Relevant bibliographies by topics / Solution Combustion Synthesi

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Academic literature on the topic 'Solution Combustion Synthesi'

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Published: 14 March 2023

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Journal articles on the topic "Solution Combustion Synthesi"

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Zhou, Qilai, Yue Gao, Lihong Xue, Heping Li, and Youwei Yan. "ICONE23-1090 SINGLE STEP FABRICATION OF NANO-SIZED Li4SiO4 BREEDER BY MICROWAVE-INDUCED SOLUTION COMBUSTION SYNTHESIS." Proceedings of the International Conference on Nuclear Engineering (ICONE) 2015.23 (2015): _ICONE23–1—_ICONE23–1. http://dx.doi.org/10.1299/jsmeicone.2015.23._icone23-1_47.

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Lazo, A., C. Paucarchuco, and H. Loro. "SÍNTESIS DE YAIO3 (YAP) POLICRISTALINO POR EL MÉTODO DE COMBUSTIÓN EN SOLUCIÓN." Revista Cientifica TECNIA 27, no. 1 (January 4, 2018): 61. http://dx.doi.org/10.21754/tecnia.v27i1.126.

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Se presenta el método de combustión en solución y su aplicación para la síntesis de YAlO3 (YAP), fueron usados como combustibles para la reacción de combustión y síntesis la urea y glicina, del YAP. Usando las técnicas de difracción de rayos X (XRD) por el método del polvo y microscopia electrónica de barrido (MEB) fueron analizadas la parte estructural y morfológica de las muestras obtenidas. Los difractogramas de Rayos X muestran una excelente correspondencia con lo reportado en la literatura para este material. Se suministran también los resultados de las muestras de material YAlxCrx‐1O3, dopado con Cr3+ con x = 0.001, 0.01, que exhiben picos de difracción dominantes debidos a la fase ortorrómbica de YAlO3 Palabras clave.- YAP, YAlO3, Combustion method. ABSTRACT The solution‐combustion process is presented, as well as its application to the synthesis of YAlO3 (YAP). Urea and glycine were used as fuel for the combustion reaction and synthesis of the YAP. The structure and morphology of the obtained sample were analyzed using the X‐ray diffraction (XRD) powder method and scanning electron microscopy (SEM). The X‐ray patterns showed an excellent agreement with data reported in the literature for this material. Results are also given for samples of YAlxCrx‐1O3 doped with Cr3+, with x = 0.001, 0.01, which showed dominant diffraction peaks due to the orthorhombic phase of YAlO3. Keywords.- YAP, YAlO3, combustion method.
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Astuti, Yayuk, Prisca Putri Elesta, Didik Setyo Widodo, Hendri Widiyandari, and Ratna Balgis. "Hydrazine and Urea Fueled-Solution Combustion Method for Bi2O3 Synthesis: Characterization of Physicochemical Properties and Photocatalytic Activity." Bulletin of Chemical Reaction Engineering & Catalysis 15, no. 1 (October 19, 2019): 104–11. http://dx.doi.org/10.9767/bcrec.15.1.5483.104-111.

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Bismuth oxide synthesis using solution combustion method fuelled by hydrazine and urea has been conducted. This study aims to examine the effect of the applied fuels, urea and hydrazine, on product characteristics and photocatalytic activity in degrading rhodamine B dye. Bismuth oxide synthesis was initiated by dissolving bismuth nitrate pentahydrate (Bi(NO3)3.5H2O) in a nitric acid solvent. Fuel was added and then stirred. The solution formed was heated at 300 ºC for 8 hours. The product obtained was then calcined at 700 ºC for 4 hours. Bismuth oxide synthesized with urea (BO1) and hydrazine (BO2) as fuels both obtained form of yellow powder. The formation of bismuth oxide is indicated by the vibrations of the Bi–O–Bi and Bi–O groups and the crystal structure of a-Bi2O3 in both products. Photocatalytic activity test showed that BO1 has a photocatalyst activity in degrading rhodamine B higher than that of BO2 with constant values of 3.83×10-5 s-1 and 3.43×10-5 s-1, respectively. The high photocatalytic activity can be examined through several factors, such as: band gap values, crystal structure, morphology, and surface area, acquired as a result of the use of different fuels in the synthesis process. Copyright © 2020 BCREC Group. All rights reserved
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Jung, Choong Hwan, Ji Yeon Park, and Woo Seog Ryu. "Synthesis and Dilatometric Study of Ca(Sr, La)TiO3 Prepared by Solution Combustion Synthesis (SCS)." Solid State Phenomena 119 (January 2007): 107–10. http://dx.doi.org/10.4028/www.scientific.net/ssp.119.107.

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La and Sr have recognized as elements of high level radioactive wastes immobilized by solid solution with CaTiO3. For forming solid solution with CaTiO3, the solution combustion synthesis (SCS) process was applied and the powder characteristics and sinterability were investigated. The proper selection of the type and the composition of fuels are important to get the crystalline of CaTiO3. When glycine or the mixtures of urea+citric acid with stoichiometric composition was used, the solid solutions of Ca(La, Sr)TiO3 were entirely produced. The combustion synthesized powder seemed to have a good sinterability with the linear shrinkage of more than 23% up to 1400oC, while that of the solid state reacted powder was less than 19% at the same conditions.
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Mukasyan, Alexander S., Paul Epstein, and Peter Dinka. "Solution combustion synthesis of nanomaterials." Proceedings of the Combustion Institute 31, no. 2 (January 2007): 1789–95. http://dx.doi.org/10.1016/j.proci.2006.07.052.

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Yin, Ziyang, Si Li, Xiang Li, Wuyang Shi, Wei Liu, Zhengxia Gao, Mengya Tao, Chengliang Ma, and Yuan Liu. "A review on the synthesis of metal oxide nanomaterials by microwave induced solution combustion." RSC Advances 13, no. 5 (2023): 3265–77. http://dx.doi.org/10.1039/d2ra07936d.

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Microwave-induced solution combustion synthesis is a new method of nanomaterials preparation based on traditional solution combustion synthesis. The method can rapidly prepare a wide variety of nanomaterials.
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Kata, D., M. Ohyanagi, and Z. A. Munir. "Induction-field-activated self-propagating high-temperature synthesis of AlN–SiC solid solutions in the Si3N4–Al–C system." Journal of Materials Research 15, no. 11 (November 2000): 2514–25. http://dx.doi.org/10.1557/jmr.2000.0361.

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The synthesis of AlN–SiC solid solutions from Si3N4, Al, and C was investigated using the induction-field-activated/self-propagating high-temperature synthesis/static pseudo-isostatic compaction technique. Careful x-ray diffraction analyses were made on the products of combustion to determine reaction routes. Optical microscopy as well as scanning electron microscopy with an electron probe microanalysis was used for microstructural analysis. It was found that initially molten aluminum reacted with silicon nitride producing an Al–Si alloy. At higher temperatures, aluminum evaporated from the Al–Si liquid and the synthesis of AlN via a vapor phase process took place. Subsequently, dissolution of AlN into molten Si resulted in the formation of an AlN–SiC solid solution from the Al–N–Si–C liquid phase. However, below 1850 °C, the resulting solid solution of 4AlN–3SiC was not fully crystallized. Combustion temperatures above or equal to 1850 °C were required to prepare a highly crystallized solid solution with a morphology exhibiting hexagonal platelets. Based on these observations, a model for the formation of AlN–SiC solid solution is proposed.
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Ashok, Anchu, Anand Kumar, and Faris Tarlochan. "Surface Alloying in Silver-Cobalt through a Second Wave Solution Combustion Synthesis Technique." Nanomaterials 8, no. 8 (August 9, 2018): 604. http://dx.doi.org/10.3390/nano8080604.

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Herein, we report the synthesis of silver-cobalt nanopowders using three different modes of solution combustion synthesis, and we present the effects of the synthesis conditions on particle morphology. The synthesized nanoparticles were characterized using X-ray diffraction (XRD), Scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), UV-Visible spectrophotometer (UV-vis), Transmission electron microscopy (TEM), and X-Ray Photoelectron Spectroscopy (XPS) to understand the structural and elemental properties. When Co is synthesized over Ag in a second wave of combustion, peak shifts observed in XRD and XPS show a change in the cell parameters and prove the existence of a strong electronic interaction between Ag and Co. Better control of mixing and alloying through the second wave combustion synthesis mode (SWCS) was evident. The sequence of combustion affects the structure and composition of the material. SWCS reduces the amount of carbon content, as compared to single-stage combustion, and the combustion of carbon is followed by a rearrangement of atoms.
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Ianoş, Robert. "An efficient solution for the single-step synthesis of 4CaO·Al2O3·Fe2O3 powders." Journal of Materials Research 24, no. 1 (January 2009): 245–52. http://dx.doi.org/10.1557/jmr.2009.0019.

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Single-phase nanocrystalline 4CaO·Al2O3·Fe2O3 powders were prepared directly from the combustion reaction using a new cost-effective, time-saving, and environmentally friendly version of solution combustion synthesis. Instead of a single fuel, a fuel mixture of urea and β-alanine was used. It was shown by x-ray diffraction, energy-dispersive x-ray analysis, thermogravimetric analysis, and optical microscopy that this new version of the solution combustion synthesis allows the maximization of the exothermic effect associated with the combustion reaction. On the other hand, it was shown that the traditional version of combustion synthesis involving the use of a single fuel, such as urea or β-alanine, does not ensure the formation of Ca4Al2Fe2O10 unless subsequent thermal treatments are applied. It was suggested that the occurrence of combustion reactions cannot be regarded only in terms of adiabatic temperature, as the kinetic aspects overrule the thermodynamic ones.
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Amosov, Aleksandr P., Vladislav A. Novikov, Egor M. Kachkin, Nikita A. Kryukov, Alexander A. Titov, Ilya M. Sosnin, and Dmitry L. Merson. "The Solution Combustion Synthesis of ZnO Powder for the Photodegradation of Phenol." Ceramics 5, no. 4 (November 3, 2022): 928–46. http://dx.doi.org/10.3390/ceramics5040067.

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Nanoscale and submicron powder of zinc oxide (ZnO) is known as a highly efficient photocatalyst that is promising for solving the problem of wastewater treatment from toxic organic pollutants including phenol and its derivatives. The results of laboratory studies of ZnO preparation by a simple, energy-saving, and highly productive method of solution–combustion synthesis from a mixture of solutions of zinc nitrate and glycine, as well as the use of the ZnO powder synthesized by combustion for the photocatalytic decomposition of phenol, are presented. The modes and characteristics of combustion, phase composition, chemical composition, and structure of the combustion product at different ratios of glycine with zinc nitrate were determined. It is shown that calcination at 650 °C reduces the content of carbon impurity in the combustion product to ~1 wt.% and leads to obtaining ZnO powder in the form of porous agglomerates up to 100 μm in size sintered from crystalline nanoscale and submicron ZnO particles with an average crystallite size of 44 nm. The ZnO powder exhibits high photocatalytic activity, leading to the almost complete degradation of phenol in an aqueous solution under the action of ultraviolet irradiation in less than 4 h.
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Dissertations / Theses on the topic "Solution Combustion Synthesi"

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MARIN, FIGUEREDO MIGUEL JOSE. "Metal Oxide Catalysts for the Abatement of Volatile Organic Compounds and Carbonaceous Particulate Matter." Doctoral thesis, Politecnico di Torino, 2022. http://hdl.handle.net/11583/2966339.

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Topolski, Diogo Kramer. "Obtenção de espinélio MgAl2O4 nanoestruturado através de síntese contínua por combustão em solução." reponame:Biblioteca Digital de Teses e Dissertações da UFRGS, 2010. http://hdl.handle.net/10183/116606.

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Este trabalho teve por objetivo investigar a obtenção de espinélio MgAl2O4 nanoestruturado através da síntese contínua por combustão em solução e sua caracterização por diferentes técnicas. Incluso neste estudo a influência do tipo de combustível e a razão combustível-oxidante no tamanho do cristalito. As partículas de espinélio MgAl2O4 foram sintetizadas utilizando-se os precursores químicos nitrato de alumínio e nitrato de magnésio como fonte dos cátions metálicos. Uréia, glicina e sacarose foram empregadas como agentes redutores, com diferentes valores da razão combustível-oxidante para a sacarose. Estes parâmetros foram relacionados com sua influência no tamanho de cristalito, tamanho de partícula e área superficial. Na caracterização do pó obtido, foram utilizadas técnicas como análise termodiferencial (ATD) e termogravimétrica (ATG), granulometria por difração de laser (GDL), análise de área superficial (BET), análise cristalográfica por difração de raios X (DRX), morfologia por microscopia eletrônica de varredura (MEV). As reações químicas da síntese contínua por combustão em solução resultaram na formação in situ de fases cristalinas para reações estequiométricas de uréia, glicina e sacarose e as deficientes de sacarose. Preponderância de fase amorfa ocorreu nas reações com excesso de sacarose para o pó como-sintetizado. A totalidade de fase cristalina foi obtida após um tratamento térmico a 900°C do pó como-sintetizado. Os pós de espinélio MgAl2O4 obtidos apresentaram-se como constituídos de cristalitos nanométricos, dispostos na forma de agregados de tamanho micrométrico. O tamanho de cristalito médio, calculado pelo método Single Line, a partir de dados de análises por DRX, foi de 13 nm. A área superficial média dos pós calcinados medida pelo método BET foi de 54 g/m2 Por análise granulométrica constatou-se um Tamanho de partícula médio de 17 μm para o pó como-sintetizado e 17,1 μm para o calcinado a 900ºC. As análises por MEV confirmaram a agregação das partículas do pó sintetizado, a partir de partículas preponderantemente esféricas e algumas com morfologia irregular.
This study has investigated a continuous solution combustion synthesis technique to obtain the nanostructured MgAl2O4 spinel powder and their characterize them by different tecniques. This study has also included the investigation of the influence of different kinds of fuel and fuel-to-oxidant ratio on crystallite size. The MgAl2O4 spinel powder was performed using aluminum nitrate and magnesium nitrate to obtain the metallic ions. Urea, glycine and sucrose were used like fuel, with several fuel-to-oxidant ratio. These parameters were correlating with powders characteristics, like crystallite size, particle size and superficial area. The techniques used for powder characterization included differential thermal analyzer (DTA), thermogravimetric analyzer (TGA), particles size analyzer (PSA), surface area by BET analysis, X-ray diffraction (XRD) and scanning electron microscopy (SEM). The chemical reactions of solution combustion resulted on crystalline phase to the reactions with urea, glycine and sucrose (to desabilites on fuel and stoichiometric) and amorphous phase formation of MgAl2O4 in situ for as-synthesized powder. The crystalline phase formation of spinel MgAl2O4 was only succeeded obtained after a thermal treatment of as-synthesized powder under 900°C.The spinel MgAl2O4 powders obtained were composed of nano-size crystallites, but in micrometer-sized aggregates. The mean particle size calculated, via Single Line method, using XRD was 13 nm. PSA indicated that the synthesized powders contain a mean aggregates size with a tri mode distribution of around 17.1 μm. SEM analyses confirmed that the as-synthesized powders are composed of particles aggregation. They have an irregular morphology and nano-size crystallites.
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Giangolini, Matteo. "Production and characterization of tin oxide thin films deposited via solution combustion synthesis." Master's thesis, Alma Mater Studiorum - Università di Bologna, 2018. http://amslaurea.unibo.it/15816/.

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The main goal of this thesis work is the production and characterization of Tin oxide thin film deposited via Solution Combustion Synthesis (SCS). Different precursors are used in order to study the effect of the chemical nature of the reagent on the structural, morphological and electrical properties of the thin films. Tin oxide was chosen because is one of the most promising candidates for p-type oxide. In fact, the semiconductor oxides reported in the literature are mostly limited to n-type and there is a need for solution processed p-type oxide semiconductors to achieve Complementary Metal Oxide Semiconductors (CMOS) using all oxide materials. Anyway, the production window of solution processed for p-type SnO is narrow and Silver doping will be used to enhance the probability to get it. If production of p-type Tin oxide will not be achieved, the work will be focused on n-type SnO2 and on the optimisation of devices made with this material, either Thin Film Transistors (TFTs) or Transparent Conductive Oxides (TCOs). Samples made in this work show good optical properties, like transmittance over 80% and energy gap values around 3.79 eV, but none of them turned out to be a p-type oxide or a good TFT. Samples annealed at higher temperatures have good electrical conductivity properties, which could lead to a future study in order to optimise these materials for TCO purposes.
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Nascimento, Cássia Costa. "Síntese de cerâmicas tipo perovskita com potencial uso em células solares." Universidade Federal de São Carlos, 2017. https://repositorio.ufscar.br/handle/ufscar/8819.

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Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
Visible light accounts for the biggest fraction of the solar irradiance. One of the strategies for achieving higher photovoltaic power conversion efficiency is the application of low band-gap materials (Eg ideal≈1.4 eV) capable of absorbing this fraction of the solar spectrum. Ferroelectric semiconductors have been studied in this field due to the above-bandgap generated photovoltages and their ferroelectric polarization-driven carrier separation. Ferroelectric oxides usually present wide bandgaps which allow the absorption of only 8-20% of the solar spectrum. However, the development of new ferroelectric materials, particularly KBNNO [KNbO3]0,9[BaNi0,5Nb0,5O3-δ ]0,1 (Eg = 1.39 eV) and KBiFe2O5 (Eg=1,60 eV), has encouraged the use of such materials in solar cells. Simple synthesis routes, with short steps, time and temperatures are essential for the future progress of the application of such ferroelectric oxides in solar cells. KBNNO and KBiFe2O5 require high crystallization temperatures, which reduce the number of potential substrates and electrode materials that could be used in devices, as polymer-based flexible ones. Obtaining this oxides in a high surface-area powder form might be a strategy to further incorporation in solar cells composed of low-temperature processing materials. This work reports for the first time synthesis of KBNNO and KBiFe2O5 by solution combustion (SCS). Characterization by WAXD, SEM, EDS, TG/DSC and Diffuse Reflectance UV-Vis Spectroscopy and dielectric constants indicates the success of the synthesis. The optical properties show the visible-light absorption contribution and band-gaps closer to the ideal magnitude for solar applications compared to the non doped materials. The SCS was shown as an effective route to obtaining the phase. Furthermore, it is possible to improve it in order to produce powders with smaller particle size and absent of secondary phases.
A luz visível representa a fração mais relevante da radiação solar. Desta maneira, busca-se empregar nas camadas ativas das células solares materiais com baixos band-gaps (Eg ideal ≈1,4 eV), capazes de absorver fótons nessa região do espectro. Semicondutores ferroelétricos com estrutura da perovskita ou estruturas relacionadas têm sido estudados nesse campo devido ao potencial de obtenção de voltagens superiores à magnitude de seus band-gaps e à contribuição na separação de portadores de cargas decorrente da polarização intrínseca presente nesses materiais. Óxidos ferroelétricos geralmente possuem Eg elevados (2,7-4 eV), permitindo o aproveitamento de somente 8-20% do espectro solar. No entanto, o desenvolvimento de novos semicondutores ferroelétricos, particularmente a KBNNO [KNbO3]0,9[BaNi0,5Nb0,5O3-δ ]0,1 (Eg=1,39 eV) e KBiFe2O5 (Eg=1,60 eV), tem encorajado a aplicação desses materiais em células solares. Rotas de síntese simples, com etapas, tempos e temperaturas reduzidas são essenciais para o progresso futuro da aplicação de tais óxidos ferroelétricos em células solares. A KBNNO e KBiFe2O5 cristalizam em temperaturas mais elevadas do que perovskitas orgânico-inorgânicas, o que reduz a possibilidade de fabricação de dispositivos na presença de substratos e eletrodos sensíveis à temperatura, como substratos poliméricos flexíveis. Assim, a obtenção desses óxidos na forma de pós de elevada área superficial pode ser uma estratégia para posterior incorporação em dispositivos contendo materiais processados a baixas temperaturas. Neste trabalho, reporta-se pela primeira vez a síntese da KBNNO e KBiFe2O5 por combustão em solução. Caracterizações por DRX, MEV, EDS, TG/DSC, Espectroscopia UV-Vis e constantes dielétricas indicam a obtenção das fases com sucesso. As propriedades ópticas confirmam contribuição na absorção da luz visível com respeito aos materiais não dopados, KNbO3 e BiFeO3. A síntese por combustão em solução se mostra efetiva para obtenção das fases, mas passível de melhorias para produção de pós com menor tamanho de partícula e sem a presença de fases secundárias.
CNPq: 155305/2014-0
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Toniolo, Juliano Cantarelli. "Influência da razão combustível-oxidante nas características de óxidos nanoestruturados sintetizados por combustão em solução." reponame:Biblioteca Digital de Teses e Dissertações da UFRGS, 2009. http://hdl.handle.net/10183/16479.

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Com o aumento do uso do método de síntese por combustão em solução para obtenção de pós cerâmicos, há uma crescente percepção da necessidade de se entender as características únicas deste processo. Esta tese apresenta uma investigação baseada na obtenção de diferentes pós nanoestruturados: Al2O3-α (alumina), Cr2O3 (crômia), Fe2O3-α (hematita), Fe3O4 (magnetita), NiO (bunsenita) e CoO, Co3O4 (óxidos de cobalto), como opção para futuras aplicações. Estes foram caracterizados via ATD, BET, DRX, MET, MEV, VSM, XPS e FTIR. O foco particular deste trabalho é o estudo da razão combustível-oxidante e sua influência nas características dos materiais resultantes. Outros parâmetros de combustão foram identificados e também devidamente avaliados, tais como: tipo de chama, temperatura, gases gerados e composição química dos reagentes precursores. O cálculo termodinâmico da reação de combustão em solução mostrou que, quando a razão combustível-oxidante aumenta, obtêm-se uma elevação da temperatura de chama adiabática e da quantidade de gás produzida, definindo características do particulado como morfologia, tamanho de cristalito, área superficial e nível de agregação. A formação dos óxidos e metais seguiu um comportamento termodinâmico esperado, conforme energia livre de Gibbs. Menores tamanhos de cristalito foram obtidos sempre na condição deficiente em combustível para todos os sistemas estudados. Já a temperatura foi o principal parâmetro de reação que governou a taxa de crescimento e concorreu com a geração de gases para a formação dos cristalitos em certas condições redutoras. Os resultados deste trabalho melhoraram significativamente o entendimento do efeito da razão combustível-oxidante no comportamento das características físicas dos pós. Esta correlação foi avaliada com intuito de fornecer base de conhecimento para possível aplicação desta tecnologia na otimização ou desenvolvimento de novos sistemas de pós.
With the increasing use of solution combustion synthesis method for powder obtaining, there is a growing realization of the need to understand the unique characteristics of this process. This thesis presents the novel investigation of this technique specifically based upon some nanostructured powders such as α - Al2O3 (alumina), Cr2O3 (eskolite), α - Fe2O3 (hematite), Fe3O4 (magnetite), NiO (bunsenite), and CoO, Co3O4 (cobalt oxides) as a core option for future applications. These were characterized via DTA, BET, XRD, TEM, SEM, VSM, XPS, and FTIR. The particular focus of this work is based on the study of the fuel-to-oxidant ratio influence to the characteristics of the resulting materials. Other combustion parameters were identified and also proper appraised as flame type, temperature, gas generation, and chemical composition of precursor reagents. The thermodynamic calculation of the combustion reaction shows that as fuel-tooxidant ratio increases the amount of gas produced, and adiabatic flame temperature also increases. Powder characteristics as morphology, crystallite size, surface area and aggregation degree are mainly governed by the flame temperature, and generation of gases. The oxide and metals formation followed a thermodynamic behavior as expected, conform to Gibbs free energy. Lower crystallite sizes were always obtained by fuel-lean condition for all studied systems. The temperature was the main reaction parameter controlling the growth rate, while it competed with generation of gases to form crystallites under certain reducing conditions. The outcomes of this work have significantly improved the understanding of the fuelto- oxidant ratio effects on the behavior of the physical characteristics of powders. This correlation has been drawn in order to provide a knowledge basis for possible application of this technology to optimize or develop new powder systems.
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Goujon, Pierre-Andre. "Synthèse par flash combustion et voie solide de formulations céramiques diélectriques dans le diagramme de phase ternaire CaO/ZrO2/TiO2." Thesis, Normandie, 2020. http://www.theses.fr/2020NORMC225.

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Le domaine de composition Ca(ZrxTi1-x)O3 a été étudié afin de mieux apprécier ses propriétés diélectriques ; dans le but d'applications pour condensateurs céramiques multicouches à armatures en métaux non nobles. La synthèse de tout ce domaine est mal connue, que ce soit par voie solide, ou par flash combustion. L’étude et l’optimisation (mélangeage/broyage, température de chamottage) de la synthèse par voie solide a permis la synthèse d’échantillons monophasés de la phase pérovskite tout le long du domaine de composition. L’étude de la synthèse par flash combustion a d’abord déterminé que le combustible le plus efficace pour la synthèse était la glycine, puis que l’apport de titane permettant la formation de la phase la plus performante est le nitrate de Titane (TiO(NO3)2) synthétisé à partir du butoxyde de titane.La densification des poudres obtenues par ces deux méthodes a été étudiée et comparée. Ces essais ont permis de comparer plusieurs paramètres sur la densification des échantillons. Ces paramètres sont le mode d’élaboration, le ratio Zr/Ti, ainsi que l’atmosphère de frittage. Des ajouts de frittages seront également testés sur deux compositions : CaZrO3 et Ca(Zr0,8Ti0,2)O3. Ces compositions ont été choisies car elles sont pauvres en titane, ce qui évite la réduction de cet élément qui transformerait le condensateur en semi-conducteur lors d’un frittage sous atmosphère réductrice. Cette étude comparative de ces différents paramètres porte également sur les propriétés diélectriques des échantillons ainsi produits
The compositional domain Ca(ZrxTi1-x)O3 has been studied in order to understand the formation of solid solution between CaTiO3 and CaZrO3. The aim of this study is the application of such formulations for multilayer ceramic capacitors with non-nobles metal armatures. The synthesis on the line CaTiO3/CaZrO3 is poorly known, either by solid state or by flash-combustion. The study and optimization (mixing/grinding, temperature of calcination) of the solid-state synthesis has allowed the synthesis of single-phase samples made of the perovskite phase along the whole compositional range. The study of the solution-combustion synthesis first determined that the most efficient fuel for the synthesis was glycine, then the fact that the titanium input allowing the formation of the purest phase is TiO(NO3)2, synthesized from titanium butoxide.The densification of the powders obtained by these two methods was studied and compared. These tests allowed to compare several parameters on the densification of the samples. These parameters are the powders’ method of elaboration, the Zr/Ti ratio and the sintering atmosphere. Sintering adds were also be tested on two compositions: CaZrO3 and Ca(Zr0.8Ti0.2)O3. These compositions have been chosen because they are weak in titanium, which avoids reduction and appearance of semi-conduction of Ti that would transform the capacitor into a p-semiconductor during sintering in a reducing atmosphere. This comparative study of these different parameters also deals with the dielectric properties of the samples thus produced
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Pradal, Nathalie. "Synthèses, mise en forme et caractérisations de luminophores nanostructurés pour une nouvelle génération de dispositifs d'éclairage sans mercure." Phd thesis, Université Blaise Pascal - Clermont-Ferrand II, 2012. http://tel.archives-ouvertes.fr/tel-00775908.

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Le marché de l'éclairage est un marché de masse à diffusion large en pleine mutation face aux nouvelles contraintes environnementales. Il s'inscrit dans une démarche de préservation de l'environnement avec une volonté européenne de voir sa consommation énergétique réduite de 20% d'ici 2020. Les luminophores jouent un rôle prépondérant dans les performances des systèmes d'éclairage utilisant comme sources d'excitations des LEDs bleues ou UV, ou encore un plasma (Xe-Ne), où ils permettent de convertir les photons incidents (VUV, UV ou bleus) en lumière visible. Dans le cadre de cette thèse, nous nous sommes intéressés à la production de lumière blanche. Pour obtenir une couleur la plus proche du blanc idéal et répondant aux mieux au cahier des charges de l'éclairage domestique, une amélioration des performances des luminophores utilisés classiquement est nécessaire. Au cours de ces travaux nous avons porté notre attention sur deux aluminates de formulations Y3Al5O12 dopé Ce3+ (YAG :Ce) et BaMgAl10O17 dopé Eu2+ (BAM :Eu). L'aspect novateur repose d'une part sur la synthèse de ces luminophores sous forme de nanoparticules par des voies de synthèse originales (la voie solvothermale et la combustion assistée par micro-ondes respectivement) et d'autre part sur leur mise en forme (revêtements composites " luminophores/polymère "). Plusieurs techniques expérimentales (DRX, IR, Mössbauer, aimantation, MEB, MET,...) ont été utilisées afin de caractériser leurs propriétés structurales et morphologiques. L'étude des performances optiques de ces luminophores enregistrées sous excitations bleue, UV et/ou VUV nous a permis de mettre en évidence leur utilisation potentielle dans les nouveaux dispositifs d'éclairage : associés à d'autres luminophores (rouge pour le YAG :Ce; rouge et vert pour le BAM :Eu) en proportions adéquates, il est possible de générer de la lumière blanche présentant les propriétés escomptées.
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Volkmer, Tiago Moreno. "Obtenção e caracterização de α-fosfato tricálcico por síntese de combustão e aplicação em cimentos ósseos e arcabouços de criogéis." reponame:Biblioteca Digital de Teses e Dissertações da UFRGS, 2011. http://hdl.handle.net/10183/34762.

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Os cimentos de fosfato de cálcio apresentam uma série de vantagens de utilização em ortopedia e traumatologia, sendo as mais destacadas a sua biocompatibilidade e bioatividade, as quais permitem a osteocondução dos tecidos ósseos e o endurecimento “in situ”, permitindo maior facilidade de manipulação. Entretanto; através dos métodos convencionais de reação no estado sólido há uma grande dificuldade em se obter a fase α- fosfato tricálcico pura. Com o desenvolvimento deste trabalho foi possível sintetizar a fase α-fosfato tricálcico nanoestruturado com elevado grau de pureza, utilizando-se o método de síntese de combustão em solução. Após os estudos da influência do pH, da natureza do combustível (uréia ou glicina) e dos teores estequiométricos de combustível (0,75; 1,0; 1,5 e 2,0) foi possível definir os melhores parâmetros de síntese (pH 1,5 e combustível uréia em teor duas vezes maior do que o estequiométrico). Com a definição dos parâmetros ótimos de reação, estudou-se a viabilidade de sua utilização como cimento de fosfato de cálcio. Nesta etapa verificou-se a influência do tamanho de partícula através do tempo de moagem. Para tempo de moagem de 180 minutos foram obtidos valores de resistência mecânica à compressão de até 30,4 MPa. Porém após a imersão em solução de plasma sanguineo simulado (SBF) em tempos crescentes de até 28 dias, ocorreu a diminuição desta propriedade o que é indicativo da alta solubilidade dos pós de α-fosfato tricálcico obtidos via síntese de combustão em solução. O ensaio de citotoxicidade In Vitro demonstrou que o CFC sintetizado neste trabalho não apresentou efeito tóxico para as células. Na sequência do trabalho, investigou-se a viabilidade da aplicação do CFC como substituto ósseo e como carga cerâmica em criogéis poliméricos para utilização em engenharia de tecidos. Inicialmente utilizou-se o sistema dimetilaminoetil metacrilato (DMAEMA) com a adição de 5% de um ácido acrílico (ácido acrílico ou ácido metacrílico), porém tal sistema se mostrou muito instável e apresentou baixa reprodutibilidade. Dessa forma, substituiu-se o ácido acrílico pelo monômero hidroxietil metacrilato (HEMA), pelo fato de o último possuir maior estabilidade química e melhores propriedades mecânicas. Com o uso deste sistema foram obtidos arcabouços porosos através do método de criopolimerização com porosidade de até 75% e poros de até 1 milímetro de diâmetro. A adição de α-fosfato tricálcico às estruturas porosas pouco influenciou nas propriedades físicas da rede polimérica e nas propriedades mecânicas dos arcabouços porosos, porém aumentou significativamente a biocompatibilidade destes, permitindo a adesão e a proliferação de células tronco mesenquimais. A presença de colágeno do tipo I e de fosfatase alcalina são bons indicativos de que as células tronco mesenquimais estão se diferenciando em tecido ósseo e demonstram o potencial destes materiais para o seu uso como biomaterial e mais especificamente como substitutos ósseos.
The calcium phosphate cements have a large number of advantages regarding its use in orthopedics and traumatology, being the most prominent its biocompatibility and bioactivity, which allows the osteoconductive of bone tissue and in situ hardening, allowing greater ease of handling. However, the use of conventionals synthesis methods, e.g. solid state reactions, brings great difficulty to the obtainment of highly pure α- tricalcium phosphate phase. In this thesis, the use of the solution combustion synthesis method allowed to synthesize nanostructured α-tricalcium phosphate with high purity. Further studies on pHs influence, fuel natures (urea or glycine) and fuel ratio (0.75, 1.0, 1.5 and 2.0) allowed to define the best synthesis parameters (pH 1.5 and urea fuel content in two times higher than the stoichiometric). After choosing the best paramaters to the obtainment of higly pure α-tricalcium phosphate, we studied the feasibility of their use as calcium phosphate cement (CFC) by studing the influence of particle size by increasing the milling time from 30 to 180 minutes. The better results were found for the milling time of 180 minutes. Compressives strength of up to 30.4 Mpa were obtained for this formulation. However, after soaking the calcium phosphate cements in simulated blood plasma (SBF) in growing times up to 28 days, a decrease in the compressive strenght was noticed, which is an indicative of the high solubility of the α-tricalcium phosphate powders obtained by solution combustion synthesis. After the obtainment of the calcium phosphate cements, its application as bone substitute and as ceramic load in polymeric cryogels for use in tissue engineering were studied. Initially, the system dimethylaminoethyl methacrylate (DMAEMA) with 5% of an acrylic acid (acrylic acid or methacrylic acid) was used, but due its great instability and lack of reproductbility this system was abandoned. Since it has greater chemical stability and good mechanical properties, the monomer hydroxyethyl methacrylate (HEMA) was chosen as pair to the DMAEMA monomer. With the use of this polymeric system, porous scaffolds with porosity of up to 75% and pores up to 1 mm in diameter were obtained by the method of cryopolymerization. The addition of α-tricalcium phosphate to the porous scaffolds did not showed a significant influence on physical properties of the polymer network nether on mechanical properties of porous structures. However, it increased significantly the biocompatibility of the scaffolds, allowing the adhesion and proliferation of mesenchymal stem cells. The presence of type I collagen and alkaline phosphatase are good indicators that mesenchymal stem cells are differentiating into bone tissue and demonstrate the potential application of these materials as biomaterials, more specifically as bone substitutes.
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SETZ, LUIZ F. G. "Processamento coloidal de cromito de lantanio." reponame:Repositório Institucional do IPEN, 2009. http://repositorio.ipen.br:8080/xmlui/handle/123456789/11522.

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Tese (Doutoramento)
IPEN/T
Instituto de Pesquisas Energeticas e Nucleares - IPEN-CNEN/SP
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Soares, Maria Rosa Nunes. "Development of Zirconia based phosphors for application in lighting and as luminescent bioprobes." Doctoral thesis, Universidade de Aveiro, 2016. http://hdl.handle.net/10773/15884.

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Doutoramento em Nanociências e Nanotecnologia
The strong progress evidenced in photonic and optoelectronic areas, accompanied by an exponential development in the nanoscience and nanotechnology, gave rise to an increasing demand for efficient luminescent materials with more and more exigent characteristics. In this field, wide band gap hosts doped with lanthanide ions represent a class of luminescent materials with a strong technological importance. Within wide band gap material, zirconia owns a combination of physical and chemical properties that potentiate it as an excellent host for the aforementioned ions, envisaging its use in different areas, including in lighting and optical sensors applications, such as pressure sensors and biosensors. Following the demand for outstanding luminescent materials, there is also a request for fast, economic and an easy scale-up process for their production. Regarding these demands, laser floating zone, solution combustion synthesis and pulsed laser ablation in liquid techniques are explored in this thesis for the production of single crystals, nanopowders and nanoparticles of lanthanides doped zirconia based hosts. Simultaneously, a detailed study of the morphological, structural and optical properties of the produced materials is made. The luminescent characteristics of zirconia and yttria stabilized zirconia (YSZ) doped with different lanthanide ions (Ce3+ (4f1), Pr3+ (4f2), Sm3+ (4f5), Eu3+ (4f6), Tb3+ (4f8), Dy3+ (4f9), Er3+ (4f11), Tm3+ (4f12), Yb3+ (4f13)) and co-doped with Er3+,Yb3+ and Tm3+,Yb3+ are analysed. Besides the Stokes luminescence, the anti- Stokes emission upon infrared excitation (upconversion and black body radiation) is also analysed and discussed. The comparison of the luminescence characteristics in materials with different dimensions allowed to analyse the effect of size in the luminescent properties of the dopant lanthanide ions. The potentialities of application of the produced luminescent materials in solid state light, biosensors and pressure sensors are explored taking into account their studied characteristics.
O progresso observado nas últimas décadas na área da fotónica e optoelectrónica, acompanhado de um desenvolvimento exponencial nas áreas da nanociência e nanotecnologia, resulta numa constante procura por materiais luminescentes eficientes com características cada vez mais exigentes. Matrizes de largo hiato energético dopadas com iões lantanídeos assumem-se, atualmente, como uma classe de materiais luminescentes de elevada importância tecnológica. Dentro destas, a zircónia apresenta uma combinação de propriedades químicas e físicas que a potenciam como matriz para a incorporação dos iões mencionados, tendo em vista o seu uso em diversas áreas, destacando-se as aplicações em iluminação e sensores óticos, entre os quais sensores de pressão e biossensores. Associada à necessidade de materiais luminescentes com características superiores, encontra-se a necessidade de técnicas de produção rápidas, económicas e com potencial para produção em larga escala. Tendo em conta estas necessidades, técnicas como a fusão de zona com laser, combustão em solução e ablação laser em meio líquido são exploradas neste trabalho para a produção de monocristais, nanopós e nanopartículas de matrizes à base de zircónia intencionalmente dopadas com lantanídeos. Em simultâneo, é realizado um estudo detalhado das propriedades morfológicas, estruturais e óticas dos materiais produzidos. São estudadas as características luminescentes de matrizes de zircónia (ZrO2) e zircónia estabilizada com ítrio (YSZ) dopadas com vários iões lantanídeos (Ce3+ (4f1), Pr3+ (4f2), Sm3+ (4f5), Eu3+ (4f6), Tb3+ (4f8), Dy3+ (4f9), Er3+ (4f11), Tm3+ (4f12), Yb3+ (4f13)) e co-dopadas com Er3+,Yb3+ e Tm3+,Yb3+. Para além da luminescência de Stokes, foi avaliada e discutida a emissão anti-Stokes (upconversion e radiação de corpo negro) sob excitação no infravermelho. A comparação da luminescência em materiais com diferentes dimensões permitiu analisar o efeito do tamanho nas propriedades luminescentes dos iões dopantes. A discussão do trabalho é acompanhada por uma integração dos resultados visando as aplicações destes materiais luminescentes em emissores do estado sólido, biossensores e sensores de pressão.
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Books on the topic "Solution Combustion Synthesi"

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González-Cortés, Sergio L. Solution Combustion Synthesis of Nanostructured Solid Catalysts for Sustainable Chemistry. WORLD SCIENTIFIC (EUROPE), 2020. http://dx.doi.org/10.1142/q0257.

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Gonzalez-Cortes, Sergio. Solution Combustion Synthesis of Nanostructured Solid Catalysts for Sustainable Chemistry. World Scientific Publishing UK Limited, 2020.

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Book chapters on the topic "Solution Combustion Synthesi"

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Yermekova, Zhanna, German Trusov, and Sergey I. Roslyakov. "Spray Solution Combustion Synthesis of NiCu Hollow Spheres." In Lecture Notes in Mechanical Engineering, 11–17. Singapore: Springer Singapore, 2022. http://dx.doi.org/10.1007/978-981-16-9632-9_2.

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Zhang, Cheng, Yi Kun Liao, and Dan Yu Jiang. "Synthesis of Ultrafine GSAG:Ce Phosphor by Solution Combustion." In High-Performance Ceramics V, 386–87. Stafa: Trans Tech Publications Ltd., 2008. http://dx.doi.org/10.4028/0-87849-473-1.386.

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Bansal, Narottam P., and Zhimin Zhong. "Synthesis of Sm0.5Sr0.5CoO3-Xand La0.6Sr0.4CoO3-XNanopowders by Solution Combustion Process." In Progress in Nanotechnology, 103–12. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2014. http://dx.doi.org/10.1002/9780470588246.ch17.

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Bera, Parthasarathi, and Singanahally T. Aruna. "Solution Combustion Synthesis, Characterization, and Catalytic Properties of Oxide Materials." In Nanotechnology in Catalysis, 91–118. Weinheim, Germany: Wiley-VCH Verlag GmbH & Co. KGaA, 2017. http://dx.doi.org/10.1002/9783527699827.ch5.

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Puszynski, Jan A., Shivanee R. Dargar, and Berthold E. Liebig. "Combustion Synthesis of Ceramic Composites and Solid Solutions from Nanoreactants." In Ceramic Transactions Series, 11–21. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2012. http://dx.doi.org/10.1002/9781118407820.ch2.

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Aruna, S. T., and M. Shilpa. "Solution Combustion Synthesis of Calcium Phosphate-Based Bioceramic Powders for Biomedical Applications." In Nanomaterials and Their Biomedical Applications, 175–96. Singapore: Springer Singapore, 2021. http://dx.doi.org/10.1007/978-981-33-6252-9_7.

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Yilmaz, Esma, M. Seref Sonmez, Bora Derin, Filiz Cinar Sahin, and Onuralp Yucel. "Synthesis of Mn2O3 Nanopowders with Urea and Citric Acid by Solution Combustion Route." In TMS 2017 146th Annual Meeting & Exhibition Supplemental Proceedings, 39–46. Cham: Springer International Publishing, 2017. http://dx.doi.org/10.1007/978-3-319-51493-2_5.

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Jithin, P. V., and Joji Kurian. "Structural Study of Ethylene Glycol-Assisted Solution Combustion Synthesis of Strontium Doped LaMnO3." In Nanostructured Smart Materials, 159–69. First edition.: Apple Academic Press, 2021. http://dx.doi.org/10.1201/9781003130468-10.

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Jung, Choong Hwan, Ji Yeon Park, and Woo Seog Ryu. "Synthesis and Dilatometric Study of Ca(Sr, La)TiO3 Prepared by Solution Combustion Synthesis (SCS)." In Solid State Phenomena, 107–10. Stafa: Trans Tech Publications Ltd., 2007. http://dx.doi.org/10.4028/3-908451-27-2.107.

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Wang, C. M., and S. L. Chung. "Dye-Sensitized Solar Cell Using a Tio2 Nanocrystalline Film Electrode Prepared by Solution Combustion Synthesis." In Proceedings of ISES World Congress 2007 (Vol. I – Vol. V), 1361–65. Berlin, Heidelberg: Springer Berlin Heidelberg, 2008. http://dx.doi.org/10.1007/978-3-540-75997-3_277.

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Conference papers on the topic "Solution Combustion Synthesi"

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Sai Kumar, V. Sesha, K. Venkateswara Rao, T. Krishnaveni, A. Shiva Kishore Goud, and P. Ranjith Reddy. "Solution combustion synthesis and characterization of nanosized bismuth ferrite." In SOLID STATE PHYSICS: Proceedings of the 56th DAE Solid State Physics Symposium 2011. AIP, 2012. http://dx.doi.org/10.1063/1.4710018.

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Menon, Sumithra Sivadas, R. Anitha, Bhavana Gupta, K. Baskar, and Shubra Singh. "Synthesis of GaN:ZnO solid solution by solution combustion method and characterization for photocatalytic application." In DAE SOLID STATE PHYSICS SYMPOSIUM 2015. Author(s), 2016. http://dx.doi.org/10.1063/1.4947679.

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Patil, Sarika P., Shital P. Patil, V. R. Puri, and L. D. Jadhav. "Synthesis and characterization of pure Cu and CuO nano particles by solution combustion synthesis." In PROCEEDING OF INTERNATIONAL CONFERENCE ON RECENT TRENDS IN APPLIED PHYSICS AND MATERIAL SCIENCE: RAM 2013. AIP, 2013. http://dx.doi.org/10.1063/1.4810699.

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Ullaha, Sana, Fabio De Matteis, Rita Branquinho, Elvira Fortunato, Rodrigo Martins, and Ivan Davoli. "A combination of solution synthesis & solution combustion synthesis for highly conducting and transparent Aluminum Zinc Oxide thin films." In 2015 IEEE 15th International Conference on Nanotechnology (IEEE-NANO). IEEE, 2015. http://dx.doi.org/10.1109/nano.2015.7388919.

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Basha, Md Hussain, N. O. Gopal, J. L. Rao, H. Nagabhushana, B. M. Nagabhushana, and R. P. S. Chakradhar. "Development and characterization of Mn2+-doped MgO nanoparticles by solution combustion synthesis." In NANOFORUM 2014. AIP Publishing LLC, 2015. http://dx.doi.org/10.1063/1.4917793.

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Verma, Naveen, Bernabe Mari, Krishan Chander Singh, Jitender Jindal, Miguel Mollar, and Suprabha Yadav. "Luminescence properties of ZnMoO4:Eu3+:Y3+ materials synthesized by solution combustion synthesis method." In 5TH NATIONAL CONFERENCE ON THERMOPHYSICAL PROPERTIES: (NCTP‐09). American Institute of Physics, 2016. http://dx.doi.org/10.1063/1.4945242.

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Verma, Naveen, Bernabe Mari, Krishan Chander Singh, Jitender Jindal, Miguel Mollar, and Suprabha Yadav. "Luminescence properties of ZnMoO4:Eu3+:Y3+ materials synthesized by solution combustion synthesis method." In 5TH NATIONAL CONFERENCE ON THERMOPHYSICAL PROPERTIES: (NCTP‐09). American Institute of Physics, 2016. http://dx.doi.org/10.1063/1.4945250.

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Nehru, L. C., and C. Sanjeeviraja. "Microwave-assisted solution combustion synthesis of nanostructured Zn[sub 2]SnO[sub 4]." In PROCEEDING OF INTERNATIONAL CONFERENCE ON RECENT TRENDS IN APPLIED PHYSICS AND MATERIAL SCIENCE: RAM 2013. AIP, 2013. http://dx.doi.org/10.1063/1.4810090.

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Thomas, Nygil, Dyna Maria Michael, Jasmine Thomas, and Ebin Sebastian. "Ultra fast synthesis of nanocrystalline metal oxides using microwave assisted solution combustion method." In 16TH INTERNATIONAL CONFERENCE ON CONCENTRATOR PHOTOVOLTAIC SYSTEMS (CPV-16). AIP Publishing, 2020. http://dx.doi.org/10.1063/5.0029898.

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Ziegler, D., A. Marchisio, G. Ercolino, S. Specchia, and J. M. Tulliani. "P1GS.19 - Cobalt spinel via solution combustion synthesis as an ammonia sensing material." In 17th International Meeting on Chemical Sensors - IMCS 2018. AMA Service GmbH, Von-Münchhausen-Str. 49, 31515 Wunstorf, Germany, 2018. http://dx.doi.org/10.5162/imcs2018/p1gs.19.

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