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Journal articles on the topic 'Single particle ICP-MS/MS'

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Author: Grafiati

Published: 31 August 2024

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1

Bustos, Antonio R. Montoro, and Michael R. Winchester. "Single-particle-ICP-MS advances." Analytical and Bioanalytical Chemistry 408, no. 19 (May 21, 2016): 5051–52. http://dx.doi.org/10.1007/s00216-016-9638-1.

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2

Mitrano, Denise M., Angela Barber, Anthony Bednar, Paul Westerhoff, Christopher P. Higgins, and James F. Ranville. "Silver nanoparticle characterization using single particle ICP-MS (SP-ICP-MS) and asymmetrical flow field flow fractionation ICP-MS (AF4-ICP-MS)." Journal of Analytical Atomic Spectrometry 27, no. 7 (2012): 1131. http://dx.doi.org/10.1039/c2ja30021d.

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3

Correia, Manuel, Toni Uusimäki, Allan Philippe, and Katrin Loeschner. "Challenges in Determining the Size Distribution of Nanoparticles in Consumer Products by Asymmetric Flow Field-Flow Fractionation Coupled to Inductively Coupled Plasma-Mass Spectrometry: The Example of Al2O3, TiO2, and SiO2 Nanoparticles in Toothpaste." Separations 5, no. 4 (November 27, 2018): 56. http://dx.doi.org/10.3390/separations5040056.

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According to the current European regulation on cosmetics, any ingredient present as a nanomaterial should be indicated in the ingredient list. There is a need for analytical methods capable of determining the size of the relevant ingredients and thus assessing if these are nanomaterials or not. An analytical method based on asymmetric flow field-flow fractionation (AF4) and inductively coupled plasma-mass spectrometry (ICP-MS) was developed to determine the size of particles present in a commercial toothpaste. Multi-angle light scattering (MALS) was used for on-line size determination. The number-based particle size distributions (PSDs) of the particles were retrieved upon mathematical conversion of the mass-based PSDs recovered from the AF4-ICP-MS fractograms. AF4-ICP-MS allowed to separate and detect Al2O3 and TiO2 particles in the toothpaste and to retrieve a correct TiO2 number-based PSD. The potential presence of particles in the lower size range of the Al2O3 mass-based PSD had a strong impact on sizing and nanomaterial classification upon conversion. AF4 coupled with ICP-MS and MALS was found to be a powerful approach for characterization of different particles in a multiple-particle system such as toothpaste. Confirmation of particle size by a secondary method such as single particle ICP-MS or hydrodynamic chromatography was crucial.

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4

Yongyang, Su, Wang Wei, Li Zhiming, Deng Hu, Zhou Guoqing, Xu Jiang, and Ren Xiangjun. "Direct detection and isotope analysis of individual particles in suspension by single particle mode MC-ICP-MS for nuclear safety." Journal of Analytical Atomic Spectrometry 30, no. 5 (2015): 1184–90. http://dx.doi.org/10.1039/c4ja00339j.

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5

Walbrück, Katharina, Fabian Kuellmer, Steffen Witzleben, and Klaus Guenther. "Synthesis and Characterization of PVP-Stabilized Palladium Nanoparticles by XRD, SAXS, SP-ICP-MS, and SEM." Journal of Nanomaterials 2019 (April 17, 2019): 1–7. http://dx.doi.org/10.1155/2019/4758108.

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Due to increased emissions of palladium nanoparticles in recent years, it is important to develop analytical techniques to characterize these particles. The synthesis of defined and stable particles plays a key role in this process, as there are not many materials commercially available yet which could act as reference materials. Polyvinylpyrrolidone- (PVP-) stabilized palladium nanoparticles were synthesized through the reduction of palladium chloride by tetraethylene glycol (TEG) in the presence of KOH. Four different methods were used for particle size analysis of the palladium nanoparticles. Palladium suspensions were analyzed by scanning electron microscopy (SEM), small angle X-ray scattering (SAXS), single-particle ICP-MS (SP-ICP-MS), and X-ray diffraction (XRD). Secondary particles between 30 nm and 130 nm were detected in great compliance with SAXS and SP-ICP-MS. SEM analysis showed that the small particulates tend to form agglomerates.

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6

Kajner, Gyula, Ádám Bélteki, Martin Cseh, Zsolt Geretovszky, Tibor Ajtai, Lilla Barna, Mária A. Deli, Bernadett Pap, Gergely Maróti, and Gábor Galbács. "Design, Optimization, and Application of a 3D-Printed Polymer Sample Introduction System for the ICP-MS Analysis of Nanoparticles and Cells." Nanomaterials 13, no. 23 (November 25, 2023): 3018. http://dx.doi.org/10.3390/nano13233018.

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Commonly used sample introduction systems for inductively coupled plasma mass spectrometry (ICP-MS) are generally not well-suited for single particle ICP-MS (spICP-MS) applications due to their high sample requirements and low efficiency. In this study, the first completely 3D-printed, polymer SIS was developed to facilitate spICP-MS analysis. The system is based on a microconcentric pneumatic nebulizer and a single-pass spray chamber with an additional sheath gas flow to further facilitate the transport of larger droplets or particles. The geometry of the system was optimized using numerical simulations. Its aerosol characteristics and operational conditions were studied via optical particle counting and a course of spICP-MS measurements, involving nanodispersions and cell suspensions. In a comparison of the performance of the new and the standard (quartz microconcentric nebulizer plus a double-pass spray chamber) systems, it was found that the new sample introduction system has four times higher particle detection efficiency, significantly better signal-to-noise ratio, provides ca. 20% lower size detection limit, and allows an extension of the upper limit of transportable particle diameters to about 25 µm.

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7

Meng, Ziwei, Lingna Zheng, Hao Fang, Pu Yang, Bing Wang, Liang Li, Meng Wang, and Weiyue Feng. "Single Particle Inductively Coupled Plasma Time-of-Flight Mass Spectrometry—A Powerful Tool for the Analysis of Nanoparticles in the Environment." Processes 11, no. 4 (April 17, 2023): 1237. http://dx.doi.org/10.3390/pr11041237.

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Single-particle inductively coupled plasma-mass spectrometry (SP-ICP-MS) has emerged as an important tool for the characterization of inorganic nanoparticles (NPs) in the environment. Although most SP-ICP-MS applications rely on the quadrupole ICP-MS (ICP-QMS), it is limited by the slow scanning speed of the quadrupole. Recent advancements in instrumentation have led to the development of inductively coupled plasma time-of-flight mass spectrometry (ICP-TOF-MS) which offers a viable solution. In this review, we discuss the recent advances in instrumentation and methodology of ICP-TOF-MS, followed by a detailed discussion of the applications of SP-ICP-TOFMS in analyzing NPs in the environment. SP-ICP-TOFMS has the potential to identify and quantify both anthropogenic and natural NPs in the environment, providing valuable insights into their occurrence, fate, behavior, and potential environmental risks.

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8

Franze, Bastian, Ingo Strenge, and Carsten Engelhard. "Separation and detection of gold nanoparticles with capillary electrophoresis and ICP-MS in single particle mode (CE-SP-ICP-MS)." Journal of Analytical Atomic Spectrometry 32, no. 8 (2017): 1481–89. http://dx.doi.org/10.1039/c7ja00040e.

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9

Rua-Ibarz, Ana, Eduardo Bolea-Fernandez, Guillermo Pozo, Xochitl Dominguez-Benetton, Frank Vanhaecke, and Kristof Tirez. "Characterization of iron oxide nanoparticles by means of single-particle ICP-mass spectrometry (SP-ICP-MS) – chemical versus physical resolution to overcome spectral overlap." Journal of Analytical Atomic Spectrometry 35, no. 9 (2020): 2023–32. http://dx.doi.org/10.1039/d0ja00183j.

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In this work, different single-particle ICP-MS (SP-ICP-MS) approaches, relying on either chemical or physical resolution to overcome spectral overlap, have been assessed for their utility in the characterization of iron oxide nanoparticles (IONPs).

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10

Venkatesan, Arjun K., Blanca T. Rodríguez, Aurelie R. Marcotte, Xiangyu Bi, Jared Schoepf, James F. Ranville, Pierre Herckes, and Paul Westerhoff. "Using single-particle ICP-MS for monitoring metal-containing particles in tap water." Environmental Science: Water Research & Technology 4, no. 12 (2018): 1923–32. http://dx.doi.org/10.1039/c8ew00478a.

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11

Han, Juan, Xu Wu, Julia Xiaojun Zhao, and David T. Pierce. "An Unprecedented Metal Distribution in Silica Nanoparticles Determined by Single-Particle Inductively Coupled Plasma Mass Spectrometry." Nanomaterials 14, no. 7 (April 6, 2024): 637. http://dx.doi.org/10.3390/nano14070637.

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Metal-containing nanoparticles are now common in applications ranging from catalysts to biomarkers. However, little research has focused on per-particle metal content in multicomponent nanoparticles. In this work, we used single-particle inductively coupled plasma mass spectrometry (ICP-MS) to determine the per-particle metal content of silica nanoparticles doped with tris(2,2′-bipyridyl)ruthenium(II). Monodispersed silica nanoparticles with varied Ru doping levels were prepared using a water-in-oil microemulsion method. These nanoparticles were characterized using common bulk-sample methods such as absorbance spectroscopy and conventional ICP-MS, and also with single-particle ICP-MS. The results showed that averaged concentrations of metal dopant measured per-particle by single-particle ICP-MS were consistent with the bulk-sample methods over a wide range of dopant levels. However, the per-particle amount of metal varied greatly and did not adhere to the usual Gaussian distribution encountered with one-component nanoparticles, such as gold or silver. Instead, the amount of metal dopant per silica particle showed an unexpected geometric distribution regardless of the prepared doping levels. The results indicate that an unusual metal dispersal mechanism is taking place during the microemulsion synthesis, and they challenge a common assumption that doped silica nanoparticles have the same metal content as the average measured by bulk-sample methods.

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12

Jreije, Ibrahim, Agil Azimzada, Madjid Hadioui, and Kevin J. Wilkinson. "Measurement of CeO2 Nanoparticles in Natural Waters Using a High Sensitivity, Single Particle ICP-MS." Molecules 25, no. 23 (November 25, 2020): 5516. http://dx.doi.org/10.3390/molecules25235516.

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As the production and use of cerium oxide nanoparticles (CeO2 NPs) increases, so does the concern of the scientific community over their release into the environment. Single particle inductively coupled plasma mass spectrometry is emerging as one of the best techniques for NP detection and quantification; however, it is often limited by high size detection limits (SDL). To that end, a high sensitivity sector field ICP-MS (SF-ICP-MS) with microsecond dwell times (50 µs) was used to lower the SDL of CeO2 NPs to below 4.0 nm. Ag and Au NPs were also analyzed for reference. SF-ICP-MS was then used to detect CeO2 NPs in a Montreal rainwater at a concentration of (2.2 ± 0.1) × 108 L−1 with a mean diameter of 10.8 ± 0.2 nm; and in a St. Lawrence River water at a concentration of ((1.6 ± 0.3) × 109 L−1) with a higher mean diameter (21.9 ± 0.8 nm). SF-ICP-MS and single particle time of flight ICP-MS on Ce and La indicated that 36% of the Ce-containing NPs detected in Montreal rainwater were engineered Ce NPs.

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13

Barber, Angela, Sun Kly, Matthew G. Moffitt, Logan Rand, and James F. Ranville. "Coupling single particle ICP-MS with field-flow fractionation for characterizing metal nanoparticles contained in nanoplastic colloids." Environmental Science: Nano 7, no. 2 (2020): 514–24. http://dx.doi.org/10.1039/c9en00637k.

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Composite particles containing metallic nanoparticles in a polymer matrix, which simulate environmentally-transformed nanoparticles, are effectively characterized by combining field-flow fractionation with single particle ICP-MS.

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14

Guo, Xiaoman, Sina Alavi, Elham Dalir, Jingmin Dai, and Javad Mostaghimi. "Time-resolved particle image velocimetry and 3D simulations of single particles in the new conical ICP torch." Journal of Analytical Atomic Spectrometry 34, no. 3 (2019): 469–79. http://dx.doi.org/10.1039/c8ja00407b.

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15

Bolea-Fernandez, Eduardo, Diego Leite, Ana Rua-Ibarz, Lieve Balcaen, Maite Aramendía, Martín Resano, and Frank Vanhaecke. "Characterization of SiO2nanoparticles by single particle-inductively coupled plasma-tandem mass spectrometry (SP-ICP-MS/MS)." Journal of Analytical Atomic Spectrometry 32, no. 11 (2017): 2140–52. http://dx.doi.org/10.1039/c7ja00138j.

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16

Kaňa, Antonín, Martin Loula, Richard Koplík, Magda Vosmanská, and Oto Mestek. "Peak bordering for ultrafast single particle analysis using ICP-MS." Talanta 197 (May 2019): 189–98. http://dx.doi.org/10.1016/j.talanta.2019.01.030.

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17

Montaño, Manuel D., John W. Olesik, Angela G. Barber, Katie Challis, and James F. Ranville. "Single Particle ICP-MS: Advances toward routine analysis of nanomaterials." Analytical and Bioanalytical Chemistry 408, no. 19 (June 23, 2016): 5053–74. http://dx.doi.org/10.1007/s00216-016-9676-8.

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18

Joo, Nayoung, and H. B. Lim. "Density Determination of Au Nanoparticles Using Single Particle ICP‐MS." Bulletin of the Korean Chemical Society 40, no. 11 (October 15, 2019): 1087–92. http://dx.doi.org/10.1002/bkcs.11875.

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19

Ferraris, Francesca, Carlos Adelantado, Andrea Raggi, Sara Savini, Mohammed Zougagh, Ángel Ríos, and Francesco Cubadda. "An ICP-MS-Based Analytical Strategy for Assessing Compliance with the Ban of E 171 as a Food Additive on the EU Market." Nanomaterials 13, no. 22 (November 15, 2023): 2957. http://dx.doi.org/10.3390/nano13222957.

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A method was developed for the determination of total titanium in food and food supplements by inductively coupled plasma mass spectrometry (ICP-MS) after microwave-assisted acid digestion of samples. Five food supplements, including one certified reference material, and 15 food products were used for method development. Key factors affecting the analytical results, such as the composition of the acid mixture for sample digestion and the bias from spectral interferences on the different titanium isotopes, were investigated. Resolution of interferences was achieved by ICP-MS/MS with ammonia adduct formation and viable conditions for control laboratories equipped with standard quadrupole instruments were identified. The method was successfully validated and enables rapid screening of samples subject to confirmatory analysis for the presence of TiO2 particles. For the latter, single-particle ICP-MS (spICP-MS) analysis after chemical extraction of the particles was used. The two methods establish a viable analytical strategy for assessing the absence of titania particles in food products on the EU market following the E 171 ban as a food additive.

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20

Trujillo, Celia, Josefina Pérez-Arantegui, Ryszard Lobinski, and Francisco Laborda. "Improving the Detectability of Microplastics in River Waters by Single Particle Inductively Coupled Plasma Mass Spectrometry." Nanomaterials 13, no. 10 (May 9, 2023): 1582. http://dx.doi.org/10.3390/nano13101582.

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Detection of microplastics in environmental samples requires fast, sensitive and selective analytical techniques, both in terms of the size of the microparticles and their concentration. Single particle inductively coupled plasma mass spectrometry (SP-ICP-MS) allows the detection of plastic particles down to ca. 1 µm and down to concentrations of 100 particles per mL. In SP-ICP-MS, detection of carbon-containing particles is hampered by the presence of other forms of carbon (carbonates, organic matter, microorganisms…). An acidic pre-treatment of river water samples with 10% (v/v) nitric acid for 24 h allowed the reduction of the presence of dissolved carbon to ultrapure water levels and the digestion of potential microorganisms in the samples, recovering polystyrene microparticles up to 80%. Carbon-containing particles were detected in most of the samples analysed from Spanish and French Pyrenean rivers. The presence of microplastics in these samples was confirmed by Raman microscopy and their morphology was defined by electron microscopy combined with energy-dispersive X-ray spectroscopy. The developed SP-ICP-MS method is suitable for the rapid screening of river waters for the presence of microplastics, which can then be analysed by inherently slower but more selective techniques (e.g., Raman microscopy).

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21

Mozhayeva, Darya, and Carsten Engelhard. "A critical review of single particle inductively coupled plasma mass spectrometry – A step towards an ideal method for nanomaterial characterization." Journal of Analytical Atomic Spectrometry 35, no. 9 (2020): 1740–83. http://dx.doi.org/10.1039/c9ja00206e.

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The critical review discusses instrumental developments in single particle ICP-MS (spICP-MS) of recent years step-by-step. Nanoanalysis application papers from the literature are summarized in a tabular form including important experimental parameters.

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22

Lee, Wan-Waan, and Wing-Tat Chan. "Calibration of single-particle inductively coupled plasma-mass spectrometry (SP-ICP-MS)." Journal of Analytical Atomic Spectrometry 30, no. 6 (2015): 1245–54. http://dx.doi.org/10.1039/c4ja00408f.

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23

Hebert, Deja, Jenny Nelson, Brooke N. Diehl, and Phoebe Zito. "Single-Particle ICP-MS/MS Application for Routine Screening of Nanoparticles Present in Powder-Based Facial Cosmetics." Nanomaterials 13, no. 19 (September 30, 2023): 2681. http://dx.doi.org/10.3390/nano13192681.

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The short- and long-term impacts of nanoparticles (NPs) in consumer products are not fully understood. Current European Union (EU) regulations enforce transparency on products containing NPs in cosmetic formulations; however, those set by the U.S. Food and Drug Administration are lacking. This study demonstrates the potential of single-particle inductively coupled plasma tandem mass spectrometry (spICP-MS/MS) as a screening method for NPs present in powder-based facial cosmetics (herein referred to as FCs). A proposed spICP-MS/MS method is presented along with recommended criteria to confirm particle presence and particle detection thresholds in seven FCs. FC products of varying colors, market values, and applications were analyzed for the presence of Bi, Cr, Mg, Mn, Pb, Sn, Ag, Al, and Zn NPs based on their ingredient lists as well as those commonly used in cosmetic formulations. The presence of NPs smaller than 100 nm was observed in all FC samples, and no correlations with their presence and market value were observed. Here, we report qualitative and semi-quantitative results for seven FC samples ranging in color, brand, and shimmer.

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24

Newman, Karla, Chris Metcalfe, Jonathan Martin, Holger Hintelmann, Phil Shaw, and Ariane Donard. "Improved single particle ICP-MS characterization of silver nanoparticles at environmentally relevant concentrations." Journal of Analytical Atomic Spectrometry 31, no. 10 (2016): 2069–77. http://dx.doi.org/10.1039/c6ja00221h.

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25

Manard, Benjamin T., Veronica C. Bradley, C. Derrick Quarles, Lyndsey Hendriks, Daniel R. Dunlap, Cole R. Hexel, Patrick Sullivan, and Hunter B. Andrews. "Towards Automated and High-Throughput Quantitative Sizing and Isotopic Analysis of Nanoparticles via Single Particle-ICP-TOF-MS." Nanomaterials 13, no. 8 (April 9, 2023): 1322. http://dx.doi.org/10.3390/nano13081322.

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The work described herein assesses the ability to characterize gold nanoparticles (Au NPs) of 50 and 100 nm, as well as 60 nm silver shelled gold core nanospheres (Au/Ag NPs), for their mass, respective size, and isotopic composition in an automated and unattended fashion. Here, an innovative autosampler was employed to mix and transport the blanks, standards, and samples into a high-efficiency single particle (SP) introduction system for subsequent analysis by inductively coupled plasma–time of flight–mass spectrometry (ICP-TOF-MS). Optimized NP transport efficiency into the ICP-TOF-MS was determined to be >80%. This combination, SP-ICP-TOF-MS, allowed for high-throughput sample analysis. Specifically, 50 total samples (including blanks/standards) were analyzed over 8 h, to provide an accurate characterization of the NPs. This methodology was implemented over the course of 5 days to assess its long-term reproducibility. Impressively, the in-run and day-to-day variation of sample transport is assessed to be 3.54 and 9.52% relative standard deviation (%RSD), respectively. The determination of Au NP size and concentration was of <5% relative difference from the certified values over these time periods. Isotopic characterization of the 107Ag/109Ag particles (n = 132,630) over the course of the measurements was determined to be 1.0788 ± 0.0030 with high accuracy (0.23% relative difference) when compared to the multi-collector–ICP-MS determination.

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26

Gundlach-Graham, Alexander, and Kamyar Mehrabi. "Monodisperse microdroplets: a tool that advances single-particle ICP-MS measurements." Journal of Analytical Atomic Spectrometry 35, no. 9 (2020): 1727–39. http://dx.doi.org/10.1039/d0ja00213e.

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Controlled introduction of monodisperse microdroplets is tool that can be used to improve single-particle ICP-MS measurements. Microdroplet-based signals are used for calibration, and also enable us to devise and validate data analysis strategies.

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27

Sötebier, Carina A., Daniel J. Kutscher, Lothar Rottmann, Norbert Jakubowski, Ulrich Panne, and Jörg Bettmer. "Combination of single particle ICP-QMS and isotope dilution analysis for the determination of size, particle number and number size distribution of silver nanoparticles." Journal of Analytical Atomic Spectrometry 31, no. 10 (2016): 2045–52. http://dx.doi.org/10.1039/c6ja00137h.

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28

Shaw, P., and A. Donard. "Nano-particle analysis using dwell times between 10 μs and 70 μs with an upper counting limit of greater than 3 × 107 cps and a gold nanoparticle detection limit of less than 10 nm diameter." Journal of Analytical Atomic Spectrometry 31, no. 6 (2016): 1234–42. http://dx.doi.org/10.1039/c6ja00047a.

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29

Clark, Nathaniel J., Robert Clough, David Boyle, and Richard D. Handy. "Development of a suitable detection method for silver nanoparticles in fish tissue using single particle ICP-MS." Environmental Science: Nano 6, no. 11 (2019): 3388–400. http://dx.doi.org/10.1039/c9en00547a.

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A strong alkali extraction technique and suitable single particle ICP-MS method is described for the routine quantifying of particle number concentration, particle size and particle mass concentration for silver nanomaterials in fish tissue.

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30

Cosmi, Marzia, Nathaly Gonzalez-Quiñonez, Pablo Tejerina Díaz, Ángel Manteca, Elisa Blanco-González, Jörg Bettmer, María Montes-Bayón, and Mario Corte-Rodriguez. "Evaluation of nanodebris produced by in vitro degradation of titanium-based dental implants in the presence of bacteria using single particle and single cell inductively coupled plasma mass spectrometry." Journal of Analytical Atomic Spectrometry 36, no. 9 (2021): 2007–16. http://dx.doi.org/10.1039/d1ja00154j.

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31

Kantorová, Věra, Martin Loula, Antonín Kaňa, and Oto Mestek. "Determination of silver nanoparticles in cosmetics using single particle ICP-MS." Chemical Papers 75, no. 11 (July 8, 2021): 5895–905. http://dx.doi.org/10.1007/s11696-021-01763-z.

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32

Huang, Yingyan, Judy Tsz-Shan Lum, and Kelvin Sze-Yin Leung. "Single particle ICP-MS combined with internal standardization for accurate characterization of polydisperse nanoparticles in complex matrices." Journal of Analytical Atomic Spectrometry 35, no. 10 (2020): 2148–55. http://dx.doi.org/10.1039/d0ja00180e.

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33

Lockwood, Thomas E., Raquel Gonzalez de Vega, and David Clases. "An interactive Python-based data processing platform for single particle and single cell ICP-MS." Journal of Analytical Atomic Spectrometry 36, no. 11 (2021): 2536–44. http://dx.doi.org/10.1039/d1ja00297j.

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A data processing platform was developed for the analysis of single particle and single cell ICP-MS data sets. All functions are embedded in a GUI and enable signal recognition, accumulation and calibration via dedicated pathways and filters.

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34

Tuoriniemi, Jani, Geert Cornelis, and Martin Hassellöv. "A new peak recognition algorithm for detection of ultra-small nano-particles by single particle ICP-MS using rapid time resolved data acquisition on a sector-field mass spectrometer." Journal of Analytical Atomic Spectrometry 30, no. 8 (2015): 1723–29. http://dx.doi.org/10.1039/c5ja00113g.

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35

Meermann, Björn, and Francisco Laborda. "Analysis of nanomaterials by field-flow fractionation and single particle ICP-MS." Journal of Analytical Atomic Spectrometry 30, no. 6 (2015): 1226–28. http://dx.doi.org/10.1039/c5ja90019k.

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36

Holbrook, Timothy Ronald, Doriane Gallot-Duval, Thorsten Reemtsma, and Stephan Wagner. "Machine learning: our future spotlight into single-particle ICP-ToF-MS analysis." Journal of Analytical Atomic Spectrometry 36, no. 12 (2021): 2684–94. http://dx.doi.org/10.1039/d1ja00213a.

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Using the multi-element capabilities of single-particle ICP-ToF-MS in combination with a laser ablation and machine learning algorithms, environmentally relevant road runoff samples were characterized.

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37

Lankone, Ronald S., Jingjing Wang, James F. Ranville, and D. Howard Fairbrother. "Photodegradation of polymer-CNT nanocomposites: effect of CNT loading and CNT release characteristics." Environmental Science: Nano 4, no. 4 (2017): 967–82. http://dx.doi.org/10.1039/c6en00669h.

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38

Toncelli, Claudio, Kyriaki Mylona, Manolis Tsapakis, and Spiros A. Pergantis. "Flow injection with on-line dilution and single particle inductively coupled plasma – mass spectrometry for monitoring silver nanoparticles in seawater and in marine microorganisms." Journal of Analytical Atomic Spectrometry 31, no. 7 (2016): 1430–39. http://dx.doi.org/10.1039/c6ja00011h.

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39

Hendriks, Lyndsey, Benita Ramkorun-Schmidt, Alexander Gundlach-Graham, Julian Koch, Robert N. Grass, Norbert Jakubowski, and Detlef Günther. "Single-particle ICP-MS with online microdroplet calibration: toward matrix independent nanoparticle sizing." Journal of Analytical Atomic Spectrometry 34, no. 4 (2019): 716–28. http://dx.doi.org/10.1039/c8ja00397a.

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Microdroplets with known concentrations of element standards are introduced concomitant with NP-containing solutions into the ICP to provide online matrix-matched calibration of analyte NPs for single-particle-ICP-TOFMS.

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40

Zhang, Huiling, Yuxiong Huang, Jianqiang Gu, Arturo Keller, Yuwei Qin, Yue Bian, Kun Tang, Xiaolei Qu, Rong Ji, and Lijuan Zhao. "Single particle ICP-MS and GC-MS provide a new insight into the formation mechanisms during the green synthesis of AgNPs." New Journal of Chemistry 43, no. 9 (2019): 3946–55. http://dx.doi.org/10.1039/c8nj06291a.

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41

Semenova, Daria, and Yuliya E. Silina. "The Role of Nanoanalytics in the Development of Organic-Inorganic Nanohybrids—Seeing Nanomaterials as They Are." Nanomaterials 9, no. 12 (November 23, 2019): 1673. http://dx.doi.org/10.3390/nano9121673.

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The functional properties of organic-inorganic (O-I) hybrids can be easily tuned by combining system components and parameters, making this class of novel nanomaterials a crucial element in various application fields. Unfortunately, the manufacturing of organic-inorganic nanohybrids still suffers from mechanical instability and insufficient synthesis reproducibility. The control of the composition and structure of nanosurfaces themselves is a specific analytical challenge and plays an important role in the future reproducibility of hybrid nanomaterials surface properties and response. Therefore, appropriate and sufficient analytical methodologies and technical guidance for control of their synthesis, characterization and standardization of the final product quality at the nanoscale level should be established. In this review, we summarize and compare the analytical merit of the modern analytical methods, viz. Fourier transform infrared spectroscopy (FTIR), RAMAN spectroscopy, surface plasmon resonance (SPR) and several mass spectrometry (MS)-based techniques, that is, inductively coupled plasma mass spectrometry (ICP-MS), single particle ICP-MS (sp-ICP-MS), laser ablation coupled ICP-MS (LA-ICP-MS), time-of-flight secondary ion mass spectrometry (TOF-SIMS), liquid chromatography mass spectrometry (LC-MS) utilized for characterization of O-I nanohybrids. Special attention is given to laser desorption ionization mass spectrometry (LDI-MS) as a reliable nanoanalytical platform for characterization of O-I hybrid nanomaterials, their quality, design verification and validation.

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Navratilova, Jana, Antonia Praetorius, Andreas Gondikas, Willi Fabienke, Frank von der Kammer, and Thilo Hofmann. "Detection of Engineered Copper Nanoparticles in Soil Using Single Particle ICP-MS." International Journal of Environmental Research and Public Health 12, no. 12 (December 10, 2015): 15756–68. http://dx.doi.org/10.3390/ijerph121215020.

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Loula, Martin, Antonín Kaňa, and Oto Mestek. "Non-spectral interferences in single-particle ICP-MS analysis: An underestimated phenomenon." Talanta 202 (September 2019): 565–71. http://dx.doi.org/10.1016/j.talanta.2019.04.073.

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Lee, Sungyun, Xiangyu Bi, Robert B. Reed, James F. Ranville, Pierre Herckes, and Paul Westerhoff. "Nanoparticle Size Detection Limits by Single Particle ICP-MS for 40 Elements." Environmental Science & Technology 48, no. 17 (August 22, 2014): 10291–300. http://dx.doi.org/10.1021/es502422v.

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Long, Chen-lu, Zhao-guang Yang, Yuan Yang, Hai-pu Li, and Qiang Wang. "Determination of gold nanoparticles in natural water using single particle-ICP-MS." Journal of Central South University 23, no. 7 (July 2016): 1611–17. http://dx.doi.org/10.1007/s11771-016-3215-9.

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SUZUKI, Yoshinari, Masae HARIMOTO, Miki TAKAHASHI, Hiroshi AKIYAMA, Akihiko HIROSE, and Tomoaki TSUTSUMI. "Analysis of Silver-containing Nanoparticles in Oysters Using Single-particle ICP-MS." Journal of Environmental Chemistry 34 (2024): 9–20. http://dx.doi.org/10.5985/jec.34.9.

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Strenge, I., and C. Engelhard. "Capabilities of fast data acquisition with microsecond time resolution in inductively coupled plasma mass spectrometry and identification of signal artifacts from millisecond dwell times during detection of single gold nanoparticles." Journal of Analytical Atomic Spectrometry 31, no. 1 (2016): 135–44. http://dx.doi.org/10.1039/c5ja00177c.

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Suwanroek, Wanida, Jitapa Sumranjit, Tuksadon Wutikhun, and Atitaya Siripinyanond. "Use of single particle inductively coupled plasma mass spectrometry for the study of zinc oxide nanoparticles released from fabric face masks." Journal of Analytical Atomic Spectrometry 37, no. 4 (2022): 759–67. http://dx.doi.org/10.1039/d1ja00447f.

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An analytical method based on single particle inductively coupled plasma mass spectrometry (SP-ICP-MS) was developed to study the release of ZnO nanoparticles from fabric face mask samples upon washing.

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Marigliano, Lucile, Bruno Grassl, Joanna Szpunar, Stéphanie Reynaud, and Javier Jiménez-Lamana. "Nanoplastic Labelling with Metal Probes: Analytical Strategies for Their Sensitive Detection and Quantification by ICP Mass Spectrometry." Molecules 26, no. 23 (November 24, 2021): 7093. http://dx.doi.org/10.3390/molecules26237093.

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The detection and quantification of nanoplastics in aquatic environments is one of the major challenges in environmental and analytical research nowadays. The use of common analytical techniques for this purpose is not only hampered by the size of nanoplastics, but also because they are mainly made of carbon. In addition, the expected concentrations in environmental samples are below the detection limit of the majority of analytical techniques. In this context, the great detection capabilities of Inductively Coupled Plasma Mass Spectrometry (ICP-MS) in its Single Particle mode (SP-ICP-MS) have made of this technique a good candidate for the analysis of nanoplastics. Since the monitoring of carbon by ICP-MS faces several difficulties, the use of metal tags, taking advantage of the great potential of nanoplastics to adsorb chemical compounds, has been proposed as an alternative. In this perspectives paper, three different strategies for the analysis of polystyrene (PS) nanoplastics by SP-ICP-MS based on the use of metals species (ions, hydrophobic organometallic compound, and nanoparticles) as tags are presented and discussed. Advantages and disadvantages of each strategy, which rely on the labelling process, are highlighted. The metal nanoparticles labelling strategy is shown as a promising tool for the detection and quantification of nanoplastics in aqueous matrices by SP-ICP-MS.

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Aureli, Federica, Maria Ciprotti, Marilena D’Amato, Emanueli do Nascimento da Silva, Stefano Nisi, Daniele Passeri, Angela Sorbo, Andrea Raggi, Marco Rossi, and Francesco Cubadda. "Determination of Total Silicon and SiO2 Particles Using an ICP-MS Based Analytical Platform for Toxicokinetic Studies of Synthetic Amorphous Silica." Nanomaterials 10, no. 5 (May 6, 2020): 888. http://dx.doi.org/10.3390/nano10050888.

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Synthetic amorphous silica (SAS), manufactured in pyrogenic or precipitated form, is a nanomaterial with a widespread use as food additive (E 551). Oral exposure to SAS results from its use in food and dietary supplements, pharmaceuticals and toothpaste. Recent evidence suggests that oral exposure to SAS may pose health risks and highlights the need to address the toxic potential of SAS as affected by the physicochemical characteristics of the different forms of SAS. For this aim, investigating SAS toxicokinetics is of crucial importance and an analytical strategy for such an undertaking is presented. The minimization of silicon background in tissues, control of contamination (including silicon release from equipment), high-throughput sample treatment, elimination of spectral interferences affecting inductively coupled plasma mass spectrometry (ICP-MS) silicon detection, and development of analytical quality control tools are the cornerstones of this strategy. A validated method combining sample digestion with silicon determination by reaction cell ICP-MS is presented. Silica particles are converted to soluble silicon by microwave dissolution with mixtures of HNO3, H2O2 and hydrofluoric acid (HF), whereas interference-free ICP-MS detection of total silicon is achieved by ion-molecule chemistry with limits of detection (LoDs) in the range 0.2–0.5 µg Si g−1 for most tissues. Deposition of particulate SiO2 in tissues is assessed by single particle ICP-MS.

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