Academic literature on the topic 'Temperature-modulated DSC'

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Journal articles on the topic "Temperature-modulated DSC"

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Mesquida, Patrick, Andrä le Coutre, and Jan K. Krüger. "Temperature modulated DSC at intermediate-low temperatures." Thermochimica Acta 330, no. 1-2 (May 1999): 137–44. http://dx.doi.org/10.1016/s0040-6031(99)00028-3.

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Fraga, Iria, S. Montserrat, and J. M. Hutchinson. "TOPEM, a new temperature modulated DSC technique." Journal of Thermal Analysis and Calorimetry 87, no. 1 (January 2007): 119–24. http://dx.doi.org/10.1007/s10973-006-7969-4.

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Schawe, J. E. K., T. Hütter, C. Heitz, I. Alig, and D. Lellinger. "Stochastic temperature modulation: A new technique in temperature-modulated DSC." Thermochimica Acta 446, no. 1-2 (July 2006): 147–55. http://dx.doi.org/10.1016/j.tca.2006.01.031.

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Kanari, Katsuhiko, and Takeo Ozawa. "Simulation of temperature modulated DSC of temperature dependent heat capacity." Thermochimica Acta 304-305 (November 1997): 201–7. http://dx.doi.org/10.1016/s0040-6031(97)00173-1.

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Chen, W. "Study of crystallization kinetics by temperature-modulated DSC." Polymer 41, no. 11 (May 2000): 4119–25. http://dx.doi.org/10.1016/s0032-3861(99)00621-7.

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Righetti, Maria. "Crystallization of Polymers Investigated by Temperature-Modulated DSC." Materials 10, no. 4 (April 24, 2017): 442. http://dx.doi.org/10.3390/ma10040442.

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Boller, A., I. Okazaki, K. Ishikiriyama, G. Zhang, and B. Wunderlich. "Determination of cell asymmetry in temperature-modulated DSC." Journal of thermal analysis 49, no. 2 (August 1997): 1081–88. http://dx.doi.org/10.1007/bf01996796.

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MENG, F., S. SCHRICKER, W. BRANTLEY, D. MENDEL, R. RASHID, H. FIELDSJR, K. VIG, and S. ALAPATI. "Differential scanning calorimetry (DSC) and temperature-modulated DSC study of three mouthguard materials☆." Dental Materials 23, no. 12 (December 2007): 1492–99. http://dx.doi.org/10.1016/j.dental.2007.01.006.

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Kotera, M., T. Nishino, and K. Nakamae. "Imidization processes of aromatic polyimide by temperature modulated DSC." Polymer 41, no. 10 (May 2000): 3615–19. http://dx.doi.org/10.1016/s0032-3861(99)00546-7.

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Boller, A., Y. Jin, and B. Wunderlich. "Heat capacity measurement by modulated DSC at constant temperature." Journal of Thermal Analysis 42, no. 2-3 (August 1994): 307–30. http://dx.doi.org/10.1007/bf02548519.

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Dissertations / Theses on the topic "Temperature-modulated DSC"

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Chen, Lu Guang, and s3064076@student rmit edu au. "Thermo-Optical Properties of Polymer Dispersed Liquid Crystals." RMIT University. Applied Science, 2007. http://adt.lib.rmit.edu.au/adt/public/adt-VIT20080206.114823.

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Abstract:
Polymer dispersed liquid crystal (PDLC) films, consisting of micro-sized domains of a liquid crystal dispersing in a polymer matrix, serve as the basis of a variety of high-efficiency electro-optical effects. The thermo-optical properties of the PDLCs were investigated in this thesis. The thermal properties and the morphologies of four low molar mass mesogens were studied by DSC and polarized optical microscope (POM). There were significant super cooling/heating effects on the first order phase transitions but not on the mesophase transitions. The structural effects on the transition temperature were investigated. Between the two 4-alkoxybenzoic acids mesogens, the clearing temperature of 4-(octyloxy)benzoic acid was higher than 4-(decyloxy)benzoic acid because of the increasing chain length. Trans-4-methoxycinnamic acid had the highest melting temperature among the four mesogens despite the molar mass because the carboxylic acid termini of trans-4-methoxycinnamic acid gave rise to strong intermolecular attractions. The smectic phases of 4-(octyloxy)benzoic acid were classified as head-to-head bilayer orientational smectic structures, SmA2 and SmC2, respectively, by wide angle X-ray diffraction through measuring the d spacing of the liquid crystal. The total solubility parameter was used to evaluate matching a polymer-LC-solvent combination. PDLC films were prepared by the solvent induced phase separation method and suitable morphologies were achieved by thermal induced phase separation. The phase transition temperatures of PDLCs were shifted to a lower temperature due to the polymer dispersion effects. Different mesophases were observed in PDLC films when LC exhibited different mesophases. The LC fractions in the droplets were calculated from the nematic to isotropic enthalpies through the Smith equation. Two factors, thermal cooling rate and the LC concentration, which affect the size of the droplet dispersed in the polymer matrix, were investigated in the PVC dispersed 4,4'-azoxyanisole. The phase transitions of pHEMA dispersed 4-(octyloxy)benzoic acid and PVC dispersed 4,4'-azoxyanisole were investigated by TMDSC and quasi-isothermal TMDSC. The TMDSC results were analysed by the two approaches, reversing and non-reversing heat flow and complex heat capacity. The results of the phase transitions of the two PDLCs illustrated that in the PDLCs it involved both non-reversing, melting, and reversing, clearing and the transition between two mesophases. In the non-reversing transition, the transition temperature would be affected by super cooling/heating and the results obtained in the experiments were dependent on the experimental conditions, such as the heating or cooling rate, sample size and purge gas flow rate. However, in the reversing transition process, there were no super cooling/heating effects observed and it seemed that the experimental conditions were not so critical. Results could be monitored by Lissajous figures obtained from the quasi-isothermal TMDSC. The plots of modulated heat flow versus the derivative of modulated temperature can be used to alert to unfavorable experimental conditions where loss of system linearity could be seen.
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Book chapters on the topic "Temperature-modulated DSC"

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Wagner, Matthias. "Temperature-Modulated DSC." In Thermal Analysis in Practice, 287–98. München: Carl Hanser Verlag GmbH & Co. KG, 2017. http://dx.doi.org/10.3139/9781569906446.016.

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Ebeid, El-Zeiny M., and Mohamed B. Zakaria. "Temperature-modulated DSC (TMDSC)." In Thermal Analysis, 41–128. Elsevier, 2021. http://dx.doi.org/10.1016/b978-0-323-90191-8.00005-1.

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Conference papers on the topic "Temperature-modulated DSC"

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Matsuda, Yu, Yasuteru Fukawa, Mitsuru Kawashima, Seiji Kojima, Michio Tokuyama, Irwin Oppenheim, and Hideya Nishiyama. "Fragility Variation of Lithium Borate Glasses Studied by Temperature-Modulated DSC." In COMPLEX SYSTEMS: 5th International Workshop on Complex Systems. AIP, 2008. http://dx.doi.org/10.1063/1.2897785.

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Paniez, Patrick J., S. Brun, and S. Derrough. "Modulated-temperature DSC (MT-DSC): a new technique for the extensive thermal characterization of complex chemically amplified systems." In Microlithography '97, edited by Regine G. Tarascon-Auriol. SPIE, 1997. http://dx.doi.org/10.1117/12.275816.

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