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Journal articles on the topic 'Tin hydride'

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Published: 4 June 2021
Last updated: 2 February 2022

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1

Light, James, and Ronald Breslow. "A water soluble tin hydride reagent." Tetrahedron Letters 31, no. 21 (1990): 2957–58. http://dx.doi.org/10.1016/s0040-4039(00)88997-2.

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2

Belletire, J. L., and N. O. Mahmoodi. "Direct butyrolactone production using tin hydride." Tetrahedron Letters 30, no. 33 (January 1989): 4363–66. http://dx.doi.org/10.1016/s0040-4039(00)99361-4.

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3

Torvisco, Ana, Judith Binder, Melanie Wolf, Cathrin Zeppek, Hans-Georg Stammler, Norbert Mitzel, and Frank Uhlig. "Crystallographic studies of novel aryl heavy Group 14/15 halides and hydrides." Acta Crystallographica Section A Foundations and Advances 70, a1 (August 5, 2014): C676. http://dx.doi.org/10.1107/s2053273314093231.

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A series of novel aryl (phenyl, tolyl, xylyl, mesityl, naphthyl, anthracenyl) heavy Group 14 and 15 halides (Cl, Br) and hydrides have been synthesized and structurally characterized via X-ray diffraction. Depending on the nature of the aryl substituent, these compounds display a range of non-covalent intermolecular interactions in the form of edge to face, π-π stacking and C-H···π interactions resulting in discrete arrangements in the solid state. The strength of these interactions as well as halide or hydride substituent effects and their consequences on resulting structural parameters will be highlighted and discussed. In addition, in situ crystallization techniques were employed to elucidate the structures of highly air sensitive novel aryl tin and silicon hydride species.
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4

Martin, F., FM Corrigan, Ofx Donard, J. Kelly, Jao Besson, and DF Horrobin. "Organotin compounds in trimethyltin-treated rats and in human brain in Alzheimer's Disease." Human & Experimental Toxicology 16, no. 9 (September 1997): 512–15. http://dx.doi.org/10.1177/096032719701600906.

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As blood tin concentrations are elevated in Alzheimer's disease and as some low molecular weight organotin compounds are neurotoxic, we have attempted to detect organotins in brain in Alzheimer's Disease. First we measured the concentration of trimethyltin (TMT) in the brains of rats which had been exposed to memory- impairing concentrations of TMT and, as the method of linking hydride generation, cryogenic trapping, gas chromatographic separation and atomic absorption spec trophotometric detection permitted the measurements of organotin compounds when the total tin was greater than 0.2 nanograms, we applied these techniques to human brain tissue, some of which showed neuropathological evidence of Alzheimer's Disease. No low molecular weight organotin compounds were detected in the human brain tissue, but it is possible that tin may be complexed with large organic molecules, the hydrides of which would not be volatile, but which could be identified by liquid chromatography.
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5

Weiß, Sebastian, Max Widemann, Klaus Eichele, Hartmut Schubert, and Lars Wesemann. "Low valent lead and tin hydrides in reactions with heteroallenes." Dalton Transactions 50, no. 14 (2021): 4952–58. http://dx.doi.org/10.1039/d1dt00542a.

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6

Novák, Miroslav, Libor Dostál, Zdenka Růžičková, Stefan Mebs, Jens Beckmann, and Roman Jambor. "From Monomeric Tin(II) Hydride to Nonsymmetric Distannyne." Organometallics 38, no. 12 (June 5, 2019): 2403–7. http://dx.doi.org/10.1021/acs.organomet.9b00215.

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7

Curran, Dennis P., and Churl Min Seong. "The Tin Hydride Reductive Decyanation of Geminal Dinitriles." Synlett 1991, no. 02 (1991): 107–8. http://dx.doi.org/10.1055/s-1991-20644.

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8

LIGHT, J., and R. BRESLOW. "ChemInform Abstract: A Water Soluble Tin Hydride Reagent." ChemInform 22, no. 23 (August 23, 2010): no. http://dx.doi.org/10.1002/chin.199123211.

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9

Studer, Armido, and Stephan Amrein. "Tin Hydride Substitutes in Reductive Radical Chain Reactions." Synthesis 2002, no. 07 (2002): 835–49. http://dx.doi.org/10.1055/s-2002-28507.

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10

Kerschl, Susanna, and Bernd Wrackmeyer. "Notizen: Versuche zur Herstellung eines Alkenyl(dimethyl)zinnhydrids: Gibt es eine intramolekulare Sn–H–B-Brücke?/ Attempts at the Synthesis of an Alkenyl(dimethyl)tin Hydride: Is there an Intramolecular Sn–H–B Bridge?" Zeitschrift für Naturforschung B 42, no. 8 (August 1, 1987): 1047–49. http://dx.doi.org/10.1515/znb-1987-0820.

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Abstract2-(E)-Dim ethyl(chloro)stannyl-3-diethylboryl-2- pentene (lc) reacts with trimethyltin hydride (3) to give the corresponding alkenyl(dim ethyl)tin hydride (2). Compound 2 has been characterized by 1H, 11B, 13C, 119Sn NMR . Neither the NMR nor the IR data are in support of an intramolecular Sn-H-B bridge.
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11

Rončević, Sanda, Anica Benutić, Ivan Nemet, and Buga Gabelica. "Tin Content Determination in Canned Fruits and Vegetables by Hydride Generation Inductively Coupled Plasma Optical Emission Spectrometry." International Journal of Analytical Chemistry 2012 (2012): 1–7. http://dx.doi.org/10.1155/2012/376381.

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Tin content in samples of canned fruits and vegetables was determined by hydride generation inductively coupled plasma atomic emission spectrometry (HG-ICP-OES), and it was compared with results obtained by standard method of flame atomic absorption spectrometry (AAS). Selected tin emission lines intensity was measured in prepared samples after addition of tartaric acid and followed by hydride generation with sodium borohydride solution. The most favorable line at 189.991 nm showed the best detection limit (1.9 μg L−1) and limit of quantification (6.4 μg kg−1). Good linearity and sensitivity were established from time resolved analysis and calibration tests. Analytical accuracy of 98–102% was obtained by recovery study of spiked samples. Method of standard addition was applied for tin determination in samples from fully protected tinplate. Tin presence at low-concentration range was successfully determined. It was shown that tenth times less concentrations of Sn were present in protected cans than in nonprotected or partially protected tinplate.
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12

Fu, Gregory C. "New applications of organometallic catalysts in organic chemistry." Pure and Applied Chemistry 74, no. 1 (January 1, 2002): 33–36. http://dx.doi.org/10.1351/pac200274010033.

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13

Gastaldi, Stéphane, and Didier Stien. "PAH-supported tin hydride: a new tin reagent easily removable from reaction mixtures." Tetrahedron Letters 43, no. 24 (June 2002): 4309–11. http://dx.doi.org/10.1016/s0040-4039(02)00801-8.

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14

Matsuo, Takashi, Kunihiko Komatsuzaki, Takanori Tsuji, and Takashi Hayashi. "Reaction of cobalt porphycene with hydride reagents: spectroscopic detection of Co–H porphycene species and formation of Co–SnR3 porphycene species." Journal of Porphyrins and Phthalocyanines 16, no. 05n06 (May 2012): 616–25. http://dx.doi.org/10.1142/s1088424612500587.

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The reaction of tetrapropylporphycenatocobalt(III) with tributyltin hydride generates a cobalt(III)–hydride porphycene detectable by UV-vis spectroscopy under diluted conditions, whereas it is impossible to characterize hydride species of cobalt porphyrins. One of the reasons for the stability of the porphycene hydride species is that the porphycene ring has a lower LUMO energy level due to the decrease in the symmetry of the ligand character. However, the hydride species in a highly concentrated solution of the complex is easily converted into the cobalt(II) species via dimerization or reaction of the hydride with excess tributyltin hydride through hemolysis of the Sn–H/Co–H bonds. When the Co(III) porphycene is reacted with LiBHEt3 , the final product is the cobalt(III)–ethyl complex formed by β-rearrangement during the reaction of the hydride species and diethylborane in a solvent cage. In the reaction of tetrakistrifluoromethylporphycenatocobalt(III) with tributyltin hydride, the dominant reaction pathway includes one-electron reduction of the porphycene ring together with radical coupling of the tin reagent rather than the net hydride transfer. This finding suggests that the delicate control of the LUMO energy level influences the stability of the hydride species. The tetrapropylporphycenatocobalt(III) complex with tributyltin or triphenyltin hydride in the presence of AIBN produces the corresponding Co(III)– trialkyltin complex. This complex was characterized by 1H NMR spectroscopy.
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15

Tanaka, Hideo, Hiroaki Suga, Hidenori Ogawa, A. K. M. Abdul Hai, Sigeru Torii, Anny Jutand, and Christian Amatore. "Electrooxidative initiation of tin hydride-promoted radical chain reactions." Tetrahedron Letters 33, no. 43 (October 1992): 6495–98. http://dx.doi.org/10.1016/s0040-4039(00)79024-1.

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16

Vedejs, E., S. M. Duncan, and A. R. Haight. "An internally activated tin hydride with enhanced reducing ability." Journal of Organic Chemistry 58, no. 11 (May 1993): 3046–50. http://dx.doi.org/10.1021/jo00063a024.

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17

Jana, Anukul, Herbert W Roesky, Carola Schulzke, and Alexander Döring. "Reactions of Tin(II) Hydride Species with Unsaturated Molecules." Angewandte Chemie International Edition 48, no. 6 (January 26, 2009): 1106–9. http://dx.doi.org/10.1002/anie.200805595.

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18

Jana, Anukul, Herbert W Roesky, Carola Schulzke, and Alexander Döring. "Reactions of Tin(II) Hydride Species with Unsaturated Molecules." Angewandte Chemie 121, no. 6 (January 26, 2009): 1126–29. http://dx.doi.org/10.1002/ange.200805595.

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19

Miller, Benjamin L., and James W. Hershberger. "Preparation of a highly functionalized polystyrene-bound tin hydride." Journal of Polymer Science Part C: Polymer Letters 25, no. 5 (May 1987): 219–21. http://dx.doi.org/10.1002/pol.1987.140250505.

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20

Suarez-Vazquez, Santiago I., and Makoto Nanko. "Fabrication and Consolidation of TiNx by Pulsed Electric Current Sintering." Materials Science Forum 761 (July 2013): 55–58. http://dx.doi.org/10.4028/www.scientific.net/msf.761.55.

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A new and simple method is proposed to fabricate fully dense and single fcc phase of substoichiometric titanium nitride (TiNx). Powders mixture composed of titanium hydride (TiH2) and titanium nitride (TiN) was consolidated by using pulsed electric current sintering. All samples showed relative density values higher than 98% with larger grain size at lower nitrogen concentration. Lattice parameter increased linearly with increasing [N]/[Ti] ratio. In addition, TiNx with substoichiometric compositions was more easily densified than stoichiometric TiN. The addition of TiH2 improves the sinterability of the samples preserving the fcc phase characteristic of TiN.
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21

Khyzhnyak, V. G., A. I. Dudka, I. I. Bilyk, O. V. Khyzhnyak, and M. V. Arshuk. "Protective Coatings on Steel Tytanoalitovani 40X13." Фізика і хімія твердого тіла 16, no. 3 (September 15, 2015): 593–98. http://dx.doi.org/10.15330/pcss.16.3.593-598.

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Past studies on application to the surface of steel 40X13 multi tytanoalitovanyh coatings in containers of consumable shutter using a mixture of powders of titanium, aluminum; titanium hydride; tytanoalituvannya steel 40X13 with pre-deposited TiN layer; tytanoalituvannya pre-nitrided steel among ammonia. The possibility of forming coatings on steel 40X13 involving compounds Ti4Fe2O, FeTiAl, TiN, TiC and transition zone. Established distribution of chemical elements and microhardness thickness diffusion coatings. The maximum microhardness detected for layers Tees - 31,0-34,0 GPa; TiN layers for - 19,5-22,5 GPa; for the zone Ti4Fe2O, FeTiAl - 5,0-7,0 GPa.
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22

Real, Julio, Esther Prat-Gil, Montserrat Pagès-Barenys, Alfonso Polo, Joan F. Piniella, and Ángel Álvarez-Larena. "Platinum phosphinothiolato hydride complexes: synthesis, structure and evaluation as tin-free hydroformylation catalysts." Dalton Transactions 45, no. 9 (2016): 3964–73. http://dx.doi.org/10.1039/c5dt04107d.

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23

Aicher, Frederik S. W., Klaus Eichele, Hartmut Schubert, and Lars Wesemann. "Complete Hydrogen Transfer: Tin Hydride Reactivity toward Adamantylisonitrile and Benzonitrile." Organometallics 37, no. 11 (May 29, 2018): 1773–80. http://dx.doi.org/10.1021/acs.organomet.8b00207.

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24

Studer, Armido, and Stephan Amrein. "ChemInform Abstract: Tin Hydride Substitutes in Reductive Radical Chain Reactions." ChemInform 33, no. 34 (May 20, 2010): no. http://dx.doi.org/10.1002/chin.200234285.

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25

CURRAN, D. P., and C. M. SEONG. "ChemInform Abstract: The Tin Hydride Reductive Decyanation of Geminal Dinitriles." ChemInform 22, no. 16 (August 23, 2010): no. http://dx.doi.org/10.1002/chin.199116122.

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26

Gastaldi, Stephane, and Didier Stien. "ChemInform Abstract: PAH-Supported Tin Hydride: A New Tin Reagent Easily Removable from Reaction Mixtures." ChemInform 33, no. 34 (May 20, 2010): no. http://dx.doi.org/10.1002/chin.200234062.

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27

Fu, Qi Jia, and Shik Chi Tsang. "Tin and tin–titanium as catalyst components for reversible hydrogen storage of sodium aluminium hydride." Fuel 85, no. 14-15 (October 2006): 2141–47. http://dx.doi.org/10.1016/j.fuel.2006.03.017.

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28

Savvakin, D. G., and D. V. Oryshych. "Evolution of Phase Composition and Microstructure upon Synthesis of Zr—Sn Alloy from Zirconium Hydride and Tin Powders." METALLOFIZIKA I NOVEISHIE TEKHNOLOGII 37, no. 4 (August 17, 2016): 559–69. http://dx.doi.org/10.15407/mfint.37.04.0559.

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29

Krull, Ira S., and Kenneth W. Panaro. "Trace Analysis and Speciation for Methylated Organotins by HPLC-Hydride Generation-Direct Current Plasma Emission Spectroscopy (HPLC-HY-DCP)." Applied Spectroscopy 39, no. 6 (November 1985): 960–68. http://dx.doi.org/10.1366/0003702854249402.

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Total tin determinations can be accomplished at trace levels (10–25 ppb) by a continuous on-line hydride generation (HY), followed by direct current plasma (DCP) emission spectroscopy (HY-DCP). This approach is applicable for organotin compounds such as mono-, di-, and trimethyltin chloride, as well as stannous and stannic cations. HY-DCP methods of total tin analysis have been applied to a number of spiked and actual samples. Detection limits, calibration plots, sensitivities, and related analytical parameters have been evaluated. Organotin analysis and speciation can be accomplished by the interfacing of this HY-DCP step with high-performance liquid chromatography (HPLC), with the use of a polymeric PRP-1 type column with an acidic, ionic mobile phase, usually containing a suitable ion-pairing reagent. The overall speciation approach, HPLC-HY-DCP, has been evaluated with regard to separation conditions; detection limits; sensitivities; calibration plots; and applications to spiked water, clam juice, seawater, and tuna fish samples. The results suggest the suitability and reliability of this HPLC-HY-DCP approach for individual tin species. Other metal species capable of forming a hydride derivative on-line, in a continuous fashion, may also be suitable for speciation by HPLC-HY-DCP.
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30

Enholm, Eric J., and Zhaozhong J. Jia. "Reactions of Tin(IV) Enolates and Radicals Derived from the Tin Hydride Scission of Cyclopropyl Ketones." Journal of Organic Chemistry 62, no. 16 (August 1997): 5248–49. http://dx.doi.org/10.1021/jo970914c.

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31

Jagielska-Wiaderek, Karina, Henryk Bala, and Tadeusz Wierzchon. "Corrosion depth profiles of nitrided titanium alloy in acidified sulphate solution." Open Chemistry 11, no. 12 (December 1, 2013): 2005–11. http://dx.doi.org/10.2478/s11532-013-0342-0.

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AbstractThick (400 µm) glow-discharge nitrided layers, TiN+Ti2N + αTi(N) type, have been produced on the Ti-1Al-1Mn titanium alloy. Using a progressive thinning method, the polarization characteristics at different depths of nitrided layers have been measured. From the plots of obtained potentiodynamic polarization curves the depth profiles of characteristic anodic and cathodic currents (at potentials corresponding to (a) hydride formation, (b) hydrogen evolution, (c) primary passivation, (d) oxygen evolution and (e) secondary passivation) as well as polarization resistance have been determined in 0.5 M Na2SO4 solution acidified to pH = 2. The anomalously high slope of the polarization curves in the cathodic region has been ascribed to the formation of titanium hydride. It has been shown that outer nitrided layers (up to 25 µm) exhibit excellent acid corrosion resistance owing to strong inhibition of the anodic process by TiN phase. Corrosion resistance of deeper situated layers gradually decreases and at depths of 250–370 µm the corrosion process is accelerated by presence of TiO2 precipitations. Nitrided layers, unlike the alloy core, allow oxygen evolution on the oxy-nitrided surface at potential of +1.6 V and at more positive potentials gradual transformation of the surfacial film into TiO2 takes place. Secondary passivation on nitrided titanium is less efficient than that in the absence of Ti-N species.
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32

Protsky, A. N., B. M. Bulychev, G. L. Soloveichik, and V. K. Belsky. "Interaction of tin methylchlorides SnMenCl4−n with molybdenum hydride bis(cyclopentadienyl)." Inorganica Chimica Acta 115, no. 2 (May 1986): 121–28. http://dx.doi.org/10.1016/s0020-1693(00)84402-3.

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33

Alvarez, George H., and Stephen G. Capar. "Determination of tin in foods by hydride generation-atomic absorption spectrometry." Analytical Chemistry 59, no. 3 (February 1987): 530–33. http://dx.doi.org/10.1021/ac00130a036.

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34

VEDEJS, E., S. M. DUNCAN, and A. R. HAIGHT. "ChemInform Abstract: An Internally Activated Tin Hydride with Enhanced Reducing Ability." ChemInform 24, no. 37 (August 20, 2010): no. http://dx.doi.org/10.1002/chin.199337130.

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35

Wiesemann, Markus, Mark Niemann, Johannes Klösener, Beate Neumann, Hans-Georg Stammler, and Berthold Hoge. "Tris(pentafluoroethyl)stannane: Tin Hydride Chemistry with an Electron-Deficient Stannane." Chemistry - A European Journal 24, no. 11 (January 30, 2018): 2699–708. http://dx.doi.org/10.1002/chem.201705068.

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36

TANAKA, H., H. SUGA, H. OGAWA, A. K. M. A. HAI, and S. TORII. "ChemInform Abstract: Electrooxidative Initiation of Tin Hydride-Promoted Radical Chain Reactions." ChemInform 24, no. 14 (August 20, 2010): no. http://dx.doi.org/10.1002/chin.199314041.

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37

Klingler, Robert J., Ira Bloom, and Jerome W. Rathke. "Thermodynamics for the addition of a tin hydride to carbon dioxide." Organometallics 4, no. 10 (October 1985): 1893–94. http://dx.doi.org/10.1021/om00129a036.

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38

Clive, Derrick L. J., and Jian Wang. "A Tin Hydride Designed To Facilitate Removal of Tin Species from Products of Stannane-Mediated Radical Reactions." Journal of Organic Chemistry 67, no. 4 (February 2002): 1192–98. http://dx.doi.org/10.1021/jo010885c.

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39

Tsuda, Taizo, Minoru Wada, Shigeru Aoki, and Yoshihiro Matsui. "Determination of Inorganic Tin in Biological Samples by Hydride Generation-Atomic Absorption Spectrometry after Silica Gel Cleanup." Journal of AOAC INTERNATIONAL 71, no. 2 (March 1, 1988): 373–74. http://dx.doi.org/10.1093/jaoac/71.2.373.

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Abstract A method is described for the determination of inorganic tin in biological samples by hydride generation-atomic absorption spectrometry (HG-AAS). A sample is extracted with ethyl acetate after addition of HC1 and NaCl. The concentrated extract is passed through a silica gel column. The column is washed with ethanol, water, and 0.2N HC1 successively, and then inorganic tin is eluted with 2N HC1 and measured by HG-AAS. Recoveries from fish muscle spiked with 0.1 ng/g Sn4+ are 78.9 ± 4.2% (average ± standard deviation, n = 5). The detection limit is 0.01 jug/g as Sn.
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40

Oh, Seung Jin, Changheui Jang, Jun Hwan Kim, and Yong Hwan Jeong. "Microstructure and hydride embrittlement of zirconium model alloys containing niobium and tin." Materials Science and Engineering: A 528, no. 10-11 (April 2011): 3771–76. http://dx.doi.org/10.1016/j.msea.2011.01.093.

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41

Nakamura, Eiichi, Daisuke Machii, and Tsuyoshi Inubushi. "Homogeneous sonochemistry in radical-chain reactions. Sonochemical hydrostannation and tin hydride reduction." Journal of the American Chemical Society 111, no. 17 (August 1989): 6849–50. http://dx.doi.org/10.1021/ja00199a059.

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42

Baillargeon, Victor P., and J. K. Stille. "Palladium-catalyzed formylation of organic halides with carbon monoxide and tin hydride." Journal of the American Chemical Society 108, no. 3 (February 1986): 452–61. http://dx.doi.org/10.1021/ja00263a015.

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43

Jana, Anukul, Herbert W. Roesky, Carola Schulzke, and Prinson P. Samuel. "Reaction of Tin(II) Hydride with Compounds Containing Aromatic C−F Bonds†." Organometallics 29, no. 21 (November 8, 2010): 4837–41. http://dx.doi.org/10.1021/om1000106.

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44

Erickson, Jeremy D., Ting Yi Lai, David J. Liptrot, Marilyn M. Olmstead, and Philip P. Power. "Catalytic dehydrocoupling of amines and boranes by an incipient tin(ii) hydride." Chemical Communications 52, no. 94 (2016): 13656–59. http://dx.doi.org/10.1039/c6cc06963k.

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{ArMe6Sn(μ-OMe)}2 (1, ArMe6 = C6H3-2,6-(C6H2-2,4,6-Me3)2) and {AriPr4Sn(μ-OMe)}2 (2, AriPr4 = C6H3-2,6-(C6H3-2,6-iPr2)2) facilitate the dehydrocoupling of ammonia, 1° and 2° amines with HBpin. 2 catalyzes the reactions faster than 1 but is limited to 1° amines. Synthesis and characterization of a tin(ii) amide and amide-hydride give insight into the catalytic mechanism.
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45

Dodero, Verónica I., Terence N. Mitchell, and Julio C. Podestá. "Synthesis and Free Radical Addition Reactions of Tris[(phenyldimethylsilyl)methyl]tin Hydride." Organometallics 22, no. 4 (February 2003): 856–60. http://dx.doi.org/10.1021/om020936b.

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46

Yokoi, Katuhiko, Mieko Kimura, Hideo Hirakata, Yoshimichi Someya, Kenji Sekine, and Yoshinori Itokawa. "Determination of tin in urine by gaseous hydride generation-atomic absorption spectrophotometry." Nippon Eiseigaku Zasshi (Japanese Journal of Hygiene) 42, no. 4 (1987): 881–86. http://dx.doi.org/10.1265/jjh.42.881.

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47

Blanton, James R., and Joseph M. Salley. "Reducing alkyl halides using a polymer-bound crown ether/tin hydride cocatalyst." Journal of Organic Chemistry 56, no. 2 (January 1991): 490–91. http://dx.doi.org/10.1021/jo00002a004.

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48

ENHOLM, E. J., and Z. J. JIA. "ChemInform Abstract: Reactions of Tin(IV) Enolates and Radicals Derived from the Tin Hydride Scission of Cyclopropyl Ketones." ChemInform 28, no. 51 (August 2, 2010): no. http://dx.doi.org/10.1002/chin.199751087.

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49

Morris, Louis J., Nasir A. Rajabi, Mary F. Mahon, Ian Manners, Claire L. McMullin, and Michael S. Hill. "Synthesis and reactivity of alkaline-earth stannanide complexes by hydride-mediated distannane metathesis and organostannane dehydrogenation." Dalton Transactions 49, no. 30 (2020): 10523–34. http://dx.doi.org/10.1039/d0dt02406f.

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50

Mercier, Cédric, Raphaël Schneider, Patrick Willmann, and Denis Billaud. "Influence of the C/Sn Ratio on the Synthesis and Lithium Electrochemical Insertion of Tin-Supported Graphite Materials Used as Anodes for Li-Ion Batteries." International Journal of Electrochemistry 2011 (2011): 1–8. http://dx.doi.org/10.4061/2011/381960.

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Abstract:
Novel composites consisting of tin particles associated to graphite were prepared by chemical reduction of tin(+2) chloride byt-BuONa-activated sodium hydride in the presence of graphite. The samples obtained using various C/Sn ratios were investigated by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), and elemental analyses. The largest tin particles associated to graphite layers were observed for the material with a C/Sn ratio of 16. For the materials with C/Sn ratios of 42 and 24, SEM and TEM experiments demonstrated that Sn aggregates of ca. 250 nm length and composed of Sn particles with an average diameter of ca. 50 nm were homogeneously distributed at the surface of graphite. Electrodes prepared from theC/Sn=42material exhibit a high reversible capacity of over 470 mAhg−1up to twenty cycles with stable cyclic performances.
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