Relevant bibliographies by topics / Synthesis of nitrosyl compound

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Academic literature on the topic 'Synthesis of nitrosyl compound'

Author: Grafiati
Published: 4 June 2021
Last updated: 10 February 2022

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Journal articles on the topic "Synthesis of nitrosyl compound"

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De Vries, Nadine, Jessica Cook, Alan Davison, Terrence Nicholson, and Alun G. Jones. "Synthesis and characterization of a technetium(III) nitrosyl compound: Tc(NO)(Cl)(SC10H13)3." Inorganic Chemistry 29, no. 5 (March 1990): 1062–64. http://dx.doi.org/10.1021/ic00330a030.

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Legzdins, Peter, Kevin M. Smith, and Steven J. Rettig. "Synthesis, characterization, and properties of some cyclopentadienyl molybdenum nitrosyl benzyl complexes." Canadian Journal of Chemistry 79, no. 5-6 (May 1, 2001): 502–9. http://dx.doi.org/10.1139/v00-158.

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Reaction of CpMo(NO)(CH2Ph)Cl with Me2Mg, Ph2Mg, or PhCCLi reagents in THF affords the corresponding alkyl, aryl, or alkynyl CpMo(NO)(CH2Ph)R (R = hydrocarbyl) complexes as orange powders in good yields. Unlike related 16-electron CpMo(NO)R2 complexes, these 18-electron species exhibit good thermal stability due to their η2-benzyl-Mo interactions. Treatment of CpMo(NO)(CH2Ph)Cl with Na(DME)Cp provides dark green Cp2Mo(NO)(CH2Ph), whose solid-state molecular structure has been established by a single-crystal X-ray crystallographic analysis. The two Cp rings display different binding modes to the Mo atom, while the benzyl ligand is coordinated to the metal centre in an η1 fashion. The triflate complex, CpMo(NO)(CH2Ph)(OTf), is obtained by addition of AgOTf to the benzyl chloride precursor. The covalent Mo—OTf bond in this compound can be disrupted by the addition of Lewis bases (L) such as PPh3 or pyridine, leading to the corresponding [CpMo(NO)(CH2Ph)(L)][OTf] salts. Attempts to generate neutral benzylidene complexes by deprotonation of [CpMo(NO)(CH2Ph)(PPh3)][OTf] have not yet been successful.Key words: nitrosyl, molybdenum, benzyl, hydrocarbyl, triflate.
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Vogel, Sabine, Gottfried Huttner, Laszlo Zsolnai, and Christiane Emmerich. "H2NNH- und H2NO- als η2-koordinierte Liganden in Tripod-Cobalt-Komplexen / H2NNH- and H2NO- as η2-Coordinated Ligands in Tripod Cobalt Complexes." Zeitschrift für Naturforschung B 48, no. 3 (March 1, 1993): 353–63. http://dx.doi.org/10.1515/znb-1993-0315.

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The complex cation [tripod Co η2-(NH2O)]+, 2, (tripod = CH3C(CH2PPh2)3) containing an η2-coordinated NH2O−-ligand is an isoelectronic equivalent to the recently reported complex [tripod Co η2-(Ν2Η3)]+, 1, which contains side-on coordinated N2H3− [1,4]. The structures of the two cations 1 and 2 are almost superimposable.The structural discrimination between the NH2- and O- parts of the η2-NH2O--ligand in 2 has been corroborated by the synthesis and X-ray analysis of the cations [tripod Co η2-(NMe2O)]+, 3, and [tripod Co Cl (NH2OMe)]+, 4. The hydroxylamido(1–) compound 2 upon treatment with air transforms into the nitrosyl compound [tripod Co (NO)], 5, the structure of which has also been determined.
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Balasekaran, S. M., A. Hagenbach, M. Drees, and U. Abram. "[TcII(NO)(trifluoroacetate)4F]2−– synthesis and reactions." Dalton Trans. 46, no. 39 (2017): 13544–52. http://dx.doi.org/10.1039/c7dt03084c.

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Cs(NBu4)[Tc(NO)(OOCCF3)4F] can act as a precursor for the synthesis of further Tc(ii) and Tc(i) nitrosyl complexes with trifluoroacetato or fluorido ligands. The Tc(i) compounds show unusual99Tc NMR chemical shifts.
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Pratihar, Pampa, Anup Kumar Dasmahapatra, and Chittaranjan Sinha. "Arylazoimidazole compounds of rhenium nitrosyl: Synthesis, spectral characterization and reactivity." Polyhedron 26, no. 6 (April 2007): 1217–21. http://dx.doi.org/10.1016/j.poly.2006.10.029.

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Klimochkin, Yuri, Ilya Tkachenko, and Victor Rybakov. "Convenient Synthesis of Ethyl 5-Oxohomoadamantane-4-carboxylate: A Useful Precursor of Polyfunctional Homoadamantanes." Synthesis 51, no. 06 (November 8, 2018): 1482–90. http://dx.doi.org/10.1055/s-0037-1610312.

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A facile and convenient synthesis of ethyl 5-oxohomoadamantane-4-carboxylate is reported, and its chemical properties as a cage analogue of acetoacetic ester are investigated. Various derivatives of homoadamantane were synthesized through the reaction of 5-oxohomoadamantane-4-carboxylate with electrophilic agents, binucleophiles, and hydrazoic acid. Some new unusual products were obtained by the reaction of that β-keto ester with nitric acid and nitrosyl chloride. Cage compounds synthesized could be used as precursors for the diverse condensed heterocyclic compounds with potential viral ion channel abrogating activity that possess conformationally rigid lipophilic moieties.
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Keerthi Kumar, Chinnagiri T., Jathi Keshavayya, Tantry N. Rajesh, Sanehalli K. Peethambar, and Angadi R. Shoukat Ali. "Synthesis, Characterization, and Biological Activity of 5-Phenyl-1,3,4-thiadiazole-2-amine Incorporated Azo Dye Derivatives." Organic Chemistry International 2013 (August 18, 2013): 1–7. http://dx.doi.org/10.1155/2013/370626.

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5-Phenyl-1,3,4-thiadiazole-2-amine has been synthesized by single step reaction. A series of heterocyclic azodyes were synthesized by diazotisation of 5-phenyl-1,3,4-thiadiazole-2-amine by nitrosyl sulphuric acid followed by coupling with different coupling compounds such as 8-hydroxyquinoline, 2,6-diaminopyridine, 2-naphthol, N,N-dimethyl aniline, resorcinol, and 4,6-dihydroxypyrimidine. The dyes were characterized by UV-Vis, IR, 1H-NMR, 13C NMR, and elemental analysis. The synthesized compounds were also screened for biological activity.
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Vassilyeva, O., E. Buvaylo, and B. Skelton. "DIRECT SYNTHESIS AND CRYSTAL STRUCTURE OF BIS(BROMIDO-BIS(1,10 PHENANTHROLINE)-COPPER(II)) NITROPRUSSIDE DIMETHYLFORMAMIDE SOLVATE." Bulletin of Taras Shevchenko National University of Kyiv. Chemistry, no. 1(55) (2018): 15–18. http://dx.doi.org/10.17721/1728-2209.2018.1(55).3.

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The title compound, [Cu(C12H8N2)2Br]2[Fe(CN)5(NO)]·C3H7NO, was prepared by the self-assembly of nitroprusside anion and Cu cation containing a bidentate amine in the reaction of copper powder and sodium nitroprusside with NH4Br and 1,10-phenanthroline (phen) in dimethylformamide (DMF). The complex is formed of discrete [Cu(phen)2Br]+ cations, nitroprusside [Fe(CN)5(NO)]2– anions and DMF molecules of crystallization. The cation has no crystallographically imposed symmetry; the metal atom coordinates two nitrogen atoms of two phen molecules and bromide ion. The copper coordination geometry is intermediate between a square pyramid and a trigonal bipyramid. The [Fe(CN)5(NO)]2– anion is located on an inversion centre with the nitrosyl group modelled as disordered with one of the CN groups. The DMF solvent molecule was found to be disordered about the crystallographic inversion centre; geometries were restrained to ideal values. In the solid state, alternating layers of cations and of anions plus DMF molecules are stacked along the b axis.
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Vogler, Stefan, Kurt Dehnicke, and Dieter Fenske. "[Na-15-Krone-5] [ReF2Cl2(NO)2]; Synthese, IR-Spektrum und Kristallstruktur / [Na-15-Crown-5][ReF2Cl2(NO)2]; Synthesis, IR Spectrum, and Crystal Structure." Zeitschrift für Naturforschung B 44, no. 11 (November 1, 1989): 1393–96. http://dx.doi.org/10.1515/znb-1989-1112.

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[Na-15-crown-5][ReF2Cl2(NO)2] has been prepared by the reaction of ReCl3(NO)2 with sodium fluoride in acetonitrile suspension in the presence of 15-crown-5. It forms green, slightly moisture sensitive crystals, which were characterized by IR spectroscopy as well as by an X-ray structure determination. Space group P21/c, Z = 4, 4821 observed unique reflexions, R = 0.040. Lattice dimensions at —60 °C: a = 1024.6(7), b = 801.4(4), c = 2386.6(12) pm; β = 99.90(4)°. The compound forms ion pairs via two Na—F contacts with bond lengths of 239.8 and 233.4 pm. Thus the sodium ion is seven-coordinate by the five oxygen atoms of the crown ether molecule and by two fluorine ligands of the [ReF2Cl2(NO)2]- unit. The nitrosyl groups of the anion are in transposition to the fluorine atoms and in cis-position to one another (symmetry C2v).
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Smékal, Zdeněk, Jiří Kameníček, Ingrid Svoboda, and Albert Escuer. "Synthesis, Crystal Structure and Magnetic Properties of Novel Complex [μ-(NC)-Fe(CN)3(NO)-μ-(CN)-Cu(ept)]n·4nH2O (ept = N-(2-Aminoethyl)propane-1,3-diamine)." Collection of Czechoslovak Chemical Communications 66, no. 10 (2001): 1490–98. http://dx.doi.org/10.1135/cccc20011490.

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The novel complex [μ-(NC)-Fe(CN)3(NO)-μ-(CN)-Cu(ept)]n·4nH2O (ept = N-(2-aminoethyl)- propane-1,3-diamine) was obtained by the reaction of Cu(ClO4)2·6H2O with N-(2-amino- ethyl)propane-1,3-diamine and Na2[Fe(CN)5NO]·2H2O in water. This compound was characterized by IR, UV-VIS and EPR spectroscopies and magnetic measurement. Single-crystal X-ray structure analysis revealed that the title complex has a one-dimensional polymeric structure containing hexacoordinate iron(II) with five cyanide ligands (two of them, in trans position, bridging) and one nitrosyl group, and pentacoordinate copper(II) with N-(2-aminoethyl)propane-1,3-diamine and two sites occupied by bridging cyanide ligands. Magnetic investigation revealed a very weak antiferromagnetic interaction between the copper atoms (superexchange interaction parameter J = -1.7(1) cm-1; H = -JSiSi+1) within the chain through the diamagnetic [Fe(CN)5NO]2- ions.
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Dissertations / Theses on the topic "Synthesis of nitrosyl compound"

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Sherman, D. J. "Studies on some platinum metal compounds." Thesis, University of Oxford, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.382671.

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Lambert, Ronald J. W. "The bonding, synthesis and electrochemistry of some iron-sulphur-nitrosyl compounds." Thesis, University of St Andrews, 1990. http://hdl.handle.net/10023/14972.

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Salts of the bls(μ-thiosulphato-S)-bis(dinitrosylferrate)(2-) anion, [Fe2(S2o3)2(NO)4]2- can be prepared by the reaction of iron(ll)/thiosulphate mixtures with nitrite ion. The crystal structure of {(Ph3P)2N}2[ Fe2(S203)2(NO)4] reveals it to adopt a trans structure. 15N n.m.r. studies of this salt also show it to adopt the trans structure in solution. The anion reacts with thiolate ion, RS-, to provide good yields of Fe2(SR)2(NO)4; e.p.r. studies show the mononitrosyl [Fe(N0)(SR)3]3− to be a major intermediate in this reaction. Salts of the Black Roussin ion, [Fe4S3(NO)7]- react with aryldiazonium salts, ArN2+ , to produce Fe2(SAr)2(NO)4. 13C n.m.r. studies of Fe2(SC6H4F)2(NO)4 reveal it to exist in a 1:1 ratio of cis and trans isomers. Reaction of the Black anion with trialkylsulphonium or sulphoxonium salts leads to the metathesis product. The crystal structure of Me3S[Fe4S3(NO)7] shows no evidence for the closure of the iron-sulphur cage by the sulphur of the Me3S cation. Reaction of the Black anion with trialkyloxonium salts provides good yields of Fe2(SR)2(NO)4. Electrochemical studies on Fe2(SR)2(NO)4 by conventional cyclic voltammetry shows two chemically and electrochemically reversible one electron reductions to produce [Fe2(SR)2(NO)4]− and [Fe2(SR)2(NO)4]2−. The monoanion is a paramagnetic complex with g= 1.995; coupling to four equivalent nitrogens shows the presence of a delocalised electron. The electrochemical behaviour of the dianion is dependent on the electrode material; reversible on a glassy carbon electrode but quasi-reversible on platinum. Fe2(SR)2(NO)4 also exhibits a three electron oxidation; the anodic current of which increases in the presence of primary amines. Electrochemical studies on the Black Roussin ion and its selenium analogue [Fe4Se3(NO)7]− show similar electrochemical responses: three reversible one electron reductions and an irreversible multielectron oxidation. Extended Huckel molecular orbital calculations on [Fe2S2(NO)4]2− , Fe2(SMe)2(NO)4 and [Fe2(S203)2(N0)4]2− reveal little direct Fe-Fe interaction in these complexes. Reduction or oxidation would result in the addition or removal of electron density from orbitals of mainly Fe-S character. An electrochemical study of Fe(NO)(S2C N R2)2 by cyclic voltammetry shows a reversible one electron reduction and an Irreversible oxidation in tetrahydrofuran and dichloromethane. In acetonitrile the reduction of the complex is coupled to a chemical step making the reduction chemically irreversible at low scan rates. The observed variation of E with R is due to the inductive effect of R.
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Yousif-Ross, Sue A. "Studies toward the synthesis of phosphido-bridged iron carbonyl and nitrosyl compounds /." The Ohio State University, 1988. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487596307356516.

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Leung, Hiu-chi, and 梁曉詞. "Syntheses, reactivities and biological activities of ruthenium azido, nitrido and nitrosyl complexes supported by tetradentate tertiaryamine ligands." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2010. http://hub.hku.hk/bib/B43703732.

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Eroy-Reveles, Aura Alegra. "Synthesis of photoactive manganese nitrosyl compounds and materials for the light controlled release of nitric oxide /." Diss., Digital Dissertations Database. Restricted to UC campuses, 2008. http://uclibs.org/PID/11984.

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Legoupy, Stéphanie. "Synthèse et réactivité de nouveaux complexes organométalliques chiraux du rhénium." Rennes 1, 1997. http://www.theses.fr/1997REN10148.

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Le travail présenté dans ce mémoire concerne la synthèse et la réactivité de complexes du rhénium. De nouveaux complexes organométalliques chiraux du rhénium des alcools propargyliques et homoallylique ont été synthétisés. Des alcools allyliques secondaires et 1,2-disubstitues ont été coordonnés à l'entité chirale (#5C#5H#5)Re(No)(Pph#3)#+Bf#4#-. Dans le cas du 3-buten-2-ol complexe, les deux diastéréoisomères ont pu été séparés. L'étude de la réactivité de ces complexes du rhénium a montré qu'ils sont compatibles avec des réactions d'oxydation, de Wittig, de réduction, d'estérification, de chloration, de bromation et de fluoration. L'entité organométallique (#5C#5H#5)Re(No)(Pph#3)#+Bf#4#- s'est montrée un bon groupement protecteur d'une seule double liaison au cours de ces réactions. Les substitutions allyliques, catalysées par un acide de Lewis, sur les complexes du rhénium des alcools allyiques ont été étudiées. Quelque soit le nucléophile, ces réactions sont régio- et stéréosélectives et se font avec rétention de configuration. Un mécanisme impliquant un complexe -allyl dicationique du rhénium a été proposé. Le rôle activateur du rhénium a été mis en évidence.
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Richter-Addo, George Bannerman. "Synthetic utilization of the redox properties of some group 6 organometallic nitrosyl complexes." Thesis, University of British Columbia, 1988. http://hdl.handle.net/2429/29174.

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The redox behavior of a series of organometallic complexes containing Cp'M(NO) groups (Cp' = ƞ⁵-C₅H₅(Cp) or ƞ⁵-C₅Me₅(Cp*) ; M = Mo or W) has been investigated both by cyclic voltammetry and by chemical means. The neutral 16-electron Cp'Mo(N0)X₂ compounds (X = CL, Br or I) undergo a single, essentially reversible, one-electron reduction in CH₂CL₂/O.1M [n-Bu₄N]PF₆ at relatively low potentials (<-0.1 V vs SCE). The electrochemically observed reductions can be effected on a preparative scale by employing CP₂C0 as the chemical reductant. The isolable 17-electron [Cp'Mo (NO)X₂]•⁻ radical anions are cleanly reconverted to their 16-electron neutral precursors by treatment with [Cp₂Fe]BF₄. In contrast, the Cp'W(NO)I₂ compounds undergo rapid decomposition to their [Cp'W(NO)I]₂ monohalo dimers upon electrochemical reduction. Electrophiles NE⁺ (E = O or ϱ-O₂NC₆H₄N) undergo unprecedented insertions into the Cr-C ϭ-bonds of CpCr(NO)₂R complexes (R = Me, CH₂SiMe₃ or Ph) to afford [CpCr(N0)₂{N(E)R}]⁺ cationic complexes. Present evidence is consistent with these insertions occurring via charge-controlled, intermolecular attacks by NE⁺ at the Cr-R groups in classical SE2 processes. The newly-formed N(E)R ligands function as Lewis bases through nitrogen atoms toward the formally 16-electron [CpCr(NO)₂]⁺ cations and may be displaced from the chromium's coordination sphere by the more strongly coordinating CL⁻ anion. The resulting CpCr(NO)₂CL can be reconverted to CpCr(NO)₂R. thereby completing a cycle by regenerating the initial organometallic reactant. The entire sequence of stoichiometric reactions forming the cycle thus constitutes a selective method for the formation of new carbon-nitrogen bonds, the net organic conversions mediated by the CpCr(NO)₂ group being NE⁺ + R⁻ → N(E)R. The electrophilic [Cp'M(NO)₂]⁺ cations (Cp'=Cp or Cp* ; M = Cr, Mo or W) condense with methyl propiolate and 2,3-dimethyl-2-butene to afford cationic organometallic lactone complexes. These complexes undergo facile ⍜-dealkylation to yield the neutral Cp'M(NO)₂(ƞ¹-lactone) derivatives. Furthermore, the neutral Cp'W(NO)₂(ƞ¹-lactone) compounds decompose in air to their Cp'W(O)₂(ƞ¹-lactone) dioxo products.
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Rahman, Mohammad Saifur. "SYNTHESIS AND PHOTOCHEMICAL STUDIES OF NEW PHOTOACTIVATABLE NITROXYL (HNO)-RELEASING COMPOUNDS." Kent State University / OhioLINK, 2019. http://rave.ohiolink.edu/etdc/view?acc_num=kent1574853859162083.

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Leung, Hiu-chi. "Syntheses, reactivities and biological activities of ruthenium azido, nitrido and nitrosyl complexes supported by tetradentate tertiary amine ligands." Click to view the E-thesis via HKUTO, 2010. http://sunzi.lib.hku.hk/hkuto/record/B43703732.

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Sharp, William Brett. "Synthesis and ligand reactivity of group 6 organometallic nitrosyl complexes." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 2001. http://www.collectionscanada.ca/obj/s4/f2/dsk3/ftp04/NQ61173.pdf.

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Books on the topic "Synthesis of nitrosyl compound"

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Rubenchik, Boris Lʹvovich. Obrazovanie kant͡s︡erogenov iz soedineniĭ azota. Kiev: Nauk. dumka, 1990.

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Keller, Antoni. Kompleksy nitrozylowe molibdenu w syntezie organicznej: Reakcje metatezy, polimeryzacji i izomeryzacji olefin. Wrocław: Wydawn. Uniwersytetu Wrocławskiego, 1993.

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Vermerris, Wilfred. Phenolic compound biochemistry. Dordrecht: Springer, 2008.

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Jones, Anthony C. CVD of compound semiconductors: Precursor synthesis, development and applications. Weinheim, Germany: VCH, 1997.

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M, Villalgordo José, ed. Solid-supported combinatorial and parallel synthesis of small-molecular-weight compound libraries. [New York]: Pergamon, 1998.

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Soares-Sello, Anna Mampe. Synthesis of a potential DNA binding compound containing the 2-arylindole ring system. Norwich: University of East Anglia, 1991.

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Symposium C on High Energy Ion Implantation (1991 Strasbourg, France). High energy and high dose ion implantation: Proceedings of Symposium C on High Energy Ion Implantation and Symposium D on Ion Beam Synthesis of Compound and Elemental Layers of the 1991 E-MRS Spring Conference, Strasbourg, France, May 28-31, 1991. Amsterdam: North-Holland, 1992.

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Vermerris, Wilfred, and Ralph Nicholson. Phenolic Compound Biochemistry. Springer, 2008.

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O'Brien, Paul, and Anthony C. Jones. CVD of Compound Semiconductors: Precursor Synthesis, Developmeny and Applications. Wiley & Sons, Incorporated, John, 2008.

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O'Brien, Paul, and Anthony C. Jones. CVD of Compound Semiconductors: Precursor Synthesis, Developmeny and Applications. Wiley & Sons, Limited, John, 2008.

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Book chapters on the topic "Synthesis of nitrosyl compound"

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Norton, J. R., G. Dolcetti, B. F. G. Johnson, and A. Forster. "Decacarbonyl-Di-μ-Nitrosyl-Trimetal Compounds." In Inorganic Syntheses, 39–41. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132470.ch11.

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Lane, J. D., C. J. Pickett, and D. R. Stanley. "Synthesis of Nitrosyl Complexes." In Inorganic Reactions and Methods, 118. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470145227.ch88.

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Vančik, Hrvoj. "An Overview of Synthetic Methods for Preparation of Nitrosoaromatic Compounds." In Aromatic C-nitroso Compounds, 15–35. Dordrecht: Springer Netherlands, 2013. http://dx.doi.org/10.1007/978-94-007-6337-1_2.

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Sarshar, Sepehr, and Adnan M. M. Mjalli. "Techniques for single-compound synthesis." In Annual Reports in Combinatorial Chemistry and Molecular Diversity, 19–29. Dordrecht: Springer Netherlands, 1997. http://dx.doi.org/10.1007/978-0-306-46904-6_3.

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Laude, L. D. "Non-Equilibrium Laser Compound Synthesis." In Patterns, Defects and Microstructures in Nonequilibrium Systems, 336–50. Dordrecht: Springer Netherlands, 1987. http://dx.doi.org/10.1007/978-94-009-3559-4_20.

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Kundu, Subrata, Swapna Mukherjee, and Biswajit Ghosh. "Antimalarial Compound Synthesis from Transgenic Cultures." In Reference Series in Phytochemistry, 123–52. Cham: Springer International Publishing, 2017. http://dx.doi.org/10.1007/978-3-319-28669-3_22.

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Kundu, Subrata, Swapna Mukherjee, and Biswajit Ghosh. "Antimalarial Compound Synthesis from Transgenic Cultures." In Transgenesis and Secondary Metabolism, 1–30. Cham: Springer International Publishing, 2016. http://dx.doi.org/10.1007/978-3-319-27490-4_22-1.

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Taber, Douglass F. "Best Synthetic Methods: Oxidation." In Organic Synthesis. Oxford University Press, 2013. http://dx.doi.org/10.1093/oso/9780199965724.003.0009.

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Karl A. Scheidt of Northwestern University described (Organic Lett. 2009, 11, 1651) the oxidation of primary alcohols such as 1 in the presence of an indole 2. The product 3, an active acylating agent, is readily converted to other esters and amides. K. Rajender Reddy of the Indian Institute of Chemical Technology, Hyderabad, developed (Tetrahedron Lett. 2009, 50, 2050) a protocol for the direct oxidation of a primary amine 4 to the corresponding nitrile 5. In the presence of ammonia, the same procedure converted aldehydes and primary alcohols into the nitriles. Several catalytic methods for the oxidation of alcohols to aldehydes and ketones have recently been put forward. René Grée of the Université de Rennes 1 found ( Tetrahedron Lett. 2009, 50, 1493) that ZnBr2 catalyzed the oxidation of alcohols with diethyl azodicarboxylate. Tsutomu Katsuki of Kyushu University designed (Tetrahedron Lett. 2009, 50, 3432) a Ru catalyst for the air oxidation of primary alcohols to aldehydes. Kazuaki Ishihara of Nagoya University showed (J. Am. Chem. Soc. 2009, 131, 251) that 1 mol % of 10 was sufficient to catalyze the oxidation of 6 to 7. With excess oxidant, 7 was carried on cleanly to 11. Nitroxyl radicals such as TEMPO have long been used to catalyze oxidations. Yoshiharu Iwabuchi of Tohoku University developed (J. Org. Chem. 2009, 74, 4619) a simple preparation of 13 , the most efficient such catalyst reported so far. This catalyst should also be useful for the oxidation reported by Professor Iwabuchi (Chem. Commun. 2009, 1739) of primary alcohols and aldehydes to the corresponding carboxylic acids. David S. Forbes of the University of South Alabama prepared (Tetrahedron Lett. 2009, 50, 1855) 16 by combining thioanisole with N-bromosuccinimide. The reagent 16 efficiently sulfenylated active methylene compounds. Jiri Srogl of the Academy of Sciences of the Czech Republic established (Organic Lett. 2009, 11, 843) conditions for the oxidation of primary and secondary amines to aldehydes and ketones. Olga A. Ivanova of Moscow State University demonstrated (Tetrahedron Lett. 2009, 50, 2793) that DMDO 21 could oxidize a sensitive amino cyclopropane such as 20 to the corresponding nitro compound.
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Kabalka, George W., and Rajender S. Varma. "Reduction of Nitro and Nitroso Compounds." In Comprehensive Organic Synthesis, 363–79. Elsevier, 1991. http://dx.doi.org/10.1016/b978-0-08-052349-1.00231-6.

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Li, W.-R. "Synthesis from Acyl Nitroso Compounds." In Three Carbon-Heteroatom Bonds: Esters and Lactones; Peroxy Acids and R(CO)OX Compounds; R(CO)X, X=S, Se, Te, 1. Georg Thieme Verlag KG, 2005. http://dx.doi.org/10.1055/sos-sd-021-00138.

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Conference papers on the topic "Synthesis of nitrosyl compound"

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Agafonova, N. A., E. V. Shchegolkov, Ya V. Burgart, V. I. Saloutin, and M. V. Ulitko. "Synthesis of biological active compounds based on trifluoromethylcontaining 4-nitrosopyrazoles." In VIII Information school of a young scientist. Central Scientific Library of the Urals Branch of the Russian Academy of Sciences, 2020. http://dx.doi.org/10.32460/ishmu-2020-8-0009.

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e-pot nitrosation of 1,3-diketones or their lithium salts followed by treatment of hydrazines. Reduction of the nitroso-derivatives made it possible to obtain the 4-amino-3-trifluoromethylpyrazoles chlorides. Cytotoxic activity of the compounds wase evaluated in vitro
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Plehovich, Sergey, Sergey Zelentsov, and Alexandre Plehovich. "Quantum-chemical Study of Mechanism of the Photochemical Reactions of Nitro Compounds with Sulfur - and Nitroso Containing Compounds." In The 16th International Electronic Conference on Synthetic Organic Chemistry. Basel, Switzerland: MDPI, 2012. http://dx.doi.org/10.3390/ecsoc-16-01048.

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González, Maykel, Aliuska Helguera, M. Natália Cordeiro, Miguel Cabrera Pérez, Reinaldo Ruiz, and Yunierkis Castillo. "QSAR modeling for predicting carcinogenic potency of nitroso-compounds using 0D-2D molecular descriptors." In The 11th International Electronic Conference on Synthetic Organic Chemistry. Basel, Switzerland: MDPI, 2007. http://dx.doi.org/10.3390/ecsoc-11-01361.

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Plehovitch, Sergey, Sergei Zelentsov, Dmitry Fomichev, Sergey Zelentsov, and Dmitry Ovsyannikov. "Quantum-chemical calculations of the possible formation of nitroso oxides in the course of the photooxidation reactions by nitro compounds." In The 17th International Electronic Conference on Synthetic Organic Chemistry. Basel, Switzerland: MDPI, 2013. http://dx.doi.org/10.3390/ecsoc-17-e004.

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Jih-Chao Yeh, Jhao-Ming Su, and Shyh-Liang Lou. "Synthesis of Fe3O4/hesperetin compound." In 2010 IEEE 3rd International Nanoelectronics Conference (INEC). IEEE, 2010. http://dx.doi.org/10.1109/inec.2010.5424826.

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Hamaguchi, S., T. Yamamoto, and M. Kobayashi. "Synthesis of Ternary Compound Sulfide Nanoparticles." In 2008 International Conference on Solid State Devices and Materials. The Japan Society of Applied Physics, 2008. http://dx.doi.org/10.7567/ssdm.2008.f-5-4l.

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Takano, F., H. Ofuchi, Jeung Woo Lee, K. Takita, and H. Akinaga. "Synthesis and characterization of ferromagnetic MnSiC compound." In INTERMAG Asia 2005: Digest of the IEEE International Magnetics Conference. IEEE, 2005. http://dx.doi.org/10.1109/intmag.2005.1463614.

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Kumar, P. C. Rajesh, V. Ravindrachary, K. Janardhana, H. R. Manjunath, Prakash Karegoudar, Alka B. Garg, R. Mittal, and R. Mukhopadhyay. "Synthesis and Characterization of Organic NLO Compound." In SOLID STATE PHYSICS, PROCEEDINGS OF THE 55TH DAE SOLID STATE PHYSICS SYMPOSIUM 2010. AIP, 2011. http://dx.doi.org/10.1063/1.3606340.

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Presečnik, Mojca, and Slavko Bernik. "The thermoelectric compound Ca3Co4O9 - Synthesis and characteristics." In 9TH EUROPEAN CONFERENCE ON THERMOELECTRICS: ECT2011. AIP, 2012. http://dx.doi.org/10.1063/1.4731564.

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Martinez, Doncarli, and Guiheneuc. "Compound Nerve Action Potential Modelization And Synthesis." In Proceedings of the Annual International Conference of the IEEE Engineering in Medicine and Biology Society. IEEE, 1992. http://dx.doi.org/10.1109/iembs.1992.589504.

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Reports on the topic "Synthesis of nitrosyl compound"

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Kwong, C. D. Synthesis of a naphthalene-hydroxynaphthalene polymer model compound. Office of Scientific and Technical Information (OSTI), July 1991. http://dx.doi.org/10.2172/6929711.

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Kwong, C. D. Synthesis of a naphthalene-hydroxynaphthalene polymer model compound. Office of Scientific and Technical Information (OSTI), January 1991. http://dx.doi.org/10.2172/6884708.

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Kwong, C. D. Synthesis of a naphthalene-hydroxynaphthalene polymer model compound. Office of Scientific and Technical Information (OSTI), April 1991. http://dx.doi.org/10.2172/6986489.

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Kwong, C. D. Synthesis of a naphthalene-hydroxynaphthalene polymer model compound. Office of Scientific and Technical Information (OSTI), October 1990. http://dx.doi.org/10.2172/7149929.

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Vennos, Deborah A., Michael E. Badding, and F. J. DiSalvo. Synthesis, Structure, and Properties of a New Intermetallic Compound, Ca7Ni4Sn13. Fort Belvoir, VA: Defense Technical Information Center, May 1991. http://dx.doi.org/10.21236/ada236702.

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Hall, Gabriel B., Sayandev Chatterjee, Tatiana G. Levitskaia, Thibaut J. Martin, Nathalie Wall, and Eric D. Walter. Synthesis and Characterization of Tc(I) Carbonyl Nitrosyl Species Relevant to the Hanford Tank Waste: FY 2016 Status Report. Office of Scientific and Technical Information (OSTI), November 2015. http://dx.doi.org/10.2172/1378054.

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White, C. W., J. D. Budai, and A. L. Meldrum. Ion beam synthesis of CdS, ZnS, and PbS compound semiconductor nanocrystals. Office of Scientific and Technical Information (OSTI), December 1997. http://dx.doi.org/10.2172/564245.

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Christe, Karl O., William W. Wilson, David A. Dixon, and Jerry A. Boatz. Hepta-Coordination. Synthesis and Characterization of the IOF52- Dianion, an XOF5E Compound. Fort Belvoir, VA: Defense Technical Information Center, January 1999. http://dx.doi.org/10.21236/ada408589.

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Kwong, C. D. Synthesis of a naphthalene-hydroxynaphthalene polymer model compound. Quarterly report, September 13, 1990--December 12, 1990. Office of Scientific and Technical Information (OSTI), January 1991. http://dx.doi.org/10.2172/10110983.

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Kwong, C. D. Synthesis of a naphthalene-hydroxynaphthalene polymer model compound. Quarterly report, June 13, 1990--September 12, 1990. Office of Scientific and Technical Information (OSTI), October 1990. http://dx.doi.org/10.2172/10110991.

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