Academic literature on the topic 'Pycnometer'

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Journal articles on the topic "Pycnometer"

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Sreedhara, Sudhakara Sarma, and Narasinga Rao Tata. "A Novel Method for Measurement of Porosity in Nanofiber Mat using Pycnometer in Filtration." Journal of Engineered Fibers and Fabrics 8, no. 4 (December 2013): 155892501300800. http://dx.doi.org/10.1177/155892501300800408.

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Electrospun Polymer nanofibers have a wide range of applications including automotive air filters. Large surface area, small pores, flexible and adequate porosity are widely recognized as important parameters for improving the performance of the filter media and therefore measuring the porosity of the medium is extremely important. Porosity measurement techniques such as density based method, mercury porosimetry, capillary flow porometry, image analysis are relatively inaccurate and they have some disadvantages for measuring the porosity of the nano fibers. In the present study porosity measurement for nanofiber mat using pycnometer was explored. Pycnometer is generally used to measure the density of the solids of having volumes upto 150 cc. Volume of the nanofiber was measured by pycnometer and porosity is determined as fraction of the void in total volume of the fiber. Total volume is calculated from FESEM image thickness. Various advantages of pycnometry method when compared to other techniques were discussed based on the results of porosity measurements of nanofiber mats.
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Rienitz, Olaf, Axel Pramann, and Carola Pape. "The pycnometer challenge." Analytical and Bioanalytical Chemistry 405, no. 17 (June 27, 2013): 5627–28. http://dx.doi.org/10.1007/s00216-013-7012-0.

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Rienitz, Olaf, Axel Pramann, and Carola Pape. "Solution to the pycnometer challenge." Analytical and Bioanalytical Chemistry 405, no. 27 (October 19, 2013): 8691–92. http://dx.doi.org/10.1007/s00216-013-7310-6.

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Adedeji, Akinbode A., and Michael Ngadi. "Porosity determination of deep-fat-fried coatings using pycnometer (Fried batter porosity determination by pycnometer)." International Journal of Food Science & Technology 46, no. 6 (May 3, 2011): 1266–75. http://dx.doi.org/10.1111/j.1365-2621.2011.02631.x.

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K. C. Diehl, V. A. Garwood, and C. G. Haugh. "Volume Measurement Using the Air-Comparison Pycnometer." Transactions of the ASAE 31, no. 1 (1988): 0284–87. http://dx.doi.org/10.13031/2013.30701.

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Eadkhong, Thammarong, and Sorasak Danworaphong. "On the sensitivity of an air pycnometer." Measurement 169 (February 2021): 108511. http://dx.doi.org/10.1016/j.measurement.2020.108511.

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Wyllie, Hugh A. "Syringe pycnometer for use with electronic microbalance." Analytical Chemistry 58, no. 14 (December 1986): 3269–70. http://dx.doi.org/10.1021/ac00127a081.

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Zhang, Chao, and N. Lu. "Measuring Soil-Water Density by Helium Pycnometer." Journal of Geotechnical and Geoenvironmental Engineering 144, no. 9 (September 2018): 02818002. http://dx.doi.org/10.1061/(asce)gt.1943-5606.0001929.

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Amore, Ricardo, Clóvis Pagani, Michel Nicolau Youssef, Camillo Anauate Netto, and Hugo Roberto Lewgoy. "Polymerization shrinkage evaluation of three packable composite resins using a gas pycnometer." Pesquisa Odontológica Brasileira 17, no. 3 (September 2003): 273–77. http://dx.doi.org/10.1590/s1517-74912003000300013.

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Modern restorative dentistry has been playing an outstanding role lately since composite resins, allied to adhesive systems, have been widely applied on anterior and posterior teeth restorations. The evolution of composite resins has mostly been verified due to the improvement of their aesthetic behavior and the increase in their compressive and abrasive strengths. In spite of these developments, the polymerization shrinkage inherent to the material has been a major deficiency that, so far, has been impossible to avoid. Using a gas pycnometry, this research investigated the polymerization shrinkage of three packable composite resins: Filtek P60 (3M), Prodigy Condensable (Kerr), and SureFil (Dentsply/Caulk), varying the distance from the light source to the surface of the resins (2 mm or 10 mm). The pycnometer Accupyc 1330 (Micromeritics, USA) precisely records helium displacement, allowing fast and reliable measurements of the volume of composite resin immediately before and after polymerization, without interference of temperature or humidity. Results were not found to be statistically different for the three tested resins, either for 2 mm or 10 mm-distance from the light source to the composite surface.
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Grabowski, A., R. Siuda, L. Lenc, and S. Grundas. "Evaluation of single-kernel density of scab-damaged winter wheat." International Agrophysics 26, no. 2 (April 1, 2012): 129–35. http://dx.doi.org/10.2478/v10247-012-0019-5.

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Evaluation of single-kernel density of scab-damaged winter wheatMeasurements of single-kernel mass and volume made on healthy (control) and scab-damaged samples of grain of three winter wheat varieties never resulted in lower values of mean single-kernel density for scab-damaged grain. This finding, contrary to common opinion, can be explained as being a result of the comparable magnitude of relative decrease (due to infestation) of two features (mass and volume) that define single-kernel density. The discrepancy between results presented in this paper (kernel volume was determined with an air pycnometer) and the results in some other reports (liquid pycnometers used) can result from the different methods applied for kernel volume measurements: when a liquid medium is used the surface tension effect tends to overestimate the volume, especially for scabby kernels that are known to be shrivellediepossessing voids and pores at the surface that the liquid cannot penetrate. As a consequence kernel density of scabby kernels can be significantly underestimated.
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Dissertations / Theses on the topic "Pycnometer"

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Geddis, A. M. "Rapid estimate of solid volume in large tuff cores using a gas pycnometer." Thesis, The University of Arizona, 1996. http://etd.library.arizona.edu/etd/GetFileServlet?file=file:///data1/pdf/etd/azu_e9791_1994_473_sip1_w.pdf&type=application/pdf.

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Guy, Peter John, and guyp@ebac com au. "The Solvent induced swelling behaviour of Victorian brown coals." Swinburne University of Technology. School of Engineering and Science, 2002. http://adt.lib.swin.edu.au./public/adt-VSWT20031218.142251.

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The solvent-induced swelling behaviour of Victorian brown coals was examined in detail to probe the bonding mechanisms in very low rank coals (in this case Victorian brown coal). Correlation of solvent properties with differences in observed swelling behaviour were interpreted in terms of the coal structure, and means of predicting the observed behaviour were considered. Modification of the coal structure via physical compression (briquetting), chemical digestion, thermal modification, and functional group alkylation was used to further elucidate those structural features which govern the swelling behaviour of Victorian brown coals. Briquette weathering (i.e. swelling and disintegration of briquettes when exposed to variations in humidity and temperature) was examined by making alterations to briquette feed material and observing the effects on swelling in water. The application of solubility parameter alone to prediction of coal swelling was rejected due to the many exceptions to any proposed trend. Brown coal swelling showed a minimum when the solvent electron-donor number (DN) minus its electron-acceptor number (AN) was closest to zero, i.e. when DN and AN were of similar magnitude. The degree of swelling increased either side of this point, as predicted by theory. In contrast to the solubility parameter approach (which suffers from the uncertainty caused by specific interaction between coal and solvent), the electron donor/acceptor approach is about specific interactions. It was concluded that a combination of total and three-dimensional solubility parameters and solvent electron donor/acceptor numbers may be used to predict solvent swelling of unextracted brown coals with some success. Solvent access to chemically densified coal was found to be insensitive to a reduction in pore volume, and chemical effects were dominant. Thermal modification of the digested coal resulted in reduced swelling for all solvents, indicating that the structure had adopted a minimum energy configuration due to decarboxylation and replacement of hydrogen bonds with additional covalent bonds. Swelling of oxygen-alkylated coals demonstrated that the more polar solvents are able to break relatively weak hydrogen bonded crosslinks. The large difference between the rate and extent of swelling in water (and hence weathering) of Yallourn and Morwell briquettes was shown to be almost entirely attributable to exchanged magnesium. Magnesium exchange significantly increases the rate and extent of swelling of Yallourn coal. It was also shown that the swelling of briquettes due to uptake of water by magnesium-exchanged coals is reduced significantly with controlled ageing of the briquettes. The solvent swelling behaviour of Victorian brown coals is consistent with the notion that coal is a both covalently and non-covalently crosslinked and entangled macromolecular network comprising extractable species, which are held within the network by a wide range of non-covalent, polar, electron donor/acceptor interactions. Solvents capable of significant extraction of whole brown coals are also capable of significant swelling, but not dissolution, of the macromolecular coal network, which supports the view that the network is comprised of both covalent and ionic bonding. Victorian brown coals have also been shown to exhibit polyelectrolytic behaviour due to a high concentration of ionisable surface functionalities.
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Júnior, Luiz Paulo dos Santos Salgado. ""Avaliação da contração de polimerização de uma resina composta fotopolimerizável de uso universal, variando-se a técnica de inserção do material medida por picnômetro a gás"." Universidade de São Paulo, 2004. http://www.teses.usp.br/teses/disponiveis/23/23134/tde-22092004-183442/.

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RESUMO Dada sua versatilidade e excelência estética, a resina composta é o material restaurador direto mais utilizado nas intervenções da clínica odontológica. Uso tão intenso levou pesquisadores e fabricantes a trabalharem na evolução deste material, conferindo-lhe aumento em sua resistência à compressão e abrasão, bem como melhora em seu comportamento estético. Infelizmente, um problema intrínseco da resina, a contração de polimerização é sua principal desvantagem, e caracteriza-se pela alteração volumétrica que sofre quando as moléculas de seus monômeros se unem para a formação das cadeias poliméricas. Uma das principais técnicas para combater os efeitos nocivos desta alteração volumétrica é a inserção incremental do material na cavidade a ser restaurada. Nesta pesquisa, a contração de polimerização de uma resina composta de uso universal (Charisma Heraeus Kullser) será avaliada variando-se a técnica de inserção do material na cavidade em incremento único ou três incrementos oblíquos, através do método da picnometria a gás. O picnômetro Accupyc 1330 (Micromeritics) permite medições rápidas e fiéis do volume da resina composta antes e após a fotoativação. Os resultados mostram que ocorreram diferenças estatísticas entre as duas técnicas, sendo a técnica de único incremento a que apresentou menor contração de polimerização.
Because of its versatility and aestetic excellency, composite resin is one of the most utilized direct restorative materials. Because of the resin intense use, the number of researches to improve its performance are numerous, and can be verified by the resin aestethetic behavior and its compressive and abrasion strenght increase. In spite of the mentioned developments, the polymerization shrinkage inherent of the material had been a major deficiency, and can be understood by the alteration in volume of the material after the polymerization process. In the present study, the polymerization shrinkage of the restorative material Charisma (Heraes Kulzer), was evaluated using bulk and incremental placement techniques and measured by gas pycnometer. Accupyc 1330 (Micromeritics, USA) pycnometer measures the helium displacement with great precision, allowing fast and accurate measurements of the volume of the composite resin before and after polymerization, without interference of the moisture or temperature. The results showed statistically significant diferences between the two placement techniques, with the bulk technique showing lower polymerization shrinkage than the incremental technique.
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Suleman, Riaz. "Performance of selected South African cements based on solar chamber, pycnometer, chemical and physical tests." Thesis, 2015. http://hdl.handle.net/10539/17628.

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The performance of cement in concrete can be argued to include strength, durability, economy, aesthetics as well as workability. In this research report, various local South African cements as well as a cement from Germany and Pakistan have been studied for various aspects such as strength, durability and hydration characteristics. Three curing regimes have been investigated. The curing regimes included curing in water, air and in a solar chamber to determine the strength and durability performance of the cements under study. The chemical performance of certain cements has been assessed in terms of sulphur, chloride and insoluble residue contents. Pycnometers have been utilised to determine whether the hydration characteristics can be followed for different grades of cements and mixes containing fly ash. X-ray fluorescence studies on hardened mortar have also been investigated on the mortar mixes from the pycnometer study in order to assess whether the technique may be useful to assess the hydration characteristics of the various mixes. On the whole, the strength and durability results show the importance of moisture in curing even though discrepancies were encountered. The chemical performance of the cements were found to perform satisfactorily with respect to standard codes of practice. The pycnometers may be a useful technique to assess the hydration of various mixes but require careful procedural processes. The x-ray fluorescence portion of the study revealed that the technique is not useful to assess the hydration characteristics of mortar over time. Key words: Cement, concrete, hydration, solar chamber, pycnometer, strength, durability.
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Books on the topic "Pycnometer"

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1948-, Bassett R. L., Woodhouse E. G, and U.S. Nuclear Regulatory Commission. Office of Nuclear Regulatory Research. Division of Regulatory Applications., eds. Field studies at the Apache Leap Research Site in support of alternative conceptual models. Washington, D.C: Division of Regulatory Applications, Office of Nuclear Regulatory Research, U.S. Nuclear Regulatory Commission, 1997.

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Rapid estimate of solid volume in large tuff cores using a gas pycnometer. Washington, DC: Division of Regulatory Applications, Office of Nuclear Regulatory Research, U.S. Nuclear Regulatory Commission, 1996.

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Book chapters on the topic "Pycnometer"

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Gooch, Jan W. "Pycnometer." In Encyclopedic Dictionary of Polymers, 598. New York, NY: Springer New York, 2011. http://dx.doi.org/10.1007/978-1-4419-6247-8_9651.

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Shpil’rain, E. E., K. A. Yakimovich, and A. G. Mozgovoi. "Apparatus for Continuous Measurement of Temperature Dependence of Density of Molten Metals by the Method of a Suspended Pycnometer at High Temperatures and Pressures." In Compendium of Thermophysical Property Measurement Methods, 601–24. Boston, MA: Springer US, 1992. http://dx.doi.org/10.1007/978-1-4615-3286-6_21.

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Rohen, Lázaro A., Anna C. C. Neves, Dhyemila de P. Mantovani, F. V. Carlos Maurício, Janaina da Silva Vieira, Lucas de A. Pontes, Frederico M. Margem, and Sergio Monteiro. "Hemp Fiber Density Using the Pycnometry Technique." In Characterization of Minerals, Metals, and Materials 2017, 423–28. Cham: Springer International Publishing, 2017. http://dx.doi.org/10.1007/978-3-319-51382-9_46.

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DiResta, G. R., J. Lee, N. Lau, F. Ali, J. H. Galicich, and E. Arbit. "Measurement of Brain Tissue Density Using Pycnometry." In Brain Edema VIII, 34–36. Vienna: Springer Vienna, 1990. http://dx.doi.org/10.1007/978-3-7091-9115-6_12.

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de O.R. Maciel, Natália, Carolina G. D. Ribeiro, Jordana Ferreira, Janaina da S. Vieira, Cláudio R. Marciano, Carlos Maurício Vieira, Frederico M. Margem, and Sergio N. Monteiro. "Comparative Analysis of Curaua Fiber Density Using the Geometric Characterization and Pycnometry Technique." In Characterization of Minerals, Metals, and Materials 2017, 11–19. Cham: Springer International Publishing, 2017. http://dx.doi.org/10.1007/978-3-319-51382-9_2.

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"pycnometer." In Dictionary Geotechnical Engineering/Wörterbuch GeoTechnik, 1060. Berlin, Heidelberg: Springer Berlin Heidelberg, 2014. http://dx.doi.org/10.1007/978-3-642-41714-6_164497.

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"Pycnometer." In Encyclopedic Dictionary of Polymers, 803. New York, NY: Springer New York, 2007. http://dx.doi.org/10.1007/978-0-387-30160-0_9471.

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"air pycnometer." In Dictionary Geotechnical Engineering/Wörterbuch GeoTechnik, 33. Berlin, Heidelberg: Springer Berlin Heidelberg, 2014. http://dx.doi.org/10.1007/978-3-642-41714-6_11194.

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"Pycnometry and thennoporometry." In Pore Structure of Cement-Based Materials, 210–37. CRC Press, 2005. http://dx.doi.org/10.1201/9781482271959-16.

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Bernstein, Joel. "Analytical techniques for studying and characterizing polymorphs and polymorphic transitions." In Polymorphism in Molecular Crystals, 136–214. Oxford University Press, 2020. http://dx.doi.org/10.1093/oso/9780199655441.003.0004.

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Chapter 4 deals with the analytical methods for the characterization of solid forms, including optical and hot stage microscopy, thermal methods (differential scanning calorimetry, thermal gravimetric analysis, etc.), X-ray diffraction methods (powder and single crystal methods), infrared and Raman spectroscopy, solid state nuclear magnetic resonance spectroscopy, electron microscopy, atomic force microscopy, scanning tunneling microscopy, and pycnometry (density measurements). The principles of each of these techniques are outlined, followed by representative examples of their application in the investigation and characterization of polymorphic systems. The integration of a number of analytical tools—“hyphenated techniques”—into a particular instrument is described for a number of cases, followed by a discussion of the experimental approach for determining if two samples comprise polymorphs of the same compound.
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Conference papers on the topic "Pycnometer"

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Oladiran O Fasina and (or initial) (or initial). "DOES A PYCNOMETER MEASURE THE TRUE OR APPARENT PARTICLE DENSITY OF AGRICULTURAL MATERIALS?" In 2007 Minneapolis, Minnesota, June 17-20, 2007. St. Joseph, MI: American Society of Agricultural and Biological Engineers, 2007. http://dx.doi.org/10.13031/2013.23513.

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BATISTA, ELSA, and EDUARDA FILIPE. "DATA EVALUATION AND UNCERTAINTY ANALYSIS IN AN INTERLABORATORY COMPARISON OF A PYCNOMETER VOLUME." In Advanced Mathematical and Computational Tools in Metrology. WORLD SCIENTIFIC, 2006. http://dx.doi.org/10.1142/9789812774187_0029.

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Lipchitz, Adam, Theophile Imbert, and Glenn D. Harvel. "Investigation of Fluid Dynamic Properties of Liquid Field’s Metal." In ASME 2013 Power Conference. American Society of Mechanical Engineers, 2013. http://dx.doi.org/10.1115/power2013-98224.

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The density and viscosity Field’s metal is measured in this work and compared to traditional liquid metal coolants such as sodium and lead-bismuth eutectic. Field’s metal is a eutectic of the ternary In-Bi-Sn system. The alloy is by weight percent is 51% indium, 32.5% bismuth and 16.5% tin and possesses a melting temperature of 333 K. This work experimentally measures the density and viscosity of Field’s metal for numerical modeling and thermal hydraulic applications. The density of Field’s metal is measured using a pycnometer. The density is determined for both its solid and liquid states. In its liquid state Field’s metal is found to have a linear dependence with respect to increasing temperature. The viscosity of Field’s metal is measured using a rotational viscometer. The viscosity is measured is to be 27 mPa-s at 353 K, however further investigation is required to determine a trend at higher temperatures.
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Lima, R. S., and C. P. Bergmann. "Phase Transformations on Flame Sprayed Alumina." In ITSC 1996, edited by C. C. Berndt. ASM International, 1996. http://dx.doi.org/10.31399/asm.cp.itsc1996p0765.

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Abstract Flame-sprayed coatings of alumina were produced by an oxyacetylene flame spray system in order to study the phase transformations that occurs on alumina during the spraying. The X-ray diffraction pattern of the alumina powder to be sprayed, showed the main presence of the stable phase alpha alumina and an impurity probably resulting from the process of purification of alumina. For as-sprayed coatings, phase changes occur. The X-ray diffraction pattern shows the presence of the stable form alpha alumina, but also the metastable form gamma alumina and amorphous alumina. True density measurements were done using a helium pycnometer, as an aid to observe the phase transformations. The density of the powder to be sprayed was 3.98 g/cm3 and the density of the as-sprayed coatings was 3.62 g/cm3. This change of density is linked to the phase transformation during spraying. Scanning electron microscopy (SEM) of the incident particles was made after 1 second of deposition onto glass substrates in order to observe the degree of melting of the incident particles, by analyzing their profiles (degree of flattening).
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Aydin, Elena. "DETERMINATION OF POROSITY OF SOILS WITH DIFFERENT SOIL TEXTURE USING TWO DIFFERENT PYCNOMETERS." In 19th SGEM International Multidisciplinary Scientific GeoConference EXPO Proceedings. STEF92 Technology, 2019. http://dx.doi.org/10.5593/sgem2019/3.2/s13.017.

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Gorynski, Kyle E., Mark Tobey, Daniel Enriquez, and Thomas Smagala. "Quantification and Characterization of Oil-Filled Porosity in Shales Using Basic Programmed Pyrolysis, LECO-TOC, Archimedes Bulk Density, and Helium Pycnometry Measurements." In Unconventional Resources Technology Conference. Tulsa, OK, USA: American Association of Petroleum Geologists, 2017. http://dx.doi.org/10.15530/urtec-2017-2686515.

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Rohan, P., P. Chraska, P. Ctibor, and K. Neufuss. "Relation Between Thermal Expansion Coefficient and Porosity in Thick Zircon and Alumina Coatings." In ITSC 2000, edited by Christopher C. Berndt. ASM International, 2000. http://dx.doi.org/10.31399/asm.cp.itsc2000p1067.

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Abstract For utilization of free-standing ceramic parts produced by plasma spraying it is very important to know the temperature dependence of the linear thermal expansion coefficient and its relation to the porosity of the structure. Zircon ZrSiO4 and gray alumina (96 wt % AI2O3) were plasma sprayed by the water stabilized plasma gun WSP PAL 160. Samples of both materials were cut from thick coatings with respect to their orientation to the gun axis during the gun's horizontal spraying cycling with a constant speed. Thermal expansion coefficients and the differential thermal analysis were performed using SETARAM complex measuring system (up to 1750 °C), the density/porosity was measured by several techniques, such as Archimedean weighing, helium pycnometry, etc. It was found that both, the porosity and the thermal expansion coefficient, change for different locations in the thick deposit due to the varying trajectories of individual particles/droplets in the plasma stream. Measured data for deposits are then compared with data for bulk ceramics. The dependence of the thermal expansion coefficient on porosity in a given location was determined and its general applicability for free-standing plasma spraying is then discussed in the paper.
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Reports on the topic "Pycnometer"

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Thies, C., A. M. Geddis, and A. G. Guzman. Rapid estimate of solid volume in large tuff cores using a gas pycnometer. Office of Scientific and Technical Information (OSTI), September 1996. http://dx.doi.org/10.2172/380359.

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Crupe, William E. The application of the electronic balance in high precision pycnometry. Gaithersburg, MD: National Institute of Standards and Technology, 1994. http://dx.doi.org/10.6028/nist.ir.5422.

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Taylor, James, and Cheryl Smith. The electronic balance and some gravimetric applications (the density of solids and liquids, pycnometry and mass). Gaithersburg, MD: National Institute of Standards and Technology, 1994. http://dx.doi.org/10.6028/nist.ir.5375.

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