 10 (October 8, 2021): 1025–39. http://dx.doi.org/10.2110/jsr.2020.177.

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ABSTRACT Detrital-zircon U-Pb geochronology documents a regional- to continental-scale drainage reorganization along the eastern Gulf Coastal Plain (USA) from the Late Cretaceous (Cenomanian) to the Paleocene–Eocene. We present detrital-zircon U-Pb ages and Th/U values from the Maastrichtian Ripley Formation to determine the sedimentary provenance and to provide spatiotemporal resolution of drainage reorganization. The Ripley Formation contains a 12.7% overall average abundance of detrital zircons with low (< 0.1) Th/U values relative to the underlying Cenomanian Tuscaloosa Group (3.6%), the overlying Paleocene–Eocene Wilcox Group (2.8%), an Appalachian foreland composite (2.1%), and the laterally equivalent McNairy Sandstone in the northern Mississippi Embayment (3.8%). Multidimensional scaling of detrital-zircon U-Pb spectra shows that the Ripley Formation is dissimilar from underlying and overlying Gulf Coastal Plain units, the McNairy Sandstone, and an Appalachian foreland composite sample because of differences in proportions of Appalachian (490–270 Ma) and Grenville (1250–900 Ma) zircons. We interpret the southern Appalachian Piedmont province as the principal sediment source region for the Ripley Formation to account for the elevated abundance of grains with low (< 0.1) Th/U values and unique detrital-zircon U-Pb age spectra. Results suggest a regional-scale (105 km2) drainage network, which delivered sediment to the Maastrichtian coast followed by northwestward littoral transport and eventual mixing with Appalachian foreland-derived sediment in the northern Mississippi Embayment. This study further brackets drainage reorganization along the eastern Gulf Coastal Plain and demonstrates how simple chemical–age relationships, such as zircon Th/U values coupled with U-Pb ages, can be used to evaluate sediment provenance.
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4

Hervé, Francisco, Víctor Faúndez, Manfred Brix, and Mark Fanning. "Jurassic sedimentation of the Miers Bluff Formation, Livingston Island, Antarctica: evidence from SHRIMP U–Pb ages of detrital and plutonic zircons." Antarctic Science 18, no. 2 (June 2006): 229–38. http://dx.doi.org/10.1017/s0954102006000277.

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Detrital zircon populations from two sandstone samples from the lower member (Johnsons Dock Member) of the Miers Bluff Formation at Hurd Peninsula have been dated by the Sensitive High Resolution Ion Microprobe (SHRIMP) U–Pb method. In one of the samples, zircons as young as early Middle Jurassic (Bajocian) age are present. In the second sample, the youngest detrital zircons are Middle Triassic in age. The detrital zircon age spectra indicate that Permian, early Palaeozoic and Meso- to Neoproterozoic zircon bearing rocks were present in the source areas of the Miers Bluff Formation. The sedimentary rocks are intruded by the Hespérides Point Intrusive diorite stock which yielded a U–Pb zircon crystallization age of 137.7 ± 1.4 Ma (Early Cretaceous, Valanginian). These results indicate that sedimentation of the Johnsons Dock Member of the Miers Bluff Formation is bracketed in time between the Bajocian and the Valanginian. The Miers Bluff Formation has been correlated with the Trinity Peninsula Group from the Antarctic Peninsula, based on sedimentological and structural similarity. Since the Trinity Peninsula Group is older than Middle Jurassic a direct chronological correlation is not supported by our new U–Pb zircon data. However, we suggest that the tectonic setting may have migrated in time with deposition of the pre-Middle Jurassic TPG on the peninsula, to Livingston Island where the maximum age for deposition of the MBF is Bajocian (about 170 Ma).
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5

Shi, Yu, Xi Jun Liu, and Zuo Hai Feng. "Formation Age of the Qinling Complex and the early Paleozoic Tectonic Event." Advanced Materials Research 734-737 (August 2013): 60–70. http://dx.doi.org/10.4028/www.scientific.net/amr.734-737.60.

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The Qinling orogenic belt (QOB) located between the North China Craton (NCC) and the South China Craton (SCC) is composed of the Northern Qinling Belt (NQB) and the Southern Qinling Belt (SQB). This study presents new geochemical data, zircon U-Pb ages and Hf isotopes from two rocks from the Qinling complex in the NQB. LA-ICP-MS zircon U-Pb dating results suggest that the Qinling complex was formed in early Neoproterozoic and experienced the early Paleozoic metamorphism. HighεHf(t) values of 9.0-12.0 for the early Paleozoic zircons indicated that there is mantle-derived magma intruding into the Qinling complex in the early Paleozoic.
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6

Davies, Joshua H. F. L., Jörn-Frederik Wotzlaw, Alexander P. Wolfe, and Larry M. Heaman. "Assessing the age of the Late Cretaceous Danek Bonebed with U–Pb geochronology." Canadian Journal of Earth Sciences 51, no. 11 (November 2014): 982–86. http://dx.doi.org/10.1139/cjes-2014-0136.

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An ash-rich volcaniclastic sandstone immediately underlying dinosaur-rich material from the Danek Bonebed in the Horseshoe Canyon Formation (HCF), Edmonton, Alberta, Canada, contains accessory zircon, which have been dated employing U–Pb geochronology. Both laser-ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) and chemical abrasion isotope dilution thermal ionization mass spectrometry (ID-TIMS) U–Pb analyses have been conducted. The zircon age distributions are complex with U–Pb dates ranging from Precambrian to Cretaceous. We consider the youngest ID-TIMS 206Pb/238U date of 71.923 ± 0.068 Ma as the maximum deposition age of the ash-rich sandstone, placing the overlying Danek bonebed in the early Maastrichtian. This age is compatible with the paleontological assemblage from the Danek Bonebed and the regional stratigraphy. The zircon age distribution also implies that the HCF had a complex provenance of the detritus with some Archean and Proterozoic zircons, a group of Mesozoic, and a large compliment of Cretaceous grains. The results highlight the importance of high precision geochronology in constraining the age of important fossil deposits such as the Danek Bonebed.
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7

Waight, Tod, Mikael Stokholm, Benjamin Heredia, and Tonny B. Thomsen. "U-Pb zircon and titanite age of the Christiansø granite, Ertholmene, Denmark, and correlation with other Bornholm granitoids." Bulletin of the Geological Society of Denmark 70 (March 23, 2022): 27–38. http://dx.doi.org/10.37570/bgsd-2022-70-03.

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A granitic sample from the Danish island of Christiansø in the Ertholmene island group north of Bornholm is described petrographically and geochemically, and dated using U-Pb in zircon and titanite. Zircon systematics in the sample are complicated by abundant Pb loss and a large population of zircons interpreted as being inherited. Removal of highly disturbed zircons, imprecise analyses, and assumed inherited zircons yield an upper intercept date of 1500 ± 18 Ma (MSWD = 13, n = 58). Removal of zircons with high common Pb from this population yields an identical result of 1500 ± 22 Ma (MSWD = 8, n = 34). Zircons that are ≤3% discordant give a weighted average 206Pb/238U age of 1458 ± 12 Ma (MSWD = 3.0, n = 18), and a weighted average 207Pb/206Pb age of 1495 ± 14 Ma (MSWD = 4.7, n = 19). Titanites from the sample yield a lower intercept age of 1448 ± 15 Ma (MSWD = 6.8, n = 45). The sample contains a significant number of inherited grains indicative of ages around 1.7–1.8 Ga. The relatively large MSWDs for these age determinations indicate geological complexity, likely reflecting Pb loss, and the possible presence of inherited zircons which suffered major Pb loss during incorporation in the granitic magma. The zircon and titanite dates agree reasonably well with previous age determinations on felsic lithologies from the Bornholm mainland, as well as from the Blekinge Province of southern Sweden. Petrographically and geochemically, the Christiansø granite is indistinguishable from, and can be correlated with, the A-type granites and gneisses which occur on Bornholm. The high abundance of disturbed and inherited zircons (c. 1.7–1.8 Ga) may indicate that the granite was intruded into and assimilated a nearby region of unexposed Transscandinavian Igneous Belt rocks. The somewhat altered nature of the rock, and overall disturbance of U-Pb zircon systematics, suggest alteration associated with fluid-flow along nearby faults defining the northern margin of the Sorgenfrei–Tornquist Zone.
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8

Vozárová, Anna, Miloš Šmelko, and Ilya Paderin. "Permian single crystal U-Pb zircon age of the Rožňava Formation volcanites (Southern Gemeric Unit, Western Carpathians, Slovakia)." Geologica Carpathica 60, no. 6 (December 1, 2009): 439–48. http://dx.doi.org/10.2478/v10096-009-0032-1.

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Permian single crystal U-Pb zircon age of the Rožňava Formation volcanites (Southern Gemeric Unit, Western Carpathians, Slovakia)Zircon populations from the Rožňava Formation volcanic rock complex have been analysed. Euhedral zircons from the 1stvolcanogenic horizon with fine oscillatory growth zoning, typical of magmatic origin, gave the average concordia age of 273.3 ± 2.8 Ma, with Th/U ratios in the range of 0.44-0.73. The Permian ages ranging from 266 to 284 Ma were identified in the wider, zoned or unzoned, central zircon parts, as well as in their fine-zoned oscillatory rims. The average concordia age of 275.3 ± 2.9 was obtained from the euhedral zircon population of the 2ndvolcanogenic horizon of the Rožňava Formation. The analyses were performed on zoned magmatic zircons in the age interval from 267 to 287 Ma, with Th/U ratios in the range of 0.39-0.75. In the later zircon population two inherited zircon grains were dated giving the age of 842 ± 12 Ma (Neoproterozoic) and 456 ± 7 Ma (Late Ordovician). The magmatic zircon ages document the Kungurian age of Permian volcanic activity and contemporaneous establishment of the south-Gemeric basin. The time span of volcanic activity corresponds to the collapse of the Western Carpathian Variscan foreland which expanded southward.
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9

Røhr, Torkil S., Tom Andersen, Henning Dypvik, and Ashton F. Embry. "Detrital zircon characteristics of the Lower Cretaceous Isachsen Formation, Sverdrup Basin: source constraints from age and Hf isotope data." Canadian Journal of Earth Sciences 47, no. 3 (March 2010): 255–71. http://dx.doi.org/10.1139/e10-006.

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Detrital zircons from the Lower Cretaceous Isachsen Formation of the Sverdrup Basin, Canadian Arctic Archipelago, have been dated by the U–Pb method and analyzed for Hf isotopes by laser ablation microprobe – inductively coupled plasma – mass spectrometry (LAM–ICP–MS). Five samples from four locations on Ellesmere and Axel Heiberg islands display similar ranges of U–Pb ages, with significant zircon populations at 2.8–2.6, 1.9–1.8, 1.7–1.6, and 1.2–1.0 Ga. Major hiatuses occur between 2.4 and 2.0 Ga and from 0.96 to 0.5 Ga. Low initial εHfvalues indicating recycled crust components are significant in Palaeoproterozoic (1.9–1.8 Ga) and Neoarchaean (2.8–2.6 Ga) zircon populations. Other U–Pb age populations in the studied samples are dominated by zircon with positive εHfvalues, indicating a significant contribution from mantle-derived protoliths. The εHfvalues seen within a given U–Pb age population are generally consistent, with only minor scatter among the different samples. U–Pb and Hf data closely resemble previously published data from Lower Cretaceous rocks in northern Greenland, suggesting they have the same origin. The data are also largely consistent with the East Greenland Caledonides and the Precambrian basement of Greenland and northern Canada as predominant sources of zircon for the studied sandstones. However, based on the level of similarity between data from the Wandel Sea Basin and Sverdrup Basin sediments and on previous Nd isotope work in the Sverdrup Basin, it is likely that the sediments represent redeposited lower and middle Palaeozoic sediments.
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10

Anfinson, Owen A., Andrew L. Leier, Rich Gaschnig, Ashton F. Embry, and Keith Dewing. "U–Pb and Hf isotopic data from Franklinian Basin strata: insights into the nature of Crockerland and the timing of accretion, Canadian Arctic Islands." Canadian Journal of Earth Sciences 49, no. 11 (November 2012): 1316–28. http://dx.doi.org/10.1139/e2012-067.

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New detrital zircon uranium–lead (U–Pb) ages and initial epsilon hafnium (εHf(i)) data from the Devonian clastic succession of the Canadian Arctic Islands refines the provenance of strata within the Franklinian Basin and provides constraints on the geologic evolution of the landmass responsible for the Ellesmerian Orogen. This study contributes more than 500 U–Pb ages and 32 εHf(i) values from the Blackley Formation and the Parry Islands Formation. The Middle Devonian Blackley Formation represents the onset of clastic sedimentation into the Franklinian Basin during the Devonian period. Detrital zircon from two samples yield U–Pb age populations of 380–470, 500–700, 900–2100, and 2550–3000 Ma. The population of 500–700 Ma U–Pb ages indicates a source exotic to the northern Laurentian margin and is attributed to a continental landmass located north of the present Canadian Arctic Islands (often referred to as Crockerland). This is some of the earliest evidence of 500–700 Ma detrital zircon deposition onto the northern Laurentian margin and indicates this northern landmass is at least partially accreted to Laurentia by early-Eifelian time. The Late Devonian Parry Islands Formation is the uppermost succession of Ellesmerian Orogen foreland basin sedimentation in the Franklinian Basin. Detrital zircon from four samples yield U–Pb age populations of 370–450, 470–750, 930–2100, and 2300–3200 Ma. The U–Pb ages suggest the Parry Islands Formation is derived from the northern source terrane (Crockerland) and indicate this landmass contains rocks similar to that of the east Greenland Caledonides, Pearya, and northeastern Baltica. Rim and core U–Pb double dates from the 500–700 Ma detrital zircon population and εHf(i) values from the 380–450, 520–550, and 650–710 Ma detrital zircon populations help constrain magma generation processes within Crockerland and suggest the zircons are derived from a juvenile lithosphere.
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11

Pidgeon, R. T., and W. Compston. "A SHRIMP ion microprobe study of inherited and magmatic zircons from four Scottish Caledonian granites." Earth and Environmental Science Transactions of the Royal Society of Edinburgh 83, no. 1-2 (1992): 473–83. http://dx.doi.org/10.1017/s0263593300008142.

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ABSTRACTUsing the ion microprobe SHRIMP we have analysed zircons from the Ben Vuirich, Glen Kyllachy, Inchbae and Vagastie Bridge granites from the Scottish Caledonides, in an attempt to resolve the ages of inherited zircons shown to be present in these granites by previous conventional multigrain analyses. Middle Proterozoic age components were found in inherited zircons from all four granites. Late Proterozoic (900–1,100 Ma) components have been identified in zircons from the Glen Kyllachy and Ben Vuirich granites in the Grampian Highlands. A Late Archaean age has only been detected in one zircon from the Glen Kyllachy granite. The distribution of inherited components in the granite zircon populations could reflect fundamental divisions in the age composition of granite source rocks; however, detailed assessment of this possibility must await further ion microprobe analyses on zircons from many more granites.SHRIMP isotopic and U, Th and Pb analyses were made on successive shells of zoned zircon surrounding inherited cores from the Glen Kyllachy granite to monitor chemical changes during magmatic zircon growth. Results show that zircon shells have characteristic but significantly different Th, U and Pb concentrations. Magmatic zircon from the Vagastie Bridge granite also forms as clearly defined oscillatory zoned shells around unzoned nuclei of inherited zircon. However, the distinction between magmatic and inherited zircon in zircons from the Inchbae granite is less clear. Zircons from the Ben Vuirich granite occur as euhedral, magmatic zircons, or as rounded, subhedral, inherited zircon grains. A SHRIMP age of 597 ± 11 (2σ) Ma for euhedral magmatic zircon from this granite is identical, within the uncertainty, to the conventional multigrain zircon age of 590 ± 2 (2σ) Ma reported by Rogers et al. (1989) and confirms the conclusions of those authors that sedimentation of the Dalradian sequence took place in the Precambrian.
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12

Prytchin, M. E., E. I. Soroka, and V. N. Puchkov. "Novel U-Pb isotopic zircon data on the rhyolite of the Saf’yanovskoe Cu-Zn deposit (Middle Urals)." LITHOSPHERE (Russia) 21, no. 6 (December 29, 2021): 884–93. http://dx.doi.org/10.24930/1681-9004-2021-21-6-884-893.

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Research subject. Zircons from the Saf’yanovskoe Cu-Zn deposit rhyolite (Middle Urals). For the first time, zircon U-Pb dating for the rhyolite of the ore-bearing volcanic-sedimentary rocks of the Saf’yanovskoe deposit was performed. The volcanites are characterized by an andesite-rhyodacite composition and are localized at the southern edge of the Rezhevskaya structural-formation zone (SFZ) of the Eastern Ural megazone. A number of publications assign these rocks either to the basalt-rhyolite formation of the Middle Devonian, or to the basalt-andesite-dacite-rhyolite formation of the Lower-Middle Devonian.Aim. To estimate the age of the ore-bearing volcanic rocks under study using the U-Pb SHRIMP-II isotop ic system of zircon from the rhyolite of the eastern side of the Saf’yanovskoe deposit. By its chemical composition, the rhyolite belongs to the silicic varieties of subvolcanic rocks. Methods and results. The U-Pb isotopic system of zircon was studied by 5-collector mass-spectrometer of high precision and emission of the secondary ions SHRIMP-II (ASI, Australia) in the VSЕGEI Institute. U-Pb relations were investigated by a procedure developed by I.S. Williams. The U-Pb data obtained based on 13 zircon grains showed the age of 422.8 ± 3.7 Ma. Conclusions. The U-Pb dating of zircon obtained previously from the lens-shaped andesite bodies of the western side of the Safyanovskoe deposit gave the age of 422.8 Ma, which corresponds to the Przydoli series epoch of the Upper Silurian. We established that, among the volcanic rocks of the Saf’yanovskoe deposit, the effusive formations of the Upper Silurian are present.
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13

Schiøtte, L., W. Compston, and D. Bridgwater. "U–Th–Pb ages of single zircons in Archaean supracrustals from Nain Province, Labrador, Canada." Canadian Journal of Earth Sciences 26, no. 12 (December 1, 1989): 2636–44. http://dx.doi.org/10.1139/e89-224.

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Ion-probe U–Pb dating of igneous zircons from an acid metavolcanite belonging to the Nulliak supracrustal association of the Saglek area, northern Labrador, suggests an original age of 3776 ± 8 Ma (2σ), interpreted as the deposition age of the volcanite. In accordance with the field model, this is slightly but significantly older than the previously obtained ion-probe U–Pb age of igneous zircons from the main phase of the Uivak gneisses, which carries inclusions of the supracrustal association. A secondary event of zircon growth recorded in the metavolcanite has a maximum age of 3065 ± 8 Ma (2σ).A metapelite belonging to the Weekes amphibolite supracrustal association of the Hopedale area south of Nain contains rounded, low-U zircons of 3258 ± 24 Ma (2σ) age. Occasional textural evidence suggests that some of these zircons are most likely detrital grains of igneous origin, in which case 3258 ± 24 Ma is a minimum age of the source from which the sediment was derived and a maximum age for the deposition of the sediment. However, the possibility that the age represents recrystallization of the sediment under high-grade conditions cannot be ruled out. A 2841 ± 5 Ma (2σ) age obtained on a younger generation of euhedrally zoned high-U zircons from the metapelite is within error of the published bulk zircon U–Pb age of the tonalitic component of the Kanairiktok plutonic suite that intrudes the older orthogneiss and supracrustal units in the area. These younger zircons are most likely to have grown during migmatization of the metasediment at the time of emplacement of the suite.The zircon data give no positive evidence to support correlation between the Nulliak supracrustals and the Weekes amphibolite association.
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14

Kusiak, Monika A., Daniel J. Dunkley, Richard Wirth, Martin J. Whitehouse, Simon A. Wilde, and Katharina Marquardt. "Metallic lead nanospheres discovered in ancient zircons." Proceedings of the National Academy of Sciences 112, no. 16 (April 6, 2015): 4958–63. http://dx.doi.org/10.1073/pnas.1415264112.

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Zircon (ZrSiO4) is the most commonly used geochronometer, preserving age and geochemical information through a wide range of geological processes. However, zircon U–Pb geochronology can be affected by redistribution of radiogenic Pb, which is incompatible in the crystal structure. This phenomenon is particularly common in zircon that has experienced ultra-high temperature metamorphism, where ion imaging has revealed submicrometer domains that are sufficiently heterogeneously distributed to severely perturb ages, in some cases yielding apparent Hadean (>4 Ga) ages from younger zircons. Documenting the composition and mineralogy of these Pb-enriched domains is essential for understanding the processes of Pb redistribution in zircon and its effects on geochronology. Using high-resolution scanning transmission electron microscopy, we show that Pb-rich domains previously identified in zircons from East Antarctic granulites are 5–30 nm nanospheres of metallic Pb. They are randomly distributed with respect to zircon crystallinity, and their association with a Ti- and Al-rich silica melt suggests that they represent melt inclusions generated during ultra-high temperature metamorphism. Metallic Pb is exceedingly rare in nature and previously has not been reported in association with high-grade metamorphism. Formation of these metallic nanospheres within annealed zircon effectively halts the loss of radiogenic Pb from zircon. Both the redistribution and phase separation of radiogenic Pb in this manner can compromise the precision and accuracy of U–Pb ages obtained by high spatial resolution methods.
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15

Doughty, P. Ted, and K. R. Chamberlain. "Protolith age and timing of Precambrian magmatic and metamorphic events in the Priest River complex, northern Rockies." Canadian Journal of Earth Sciences 45, no. 1 (January 1, 2008): 99–116. http://dx.doi.org/10.1139/e07-067.

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U–Pb dating of detrital zircons, magmatic zircons, and metamorphic zircon overgrowths and titanites from the Priest River complex, USA, reveal the ages of high-grade metasedimentary rocks, intrusive ages of associated igneous rocks, and the timing of Precambrian metamorphic events. Sensitive high-mass resolution ion microprobe (SHRIMP) U–Pb dates of detrital zircons from the Hauser Lake gneiss and Gold Cup Quartzite are predominately Paleoproterozoic with some Archean grains. The Hauser Lake gneiss contains detrital zircons with nearly concordant ages as young as 1511 Ma. Isotope dilution – thermal ionization mass spectrometry (ID–TIMS) and chemical abrasion – thermal ionization mass spectrometry (CA–TIMS) dating of magmatic zircon from amphibolites in the Hauser Lake Gneiss yield 1470–1430 Ma crystallization ages based on discordant data, with Cretaceous lower intercepts. The U–Pb zircon systematics are very complex and reflect multiple periods of magmatic and metamorphic growth. A combination of mechanical abrasion, chemical abrasion (CA–TIMS), and SHRIMP methods were required to identify the major geochronological components. These data, in addition to one Nd model age, strengthen correlations between the Hauser Lake Gneiss and the lower Belt–Purcell Supergroup and the Gold Cup Quartzite with the Neihart Quartzite, which underlies the Belt–Purcell Supergroup. Four SHRIMP-dated metamorphic zircon overgrowths give concordant Grenville dates with a weighted average of 1127 ± 110 Ma. This Grenville-aged metamorphic event is recorded by many isotopic systems in the Belt–Purcell basin and reflects a static thermal event, possibly driven by magmatism at depth.
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Williams, Ian S. "Some observations on the use of zircon U-Pb geochronology in the study of granitic rocks." Earth and Environmental Science Transactions of the Royal Society of Edinburgh 83, no. 1-2 (1992): 447–58. http://dx.doi.org/10.1017/s0263593300008129.

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ABSTRACTIn situ, microscale, U-Pb isotopic analyses of zircon using the SHRIMP ion microprobe demonstrate both the potential and the limitations of zircon U-Pb geochronology. Most zircons, whether from igneous or metamorphic rocks, need to be considered as mixed isotopic systems. In simple, young igneous rocks the mixing is principally between isotopically disturbed and undisturbed zircon. In polymetamorphic rocks, several generations of zircon growth can coexist, each with a different pattern of discordance. A similar situation exists for igneous rocks rich in inherited zircon, as these contain both melt-precipitated zircon and inherited components of several different ages. Microscale analysis by ion probe makes it possible to sample the record of provenance, age and metamorphic history commonly preserved within a single zircon population. It also indicates how the interpretation of conventionallymeasured bulk zircon isotopic compositions might be improved.
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17

Takehara, Lucy, Farid Chemale Júnior, Léo A. Hartmann, Ivo A. Dussin, and Koji Kawashita. "U-Pb dating by zircon dissolution method using chemical abrasion." Anais da Academia Brasileira de Ciências 84, no. 2 (June 2012): 399–405. http://dx.doi.org/10.1590/s0001-37652012000200011.

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Chemical abrasion was carried out on zircons grains of the Temora II standard for U-Pb dating prior to analyses using in situ Laser Ablation-MultiCollector Ion Coupled Plasma Mass Spectrometer (LA-ICPMS) followed by the Isotope Dissolution Thermal Ionization Mass Spectrometer (ID-TIMS) method. The proposed methodology was herein applied in order to reduce primarily the effects of secondary Pb loss, the presence of common lead and/or silicate impurities. Nine Temora II zircon grains were analyzed by the laser ablation method yielding an age of 418.3±4.3 Ma. Zircon grains of a same population were separated for chemical abrasion before dissolution and mass spectrometry analyses. Six fractions of them were separated for isotope dissolution using 235U-205Pb mixed spike after we have checked and assured the laboratory conditions of low blank values for total Pb of less than 2 pg/g. The obtained U-Pb zircon age by the ID-TIMS method was 415.7±1.8 Ma (error 0.43 %) based on four successful determinations. The results are consistent with the published ages for the Temora diorite (Temora I – 416.75±1.3 Ma; Temora II – 416.78±0.33 Ma) and established as 416±0.33 Ma. The technique is thus recommended for high precision U-Pb zircon analyses (error < 1 %), mainly for high resolution stratigraphic studies of Phanerozoic sequences.
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18

WANG, JIALIN, CHAODONG WU, ZHUANG LI, WEN ZHU, TIANQI ZHOU, JUN WU, and JUN WANG. "The tectonic evolution of the Bogda region from Late Carboniferous to Triassic time: evidence from detrital zircon U–Pb geochronology and sandstone petrography." Geological Magazine 155, no. 5 (January 16, 2017): 1063–88. http://dx.doi.org/10.1017/s0016756816001217.

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AbstractField-based mapping, sandstone petrology, palaeocurrent measurements and zircon cathodoluminescence images, as well as detrital zircon U–Pb geochronology were integrated to investigate the provenance of the Upper Carboniferous – Upper Triassic sedimentary rocks from the northern Bogda Mountains, and further to constrain their tectonic evolution. Variations in sandstone composition suggest that the Upper Carboniferous – Lower Triassic sediments displayed less sedimentary recycling than the Middle–Upper Triassic sediments. U–Pb isotopic dating using the LA-ICP-MS method on zircons from 12 sandstones exhibited similar zircon U–Pb age distribution patterns with major age groups at 360–320 Ma and 320–300 Ma, and with some grains giving ages of > 541 Ma, 541–360 Ma, 300–250 Ma and 250–200 Ma. Coupled with the compiled palaeocurrent data, the predominant sources were the Late Carboniferous volcanic rocks of the North Tianshan and Palaeozoic magmatic rocks of the Yili–Central Tianshan. There was also input from the Bogda Mountains in Middle–Late Triassic time. The comprehensive geological evidence indicates that the Upper Carboniferous – Lower Permian strata were probably deposited in an extensional context which was related to a rift or post-collision rather than arc-related setting. Conspicuously, the large range of U–Pb ages of the detrital zircons, increased sedimentary lithic fragments, fluvial deposits and contemporaneous Triassic zircon ages argue for a Middle–Late Triassic orogenic movement, which was considered to be the initial uplift of the Bogda Mountains.
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19

Breemen, O. van, and L. Corriveau. "U–Pb age constraints on arenaceous and volcanic rocks of the Wakeham Group, eastern Grenville Province." Canadian Journal of Earth Sciences 42, no. 10 (October 1, 2005): 1677–97. http://dx.doi.org/10.1139/e05-079.

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Combined sensitive high-resolution ion microprobe (SHRIMP) and thermal ionization mass spectrometry (TIMS) U–Pb zircon data from a tightly constrained stratigraphic context of the Wakeham Group provide a precise depositional age for sedimentation within this extensive basin of the Grenville Province. Metavolcanic rocks at the eastern exposure of the Wakeham Group yield ages of 1511 ± 13, 1506 ± 11, 1502 ± 9, and 1491 ± 7 Ma. A crosscutting 1493 ± 10 Ma porphyry vein marks the end of volcanism. The older two volcanic rocks rest stratigraphically above metasediments, with a 1517 ± 20 Ma maximum age of sedimentation derived from the youngest detrital zircons of an arenite. Five 1.61–1.55 Ga inherited zircons in the volcanics, reinforced by coeval inheritance in nearby plutons, indicate a Labradorian basement source to the supracrustals. The predominant arenite detrital zircons dates are in the 1.95–1.75 Ga range, however, and feature both trace element and morphological evidence for metamorphism in the source terrane. Together with zircons as old as 2.95 Ga, the detrital age spectrum is consistent with a circum-Superior provenance. The ages obtained imply that Wakeham Group volcanism and sedimentation were, at least in part, coeval with the onset of 1.52–1.46 Ga Pinwarian plutonism along the southeastern margin of Laurentia. U–Pb zircon analyses record a late Grenvillian metamorphic event around 1019 Ma. U–Pb monazite analyses from one sample yield 1010–1000 Ma ages, and the end of Grenvillian metamorphism is marked by 990 Ma U–Pb titanite ages.
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20

Skublov, Sergey G., Aleksey V. Berezin, Xian-Hua Li, Qiu-Li Li, Laysan I. Salimgaraeva, Veniamin V. Travin, and Dmitriy I. Rezvukhin. "Zircons from a Pegmatite Cutting Eclogite (Gridino, Belomorian Mobile Belt): U-Pb-O and Trace Element Constraints on Eclogite Metamorphism and Fluid Activity." Geosciences 10, no. 5 (May 21, 2020): 197. http://dx.doi.org/10.3390/geosciences10050197.

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This report presents new data on U-Pb geochronology, oxygen isotopes, and trace element composition of zircon from a pegmatite vein crosscutting an eclogite boudin on Stolbikha Island, Gridino area, Belomorian mobile belt (BMB). The zircon grains occur as two distinct populations. The predominant population is pegmatitic and shows dark cathodoluminescence (CL); about a third of this population contains inherited cores. The second zircon population is typical of granulite and exhibits a well-defined sectorial (mosaic) zoning in CL. Both the inherited cores and sectorial in CL zircons appear to have been captured from metabasites as xenocrysts during the pegmatite vein formation. A U-Pb age of 1890 ± 2 Ma for the main zircon population is interpreted as the age of the pegmatite injection. This value is close to the age threshold for the BMB eclogites (~1.9 Ga) and unambiguously defines the upper age limit for the eclogite metamorphism. The pegmatite formation is thus related to partial melting events that occurred during the retrograde amphibolite-facies metamorphism shortly after the eclogitization. A U-Pb date of 2743 ± 10 Ma obtained for the sectorial in CL zircons is considered as the age of the granulite-facies metamorphism established previously within the BMB. The values of δ18O in the zircon populations overlap in a broad range, i.e., δ18O in the pegmatitic zircons varies from 6.1‰ to 8.3‰, inherited cores show a generally higher δ18O of 6.7–8.8‰, and in the captured granulitic zircons δ18O is 6.2–7.9‰. As a result of fluid attack during the final stage of the pegmatite vein formation, the composition of the pegmatitic zircons in terms of non-formula elements (REE, Y, Ca, Sr, Ti) has become anomalous, with the content of these elements having been increased by more than tenfold in the alteration zones. Our data provide new constraints on the timing of eclogite metamorphism within the BMB and show that the late-stage pegmatite-related fluids exerted a very pronounced influence on trace element abundances in zircon, yet had no significant impact on the isotopic composition of oxygen.
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21

Xie, Lie-Wen, Jin-Hui Yang, Qing-Zhu Yin, Yue-Heng Yang, Jing-Bo Liu, and Chao Huang. "High spatial resolution in situ U–Pb dating using laser ablation multiple ion counting inductively coupled plasma mass spectrometry (LA-MIC-ICP-MS)." Journal of Analytical Atomic Spectrometry 32, no. 5 (2017): 975–86. http://dx.doi.org/10.1039/c6ja00387g.

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A new LA-MIC-ICP-MS analytical technique has been developed for the rapid measurement of 206Pb/238U zircon age (<1%, 2s) at a high spatial resolution. We show that this technique can be routinely employed to date U–Pb in small and/or complex zircons, providing a powerful tool for geochronology.
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22

KRISTOFFERSEN, MAGNUS, TOM ANDERSEN, and ARILD ANDRESEN. "U–Pb age and Lu–Hf signatures of detrital zircon from Palaeozoic sandstones in the Oslo Rift, Norway." Geological Magazine 151, no. 5 (October 29, 2013): 816–29. http://dx.doi.org/10.1017/s0016756813000885.

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AbstractU–Pb and Lu–Hf isotope analyses of detrital zircon from the latest Ordovician (Hirnantian) Langøyene Formation, the Late Silurian Ringerike Group and the Late Carboniferous Asker Group in the Oslo Rift were obtained by laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS). Overall the U–Pb dating yielded ages within the range 2861–313 Ma. The U–Pb age and Lu–Hf isotopic signatures correspond to virtually all known events of crustal evolution in Fennoscandia, as well as synorogenic intrusions from the Norwegian Caledonides. Such temporally and geographically diverse source areas likely reflect multiple episodes of sediment recycling in Fennoscandia, and highlights the intrinsic problem of using zircon as a tracer-mineral in ‘source to sink’ sedimentary provenance studies. In addition to its mostly Fennoscandia-derived detritus, the Asker Group also have zircon grains of Late Devonian – Late Carboniferous age. Since no rocks of these ages are known in Fennoscandia, these zircons are inferred to be derived from the Variscan Orogen of central Europe.
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23

Nutman, A. P., and F. Kalsbeek. "Search for Archaean basement in the Caledonian fold belt of North-East Greenland." Rapport Grønlands Geologiske Undersøgelse 162 (January 1, 1994): 129–33. http://dx.doi.org/10.34194/rapggu.v162.8254.

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SHRIMP U-Pb isotope data on zircon crystals from a gneiss sample near Danmarkshavn, where the presence of Archaean rocks has earlier been documented, show that the rock has undergone a complex history of igneous and metamorphic zircon growth. At least three generations of zircon are present with ages of c. 3000 Ma, c. 2725 Ma and 1967 ±8 Ma (2 α). Apparently the rock was formed from an Archaean protolith which underwent high grade metamorphism during the early Proterozoic. Another sample from the easternmost exposures of the Caledonian basement, collected further north, yielded only early Proterozoic zircons with an age of 1963 ± 6 Ma. Together with a SHRIMP U-Pb zircon age of 1974 ± 17 Ma reported earlier, these results give evidence of a major igneous and metamorphic event in North-East Greenland about 1965 Ma ago.
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24

Liu, Chao, Xiangdong Chang, Beilei Sun, and Fangui Zeng. "New Insight into the Depositional Age of No. 6 Coal in Heidaigou Mine, Late Paleozoic Jungar Coalfield, Inner Mongolia, China." Sustainability 14, no. 10 (May 21, 2022): 6297. http://dx.doi.org/10.3390/su14106297.

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Coal deposits can provide novel stratigraphic markers for reconstructing the evolution history of a sedimentary basin and correlating sedimentary successions. Age dating was conducted on zircons harvested from the No. 6 coal seam within the Heidaigou Mine, Inner Mongolia. Two-kilogram samples were taken, and the recovered zircons were analyzed for U–Pb isotopic and rare earth elements (REE). The REE results of the zircon grains showed that all the zircon grains were enriched in heavy rare earth elements (HREE) but depleted in light rare earth elements (LREE). In addition, zircons from the No. 6 coal seam had strongly positive Ce (Ce/Ce* = 2.4–224.6) and strongly negative Eu anomalies (Eu/Eu* = 0.1–0.6). Combined with the clear oscillatory zones in the cathodoluminescence images, all the zircon grains of the No. 6 coal were characteristic of zircons with magmatic origins. The 206Pb/238U ages of 34 zircon grains produced a narrow age population of 303–286 Ma, with a weighted average age of 293.0 ± 1.5 Ma (mean-squared weighted deviation = 1.5). Therefore, we infer that the No. 6 coal in the Heidaigou Mine was deposited during the Early Permian, and the Carboniferous–Permian boundary should be located stratigraphically lower than the No. 6 coal. The zircon U–Pb geochronology is a useful tool to determine the depositional ages of non-marine-influenced coal.
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25

STEPANYUK, L. M. "Zircon and Monazite as Geochronometers." Mineralogical Journal 44, no. 1 (2022): 41–55. http://dx.doi.org/10.15407/mineraljournal.44.01.041.

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The paper discusses the results of U-Pb isotope dating of monazites and zircons from granitoids formed under PT conditions of granulite and amphibolite facies and gneisses, and crystalline shales that are like xenoliths in these granitoids of the Ukrainian Shield. In some cases, such as the Berdychiv-type granitoids and in the Zhezhelivsky quarry, the age values of monazites and outer edges of zircons coincide well; in others, such as the granites of the Ivanivsky quarry, they differ by more than the error. In the Odessa quarry, even greater differences were found between the age of zircon (1.95-1.96 ± give errors Ga) from mafic granulite, and the age of zircon (1.99 Ga) and the age of monazite (1.89-1.83 ± Ga) of a crosscutting enderbite. The U-Pb isotope system of monazite from a vein of biotite granite common in this quarry does not meet the conditions of the Ahrens-Wetherill model. The 207Pb / 206Pb age of monazite ranges from 1909.5 to 1867.0 ± 5 Ma, i.e. by more than 40 Ma. For the Sabarivsky quarry, significant differences in the 207Pb / 206Pb age values (2015.8-1984.8 Ma), which significantly exceed the analytical error, do not allow the use of the concordia U-Pb diagram to interpret the analytical data obtained for zircons from the enderbite. It is concluded that monazite is the better mineral geochronometer, compared to zircon, to determine the age of palingenetic-anatectic granitoids. Unlike zircon, which usually inherits the relict nuclei of parent rocks, relict nuclei in monazites are an exception. However, monazite is not an ideal mineral geochronometer for determining the time of endogenous geological processes. Since the crystallization of monazite is depends on the activity of calcium in the environment, in the same rock association in rocks of different composition, monazite may crystallize at different times. The combination of radiometric studies of zircon and monazite, together with zoning of their crystals, provides ample opportunities to determine the time and duration of endogenous geological processes.
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26

Steshenko, Ekaterina N., Tamara B. Bayanova, and Pavel A. Serov. "The Paleoproterozoic Kandalaksha-Kolvitsa Gabbro-Anorthosite Complex (Fennoscandian Shield): New U–Pb, Sm–Nd, and Nd–Sr (ID-TIMS) Isotope Data on the Age of Formation, Metamorphism, and Geochemical Features of Zircon (LA-ICP-MS)." Minerals 10, no. 3 (March 10, 2020): 254. http://dx.doi.org/10.3390/min10030254.

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The paper provides new U–Pb, Sm–Nd, and Nd–Sr isotope-geochronological data on rocks of the Paleoproterozoic Kandalaksha-Kolvitsa gabbro-anorthosite complex. Rare earth element (REE) contents in zircons from basic rock varieties of the Kandalaksha-Kolvitsa area were analyzed in situ using laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS). Plots of REE distribution were constructed, confirming the magmatic origin of zircon. Temperatures of zircon crystallization were estimated using a Ti-in-zircon geochronometer. The U–Pb method with a 205Pb artificial tracer was first applied to date single zircon grains (2448 ± 5 Ma) from metagabbro of the Kolvitsa massif. The U–Pb analysis of zircon from anorthosites of the Kandalaksha massif dated the early stage of the granulite metamorphism at 2230 ± 10 Ma. The Sm–Nd isotope age was estimated on metamorphic minerals (apatite, garnet, sulfides) and whole rock at 1985 ± 17 Ma (granulite metamorphism) for the Kolvitsa massif and at 1887 ± 37 Ma (high-temperature metasomatic transformations) and 1692 ± 71 Ma (regional fluid reworking) for the Kandalaksha massif. The Sm–Nd model age of metagabbro was 3.3 Ga with a negative value of εNd = 4.6, which corresponds with either processes of crustal contamination or primary enriched mantle reservoir of primary magmas.
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27

LIU, YU, KUNGUANG YANG, ALI POLAT, and XIAO MA. "Reconstruction of the Cryogenian palaeogeography in the Yangtze Domain: constraints from detrital age patterns." Geological Magazine 156, no. 07 (August 20, 2018): 1247–64. http://dx.doi.org/10.1017/s0016756818000535.

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AbstractDetrital zircons are often used to constrain the maximum sedimentary age of strata and sedimentary provenance. This study aimed at reconstructing the Cryogenian palaeogeography of the Yangtze Domain based on U–Pb ages and Lu–Hf isotopic signatures of detrital zircons from sandstones in the southeastern part of the Yangtze Domain. U–Pb ages of the youngest detrital zircon grains from the Niuguping, Gucheng and Datangpo formations yielded average ages of 712±24 Ma, 679.2±6.2 Ma and 665.1±7.4 Ma, respectively, which are close to the depositional ages of their respective formations. An integrated study of detrital zircon Lu–Hf isotopes and U–Pb ages from three samples revealed six main peak ages in the samples from the Anhua section atc. 680 Ma,c. 780 Ma,c. 820 Ma,c. 940 Ma,c. 2000 Ma andc. 2500 Ma. The characteristics of the U–Pb ages and Hf isotopes indicate a link between the north and southeast margins of the Yangtze Domain as early asc. 680 Ma, and the provenance of the coeval sedimentary sequences in the SE Yangtze Domain was the South Qinling Block on the northern margin of the Yangtze Domain. The provenance analysis on thec. 680 Ma detritus composing upper Neoproterozoic strata in the Yangtze Domain revealed that the detritus was transported southward from South Qinling to the southeast margin of the Yangtze Domain through the Exi Strait, but was hindered by the Jiangnan Orogenic Belt.
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28

Sun, Xilin, Klaudia F. Kuiper, Yuntao Tian, Chang’an Li, Zengjie Zhang, and Jan R. Wijbrans. "Comparison of Detrital Zircon U-Pb and Muscovite 40Ar/39Ar Ages in the Yangtze Sediment: Implications for Provenance Studies." Minerals 10, no. 7 (July 20, 2020): 643. http://dx.doi.org/10.3390/min10070643.

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Detrital zircon U-Pb and muscovite 40Ar/39Ar dating are useful tools for investigating sediment provenance and regional tectonic histories. However, the two types of data from same sample do not necessarily give consistent results. Here, we compare published detrital muscovite 40Ar/39Ar and zircon U-Pb ages of modern sands from the Yangtze River to reveal potential factors controlling differences in their provenance age signals. Detrital muscovite 40Ar/39Ar ages of the major tributaries and main trunk suggest that the Dadu River is a dominant sediment contributor to the lower Yangtze. However, detrital zircon data suggest that the Yalong, Dadu, and Min rivers are the most important sediment suppliers. This difference could be caused by combined effects of lower reaches dilution, laser spot location on zircons and difference in closure temperature and durability between muscovite and zircon. The bias caused by sediment laser spot targeting a core or rim of zircon and zircon reworking should be considered in provenance studies.
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29

SANTOSH, M., A. S. COLLINS, T. MORIMOTO, and K. YOKOYAMA. "Depositional constraints and age of metamorphism in southern India: U–Pb chemical (EMPA) and isotopic (SIMS) ages from the Trivandrum Block." Geological Magazine 142, no. 3 (May 2005): 255–68. http://dx.doi.org/10.1017/s0016756805000506.

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We report U–Pb electron microprobe (zircon and monazite) and Secondary Ion Mass Spectrometry (SIMS) U–Pb (zircon) ages from a granulite-facies metapelite and a garnet–biotite gniess from Chittikara, a classic locality within the Trivandrum Block of southern India. The majority of the electron-microprobe data on zircons from the metapelite define apparent ages between 1500 and 2500 Ma with a prominent peak at 2109±22 Ma, although some of the cores are as old as 3070 Ma. Zircon grains with multiple age zoning are also detected with 2500–3700 Ma cores, 1380–1520 mantles and 530–600 Ma outer rims. Some homogeneous and rounded zircon cores yielded late Neoproterozoic ages that suggest that deposition within the Trivandrum Block belt was younger than 610 Ma. The outermost rims of these grains are characterized by early Cambrian ages suggesting metamorphic overgrowth at this time. The apparent ages of monazite grains from this locality reveal multiple provenance and polyphase metamorphic history, similar to those of the zircons. In a typical case, Palaeoproterozoic cores (1759–1967 Ma) are enveloped by late Neoproterozoic rims (562–563 Ma), which in turn are mantled by an outermost thin Cambrian rim (∼515 Ma). PbO v. ThO*2 plots for monazites define broad isochrons, with cores indicating a rather imprecise age of 1913±260 Ma (MSWD=0.80) and late Neoproterozoic/Cambrian cores as well as thin rims yielding a well-defined isochron with an age of 557±19 Ma (MSWD=0.82). SIMS U–Pb isotopic data on zircons from the garnet–biotite gneiss yield a combined core/rim imprecise discordia line between 2106±37 Ma and 524±150 Ma. The data indicate Palaeoproterozoic zircon formation with later partial or non-uniform Pb loss during the late Neoproterozoic/Cambrian tectonothermal event. The combined electron probe and SIMS data from the metapelite and garnet–biotite gneiss at Chittikara indicate that the older zircons preserved in the finer-grained metapelite protolith have heterogeneous detrital sources, whereas the more arenaceous protolith of the garnet–biotite gniess was sourced from a single-aged terrane. Our data suggest that the metasedimentary belts in southern India may have formed part of an extensive late Neoproterozoic sedimentary basin during the final amalgamation of the Gondwana supercontinent.
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30

Skublov, Sergey G., Natalia A. Rumyantseva, Qiuli Li, Boris G. Vanshtein, Dmitriy I. Rezvukhin, and Xianhua Li. "Zircon Xenocrysts from the Shaka Ridge Record Ancient Continental Crust: New U-Pb Geochronological and Oxygen Isotopic Data." Journal of Earth Science 33, no. 1 (February 2022): 5–16. http://dx.doi.org/10.1007/s12583-021-1422-2.

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AbstractOver the past two decades, a significant number of discoveries of ancient zircon xenocrysts in ocean-floor magmatic rocks have been reported. These findings provide compelling evidence for the presence of ancient continental crust within young oceanic lithosphere. Almost all finds of ancient zircon xenocrysts within oceanic crust are from the Mid-Atlantic Ridge. For other localities, however, similar data are very limited. This report presents the first age determinations (U-Pb, SHRIMP-II) and isotope-geochemical data (oxygen, trace and rare earth elements) for zircon xenocrysts from gabbro-diorites of the Shaka Ridge, in the vicinity of the Shaka fracture zone, near the western end of the Southwest Indian Ridge. The work is based on a study of bottom rock material dredged during expeditionary research on the R/V “Akademik Fedorov” (Russia) in 2016. The U-Pb isotope system of the zircon xenocrysts recorded a crystallization age of ∼2.8 Ga at an upper discordia intercept and an age of ∼600 Ma interpreted as the timing of a superimposed thermal event at a lower discordia intercept. The zircon xenocrysts show geochemical signatures of magmatic origin, i.e., fractionated REE distribution spectra with an increase in chondrite-normalized values from light to heavy REE, positive Ce anomalies and negative Eu anomalies, and high Th/U ratios (0.59–7.77). In discrimination diagrams based on a series of inter-element relationships, zircon compositions fall into the fields of zircons from rocks of continental crust, mostly granitoids. The Li content of the zircons is high (1.8 ppm–50 ppm), adding further evidence to their derivation from rocks of continental crust. During their residence within young oceanic crust, the zircon xenocrysts experienced alterations under the influence of submarine high-temperature hydrothermal fluids, which selectively affected the distribution of trace elements in the zircons and reduced the δ18O values to 1.75‰–3.15‰. The presence of obviously older zircons in Shaka gabbro-diorites clearly demonstrates the presence of ancient continental fragments and their recycling into the mantle at the western end of the Southwest Indian Ridge.
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31

Young, David N., and Lance P. Black. "U-Pb zircon dating of Proterozoic igneous charnockites from the Mawson Coast, East Antarctica." Antarctic Science 3, no. 2 (June 1991): 205–16. http://dx.doi.org/10.1017/s095410209100024x.

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We report ion-microprobe U-Pb zircon ages from charnockites of a large Proterozoic composite batholith, Mawson Coast, Australian Antarctic Territory. The charnockites crystallized from orogenic magmas of intermediate composition (mainly 54–68% SiO2) intruded into a granulite-facies metasedimentary gneiss sequence between the second and third recognized deformations. A sample of low-Ti charnockite provides an age of 954 ± 12 Ma and a high-Ti charnockite is dated at 985 ± 29 Ma (all ages quoted at 95% confidence). The age difference is not significant at the 95% confidence level. Both these ages were obtained from zircons with igneous zoning and/or morphology and thus are thought to date igneous crystallization. Zircons from a felsic gneiss xenolith within the charnockite have cores of various ages, many from 1.7 to 2.0 Ga, but with other grains between 1.0 and 1.5 Ga and a single 2.5 Ga zircon. These zircon cores are direct evidence for an early to middle Proterozoic age for the supracrustal basement sequence in this mobile belt. Many of these zircon cores are concordant but abundant discordant grains suggest a complex history of multiple Pb-loss events. Zircon rims grew at 921 ± 19 Ma, probably during the post-charnockite deformation (D3). Previously obtained Rb-Sr dates for charnockite of 886 ± 48 Ma and 910 ± 18 Ma were probably also rest during D3. A Rb-Sr isochron date of 1061 ± 36 Ma previously reported for high-Ti charnockite from Mawson Rock is thought to be erroneous, and a new date of 959 ± 58 Ma (consistent with both the igneous and reset dates above) is interpreted from those data.
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32

Compston, W. "Geological age by instrumental analysis: the 29th Hallimond Lecture." Mineralogical Magazine 63, no. 3 (June 1999): 297–311. http://dx.doi.org/10.1180/002646199548475.

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AbstractThe need in geology for in situ U-Pb age determinations of minerals is illustrated by two examples: the internal age dispersion developed within the zircon SL13 shortly after original crystallization, and the occurrence within minerals of old cores and later overgrowths. SL13 contains rare μm-sized patches of unsupported radiogenic Pb and a mainly bimodal distribution of 206Pb/238U ages otherwise. Both observations are consistent with original crystallization at 580 Ma and Pb loss at 565 Ma. Age precision is controlled by the ions counted for radiogenic Pb, and varies with instrumental sensitivity, age and U contents of the target. Laser-ablation ICPMS has similar spatial resolution and sensitivity to SIMS but consumes more sample because of much greater hole-depth in practice. Like SIMS, the measured Pb+/U+ is biased and also changes with depth so comparison with a standard mineral is necessary. Analyses of reference zircons reported here indicate that the reproducibility of Pb/U ages by ICPMS is limited by residual bias, not ion counting errors. For multipurpose ICPMS at least, the Hg background at mass 204 prohibits the measurement of 204Pb for common Pb estimation. A third micro-analytical method, ‘CHIME’, and future developments in SIMS and ICPMS are discussed briefly.
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33

ZECK, H. P., M. J. WHITEHOUSE, and J. M. UGIDOS. "496 ± 3 Ma zircon ion microprobe age for pre-Hercynian granite, Central Iberian Zone, NE Portugal (earlier claimed 618 ± 9 Ma)." Geological Magazine 144, no. 1 (October 27, 2006): 21–31. http://dx.doi.org/10.1017/s0016756806002718.

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Ion microprobe (SIMS) dating of zircon from the Miranda do Douro orthogneiss, Central Iberian Zone, Hercynian Iberian belt, defines an Early Ordovician U–Pb age of 496.0 ± 2.6 Ma (95 % conf., MSWD = 1.14) for magmatic zircon crystallization in its granitic protolith. The age contrasts with an earlier, conventional (ID-TIMS) U–Pb zircon age of 618 ± 9(95 % conf.) Ma, now thought to be an artefact of the complex zircon population. Individual SIMS ages for zircon from the rock range from 2700 to 180 Ma and comprise inherited and magmatic zircon, both concordant and common Pb-enriched, and younger, reset ages. The ID-TIMS study seems to have misinterpreted this heterogeneous population as a cogenetic suite consisting of magmatic zircon and its age-reset equivalents produced by recent Pb loss. The 496 ± 3 Ma SIMS age represents the weighted average for 26 magmatic zircon domains located by careful inspection of cathodoluminescence, secondary electron and optical microscopy images of ∼ 700 individual zircon crystals. Inherited zircon is widespread, ranging in age from 2700 to 550 Ma, with age clusters, which are statistically indistinguishable from those known from pre-Hercynian granitic basement material elsewhere in the Central Iberian Zone. Including the present age information, 582 ± 4 Ma (95 % conf., MSWD = 1.02, n = 13) and 619 ± 9 Ma (95 % conf., MSWD = 0.93, n = 7) appear as prevailing inherited zircon age components in basement intrusions in the Central Iberian Zone.
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34

Corfu, F., T. E. Krogh, and L. D. Ayres. "U–Pb zircon and sphene geochronology of a composite Archean granitoid batholith, Favourable Lake area, northwestern Ontario." Canadian Journal of Earth Sciences 22, no. 10 (October 1, 1985): 1436–51. http://dx.doi.org/10.1139/e85-150.

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U–Pb zircon and sphene data for several phases of composite batholiths in the Favourable Lake area of the Superior Province indicate two major periods of plutonism separated by a hiatus of over 200 Ma.A trondhjemite, which now forms a metamorphosed remnant within a batholith, was emplaced 2950 ± 5 Ma ago during an early plutonic event. The second and dominant plutonic period occurred between [Formula: see text] and 2711.0 ± 2.0 Ma ago; these are the ages of the earliest and the latest widespread phase of the batholiths, respectively. Ages of 2716.3 ± 1.4 and 2716 ± 4 Ma for zircons of two minor dioritic phases also fall within this interval. Metamorphic zircons about 2730 and 2715 Ma old from another unit of the batholith indicate a temporal correlation between metamorphism and main plutonic pulses.Sphenes from two samples near the margins of the batholiths yield the same age of 2711 ± 2 Ma as coexisting zircons and date the primary crystallization of the rocks. In contrast, sphenes from six samples from the interior of a batholith yield ages of 2680 ± 10 Ma, which are significantly younger than primary ages of 2950–2716 Ma of coexisting zircons. These sphene ages probably record cooling below about 500 °C during a long and complex cooling process.Several of the studied zircon populations exhibit complex discordance patterns reflecting multiple stages of Pb loss. Zircons in rocks predating the 2700–2730 Ma old metamorphic–plutonic event experienced Pb loss during this event, probably by annealing. A second low-grade event apparently caused chemical alteration of high-U zircon domains and Pb loss about 1750 Ma ago. A late stage of Pb loss affected near-surface zircon domains about 600–0 Ma ago.
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Burda, Jolanta, Aleksandra Gawęda, and Urs Klötzli. "U-Pb zircon age of the youngest magmatic activity in the High Tatra granites (Central Western Carpathians)." Geochronometria 40, no. 2 (June 1, 2013): 134–44. http://dx.doi.org/10.2478/s13386-013-0106-9.

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Abstract Detailed cathodoluminescence (CL) imaging of zircon crystals, coupled with Laser Ablation Multi-Collector Inductively Coupled Plasma Mass Spectrometry (LA-MC-ICP-MS) U-Pb zircon dating was used to develop new insights into the evolution of granitoids from the High Tatra Mountains. The zircon U-Pb results show two distinct age groups (350±5 Ma and 337±6 Ma) recorded from cores and rims domains, respectively. Obtained results point that the last magmatic activity in the Tatra granitoid intrusion occurred at ca. 330 Ma. The previously suggested age of 314 Ma reflects rather the hydrothermal activity and Pb-loss, coupled with post-magmatic shearing.
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36

Anderson, H. Elizabeth, and Donald W. Davis. "U–Pb geochronology of the Moyie sills, Purcell Supergroup, southeastern British Columbia: implications for the Mesoproterozoic geological history of the Purcell (Belt) basin." Canadian Journal of Earth Sciences 32, no. 8 (August 1, 1995): 1180–93. http://dx.doi.org/10.1139/e95-097.

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The Mesoproterozoic Purcell Supergroup (and its equivalent in the United States, the Belt Supergroup) is a thick sedimentary sequence formed in an extensional basin of uncertain age and tectonic setting. The voluminous tholeiitic Moyie sills intrude turbidites of the lower and middle Aldridge Formation, the lowest division of the Purcell Supergroup. Many of the sills were intruded into soft sediment and one intrudes the Sullivan sedimentary exhalative (SEDEX) orebody, so their age approximates that of the sediments and the Sullivan deposit. New U–Pb dates of zircon from four sills are older than previously published U–Pb zircon ages. One sill contained concordant zircons with an age of 1468 ± 2 Ma. Near concordant zircons from the other samples have similar 207Pb/206Pb ages, indicating that all of the sills crystallized at the same time. U–Pb dates of titanites from two of these sills yielded concordant dates ranging from 1090 to 1030 Ma, indicating that they have undergone a previously unrecognized Grenville-age metamorphism. The U–Pb systematics of abraded zircons from one sill indicate that they have also been affected by this event. The recognition of Grenville-age metamorphism in the Purcell (Belt) basin suggests that the prevalent 1.0–1.1 Ga Rb–Sr and K–Ar mineral and whole-rock dates from a wide variety of Purcell (Belt) igneous and sedimentary rocks are also metamorphic, and are not ages of sedimentation or "hybrid" dates reflecting partial resetting by the ca. 760 Ma Goat River orogeny. On this basis, all sedimentation in the Purcell (Belt) basin is constrained to be older than 1.1 Ga and is probably older than 1.25 Ga.
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37

STEPANYUK, L. M., L. V. SHUMLYANSKYY, S. I. KURYLO, V. O. SYOMKA, S. M. BONDARENKO, S. A. WILDE, and A. A. NEMCHIN. "The U-Pb Zircon Geochronology (LA-ICP-MS) of Geological Processes in Granulites of Middle Bouh Area. Article 3. Rock association in the lower reaches of the Yatran river." Mineralogical Journal 43, no. 1 (2021): 34–50. http://dx.doi.org/10.15407/mineraljournal.43.01.034.

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LA-ICP-MS method was applied to investigate U-Pb and Lu-Hf isotope systematics of zircon crystals from charnockitic gneiss and biotite-garnet-hypersthene enderbite that occur in the lower reaches of the Yatran river (Yatran block of the Bouh river area). According to the obtained isotope data, charnockitic gneiss hosts three zircon populations. The oldest one is represented by three crystals that have isotope age between 3125 and 3300 Ma, and εHf values between –2.3 and –7.5. The next population is well-defined, it has an age of 2038±25 Ma and large variations of Hf isotope composition: 176Hf/177Hf — from 0.28122 to 0.28261, εHf — from –9.3 до 4.6. However, the ages of most of the analyzed zircons spread along the concordia between 2300 and 2800 Ma. All zircons in this population have a similar Hf isotope composition 176Hf/177Hf = 0.28072 to 0.28092, which does not depend on the age. It is characteristic that the oldest (with preserved U-Pb isotope systematics) crystals have positive or slightly negative εHf values. Most of the U-Pb isotope analyses of zircons from enderbite fall on the discordia line that has an upper interception age of 2029 ± 18 Ma. A small number of discordant grains have 207Pb/206Pb ages up to 2500 Ma. Hafnium isotope composition in zircons from enderbite varies widely: 176Hf/177Hf = 0.28131 to 0.28151, and εHf from –6.2 to 1.8.
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38

Mortensen, J. K., J. R. Montgomery, and J. Fillipone. "U–Pb zircon, monazite, and sphene ages for granitic orthogneiss of the Barkerville terrane, east-central British Columbia." Canadian Journal of Earth Sciences 24, no. 6 (June 1, 1987): 1261–66. http://dx.doi.org/10.1139/e87-120.

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Granitic orthogneiss forms an important component of the Barkerville terrane of southeastern British Columbia. Rb–Sr whole-rock ages for the orthogneisses are ambiguous and range from Late Proterozoic to mid-Paleozoic, with large associated errors. U–Pb dating of zircon, monazite, and sphene has been employed in an attempt to establish precise crystallization ages for two of the orthogneiss bodies. U–Pb systematics for zircons from both bodies show the combined effects of inheritance of zircon cores and postcrystallization Pb loss. This complexity precludes a precise estimate of the age of emplacement of the granitic protoliths of the gneiss. The data do, however, constrain possible emplacement ages for the bodies to between 335 and 375 Ma (Late Devonian – mid-Mississippian).A U–Pb age of 174 ± 4 Ma for metamorphic sphene from one of the orthogneiss bodies is interpreted as dating the end of the second phase of deformation in the area. Two nearly concordant U–Pb ages of 114 and 117 Ma for monazite from the second body remain problematical. These data suggest either that the monazite grew during a relatively young shearing and (or) metamorphic event that locally affected the Barkerville terrane or that the closure temperatue for the U–Pb system in monazite is lower than had previously been inferred, or both.
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39

Liu, Li, and Daniel F. Stockli. "U-Pb ages of detrital zircons in lower Permian sandstone and siltstone of the Permian Basin, west Texas, USA: Evidence of dominant Gondwanan and peri-Gondwanan sediment input to Laurentia." GSA Bulletin 132, no. 1-2 (May 23, 2019): 245–62. http://dx.doi.org/10.1130/b35119.1.

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Abstract The Permian Basin of west Texas, one of the most economically significant hydrocarbon basins in the United States, formed along the southwest margin of Laurentia in the foreland of the Ouachita-Marathon orogen during the late Paleozoic. While its stratigraphic record temporally coincides with syn- and post-orogenic Ouachita-Marathon sedimentation, sediment provenance, sediment routing and dispersal, and paleo-drainage evolution have remained controversial. This study presents more than 2000 new detrital zircon U-Pb ages from 16 samples across the Permian Basin to elucidate early Permian sediment provenance and basin-fill evolution. The data show that Wolfcampian sandstones are dominated by 950–1070 Ma and 500–700 Ma detrital zircon U-Pb ages, whereas Leonardian sandstones and siltstones are dominated by 500–700 Ma and 280–480 Ma detrital zircon U-Pb ages. Most of these age clusters are not typical Laurentian basement ages, but rather indicative of a southern Gondwanan and peri-Gondwanan sources of Mexico and Central America. This interpretation is corroborated by zircons with peri-Gondwanan and Gondwanan rim-core relationships, as well as major age components of euhedral zircons, matching Maya block basement ages. Regional comparison of these new detrital zircon results with published data from Carboniferous and Permian sedimentary rocks in various terranes of Mexico and Central America, Appalachian foreland basins, Ouachita orogenic belt, midcontinent of United States, and Fort Worth Basin (Texas), indicates that most sediment influx to the Permian Basin during the early Permian (Wolfcampian and Leonardian) was derived from basement or recycled upper Paleozoic strata associated with Gondwanan and peri-Gondwanan terranes in modern Mexico and Central America. North American basements such as the Appalachian Grenville (950–1300 Ma), Granite-Rhyolite (1300–1500 Ma), and Yavapai-Mazatzal (1600–1800 Ma) provinces, appear to have provided only minor amounts of sediment. In light of depositional age constraints, the timing of Marathon-Ouachita collision, and careful detrital zircon U-Pb age spectra comparison, the sediment provenance shift from Wolfcampian to Leonardian points to a diachronous, oblique continent-continent collision between Gondwana/peri-Gondwanan terranes and Laurentia.
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40

Creaser, Robert A., Larry M. Heaman, and Philippe Erdmer. "Timing of high-pressure metamorphism in the Yukon – Tanana terrane, Canadian Cordillera: constraints from U – Pb zircon dating of eclogite from the Teslin tectonic zone." Canadian Journal of Earth Sciences 34, no. 5 (May 1, 1997): 709–15. http://dx.doi.org/10.1139/e17-057.

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Zircon from eclogite near Last Peak in the Teslin tectonic zone yielded a U–Pb isotopic age of 269 + 2 Ma (2σ), the first precise age for such a rock in the Yukon –Tanana terrane of the Canadian Cordillera. Both the morphology and geochemistry of the eclogitic zircons indicate a metamorphic origin, and the U – Pb age therefore constrains the timing of peak high-pressure metamorphism in this rock. The U – Pb age demonstrates for the first time that an Early Permian high-pressure metamorphic event occurred in rocks now making up the Teslin tectonic zone, and possibly elsewhere in the Yukon – Tanana terrane. This U – Pb age provides a new geochronologic "pin" in the evolution of the Yukon – Tanana terrane prior to its Mesozoic accretion to the North American continental margin and, combined with recent 40Ar/39Ar muscovite data, indicates that high-pressure metamorphism at this time was a relatively short-lived event.
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41

Corfu, F., and J. Wood. "U–Pb zircon ages in supracrustal and plutonic rocks; North Spirit Lake area, Northwestern Ontario." Canadian Journal of Earth Sciences 23, no. 7 (July 1, 1986): 967–77. http://dx.doi.org/10.1139/e86-098.

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The North Spirit Lake greenstone belt in the Sachigo Subprovince of the Superior Province comprises parts of three sequences of volcanic and sedimentary rocks; the main (youngest) is separated from the older sequences by an unconformity to disconformity. The belt is bounded by large granitoid batholiths and was metamorphosed under greenschist to, locally, hornblende–cordierite facies. U–Pb zircon dating was performed on volcanic, sedimentary, and plutonic rocks in order to establish an absolute chronology for the evolution of the area.A tuff breccia in the lowermost supracrustal sequence is dated at 3023 ± 2 Ma. Zircons from a tuff in the middle sequence show complex U–Pb relationships; although they do not allow a precise age determination, the data suggest that the tuff formed sometime between 2950 and 2800 Ma ago. Zircons from a quartz arenite, also in the middle sequence, yield a simple data pattern and define an age of [Formula: see text], suggesting derivation of the sediment from a uniform source of this age. A zircon analysis from a tonalitic clast in a conglomerate at the base of the upper sequence yields a minimum age of 2975 Ma. The clast may have had the same origin as the zircons in the quartz arenite. Another tonalitic clast from the same conglomerate yields a slightly older age of 3001 ± 3 Ma. No remnant of these tonalites can be recognized in the field, suggesting that they have been largely removed during subsequent erosional processes.Two subvolcanic intrusions from the upper sequence yield zircon ages of 2743 ± 2 and 2731 ± 2 Ma, respectively. A crystal tuff, also in the upper sequence, contains two generations of zircons: newly formed magmatic zircons, which date the extrusion of the tuff at 2735 ± 10 Ma, and older grains with a minimum age of 2862 Ma, which represent inherited zircons. This tuff was thus generated at least in part by anatectic melting of >2862 Ma crust.A quartz diorite from MacDowell Lake in the adjacent Berens River Subprovince yields an age of 2744 ± 2 Ma. A mafic inclusion in the quartz diorite contains amoeboidal, strongly fractured zircons, which point to an intercept age of about 2727 Ma. This age could either reflect a metamorphic event or represent a geologically meaningless mixed age.
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42

Li, Liming, Fanyan Yang, Mingtao Li, Zhirong Liang, Xuedong Ma, and Jingxiong Tian. "U–Pb zircon dating of the Paleoproterozoic khondalite series in the northeastern Helanshan region and its geological significance." Open Geosciences 14, no. 1 (January 1, 2022): 544–67. http://dx.doi.org/10.1515/geo-2022-0380.

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Abstract Petrography, zircon cathodoluminescence, and laser ablation-inductively coupled plasma mass spectrometry (LA-ICP-MS) U–Pb zircon dating were performed on the Paleoproterozoic khondalite series and the intrusive altered diabase dykes developed in the northeastern Helanshan region were analyzed. The results showed that most of the zircons in the khondalite series were detrital zircons with oscillatory zoning and a high Th/U ratio, with few metamorphic zircons having a low Th/U ratio. The 207Pb/206Pb age of the detrital zircons ranged from 3131–1980 Ma, which constrained the protolith age of the Helanshan khondalite series to after 1980 Ma. The age of the metamorphic zircons indicated two age groups as follows: 1965–1921 Ma and 1876–1820 Ma. Besides, the age of altered diabase dykes was 1865–1850 Ma. In combination with previous studies, these new metamorphic ages indicated that the metamorphic events in the northeastern Helanshan region involved the collision followed by post-collisional extension and exhumation between the Yinshan Block to the north and the Ordos Block to the south. Moreover, the 1965–1921 Ma group represented the period of the collision between the Yinshan Block and the Ordos Block and the subsequent post-collisional extension event, whereas 1876–1820 Ma indicated the period of the exhumation stage.
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43

Bortnikov, N. S., S. А. Silantiev, F. Bea, P. Montero, T. F. Zinger, S. G. Skolotnev, and E. V. Sharkov. "U-Pb dating, oxygen and hafnium isotopic ratios of zircon from rocks of oceanic core complexes at Mid-Atlantic Ridge: evidence for an interaction of young and ancient crusts at spreading of the ocean floor." Доклады Академии наук 489, no. 5 (December 20, 2019): 483–89. http://dx.doi.org/10.31857/s0869-56524895483-489.

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U-Pb age, oxygen and hafnium isotopic ratios in zircon from rocks of ocean core complexes at Mid-Atlantic Ridge have been studied using SHRIMP and MC-LA-ICP-MS techniques. U-Pb dating revealed four group of zircons: 1) 0,6-1,7 Ma, 2) 6,7-11,2 Ma, 3) 12,9-17,6 Ma, 4) 200 to 2044 Ma. The 18O values range from 4,74 to 7,2 and are distinct for zircon grains of different ages. Hafnium isotopic ratio for zircon aged from 0,6 to 17,6 Ma corresponds or is close to that of MORB from Central Atlantic. The oxygen and hafnium isotopic compositions of zircon elder than 280 Ma correspond to those of the sialic continental crust. A hypothesis of involvement of the ancient pre-Atlantic sialic (280 млн лет) and old Atlantic (7-17 Ma) crusts in a generation of the contemporary (young) oceanic crust during formation of the slow-spreading Mid-Atlantic Ridge has been proposed.
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44

Hudon, Pierre, Richard M. Friedman, Gilles Gauthier, and Jacques Martignole. "Age of the Cabonga nepheline syenite, Grenville Province, western Quebec." Canadian Journal of Earth Sciences 43, no. 9 (September 1, 2006): 1237–49. http://dx.doi.org/10.1139/e06-022.

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This study presents isotope dilution – thermal ionization mass spectrometry (ID–TIMS) U–Pb data for megacrystic zircon from the Cabonga Nepheline Syenite Complex of the Réservoir Cabonga terrane (Grenville Province). This terrane is an allochthonous slab metamorphosed under granulite-grade conditions ~1.18–1.14 Ga and transported onto migmatites of the Grenvillian Parautochthon at about 1.02 Ga. The very low uranium and lead concentrations of zircon from the Cabonga nepheline syenite (CNS) did not permit determination of a statistically significant crystallization age using laser ablation microbeam techniques. Consequently, extensive microsampling (15 zircon chips), guided by X-ray and electronic imaging, followed by ID–TIMS analyses were carried out on a single megacrystic zircon. A regression of 13 out of 15 U–Pb isotopic analyses results in a crystallization age of 1171 ± 3 Ma for the CNS. Criteria based on zircon morphologies, zoning patterns, varying Th/U ratios (0.3–0.9), and a highly fractionated Zr/Hf ratio (68) suggest an igneous derivation for the CNS. The Cabonga alkaline rocks, intruded under high-grade metamorphic conditions, preceded the onset of the widespread and ubiquitous (1.15 ± 0.01 Ga) anorthosite–mangerite–charnockite–granite magmatism in the southern part of the Grenville Province.
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45

Dinh, Sang Quang. "PETROGRAPHIC CHARACTERISTICS AND ZIRCON U-PB GEOCHRONOLOGY OF GRANITOID ROCKS IN THE SOUTHERN BÊN GIANG, QUNG NAM PROVINCE." Science and Technology Development Journal 14, no. 4 (December 30, 2011): 17–30. http://dx.doi.org/10.32508/stdj.v14i4.2024.

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The early Palaeozoic calc-alkaline granitoid association in south Nam Giang town is forming large area reaching hundreds of km2, along the east – west ductile deformation zones, which is studied in detail in diffirent geologic maps scales by the geologists (Huynh Trung and Nguyen Xuan Bao, 1981 at 1:500,000 scale or Nguyen Van Trang et al, 1986, at 1:200,000 scale). The six samples were studied in details, which are composed mainly quartz diorite and granodiorite. The samples were crushed and large zircons were extracted. The laser ablation microprobe-inductively coupled plasma mass spectrometer (LA-ICP MS) U-Pb zircon dating was carried out by standard methods at CODES, University of Tasmania-Australia. In-situ zircon U–Pb geochronology was conducted on six samples of age between 306 Ma and 278 Ma. A total of seventytwo zircons were analysed and the results exist a narrow spread in individual zircon ages between ca. 269 and 313 Ma, with significant form a coherent single age suite of 295 Ma (early Permian). As the six samples are all assigned to the same granitic suite, I have combined the individual isotopic data yields a weighted mean age from 72 analyses of 294 Ma, which represents the minimum age for the crystallisation of the south Ben Giang granite.
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46

Moser, D. E., C. L. Cupelli, I. R. Barker, R. M. Flowers, J. R. Bowman, J. Wooden, and J. R. Hart. "New zircon shock phenomena and their use for dating and reconstruction of large impact structures revealed by electron nanobeam (EBSD, CL, EDS) and isotopic U–Pb and (U–Th)/He analysis of the Vredefort domeThis article is one of a series of papers published in this Special Issue on the theme of Geochronology in honour of Tom Krogh." Canadian Journal of Earth Sciences 48, no. 2 (February 2011): 117–39. http://dx.doi.org/10.1139/e11-011.

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Integrated electron nanobeam (EBSD, CL, EDS) and isotopic measurements (U–Pb, (U–Th)/He) of zircon from the collar and centre of the 80 km wide central uplift of the 2020 ± 3 Ma Vredefort impact structure reveal new shock features in a microstructural progression related to impact basin formation and degree of U–Pb age resetting: (1) planar fractures in {1K0} and {1K2} orientation during initial shock wave compression; (2) curviplanar fractures in {1K1} orientation, now annealed, which host glassy inclusions of partial melt of the host rock; (3) microtwin lamellae in an orientation of 65° about [110], attributed to shock wave rarefaction; (4) nucleation of impact-age crystallites, possibly on microtwins, during post-shock heating by impact melt; and (5) crystal-plastic deformation linked to crater modification of the core of the central uplift. Planar fracturing and microtwinning ≥20 GPa in “cold shock” zircon in granitoid at a radial distance of 25 km failed to reset zircon age. Single-grain ID–TIMS data extend between pre-impact age of 2077 ± 11 Ma and a secondary Pb-loss event at ca. 1.0 Ga — the latter reflecting Kibaran igneous activity between 1.110 and 1.021 Ga. Age resetting by the impact event operated in an ∼15 km wide “hot shock” zone of impact-elevated temperatures ≥700 °C at the core of the central uplift. Mechanisms include internal recrystallization, defect-accelerated Pb diffusion via shock microstructures and melt films, and late crystal-plastic deformation. Igneous zircons from a 2019 ± 2 Ma foliated norite impact melt yield a mean (U–Th)/He date of 923 ± 61 Ma, indicating exposure of the present surface after this time.
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47

Allibon, James, Maria Ovtcharova, François Bussy, Michael Cosca, Urs Schaltegger, Denise Bussien, and Éric Lewin. "Lifetime of an ocean island volcano feeder zone: constraints from U–Pb dating on coexisting zircon and baddeleyite, and 40Ar/39Ar age determinations, Fuerteventura, Canary IslandsThis article is one of a series of papers published in this Special Issue on the theme of Geochronology in honour of Tom Krogh." Canadian Journal of Earth Sciences 48, no. 2 (February 2011): 567–92. http://dx.doi.org/10.1139/e10-032.

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High-precision isotope dilution – thermal ionization mass spectrometry (ID–TIMS) U–Pb zircon and baddeleyite ages from the PX1 vertically layered mafic intrusion Fuerteventura, Canary Islands, indicate initiation of magma crystallization at 22.10 ± 0.07 Ma. The magmatic activity lasted a minimum of 0.52 Ma. 40Ar/39Ar amphibole dating yielded ages from 21.9 ± 0.6 to 21.8 ± 0.3, identical within errors to the U–Pb ages, despite the expected 1% theoretical bias between 40Ar/39Ar and U–Pb dates. This overlap could result from (i) rapid cooling of the intrusion (i.e., less than the 0.3 to 0.6 Ma 40Ar/39Ar age uncertainties) from closure temperatures (Tc) of zircon (699–988 °C) to amphibole (500–600 °C); (ii) lead loss affecting the youngest zircons; or (iii) excess argon shifting the plateau ages towards older values. The combination of the 40Ar/39Ar and U/Pb datasets implies that the maximum amount of time PX1 intrusion took to cool below amphibole Tc is 0.8 Ma, suggesting PX1 lifetime of 520 000 to 800 000 Ma. Age disparities among coexisting baddeleyite and zircon (22.10 ± 0.07/0.08/0.15 Ma and 21.58 ± 0.15/0.16/0.31 Ma) in a gabbro sample from the pluton margin suggest complex genetic relationships between phases. Baddeleyite is found preserved in plagioclase cores and crystallized early from low silica activity magma. Zircon crystallized later in a higher silica activity environment and is found in secondary scapolite and is found close to calcite veins, in secondary scapolite that recrystallised from plagioclase. close to calcite veins. Oxygen isotope δ18O values of altered plagioclase are high (+7.7), indicating interaction with fluids derived from host-rock carbonatites. The coexistence of baddeleyite and zircon is ascribed to interaction of the PX1 gabbro with CO2-rich carbonatite-derived fluids released during contact metamorphism.
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48

Verhaegen, Jasper, Hilmar von Eynatten, István Dunkl, and Gert Jan Weltje. "Detrital zircon geochronology and heavy mineral analysis as complementary provenance tools in the presence of extensive weathering, reworking and recycling: the Neogene of the southern North Sea Basin." Geological Magazine 158, no. 9 (March 30, 2021): 1572–84. http://dx.doi.org/10.1017/s0016756821000133.

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AbstractHeavy mineral analysis is a long-standing and valuable tool for sedimentary provenance analysis. Many studies have indicated that heavy mineral data can also be significantly affected by hydraulic sorting, weathering and reworking or recycling, leading to incomplete or erroneous provenance interpretations if they are used in isolation. By combining zircon U–Pb geochronology with heavy mineral data for the southern North Sea Basin, this study shows that the classic model of sediment mixing between a northern and a southern source throughout the Neogene is more complex. In contrast to the strongly variable heavy mineral composition, the zircon U–Pb age spectra are mostly constant for the studied samples. This provides a strong indication that most zircons had an initial similar northern source, yet the sediment has undergone intense chemical weathering on top of the Brabant Massif and Ardennes in the south. This weathered sediment was later recycled into the southern North Sea Basin through local rivers and the Meuse, leading to a weathered southern heavy mineral signature and a fresh northern heavy mineral signature, yet exhibiting a constant zircon U–Pb age signature. Thus, this study highlights the necessity of combining multiple provenance proxies to correctly account for weathering, reworking and recycling.
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49

Schiøtte, L., W. Compston, and D. Bridgwater. "Ion probe U–Th–Pb zircon dating of polymetamorphic orthogneisses from northern Labrador, Canada." Canadian Journal of Earth Sciences 26, no. 8 (August 1, 1989): 1533–56. http://dx.doi.org/10.1139/e89-131.

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Rounded zircons included within igneous zircons from the Uivak I gneisses, northern Labrador, have ages of up to 3863 ± 12 Ma (2σ), showing the (former) existence of rocks that predate the Uivak gneisses by more than 100 Ma. The igneous zircons themselves have experienced varying amounts of early Pb loss, but age estimates based on maximum 207Pb/206Pb from three separate gneiss samples agree to within error at 3732 ± 6 Ma (2σ), which is taken as the age of emplacement of the igneous precursor to the dominant component of the Uivak gneisses. A new generation of zircons was formed during migmatization at ca. 3620 Ma. The volumetrically less important Lister gneiss was emplaced at 3235 ± 8 Ma (2σ). In the late Archaean, different parts of the gneiss complex were subjected to different grades of metamorphic overprinting. The zircon chronology of gneisses affected by granulite facies metamorphism suggests a rapid sequence of events, with simultaneous recrystallization of old zircons and growth of new U-poor zircons at 2766 ± 17 Ma (2σ), followed by partial melting at 2744 ± 4 Ma (2σ), and further recrystallization and growth of U-poor zircons afterwards. No late Archaean zircon growth has been recorded from orthogneisses unaffected by granulite fades metamorphism.
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50

Parrish, R. R., and I. Reichenbach. "Age of xenocrystic zircon from diatremes of western Canada." Canadian Journal of Earth Sciences 28, no. 8 (August 1, 1991): 1232–38. http://dx.doi.org/10.1139/e91-110.

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Abstract:
Numerous diatremes of middle and late Paleozoic age intrude miogeoclinal middle and lower Paleozoic strata in the Canadian Cordillera. In addition to abundant crustal xenoliths and conspicuous mantle-derived mineral xenocrysts, rare zircon grains are present. U–Pb dating of single zircon crystals from many of these diatremes has failed to identify the presence of cogenetic (magmatic) zircons. All dated zircon grains are interpreted as xenocrysts derived from the crust. Their morphologies range from euhedral to very rounded, and their ages range from early Paleozoic to Archean. Most ages fall between 1.8 and 2.1 Ga, with subordinate age groupings in the late Archean (ca. 2.6 Ga), Middle Proterozoic (1.0–1.1 Ga), and early Paleozoic (ca. 470 Ma, 530 Ma). The Proterozoic and Archean zircons could have been derived from either the crystalline basement or its overlying sedimentary cover of Late Proterozoic to early Paleozoic age. Paleozoic zircons were probably derived from either intrusions within the basement or sills that intrude the early Paleozoic sedimentary cover, and they signify magmatic activity possibly related to rifting of the continental margin.
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