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Relevant bibliographies by topics / Trimethylphosphin

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Academic literature on the topic 'Trimethylphosphin'

Author: Grafiati

Published: 4 June 2021

Last updated: 1 February 2022

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Journal articles on the topic "Trimethylphosphin"

1

Kreissl, F. R., W. Uedelhoven, and D. Neugebauer. "Carbonyl(cyclopentadienyl)(trimethylphosphin)tolylcarbin-komplexe von Molybdän und Wolfram." Journal of Organometallic Chemistry 344, no. 2 (April 1988): C27—C30. http://dx.doi.org/10.1016/0022-328x(88)80486-8.

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Schütt, Wolfgang, Norbert Ullrich, and Frist R. Kreiβl. "Darstellung und Reaktionen von Trimethylphosphin-sbustituierten η2-Triocarbenkomplexes des Wolframs." Journal of Organometallic Chemistry 408, no. 1 (January 1991): C5—C8. http://dx.doi.org/10.1016/0022-328x(91)80108-v.

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Steil, Peter, and Andreas Mayr. "Selektive Ligandensubstitutionsreaktionen an Carbin-Wolframkomplexen des Typs [W(CPh)Br(CO)2L2] (L = Stickstoff-Donorligand) / Selective Ligand Substitution Reactions on Carbyne Tungsten Complexes of the Type [W(CPh)Br(CO)2L2] (L = Nitrogen Donor Ligand)." Zeitschrift für Naturforschung B 47, no. 5 (May 1, 1992): 656–61. http://dx.doi.org/10.1515/znb-1992-0508.

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The reaction of [W(CPh)Br(CO)2(py)2] (1) with one equivalent of triisopropylphosphine gives [W(CPh)Br(CO)2(py)(P-i-Pr3)] (3). The reaction of 1 with two equivalents of triisopropylphosphine under irradiation with visible light affords trans-[W(CPh)Br(CO)2(P-i-Pr3)2] (4). Substitution of the pyridine ligand in 3 by other ligands L (t-butylisocyanide, trimethylphosphine and trimethylphosphite) gives the complexes [W(CPh)Br(CO)2(L)(P-i-Pr3)]. Reaction of 4 with t-butylisocyanide gives trans-[W(CPh)Br(CO)(CNCMe3)(P-i-Pr3)2]. Irradiation of [W(CPh)Br(CO)2(tmeda)] in the presence of excess trimethylphosphine gives [W(CPh)Br(CO)(PMe3)3]. The reaction of 1 with maleic anhydride gives [W(CPh)Br(CO)(C4H203)(py)2].

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4

Geboes, Yannick, Frank De Proft, and Wouter A. Herrebout. "Taking the halogen bonding–hydrogen bonding competition one step further: complexes of difluoroiodomethane with trimethylphosphine, dimethyl sulfide and chloromethane." Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials 73, no. 2 (March 14, 2017): 168–78. http://dx.doi.org/10.1107/s2052520617001354.

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To rationalize the driving factors in the competition of halogen bonding and hydrogen bonding, the complexes of the combined halogen-/hydrogen-bond donor difluoroiodomethane with the Lewis bases trimethylphosphine, dimethyl sulfide and chloromethane are studied. For all Lewis bases,ab initiocalculations lead to halogen- and hydrogen-bonded complexes. Fourier transform–IR experiments involving solutions of mixtures of difluoroiodomethane with trimethylphosphine(-d9) or dimethyl sulfide(-d6) in liquid krypton confirm the coexistence of a halogen-bonded and hydrogen-bonded complex. Also for solutions containing chloromethane, evidence of the formation of binary associations is found, but no definitive assignment of the multiple complex bands could be made. Using van't Hoff plots, the experimental complexation enthalpies for the halogen- and hydrogen-bonded complex of difluoroiodomethane with trimethylphosphine are determined to be −15.4 (4) and −10.5 (3) kJ mol−1, respectively, while for the halogen- and hydrogen-bonded complexes with dimethyl sulfide, the values are −11.3 (5) and −7.7 (6) kJ mol−1, respectively. The experimental observation that for both trimethylphospine and dimethyl sulfide the halogen-bonded complex is more stable than the hydrogen-bonded complex supports the finding that softer Lewis bases tend to favor iodine halogen bonding over hydrogen bonding.

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Kreißl, Fritz R., and Norbert Ullrich. "Elektrophile Addition des Thiomethyl-Kations an η5-Cyclopentadienyl(ethoxymethylcarben)-(nitrosyl)(trimethylphosphin)molybdän." Journal of Organometallic Chemistry 440, no. 3 (November 1992): 335–39. http://dx.doi.org/10.1016/0022-328x(92)80212-g.

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Steinborn, Dirk, Steffi Becke, Renate Herzog, Mike Günther, Robert Kircheisen, Helen Stoeckli-Evans, and Clemens Bruhn. "Heteroatomfunktionalisierte Methylgold-Komplexe: Synthese und Struktur von Chlormethyl(triphenylphosphin)- und Phenylthiomethyl(trimethylphosphin)gold." Zeitschrift für anorganische und allgemeine Chemie 624, no. 8 (August 1998): 1303–7. http://dx.doi.org/10.1002/(sici)1521-3749(199808)624:8<1303::aid-zaac1303>3.0.co;2-r.

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7

Schütt, W., E. Herdtweck, F. Hahn, and F. R. Kreißl. "Darstellung und Röntgenstrukturuntersuchung von [1-Carbonyl-1-(η5-cyclopentadienyl)-2,3-dimethyl-1-trimethylphosphin-3-trimethylphosphoranyliden-1-wolframa-2-thiacyclopropan]-tetrafluoroborat." Journal of Organometallic Chemistry 443, no. 2 (January 1993): C33—C36. http://dx.doi.org/10.1016/0022-328x(93)80311-x.

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8

Kameda, Mitsuaki, and Goji Kodama. "Reaction of Bis(trimethylphosphine)heptahydrotetraboron(1+) Cation with Trimethylphosphine." Collection of Czechoslovak Chemical Communications 62, no. 8 (1997): 1279–88. http://dx.doi.org/10.1135/cccc19971279.

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The reaction of the arachno-bis(trimethylphosphine)heptahydrotetraboron(1+) cation, B4H7 . 2 P(CH3)3+ (1), with trimethylphosphine paralleled with that of the isoelectronic arachno-trimethylphosphine-tetraborane(8), B4H8 . P(CH3)3 (2). Thus, it first gave the hypho-tris(trimethylphosphine)heptahydrotetraboron(1+) cation, B4H7 . 3 P(CH3)3+ (3), which further reacted with P(CH3)3 to finally give cleaved products, the hypho-tetrakis(trimethylphosphine)tetrahydrotriboron(1+) cation, B3H4 . 4 P(CH3)3+ (4), and trimethylphosphine-borane(3), BH3 . P(CH3)3. The effect of the ionic charges upon the reaction rates was apparent. Thus, the second reaction for 1 was rapid at room temperature while the corresponding reaction for 2 was slow and the negatively charged isoelectronic species, the B4H9 . P(CH3)3+ anion, did not undergo the second reaction. The above two hypho polyboron complex cations, 3 and 4, were characterized by 11B and 31P NMR spectroscopy. Like its isoelectronic counterparts, the cation 3 was highly fluxional; at room temperature the three B-P(CH3)3 groups were equivalent on the NMR time scale.

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Klein, Hans-Friedrich, Xiaoyan Li, Ulrich Flörke, and Hans-Jürgen Haupt. "Hydrido(acylenolato)cobalt(III)-Verbindungen mit Trimethylphosphan- Liganden: Insertionsreaktionen mit Alkinen und die ersten Carbonylcobalt(III)-Komplexe / Hydrido(acylenolato)cobalt(III) Compounds Containing Trimethylphosphane Ligands: Insertion Reactions with Alkynes and the First Carbonylcobalt(III) Complexes." Zeitschrift für Naturforschung B 55, no. 8 (August 1, 2000): 707–17. http://dx.doi.org/10.1515/znb-2000-0807.

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Abstract Formal insertion of phenylethyne into Co-H functions of mer-octahedral acyl(enolato)-cobalt(III) hydrides 1-3 proceeds under ambient conditions affording η1-vinylcobalt(III) compounds where the dianionic acyl(enolato) ligands are derived from 2-formyl-4-phenyl-cyclohexanone (4), 1-formyl-cyclohexan-2-one (5), and 3-hydroxo-2,3-diphenyl-propenal (6). Dissociation and association of trimethylphosphane results in a reversible transformation of penta-coordinate complexes 4 -6 into hexa-coordinate ones 7 -9, respectively, involving different tautomeric vinyl species. In toluene solution 9 rearranges by reductive C,C coupling into a 5,6-η2-olefin(enolato)cobalt(I) complex 10. Trimethylsilylethyne undergoes a hydrolytic desilylation reaction which is followed by reductive C,C-coupling reactions of acyl and vinyl functions selectively producing chelating η1-enolato-5,6-η2-olefin ligands in cobalt(I) com pounds 13 -16 where the (ax,eq)chelating ligands are derived from 1-formyl-cyclohexan-2-one (13), 3-hydroxo-2,3-diphenyl-propenal (14), 2-formyl-α-tetralone (15), and 2-formyl-4-tert-butyl-cyclohexanone (16). An axial position of the enolato-O donor in the trigonal bipyramidal configuration of complex 15 has been confirmed by X-ray diffraction analysis. With 1,4-bis(trimethylsilyl)buta-diyne 1,2-addition in cobalt(III) hydrides 2, 3, 11 (as deriverd from 2-formyl-α-tetralone), and 12 (as derived from 2-formyl-4-tert-butyl-cyclohexanone) produces 2-metalated vinyl groups in compounds 17 -20. Dissociation of trimethylphosphane from 17 and 19 does not activate C,C coupling at the cobalt(III) centre of penta-coordinate 21 and 22. Steric congestion in compounds 17, 18, and 20 favours exchange of trimethylphosphine for carbon monoxide affording the first octahedral carbonyl complexes of cobalt (d6) (23 -25). In the crystal and in solution a meridional configuration is adopted by complex 23 with the CO group in a position opposite to the acyl function.

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Shen, Wanling, Xin Li, and Xin Liu. "A study of oxidizing centers in carbon nanotubes by solid-state NMR." RSC Advances 5, no. 74 (2015): 60380–85. http://dx.doi.org/10.1039/c5ra07605f.

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The adsorbed trimethylphosphine is oxidized to trimethylphosphine oxide by the oxygen-containing groups on the surface of functionalized CNTs. The concentration of oxidizing center is selectively measured.

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Dissertations / Theses on the topic "Trimethylphosphin"

1

Parkin, G. "The chemistry of trimethylphosphine tungsten complexes." Thesis, University of Oxford, 1985. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.355780.

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Clayton, C. W. "The synthesis and chemistry of some novel trimethylphosphine hydride complexes of iridium." Thesis, University of Oxford, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.379909.

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3

Alper, Fatma. "Synthesis And Characterization Of Tetracarbonylpyrazinetrimethylphosphitetungsten(0) Complexes." Master's thesis, METU, 2004. http://etd.lib.metu.edu.tr/upload/12605569/index.pdf.

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In this study, the effect of a donor ligand on the stabilization of a carbonyl pyrazine tungsten complex was studied. The pentacarbonylpyrazinetungsten(0) complex could be formed from the photolysis of hexacarbonyltungsten(0) in the presence of pyrazine and could be isolated as crystalline solid. However, the complex was found to be unstable in solution, being converted to a bimetallic complex, (CO)5W(pyz)W(CO)5 and free pyrazine molecule. Two complexes exist in solution at equilibrium. The equilibrium constant could be determined by 1H-NMR spectroscopy and found to be 0.0396 at 25°
C. To test whether the introduction of a second pyrazine ligand might provide stability for the carbonyl-pyrazine-tungsten complex, W(CO)4(pyz)2 was attempted to be synthesized. The cis-W(CO)4(pyz)2 complex could be generated from the thermal substitution reaction of cis-W(CO)4(piperidine)2 with excess pyrazine in dichloromethane. However, this complex could not be isolated because of the lack of stability. The complex could only be identified by IR spectroscopy in solution. To stabilize the pentacarbonylpyrazinetungsten(0) complex, trimethylphosphite was introduced to the complex as a donor ligand. For this purpose, cis-W(CO)4[P(OCH3)3](thf), photogenerated from W(CO)5[P(OCH3)3] in tetrahydrofuran (thf), was reacted with pyrazine. The replacement of tetrahydrofuran with pyrazine (pyz) yielded cis-W(CO)4[P(OCH3)3](pyz). The complex could be isolated from the reaction solution and characterized by means of IR, 1H-, 13C-, 31P-NMR, and Mass spectroscopies. The introduction of P(OCH3)3 has proved that a donor ligand will strengthen the metal-pyrazine bond and thus stabilizes the complex. As a result of this stabilization, the complex could be isolated as the first example of tungsten pyrazine complexes that contain a donor ligand.

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4

Boga, Dilek Ayse. "Synthesis And Characterization Of Pentacarbonylacryloylferrocenetungsten(0) Complex." Master's thesis, METU, 2006. http://etd.lib.metu.edu.tr/upload/12606968/index.pdf.

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Pentacarbonylacryloylferrocenetungsten(0) complex was synthesized photochemically from hexacarbonyltungsten(0) and acryloyferrocene (acfc). UV irradiation of W(CO)6 in the presence of acryloylferrocene at 10 oC for 4 hours in n-hexane solution generates the W(CO)5(&
#61544
2-acfc) complex as the sole monosubstitution product of the photolysis, as monitored by FT-IR spectroscopy. The product complex could be isolated from the reaction solution and characterized by IR, Raman, 1H-NMR, 13C-NMR spectroscopies, mass spectrometry and elemental analysis. The complex was found to be unstable in solution and to decompose to the parent W(CO)6 complex and free acryloylferrocene molecule. The instability of the complex makes its isolation as analytically pure substance difficult. In order to stabilize the tungsten-olefin bond, trimethylphosphite was introduced as a donor ligand into the molecule. Thus, a complex containing a donor ligand in addition to the olefinic ligand was prepared starting with W(CO)6, trimethylphosphite, and acryloylferrocene. UV irradiation of W(CO)5[P(OMe)3] with acryloylferrocene in n-hexane solution at room temperature generates W(CO)4[P(OMe)3](&
#61544
2-acfc), which was isolated from the reaction solution and characterized by IR, 1H-NMR, 13C-NMR spectroscopies and mass spectrometry. The complex was found to have a cis arrangement of four CO groups in the pseudo-octahedral geometry. However, the cis-W(CO)4[P(OMe)3](&
#61544
2-acfc) complex was found to be less stable than W(CO)5(&
#61544
2-acfc).

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5

Rempe, Margaret Eileen. "Electron donor and acceptor properties of trimethylphosphine, triphenylphosphine, and related ligands with transition metals by photoelectron spectroscopy." Diss., The University of Arizona, 1994. http://hdl.handle.net/10150/186698.

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Gas-phase photoelectron spectroscopy is used to evaluate the a-donation and 1t-acceptance abilities of a series of Group 15 ligands. The free ligands PMe(3-n)Ph(n) (n=0-3), EMe₃ (E=As) and EPh₃ (E=As, Sb, Bi) are examined (Me=CH₃, Ph=C₆H₅) and the trends in lone pair ionizations are discussed. Organometallic compounds investigated include CpMn(CO)2L (L=PPh₃, AsPh₃), Cp'Mn(CO)₂L (L=PPh₃, PMe₃, AsPh₃, SbPh₃), and Mo(CO)₅L (L=PMe₃, PPh₃). Contrary to initial predictions based on electronegativities and solution pKₐ's, the trend in ionization energies for the series PMe(3-n)Ph(n) is PPh₃ < PMePh₂ < PMe₂Ph < PMe₃. The trend in first ionizations is governed by a filled-filled interaction between the lone pair and phenyl rings. The metal ionization energies of organometallic compounds containing PMe₃ and PPh₃ reflect this trend indicating that the above order is also the order of a-donation. These metal ionizations also indicate that all members of the series, PMe(3-n)Ph(n), have the same amount of π-acceptance. Just as in the phenyl containing phosphine ligands, the ligands EPh₃ exhibit filled-filled interactions between the lone pair and phenyl orbitals, but not uniformly. This filled-filled interaction decreases with the heavier elements. The order of lone pair ionizations for EPh₃ is PPh₃ < AsPh₃, SbPh₃, BiPh₃. The destabilization expected upon descent of the periodic table is offset by the effects of decreasing relaxation energy and decreasing filled-filled interactions. Metal ionizations do not strictly follow the trends of the free ligands EPh₃. These metal ionization energies coincide for organometallic compounds where E is phosphorus or arsenic. Metal ionization energies for E=Sb are very slightly stabilized compared to E=P, As. The ligands EPh₃ display the same amount of σ and π interactions in the organometallic compounds examined. It is observed that the identity of R is more important in determining σ/π interactions than the element directly bound to the metal. This work serves to bring together previous literature and current experimental results to understand the structure and bonding in the ligands ER₃ (E=P, As, Sb, Bi and R=Me, Ph).

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6

Habbadi, Nouzha. "Activation des petites molecules par les complexes du cobalt : reaction des complexes monovalents du cobalt et de la trimethylphosphine avec les alcynes vrais." Toulouse 3, 1986. http://www.theses.fr/1986TOU30073.

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La reactivite des alcynes vrais est dominee par leur acidite et en consequence leur aptitude a donner des reactions d'addition oxydante sur le centre metallique riche en electrons. Aucune oligomerisation ni polymerisation n'a ete observee. Par contre des especes originales considerees comme les intermediaires reactifs des mecanismes de polymerisation des alcynes catalysee par les metaux de transition ont ete isoles. Avec les trois alcynes utilises : le t-butylacetylene, le pentyne et le phenylacetylene, huit composes originaux ont ete mis en evidence et isoles par cristallisation fractionnee

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7

Matthews, Kelly E. "Elucidation of the aqueous equilibrium system of IrH₂(PMe₃)₃Cl and periodic trends of the iridium (III) dihydrido tris(trimethylphosphino) series, IrH₂(PMe₃)₃X." Diss., This resource online, 1994. http://scholar.lib.vt.edu/theses/available/etd-06062008-164037/.

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8

Alnagi, Omar. "Reaction de la trimethylphosphine sur les sels de cobalt (ii) : synthese des complexes pentacoordonnes cox::(2)(pme::(3))::(3) (x=c1**(-), br**(-), i**(-), ncs**(-), no::(2)**(-)), reactivite vis-a-vis de petites molecules co, no et o::(2)." Toulouse 3, 1987. http://www.theses.fr/1987TOU30048.

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Synthese et etude physicochimique des complexes. Reactivite. Etude cristallographique de la structure indiquant une geometrie de bipyramide trigonale deformee quand x**(-)=cl**(-),br**(-),i**(-),ncs**(-) et une geometrie de pyramide a base carree pour x=no::(2)**(-). Etude des substitutions par co,no et o::(2)

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9

LEPETIT, POURCELOT CHRISTINE. "Mise au point de nouveaux catalyseurs de dimerisation du propylene a base de complexes supportes du nickel : controle de la stabilite et de la selectivite par effet de ligands : influence electronique sterique et mecanistique." Paris 6, 1987. http://www.theses.fr/1987PA066489.

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10

Menu, Marie-Joëlle. "Nouveaux reactifs dans la chimie des complexes du rhodium, du chrome et du tungstene : les anions diazo rc(n::(2))**(-)." Toulouse 3, 1988. http://www.theses.fr/1988TOU30068.

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Synthese des complexes de rh, cr et w contenant le coordinat diazo en faisant reagir les sels de li des anions rc(n::(2))**(-) sur les complexes metalliques. On a isole: (pme::(3))::(4) rhc(n::(2))sime::(3) (pet::(3))::(3) rhc(n::(2))sime::(3), (pme::(3))::(2) rhc(n::(2))(s)p(n-ipr::(2))::(2). On a mis en evidence un complexe carbenique dimere possedant un groupe ylure, lors de la photolyse de (pet::(3))::(3) rhc(n::(2))sime::(3)

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Book chapters on the topic "Trimethylphosphin"

1

Werner, H., R. Feser, V. Harder, W. Hofmann, H. Neukomm, and W. D. Jones. "Cyclopentadienylbis (Trimethylphosphine) and Cyclopentadienylbis (Trimethylphosphite) Complexes of Co and Rh." In Inorganic Syntheses, 158–64. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132562.ch38.

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Werner, H., R. Feser, V. Harder, W. Hofmann, H. Neukomm, and W. D. Jones. "Cyclopentadienylbis(Trimethylphosphine) and Cyclopentadienylbis(Trimethylphosphite) Complexes of Co and Rh." In Inorganic Syntheses, 280–85. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132593.ch71.

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Markham, R. T., E. A. Dietz, D. R. Martin, O. Stelzer, and R. Schmutzler. "Trimethylphosphine." In Inorganic Syntheses, 153–55. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132470.ch41.

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Luetkens, M. L., A. P. Sattelberger, H. H. Murray, J. D. Basil, J. P. Fackler, R. A. Jones, and D. E. Heaton. "Trimethylphosphine." In Inorganic Syntheses, 7–12. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132579.ch3.

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Luetkens, M. L., A. P. Sattelberger, H. H. Murray, J. D. Basil, J. P. Fackler, R. A. Jones, and D. E. Heaton. "Trimethylphosphine." In Inorganic Syntheses, 305–10. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132593.ch76.

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Thomas, R., Klaas Eriks, R. R. Holmes, R. P. Carter, and E. Lanpher. "Trimethylphosphine." In Inorganic Syntheses, 59–63. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132401.ch18.

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Karsch, Hans Heinz, and Michele Aresta. "Trimethylphosphine Iron Complexes." In Inorganic Syntheses, 69–75. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132517.ch21.

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Kent Barefield, E., and U. Klabunde. "Pentahydridobis(trimethylphosphine)iridium(V)." In Inorganic Syntheses, 34–38. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132463.ch10.

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Labinger, J. A., J. A. Osborn, and A. Davison. "Carbonyl Trimethylphosphine Iridium(I) Complexes." In Inorganic Syntheses, 62–65. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132494.ch13.

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Miller, N. E., K. C. Nainan, G. E. Ryschkewitsch, and Goji Kodama. "Bis(trimethylphosphine)dihydroboron(III) Iodide." In Inorganic Syntheses, 135–39. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132432.ch23.

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