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Journal articles on the topic 'Synthesis of organometallics'

Author: Grafiati

Published: 4 June 2021

Last updated: 15 February 2022

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1

Nelson, John H. "Organometallics in Synthesis." Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry 26, no. 10 (November 1996): 1767–68. http://dx.doi.org/10.1080/00945719608004407.

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2

Whitby, Richard J. "Organometallics in Synthesis." Synthesis 1995, no. 06 (June 1995): 727–28. http://dx.doi.org/10.1055/s-1995-3962.

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3

Khalid, Maher, and Shireen Mohammedand Amin Kalo. "Recent Developments in Weinreb Synthesis and Their Applications." Oriental Journal of Chemistry 35, no. 6 (December 23, 2019): 1611–26. http://dx.doi.org/10.13005/ojc/350601.

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N-methoxy-N-methyl amides or Weinreb amides are worthy embranchment of amide group and their rich functional groups in organic synthesis become a strong else unfeasible conversion. Weinreb amides are produced as an intermediate product of the reaction of carboxylic acids, acid chloride or esters with organometallic reagents, which was first uncovered in 1981. The direct conversion of carboxylic acids or acid chlorides or esters to ketones or aldehydes using organometallic reagents do not lead in high yields, because the intermediate ketones are still highly reactive toward the organometallic reagent. However, after derivatization to the corresponding Weinreb Amide, reaction with organometallics does give the desired ketones, as the initial adduct is stabilized and doesn't undergo further reactions. A nucleophilic addition to the Weinreb amides results in a unique and stable five-membered cyclic tetrahedral intermediate which protects the over-addition, leading to a selective conversion.

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4

Marlett, E. M. "ELECTROCHEMICAL SYNTHESIS OF ORGANOMETALLICS." Annals of the New York Academy of Sciences 125, no. 1 (December 16, 2006): 12–24. http://dx.doi.org/10.1111/j.1749-6632.1965.tb45375.x.

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5

Seyferth, Dietmar. "Organometallics in Organic Synthesis." Organometallics 7, no. 5 (May 1, 1988): 1236. http://dx.doi.org/10.1021/om00095a603.

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6

Chaloner, Penny A. "Organometallics in organic synthesis." Journal of Organometallic Chemistry 348, no. 3 (July 1988): C45. http://dx.doi.org/10.1016/0022-328x(88)80427-3.

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7

Hanson, J. R. "Organic synthesis via organometallics." Journal of Organometallic Chemistry 426, no. 2 (March 1992): C49. http://dx.doi.org/10.1016/0022-328x(92)83056-n.

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8

Hanson, J. R. "Organic synthesis via organometallics." Journal of Organometallic Chemistry 484, no. 1-2 (December 1994): c13. http://dx.doi.org/10.1016/0022-328x(94)87214-7.

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9

Burton, Donald J., and Zhen-Yu Yang. "Fluorinated organometallics: Perfluoroalkyl and functionalized perfluoroalkyl organometallic reagents in organic synthesis." Tetrahedron 48, no. 2 (1992): 189–275. http://dx.doi.org/10.1016/s0040-4020(01)88139-4.

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10

de Meijere, Armin. "Organometallics in Organic Synthesis: Introduction." Chemical Reviews 100, no. 8 (August 2000): 2739–40. http://dx.doi.org/10.1021/cr000424b.

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11

Simon, Cotton. "Organometallics in organic synthesis 2." Polyhedron 10, no. 17 (January 1991): 2084. http://dx.doi.org/10.1016/s0277-5387(00)86039-8.

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12

Wills, Martin. "Main group organometallics in synthesis." Contemporary Organic Synthesis 1, no. 5 (1994): 339. http://dx.doi.org/10.1039/co9940100339.

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13

Wills, Martin. "Main group organometallics in synthesis." Contemporary Organic Synthesis 3, no. 3 (1996): 201. http://dx.doi.org/10.1039/co9960300201.

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14

Coldham, Iain. "Main group organometallics in synthesis." Contemporary Organic Synthesis 4, no. 2 (1997): 136. http://dx.doi.org/10.1039/co9970400136.

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15

DANKS, T. N., S. E. THOMAS, and T. GALLAGHER. "ChemInform Abstract: Organometallics in Synthesis." ChemInform 22, no. 25 (August 23, 2010): no. http://dx.doi.org/10.1002/chin.199125276.

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16

Coldham, Iain. "Main group organometallics in synthesis." Journal of the Chemical Society, Perkin Transactions 1, no. 7 (1998): 1343–64. http://dx.doi.org/10.1039/a706956a.

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17

Chaloner, Penny A. "Organometallics in Organic Synthesis 2." Journal of Organometallic Chemistry 395, no. 3 (October 1990): C53—C54. http://dx.doi.org/10.1016/0022-328x(90)85303-g.

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18

Eaborn, Colin. "Organometallics in synthesis: A manual." Journal of Organometallic Chemistry 490, no. 1-2 (March 1995): C38. http://dx.doi.org/10.1016/0022-328x(95)90301-t.

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19

Besenyei, Gábor. "Organometallics in synthesis; a manual." Reaction Kinetics and Catalysis Letters 63, no. 2 (March 1998): 409–11. http://dx.doi.org/10.1007/bf02475420.

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20

Kotha, Sambasivarao, and Milind Meshram. "Application of organometallics in organic synthesis." Journal of Organometallic Chemistry 874 (November 2018): 13–25. http://dx.doi.org/10.1016/j.jorganchem.2018.08.008.

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21

Nicholas, Kenneth M. "Transition Metal Organometallics in Organic Synthesis." Tetrahedron 56, no. 15 (April 2000): ix. http://dx.doi.org/10.1016/s0040-4020(99)01087-x.

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22

Davies, Paul W. "Organometallics: transition metals in organic synthesis." Annual Reports Section "B" (Organic Chemistry) 105 (2009): 93. http://dx.doi.org/10.1039/b822044c.

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23

Davies, Paul W. "Organometallics: transition metals in organic synthesis." Annual Reports Section "B" (Organic Chemistry) 104 (2008): 68. http://dx.doi.org/10.1039/b716606k.

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24

Afarinkia, Kamyar. "Main group organometallics in organic synthesis." Journal of the Chemical Society, Perkin Transactions 1, no. 15 (1999): 2025–46. http://dx.doi.org/10.1039/a802867b.

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25

Ghosez, L. "Stereoselective synthesis with and without organometallics." Pure and Applied Chemistry 68, no. 1 (January 1, 1996): 15–22. http://dx.doi.org/10.1351/pac199668010015.

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26

Davies, Paul W. "Organometallics: transition metals in organic synthesis." Annual Reports Section "B" (Organic Chemistry) 106 (2010): 98. http://dx.doi.org/10.1039/b927091b.

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27

BURTON, D. J., and Z. Y. YANG. "ChemInform Abstract: Fluorinated Organometallics: Perfluoroalkyl and Functionalized Perfluoroalkyl Organometallic Reagents in Organic Synthesis." ChemInform 23, no. 17 (August 22, 2010): no. http://dx.doi.org/10.1002/chin.199217330.

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28

Vasu, Dhananjayan, Angel L. Fuentes de Arriba, Jamie A. Leitch, Antoine de Gombert, and Darren J. Dixon. "Primary α-tertiary amine synthesis via α-C–H functionalization." Chemical Science 10, no. 11 (2019): 3401–7. http://dx.doi.org/10.1039/c8sc05164j.

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29

Mendoza, Abraham, and Kilian Colas. "Iterative Synthesis of Pluripotent Thioethers through Controlled Redox Fluctuation of Sulfur." Synlett 29, no. 10 (January 29, 2018): 1329–33. http://dx.doi.org/10.1055/s-0036-1591864.

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Target- and diversity-oriented syntheses are based on diverse building blocks, whose preparation requires discrete design and constructive alignment of different chemistries. To enable future automation of the synthesis of small molecules, we have devised a unified strategy that serves the divergent synthesis of unrelated scaffolds such as carbonyls, olefins, organometallics, halides, and boronic esters. It is based on iterations of a nonelectrophilic Pummerer-type C–C coupling enabled by turbo-organomagnesium amides that we have recently reported. The pluripotency of sulfur allows the central building blocks to be obtained by regulating C–C bond formation through control of its redox state.

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30

Knochel, Paul, Eike Hupe, Wolfgang Dohle, David M. Lindsay, Véronique Bonnet, Guy Quéguiner, Andreas Boudier, et al. "Functionalized main-group organometallics for organic synthesis." Pure and Applied Chemistry 74, no. 1 (January 1, 2002): 11–17. http://dx.doi.org/10.1351/pac200274010011.

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Highly functionalized Grignard-reagents can be easily obtained by an iodinemagnesim exchange reaction and further reacted with various electrophiles. Via a BZn exchange reaction, a formal Michael addition with umpolung of the reactivity can be achieved. Chiral phosphine ligands can be easily synthesized by a 2.3 sigmatropic rearrangement and used successfully in asymmetric synthesis.

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31

Mohamed, Ahmed A., Sabine N. Neal, Baraa Atallah, Nemat D. AlBab, Hussain A. Alawadhi, Yasmin Pajouhafsar, Hanan E. Abdou, et al. "Synthesis of gold organometallics at the nanoscale." Journal of Organometallic Chemistry 877 (December 2018): 1–11. http://dx.doi.org/10.1016/j.jorganchem.2018.07.032.

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32

Kollonitsch, J. "INDUSTRIAL USE OF ORGANOMETALLICS IN ORGANIC SYNTHESIS." Annals of the New York Academy of Sciences 125, no. 1 (December 16, 2006): 161–71. http://dx.doi.org/10.1111/j.1749-6632.1965.tb45387.x.

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33

COLDHAM, I. "ChemInform Abstract: Main Group Organometallics in Synthesis." ChemInform 28, no. 31 (August 3, 2010): no. http://dx.doi.org/10.1002/chin.199731238.

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34

COLDHAM, I. "ChemInform Abstract: Main Group Organometallics in Synthesis." ChemInform 29, no. 35 (June 20, 2010): no. http://dx.doi.org/10.1002/chin.199835315.

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35

WILLS, M. "ChemInform Abstract: Main Group Organometallics in Synthesis." ChemInform 26, no. 20 (August 18, 2010): no. http://dx.doi.org/10.1002/chin.199520271.

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36

Suijkerbuijk, Bart M J. M., and Robertus J M. Klein Gebbink. "Merging Porphyrins with Organometallics: Synthesis and Applications." Angewandte Chemie International Edition 47, no. 39 (September 15, 2008): 7396–421. http://dx.doi.org/10.1002/anie.200703362.

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37

Elumalai, Palani, Yong Joon Jeong, Dae Won Park, Dong Hwan Kim, Hyunuk Kim, Se Chan Kang, and Ki-Whan Chi. "Antitumor and biological investigation of doubly cyclometalated ruthenium(ii) organometallics derived from benzimidazolyl derivatives." Dalton Transactions 45, no. 15 (2016): 6667–73. http://dx.doi.org/10.1039/c5dt04400f.

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In this study, we report the synthesis, anticancer and biological properties of three doubly cyclometalated phenylbenzimidazole derived ruthenium(ii) organometallics (1–3) and their corresponding three organic ligands.

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38

Palchykov, Vitalii, Peter C. Dale, and Jeremy Robertson. "Nucleophilic vinylic substitution in bicyclic methyleneaziridines: SNVπ or SNVσ?" New Journal of Chemistry 45, no. 20 (2021): 9020–25. http://dx.doi.org/10.1039/d1nj01458g.

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A stereoselective synthesis of the monodeuterated methyleneaziridine shown allowed the stereochemical course of formal S_NV-mode ring-opening with copper-based organometallics to be assigned.

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39

Princival, Jefferson L., Alcindo A. Dos Santos, and João V. Comasseto. "Reactive organometallics from organotellurides: application in organic synthesis." Journal of the Brazilian Chemical Society 21, no. 11 (2010): 2042–54. http://dx.doi.org/10.1590/s0103-50532010001100005.

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40

Schmidlehner, Melanie, Paul-Steffen Kuhn, Carmen M. Hackl, Alexander Roller, Wolfgang Kandioller, and Bernhard K. Keppler. "Microwave-assisted synthesis of N-heterocycle-based organometallics." Journal of Organometallic Chemistry 772-773 (December 2014): 93–99. http://dx.doi.org/10.1016/j.jorganchem.2014.08.013.

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41

Davies, Paul W. "ChemInform Abstract: Organometallics: Transition Metals in Organic Synthesis." ChemInform 42, no. 18 (April 7, 2011): no. http://dx.doi.org/10.1002/chin.201118199.

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42

GIESE, B. "ChemInform Abstract: Organometallics in Organic Synthesis via Radicals." ChemInform 25, no. 31 (August 19, 2010): no. http://dx.doi.org/10.1002/chin.199431311.

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43

Afarinkia, Kamyar. "ChemInform Abstract: Main Group Organometallics in Organic Synthesis." ChemInform 30, no. 44 (June 13, 2010): no. http://dx.doi.org/10.1002/chin.199944317.

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44

Schulz, Stephan. "Low-Valent Organometallics-Synthesis, Reactivity, and Potential Applications." Chemistry - A European Journal 16, no. 22 (May 19, 2010): 6416–28. http://dx.doi.org/10.1002/chem.201000580.

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45

RICHARDS, C. J., S. E. THOMAS, and M. WILLS. "ChemInform Abstract: Organometallics in Synthesis. The Transition Elements." ChemInform 23, no. 32 (August 21, 2010): no. http://dx.doi.org/10.1002/chin.199232263.

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46

WILLS, M. "ChemInform Abstract: Organometallics in Synthesis. Main Group Elements." ChemInform 23, no. 32 (August 21, 2010): no. http://dx.doi.org/10.1002/chin.199232264.

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47

Kremsmair, Alexander, Johannes H. Harenberg, Kuno Schwärzer, Andreas Hess, and Paul Knochel. "Preparation and reactions of polyfunctional magnesium and zinc organometallics in organic synthesis." Chemical Science 12, no. 17 (2021): 6011–19. http://dx.doi.org/10.1039/d1sc00685a.

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Polyfunctional Mg and Zn organometallics can be prepared from organic halides by metal insertions, halogen/metal-exchanges or metalations with TMP-bases. These intermediates can be used in new cross-couplings, aminations or continuous flow set-ups.

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48

Shu, Xing-Zhong, Feng-Feng Pan, Peng Guo, and Xiaochuang Huang. "Synthesis of Dibenzyls by Nickel-Catalyzed Homocoupling of Benzyl Alcohols." Synthesis 53, no. 17 (March 25, 2021): 3094–100. http://dx.doi.org/10.1055/a-1467-2432.

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AbstractDibenzyls are essential building blocks that are widely used in organic synthesis, and they are typically prepared by the homocoupling of halides, organometallics, and ethers. Herein, we report an approach to this class of compounds using alcohols, which are more stable and readily available. The reaction proceeds via nickel-catalyzed and dimethyl oxalate assisted dynamic kinetic homocoupling of benzyl alcohols. Both primary and secondary alcohols are tolerated.

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49

Gonsalves, Kenneth E., He Li, R. Perez, P. Santiago, and M. Jose-Yacaman. "Synthesis of nanostructured metals and metal alloys from organometallics." Coordination Chemistry Reviews 206-207 (September 2000): 607–30. http://dx.doi.org/10.1016/s0010-8545(00)00301-5.

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50

Knochel, Paul, Eike Hupe, Wolfgang Dohle, David M. Lindsay, Veronique Bonnet, Guy Queguiner, Andreas Boudier, et al. "ChemInform Abstract: Functionalized Main-Group Organometallics for Organic Synthesis." ChemInform 33, no. 43 (May 19, 2010): no. http://dx.doi.org/10.1002/chin.200243290.

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