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Journal articles on the topic 'Reversed phase chromatography'

Author: Grafiati

Published: 4 June 2021

Last updated: 19 February 2022

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1

Hanai, Toshihiko. "Quantitative Explanation of Retention Mechanisms in Reversed-phase Mode Liquid Chromatography, and Utilization of Typical Reversed-phase Liquid Chromatography for Drug Discovery." Current Chromatography 6, no. 1 (September 18, 2019): 52–64. http://dx.doi.org/10.2174/2213240606666190619120733.

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The retention mechanism in reversed-phase liquid chromatography was quantitatively described using log P (octanol-water partition coefficient). The hydrophobic (lipophilic) interaction liquid chromatography was then used to measure the hydrophobicity of a variety of compounds. Furthermore, the technique has been used as an analytical method to determine molecular properties during the drug discovery process. However, log P values cannot be applied to other chromatographic techniques. Therefore, the direct calculation of molecular interactions was proposed to describe the general retention mechanisms in chromatography. The retention mechanisms in reversed-phase liquid chromatography were quantitatively described in silico by using simple model compounds and phases. The competitive interactions between a bonded-phase and a solvent phase clearly demonstrated the retention mechanisms in reversed-phase liquid chromatography. Chromatographic behavior of acidic drugs on a pentyl-, an octyl-, and a hexenyl-phase was quantitatively described in the in silico analysis. Their retention was based on their hydrophobicity, and hydrogen bonding and electrostatic interaction were selectivity of the hexenyl-phase. This review focuses on the quantitative explanation of the retention mechanisms in reversed-phase liquid chromatography and the practical applications in drug discovery.

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2

Figge, H., A. Deege, J. Köhler, and G. Schumburg. "Stationary phases for reversed-phase liquid chromatography." Journal of Chromatography A 351 (January 1986): 393–408. http://dx.doi.org/10.1016/s0021-9673(01)83517-2.

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3

Le Mapihan, K., J. Vial, and A. Jardy. "Reversed-phase liquid chromatography testing." Journal of Chromatography A 1088, no. 1-2 (September 2005): 16–23. http://dx.doi.org/10.1016/j.chroma.2005.02.023.

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4

Cong, Jing Xiang, Shao Yan Wang, and Hong Gao. "Separation of Liquiritin by Two-Dimensional Liquid Chromatography." Advanced Materials Research 455-456 (January 2012): 1232–38. http://dx.doi.org/10.4028/www.scientific.net/amr.455-456.1232.

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Two-dimensional liquid chromatography (2DLC) is an important technology for the separation and analysis of complex samples. Liquiritin, an important active component in licorice, was chosen as the target compound and it was separated by three kinds of off-line 2DLC, i.e. size exclusion chromatography × reversed phase chromatography, normal phase × reversed phase chromatography and reversed phase chromatography × reversed phase chromatography (SEC×RP, NP×RP and RP×RP). The chromatographic conditions were selected and the 2D systems were combined. The results show that it is feasible to separate Liquiritin from licorice extract using 2DLC. Among the 2D modes mentioned above, the highest purity of Liquiritin was obtained in the RP×RP mode, and the concentration of Liquiritin was increased most significantly in the NP×RP mode.

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5

Melander, W. R., B. K. Chen, and Cs Horváth. "Mobile phase effects in reversed-phase chromatography." Journal of Chromatography A 318 (January 1985): 1–10. http://dx.doi.org/10.1016/s0021-9673(01)90659-4.

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6

Hernandez-Torres, Maria A., John S. Landy, and John G. Dorsey. "Reversed micellar mobile phases for normal-phase chromatography." Analytical Chemistry 58, no. 4 (April 1986): 744–47. http://dx.doi.org/10.1021/ac00295a020.

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7

Molíková, Martina, and Pavel Jandera. "Characterization of stationary phases for reversed-phase chromatography." Journal of Separation Science 33, no. 4-5 (February 2, 2010): 453–63. http://dx.doi.org/10.1002/jssc.200900699.

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8

Tsuchiya, Yoshiteru. "Reversed-phase high-performance liquid chromatography." Japan journal of water pollution research 11, no. 2 (1988): 83–89. http://dx.doi.org/10.2965/jswe1978.11.83.

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9

Sentell, Karen B., and John G. Dorsey. "Retention mechanisms in reversed-phase chromatography." Journal of Chromatography A 461 (January 1989): 193–207. http://dx.doi.org/10.1016/s0021-9673(00)94287-0.

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10

Petrović, S. M., and S. Lomić. "Selectivity in Reversed-Phase Liquid Chromatography." Journal of Liquid Chromatography 12, no. 1-2 (January 1989): 59–75. http://dx.doi.org/10.1080/01483918908049190.

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11

Nelis, H. J. C. F., and A. P. De Leenheer. "Reversed-phase liquid chromatography of astacene." Journal of Chromatography A 452 (October 1988): 535–42. http://dx.doi.org/10.1016/s0021-9673(01)81477-1.

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12

Agrawal, Roopali, Sateesh Belemkar, and Chandrakant Bonde. "Orthogonal Separations in Reversed-Phase Chromatography." Chromatographia 81, no. 4 (March 6, 2018): 565–73. http://dx.doi.org/10.1007/s10337-018-3494-4.

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13

Okada, Tetsuo. "Simultaneous cation and reversed-phase chromatography." Journal of Chromatography A 607, no. 1 (August 1992): 135–38. http://dx.doi.org/10.1016/0021-9673(92)87064-f.

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14

Tanaka, Nobuo, Kazuhiro Kimata, Ken Hosoya, Hironobu Miyanishi, and Takeo Araki. "Stationary phase effects in reversed-phase liquid chromatography." Journal of Chromatography A 656, no. 1-2 (December 1993): 265–87. http://dx.doi.org/10.1016/0021-9673(93)80805-i.

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15

Despotovic, Vesna, Nemanja Trisovic, Anamarija Mandic, Gordana Uscumlic, and Tatjana Djakovic-Sekulic. "Lipophilicity assessment of some 5,5-disubstituted hydantoins by the means of reversed phase liquid chromatography." Chemical Industry and Chemical Engineering Quarterly 19, no. 1 (2013): 1–6. http://dx.doi.org/10.2298/ciceq120124037d.

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The retention of some 5,5-disubstituted hydantoins was investigated by reversed phase high performance thin-layer chromatography (RP HPTLC) and reversed phase high-pressure liquid chromatography (RP HPLC). The mobile phases were mixtures of methanol-water and acetonitrile-water in various volume fractions. In order to explore and visualize similarities and differences among the investigated compounds and chromatographic system Principal Component Analysis (PCA) was used. Results show that the experimental lipophilicity indices estimated from retention data (RM,W, logkw) and PC1 are directly correlated with logP values at a high significant statistical level.

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16

Livaja-Popovic, Dragana, Eva Loncar, Lidija Jevric, and Radomir Malbasa. "Reversed-phase thin-layer chromatography behavior of aldopentose derivatives." Chemical Industry 66, no. 3 (2012): 365–72. http://dx.doi.org/10.2298/hemind111012099l.

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Quantitative structure-retention relationships (QSRR) have been used to study the chromatographic behavior of some aldopentose. The behavior of aldopentose derivatives was investigated by means of the reversed-phase thin-layer chromatography (RP TLC) on the silica gel impregnated with paraffin oil stationary phases. Binary mixtures of methanol-water, acetone-water and dioxane-water were used as mobile phases. Retention factors, RM0, corresponding to zero percent organic modifier in the aqueous mobile phase was determined. Lipophilicity C0 was calculated as the ratio of the intercept and slope values. There was satisfactory correlation between them and log P values calculated using different theoretical procedures. Some of these correlations offer very good predicting models, which are important for a better understanding of the relationships between chemical structure and retention. The study showed that the hydrophobic parameters RM0 and C0 can be used as a measures of lipophilicity of investigated compounds.

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17

Bottoli, Carla B. G., Kenneth E. Collins, and Carol H. Collins. "Chromatographic evaluation of self-immobilized stationary phases for reversed-phase liquid chromatography." Journal of Chromatography A 987, no. 1-2 (February 2003): 87–92. http://dx.doi.org/10.1016/s0021-9673(02)01535-2.

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18

Zhu, P. L. "On the chromatography mechanism of reversed-phase liquid chromatography." Chromatographia 21, no. 4 (April 1986): 229–33. http://dx.doi.org/10.1007/bf02311893.

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19

Sharma, Bhavik, and Sushil Kumar Agarwal. "RP-HPLC Method Development and Validation for Estimation of Acebrophylline." Asian Journal of Pharmaceutical Research and Development 6, no. 6 (February 14, 2019): 66–68. http://dx.doi.org/10.22270/ajprd.v6i6.445.

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Chromatography, a separation technique, is mostly used in chemical analysis in which High-performance liquid chromatography (HPLC) is an extremely versatile technique where analytes are separated by passage through a column packed with micrometer-sized particles. Theses day reversed-phase chromatography is commonly used separation technique in HPLC. The reasons for this include the simplicity, versatility, and scope of the reversed-phase method as it is able to handle compounds of a diverse polarity and molecular mass. Reversed phase chromatography has found both analytical and preparative applications in the area of biochemical separation and purification. Molecules that possess some degree of hydrophobic character, such as proteins, peptides and nucleic acids, can be separated by reversed phase chromatography with excellent recovery and resolution. This review covers the importance of RP-HPLC in analytical method development and their strategies along with brief knowledge of critical chromatographic parameters need to be optimized for an efficient method development. Key Words- HPLC, RP-HPLC

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20

Landy, John S., and John G. Dorsey. "Characterization of micellar mobile phases for reversed-phase chromatography." Analytica Chimica Acta 178 (1985): 179–88. http://dx.doi.org/10.1016/s0003-2670(00)86267-4.

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21

Boothe, Thomas E., Ali M. Emran, Ronald D. Finn, Paresh J. Kothari, and Manhar M. Vora. "Chromatography of radiolabelled anions using reversed-phase liquid chromatographic columns." Journal of Chromatography A 333 (January 1985): 269–75. http://dx.doi.org/10.1016/s0021-9673(01)87355-6.

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22

Miyabe, Kanji. "Moment analysis of chromatographic behavior in reversed-phase liquid chromatography." Journal of Separation Science 32, no. 5-6 (March 2009): 757–70. http://dx.doi.org/10.1002/jssc.200800607.

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23

Heinisch, S., J. L. Rocca, and M. Feinberg. "Optimization of a chromatographic analysis in reversed phase liquid chromatography." Journal of Chemometrics 3, S1 (March 30, 2005): 127–37. http://dx.doi.org/10.1002/cem.1180030505.

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24

Dopico-García, M., Rosalía Noguerol-Cal, M. Castro-López, M. Cela-Pérez, Elena Piñón-Giz, Jose López-Vilariño, and M. González-Rodríguez. "Determination of polyolefin additives by reversed-phase liquid chromatography." Open Chemistry 10, no. 3 (June 1, 2012): 585–610. http://dx.doi.org/10.2478/s11532-012-0001-x.

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AbstractThis article examines the contribution of liquid chromatography to the study of polyolefin additives commonly used to obtain improved environmental resistance (antioxidants, ultraviolet light stabilizers, antistatics, and so on) and appearance enhancements (e.g. colorants). Several reversed-phase liquid chromatographic methods are summarized, and a detailed description of different detectors is provided. In addition, ways of applying these methods to analyse food contact materials and plastic toys are emphasized. Finally, the potential use of these methods is addressed which complies with European health safety regulations.

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25

Yang, R. Q., S. X. Jiang, and L. R. Chen. "Phenylvinylmethylpolysiloxane Encapsulated Stationary Phase for Reversed-Phase Liquid Chromatography." Journal of Liquid Chromatography & Related Technologies 21, no. 11 (June 1998): 1569–78. http://dx.doi.org/10.1080/10826079808001245.

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26

Arvidsson, E., J. Crommen, G. Schill, and D. Westerlund. "Indirect detection in reversed-phase liquid chromatography." Journal of Chromatography A 461 (January 1989): 429–41. http://dx.doi.org/10.1016/s0021-9673(00)94309-7.

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27

Neue, U. D. "Nonlinear Retention Relationships in Reversed-Phase Chromatography." Chromatographia 63, S13 (March 8, 2006): S45—S53. http://dx.doi.org/10.1365/s10337-006-0718-9.

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28

Manning, John N., Gregory S. Sullivan, and Paul F. Davis. "Reversed-phase liquid chromatography of elastin peptides." Journal of Chromatography B: Biomedical Sciences and Applications 487 (January 1989): 41–50. http://dx.doi.org/10.1016/s0378-4347(00)83005-4.

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29

Miyabe, Kanji, and Georges Guiochon. "Extrathermodynamic Relationships in Reversed-Phase Liquid Chromatography." Analytical Chemistry 74, no. 22 (November 2002): 5754–65. http://dx.doi.org/10.1021/ac020245p.

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30

Wilson, N. S., J. W. Dolan, L. R. Snyder, P. W. Carr, and L. C. Sander. "Column selectivity in reversed-phase liquid chromatography." Journal of Chromatography A 961, no. 2 (July 2002): 217–36. http://dx.doi.org/10.1016/s0021-9673(02)00658-1.

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31

Wilson, N. S., M. D. Nelson, J. W. Dolan, L. R. Snyder, R. G. Wolcott, and P. W. Carr. "Column selectivity in reversed-phase liquid chromatography." Journal of Chromatography A 961, no. 2 (July 2002): 171–93. http://dx.doi.org/10.1016/s0021-9673(02)00659-3.

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32

Wilson, N. S., M. D. Nelson, J. W. Dolan, L. R. Snyder, and P. W. Carr. "Column selectivity in reversed-phase liquid chromatography." Journal of Chromatography A 961, no. 2 (July 2002): 195–215. http://dx.doi.org/10.1016/s0021-9673(02)00660-x.

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33

Mehok, Anthony R., Colin T. Mant, Lajos Gera, John Stewart, and Robert S. Hodges. "Preparative reversed-phase liquid chromatography of peptides." Journal of Chromatography A 972, no. 1 (September 2002): 87–99. http://dx.doi.org/10.1016/s0021-9673(02)01076-2.

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34

Gilroy, Jonathan J., John W. Dolan, and Lloyd R. Snyder. "Column selectivity in reversed-phase liquid chromatography." Journal of Chromatography A 1000, no. 1-2 (June 2003): 757–78. http://dx.doi.org/10.1016/s0021-9673(03)00512-0.

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35

Isaksen, Morten, and George W. Francis. "Reversed-phase thin-layer chromatography of carotenoids." Journal of Chromatography A 355 (January 1986): 358–62. http://dx.doi.org/10.1016/s0021-9673(01)97338-8.

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36

Welsch, Thomas, Harald Frank, and Gyula Vigh. "Silanol effects in reversed-phase liquid chromatography." Journal of Chromatography A 506 (May 1990): 97–108. http://dx.doi.org/10.1016/s0021-9673(01)91570-5.

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37

Bartha, Ákos, and Gyula Vigh. "Studies in reversed-phase ion-pair chromatography." Journal of Chromatography A 395 (June 1987): 503–9. http://dx.doi.org/10.1016/s0021-9673(01)94138-x.

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38

Makino, Keisuke, Hiroaki Ozaki, Tetsufumi Matsumoto, Hiromasa Imaishi, Tamio Takeuchi, and Toshikazu Fukui. "Reversed-phase ion-pair chromatography of oligodeoxyribonucleotides." Journal of Chromatography A 400 (July 1987): 271–77. http://dx.doi.org/10.1016/s0021-9673(01)81621-6.

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39

Bouabdallah, S., H. Trabelsi, K. Bouzouita, and S. Sabbah. "Reversed-phase liquid chromatography of lisinopril conformers." Journal of Biochemical and Biophysical Methods 54, no. 1-3 (December 2002): 391–405. http://dx.doi.org/10.1016/s0165-022x(02)00140-9.

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40

Lepri, L., M. Del Bubba, V. Coas, and A. Cincinelli. "REVERSED-PHASE PLANAR CHROMATOGRAPHY OF RACEMIC FLAVANONES." Journal of Liquid Chromatography & Related Technologies 22, no. 1 (January 1999): 105–18. http://dx.doi.org/10.1081/jlc-100101646.

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41

JACKSON, P. T., and P. W. CARR. "ChemInform Abstract: Improving Reversed-Phase Liquid Chromatography." ChemInform 30, no. 4 (June 17, 2010): no. http://dx.doi.org/10.1002/chin.199904293.

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42

Popl, M., L. D. Ky, and J. Strnadova. "Reversed-Phase Liquid Chromatography of Some Alkaloids." Journal of Chromatographic Science 23, no. 3 (March 1, 1985): 95–100. http://dx.doi.org/10.1093/chromsci/23.3.95.

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43

Dorsey, John G., and Morteza G. Khaledi. "Hydrophobicity estimations by reversed-phase liquid chromatography." Journal of Chromatography A 656, no. 1-2 (December 1993): 485–99. http://dx.doi.org/10.1016/0021-9673(93)80815-p.

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44

Hall, J. Z., M. T. Taschuk, and M. J. Brett. "Polarity-adjustable reversed phase ultrathin-layer chromatography." Journal of Chromatography A 1266 (November 2012): 168–74. http://dx.doi.org/10.1016/j.chroma.2012.10.020.

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45

Gétaz, David, Guido Ströhlein, and Massimo Morbidelli. "Peptide pore accessibility in reversed-phase chromatography." Journal of Chromatography A 1216, no. 6 (February 2009): 933–40. http://dx.doi.org/10.1016/j.chroma.2008.12.019.

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46

Miyabe, Kanji, and Georges Guiochon. "Surface diffusion in reversed-phase liquid chromatography." Journal of Chromatography A 1217, no. 11 (March 2010): 1713–34. http://dx.doi.org/10.1016/j.chroma.2009.12.054.

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47

Kunitani, Michael, Pamela Hirtzer, Deborah Johnson, Robert Halenbeck, Albert Boosman, and Kirston Koths. "Reversed-phase chromatography of interleukin-2 muteins." Journal of Chromatography A 359 (1986): 391–402. http://dx.doi.org/10.1016/0021-9673(86)80093-0.

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48

Yamamoto, Hideko, Joseph Baumann, and Fritz Erni. "Electrokinetic reversed-phase chromatography with packed capillaries." Journal of Chromatography A 593, no. 1-2 (February 1992): 313–19. http://dx.doi.org/10.1016/0021-9673(92)80300-j.

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49

Pellett, Jackson, Patrick Lukulay, Yun Mao, William Bowen, Robert Reed, M. Ma, R. C. Munger, et al. "“Orthogonal” separations for reversed-phase liquid chromatography." Journal of Chromatography A 1101, no. 1-2 (January 2006): 122–35. http://dx.doi.org/10.1016/j.chroma.2005.09.080.

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50

Marchand, D. H., K. Croes, J. W. Dolan, L. R. Snyder, R. A. Henry, K. M. R. Kallury, S. Waite, and P. W. Carr. "Column selectivity in reversed-phase liquid chromatography." Journal of Chromatography A 1062, no. 1 (January 2005): 65–78. http://dx.doi.org/10.1016/j.chroma.2004.11.014.

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