Dissertations / Theses on the topic 'Nanodiamonds – Synthesis'
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Basso, Luca. "Laser-synthesis and optical functionalization of NV-fluorescent nanodiamonds for quantum sensing applications." Doctoral thesis, Università degli studi di Trento, 2020. http://hdl.handle.net/11572/250439.
Full textKoso, Tetyana V. [Verfasser]. "Unsaturated nanodiamonds : synthesis and functionalization of coupled diamondoids as a direct route to nanometer-sized building blocks / Tetyana V. Koso." Gießen : Universitätsbibliothek, 2013. http://d-nb.info/1065319789/34.
Full textGür, Fatih Nadi. "Plasmonic waveguides self-assembled on DNA origami templates: from synthesis to near-field characterizations." Doctoral thesis, Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2018. http://nbn-resolving.de/urn:nbn:de:bsz:14-qucosa-235762.
Full textDie Manipulation des Lichts durch die Kontrolle von Oberflächenplasmonen auf metallischen Oberflächen und Nanopartikeln gilt als vielversprechende Methode zur Überbrückung der Größen-Lücke zwischen Mikrometer-großen photonischen und nanometer-großen elektronischen Schaltkreisen. Plasmonische Wellenleiter basierend auf metallischen Nanopartikeln sind vom besonderen Interesse, da sie die Umgehung des Beugungslimits und somit eine Hochgeschwindigkeitskommunikation über kurze Distanzen in immer kleiner werdenden Schaltkreisen ermöglichen könnten. Allerdings ist die skalierbare und kostengünstige Anordnung von Partikeln eine große Herausforderung und es werden Nahfelduntersuchungen benötigt um plasmonische Interaktionen detektieren zu können. Das Ziel dieser Arbeit ist die Selbstassemblierung von multi-partikel Wellenleitern auf DNA Gerüsten. Die Verwendung von DNA-Origami bietet eine äußerst vielseitige Plattform zur skalierbaren Herstellung von Nanostrukturen mittels Selbstassemblierung und ermöglicht eine präzise Kontrolle der Anordnungen im Nanobereich. Für den Aufbau der plasmonischen Wellenleiter werden DNA-Origami Nanoröhren, bestehend aus sechs Helices als Templat für die Anbindung von monodispersen und monokristallinen Goldnanopartikeln mit einem interpartikulären Abstand von 1-2 nm verwendet. Im ersten Abschnitt dieser Arbeit werden die beeinflussenden Faktoren dieser Assemblierungsreaktion systematisch untersucht. Die Ausbeute der assemblierten Strukturen und die Besetzung der Bindungsstellen werden durch eine automatisierte und effiziente Bildanalyse von Elektronenmikroskopieaufnahmen ausgewertet. Durch die Entwicklung eines optimierten Syntheseprotokolls werden bisher unerreichte Assemblierungsausbeuten ermöglicht. Zusätzlich erfolgen die experimentelle Realisierung von Strukturen mit verschieden großen Goldnanopartikeln und unterschiedlichen interpartikulären Abständen, sowie die Anbindung von Quantenpunkten an die Wellenleiter und eine Verknüpfung der assemblierten Strukturen. Der zweite Abschnitt dieser Dissertation befasst sich mit der Untersuchung des Energietransports in selbstassemblierten Wellenleitern über einen fluoreszierenden Nanodiamanten. Dazu erfolgen hochaufgelöste Nahfeldmessungen der Wellenleiter mittels Elektronenenergieverlustspektroskopie und Kathodolumineszenz-mikroskopie. Die experimentellen Ergebnisse und zusätzlich durchgeführte Simulationen bestätigen eine durch gekoppelte Oberflächenplasmonenmoden induzierte Weitergabe der Energie innerhalb des Wellenleiters. Diese Oberflächenplasmonenmoden werden bei hoher räumlicher und spektraler Auflösung untersucht. Das hier umgesetzte Konzept der Selbstassemblierung wird den Aufbau komplexer plasmonischer Geräte für Anwendungen im Bereich der optischen Hochgeschwindigkeitsdatenübertragung, der Quanteninformations-technolgie und der Sensorik ermöglichen
Sneed, Brian D. "Synthesis and characterization of Al-Nanodiamond composite powders by high-energy ball milling." Monterey, California. Naval Postgraduate School, 2011. http://hdl.handle.net/10945/10698.
Full textHung, Chuan-Hsi. "Synthesis and Characterization of Carbonized Poly (Divinylbenzene) Microspheres for Carbon/Nanodiamond/Polymer-Based Core-Shell Materials and Applications of This Mixed-Mode Phase to High-Performance Liquid Chromatography." BYU ScholarsArchive, 2015. https://scholarsarchive.byu.edu/etd/5497.
Full text"AMINO ACID FUNCTIONALIZED NANODIAMONDS AS GENE DELIVERY VECTORS: SYNTHESIS, PHYSICOCHEMICAL CHARACTERIZATION AND CELLULAR INTERACTION STUDIES." Thesis, 2015. http://hdl.handle.net/10388/ETD-2015-09-2219.
Full textJUNE-I, WU, and 吳俊毅. "Synthesis of peptide-conjugated nanodiamonds for developing anticancer drugs and diagnostics." Thesis, 2017. http://ndltd.ncl.edu.tw/handle/nb5ap4.
Full text東海大學
化學系
105
The rapid development of nanotechnology , let it have a chance applied to Biology and Medicine. Recently a great potential of nanodiamond (ND) particles as a multimodal imaging/therapy platform has been demonstrated. Nanodiamonds (NDs) play a key role with their excellent physicochemical properties, including high biocompatibility, physical adsorption and photostabilizing activity. To combined with Biomedical Science development of drug delivery systems may be to facilitate the permeation of drugs provide the best use in medical care. In this study, the use of colon cancer and its EGFR mechanism as the goal, the nanodiamonds as a drug carrier. Here be divided into two parts, synthetic antibody-conjugated nanodiamonds and peptide-conjugated nanodiamonds. Use BCA Protein assay、MALDI-TOF MS and FTIR to identified the effect of nanodiamonds as carrier on HT-29 cells. The results show that antibody-conjugated nanodiamonds can also be successfully associated with HT-29 cells with specific binding without loss activity. The inhibition of HT-29 cells exhibited by peptide 3C-conjugated nanodiamonds is also more effective than peptide 3C. The results show that nanodiamonds as a drug carrier, has a certain potential value.
Lu, Jing-Wun, and 盧敬文. "Facile Synthesis of Titanium Sulfonate-Functionalized Nanodiamonds for Selective Enrichment of Phosphopeptides." Thesis, 2017. http://ndltd.ncl.edu.tw/handle/3889xh.
Full text國立暨南國際大學
應用化學系
105
In this work, we have developed a novel synthesis route for the production of titanium (IV) sulfonate-functionalized nanodiamonds (Ti4+-SND) as Ti4+-IMAC (Immobilized metal-ion affinity chromatography)adsorbents for selective enrichment of phosphopeptides. Nanodiamonds were first functionalized with polyarginine via EDC-mediated coupling reaction and then the titanium-sulfonate functionalization was performed by mixing with polystyrene sulfate and TiCl4 solutions. The obtained Ti4+-SNDs were used to specific capture of phosphopeptides from standard protein digests and nonfat milk digests. The results demonstrated that by taking advantage of the strong Ti4+-sulfate chelating effect and high Ti4+ loading amount, the Ti4+-SND show remarkable selectivity (β-casein/BSA = 1:1000), good sensitivity (10 fmol), and high recovery in phosphopeptide analysis. This novel approach for developing and producing IMAC adsorbents was further validated using different metal ions including Zr4+ and Fe3+. Both of the synthesized Zr4+ and Fe3+ IMAC adsorbents show excellent performance in selective enrichment of phosphopetides from complex peptide mixtures. Keywords: Polyarginine、Polystyrene sulfonate、Ti-IMAC、Phosphopeptides
Guo, Jiun-You, and 郭俊佑. "Synthesis of biocompatible and magnetic fluorescent nanodiamonds for cell manipulation and imaging." Thesis, 2014. http://ndltd.ncl.edu.tw/handle/22471857503585588079.
Full text國立暨南國際大學
應用化學系
102
Recent advances in nanotechnology for biomedical applications have rapidly growing needs for developing multifunctional nanoparticles. Here, one new class of fluorescent nanodiamond(FND) hybrids that process biocompatible, fluorescent and magnetic functionalities is presented. Magnetic iron oxide/Fluorescent nanodiamond (IO/FND) hybrids are prepared from 100 nm FNDs functionalized at the surface with polyarginine brushes to accommodate the 20 nm magnetic IOs, and then coating with a biocompatible Heparin layer. These new FND hybrids exhibit both fluorescent and magnetic properties with a maximum saturation magnetization of 4.35 emu g-1 and far-red fluorescence emission. The fluorescent intensity of FND hybrids is similar to bare FND. MTS assay reveals that FND Hybrids show have extremely low cytotoxicity toward HeLa cells. The FND hybrids are demonstrated with HeLa cell line for in vitro cellular labeling/imaging and magnetic cell manipulation. The fluorescence intensities were increased in a concentration-dependent manner by treatment with FND hybrids in HeLa cells. However, the existence of FND hybrids inside the cells did not alter cellular size distribution. The approach should be widely applicable to incorporate into a variety of biomedical applications such as hyperthermia, long-term magnetic resonance and fluorescence imaging, cell manipulation and separation.
Lin, Yi-Chen, and 林怡辰. "Facile Synthesis of Polydopamine-Coated Nanodiamonds as Both Novel SALDI Matrix and Affinity Absorbent for Ultra-Sensitive Detection of Polycyclic Aromatic Hydrocarbons." Thesis, 2017. http://ndltd.ncl.edu.tw/handle/y83538.
Full text國立暨南國際大學
應用化學系
105
Polycyclic aromatic hydrocarbons (PAHs) are notorious environmental pollutants generated primarily during the incomplete combustion of organic materials. Many PAHs have toxic, mutagenic and/or carcinogenic properties. In this work, polydopamine-coated nanodiamonds (PDA@NDs) were synthesized by in situ polymerization method and applied as a Surface-Assisted Laser Desorption Ionization, SALDI matrix for ultra-sensitive detection of PAHs by MALDI-TOF-MS. PDA@NDs exhibited low matrix background interference and high signal response for a large number of PAHs. Ultra-high sensitive detection of benzo[a]pyrene (BaP) was found to be in the low pictogram region. Furthermore, the PDA@NDs were utilized as a high affinity probe to enrich trace amount of BaP from aqueous solutions and to detect the PAHs in a real PM 2.5 sample. These results demonstrated that PDA@NDs show great potential serving both as MALDI matrix and affinity absorbent in ultra-sensitive detection of PAHs by MADI-TOF MS.
Zimmerman, John Lynn. "Chemistry of nanoscale carbon materials: Gas-phase purification of single-wall carbon nanotubes, synthesis of nanoscale carbon nitrides, and nanodiamonds in meteorite carbon with related diamond surface chemistry." Thesis, 2000. http://hdl.handle.net/1911/19578.
Full textChen, Bo-Rong, and 陳柏融. "I . Total Synthesis of Cajaninstilbene acid II. Synthesis of Nanodiamond and drugs conjugates III. Conjugation of Nanodiamond and Iressa analogue." Thesis, 2016. http://ndltd.ncl.edu.tw/handle/n36e47.
Full text國立東華大學
化學系
104
This thesis contains three topics : (1) Total Synthesis of Cajaninstilbene acid. (2) Synthesis of Nanodiamond and drugs conjugates. (3) Conjugation of Nanodiamond and Iressa analogue. First, Total Synthesis of Cajaninstilbene acid. I used cheap trans-crotonic acid as starting martial, through cyclization, and bromination to get the final product, Cajaninstilbene acid. Second, Synthesis of Nanodiamond and drugs conjugates. All-trans-retinoic acid was conjugated with Bovine serum albumin (BSA) and Nanodiamond to evaluate the biological activity. Third, Conjugation of Nanodiamond and Iressa analogue. Iressa was extended the side chain, then conjugated with Nanodiamond.
Wu, Meng-chang, and 吳孟璋. "The Synthesis of Nanodiamond Film and Its Applications." Thesis, 2006. http://ndltd.ncl.edu.tw/handle/38328868449170992824.
Full text國立雲林科技大學
電子與資訊工程研究所
94
Carbon-based materials for electron sources are of great interest due to their low threshold emission fields. These materials include diamond, nano-diamond, amorphous diamond, carbon nanofibers, tetrahedral amorphous carbon (ta-C) films, and random or oriented carbon nanotubes (CNTs). The field emission characteristics of carbon-based materials had been studied extensively, but their gas sensing characteristics deny practical applications. In this dissertation, the different electron field emission characteristics of nanodiamond film deposited onto Si substrate with low work function by a microwave plasma-chemical vapor deposition (MPCVD) reactor will be discussed. Furthermore, the different qualities of nanodiamond films will apply in gas sensing, and utilized there breakdown field to compare the influence on the sensitivity of gas sensing. It was found that field emission properties of nanodiamond film were relative to the thickness of nanodiamond film. It was suggested that good field emission performance proportional to the ratio of ID/IG. It was concluded that the nanodiamond field emitters would be the good candidate to fabricate gas sensor devices with good performance of field emission properties.
Gür, Fatih Nadi. "Plasmonic waveguides self-assembled on DNA origami templates: from synthesis to near-field characterizations." Doctoral thesis, 2017. https://tud.qucosa.de/id/qucosa%3A31000.
Full textDie Manipulation des Lichts durch die Kontrolle von Oberflächenplasmonen auf metallischen Oberflächen und Nanopartikeln gilt als vielversprechende Methode zur Überbrückung der Größen-Lücke zwischen Mikrometer-großen photonischen und nanometer-großen elektronischen Schaltkreisen. Plasmonische Wellenleiter basierend auf metallischen Nanopartikeln sind vom besonderen Interesse, da sie die Umgehung des Beugungslimits und somit eine Hochgeschwindigkeitskommunikation über kurze Distanzen in immer kleiner werdenden Schaltkreisen ermöglichen könnten. Allerdings ist die skalierbare und kostengünstige Anordnung von Partikeln eine große Herausforderung und es werden Nahfelduntersuchungen benötigt um plasmonische Interaktionen detektieren zu können. Das Ziel dieser Arbeit ist die Selbstassemblierung von multi-partikel Wellenleitern auf DNA Gerüsten. Die Verwendung von DNA-Origami bietet eine äußerst vielseitige Plattform zur skalierbaren Herstellung von Nanostrukturen mittels Selbstassemblierung und ermöglicht eine präzise Kontrolle der Anordnungen im Nanobereich. Für den Aufbau der plasmonischen Wellenleiter werden DNA-Origami Nanoröhren, bestehend aus sechs Helices als Templat für die Anbindung von monodispersen und monokristallinen Goldnanopartikeln mit einem interpartikulären Abstand von 1-2 nm verwendet. Im ersten Abschnitt dieser Arbeit werden die beeinflussenden Faktoren dieser Assemblierungsreaktion systematisch untersucht. Die Ausbeute der assemblierten Strukturen und die Besetzung der Bindungsstellen werden durch eine automatisierte und effiziente Bildanalyse von Elektronenmikroskopieaufnahmen ausgewertet. Durch die Entwicklung eines optimierten Syntheseprotokolls werden bisher unerreichte Assemblierungsausbeuten ermöglicht. Zusätzlich erfolgen die experimentelle Realisierung von Strukturen mit verschieden großen Goldnanopartikeln und unterschiedlichen interpartikulären Abständen, sowie die Anbindung von Quantenpunkten an die Wellenleiter und eine Verknüpfung der assemblierten Strukturen. Der zweite Abschnitt dieser Dissertation befasst sich mit der Untersuchung des Energietransports in selbstassemblierten Wellenleitern über einen fluoreszierenden Nanodiamanten. Dazu erfolgen hochaufgelöste Nahfeldmessungen der Wellenleiter mittels Elektronenenergieverlustspektroskopie und Kathodolumineszenz-mikroskopie. Die experimentellen Ergebnisse und zusätzlich durchgeführte Simulationen bestätigen eine durch gekoppelte Oberflächenplasmonenmoden induzierte Weitergabe der Energie innerhalb des Wellenleiters. Diese Oberflächenplasmonenmoden werden bei hoher räumlicher und spektraler Auflösung untersucht. Das hier umgesetzte Konzept der Selbstassemblierung wird den Aufbau komplexer plasmonischer Geräte für Anwendungen im Bereich der optischen Hochgeschwindigkeitsdatenübertragung, der Quanteninformations-technolgie und der Sensorik ermöglichen.
Chimowa, George. "Synthesis and characterization of nano-crystalline diamond films." Thesis, 2011. http://hdl.handle.net/10539/10410.
Full textThe objective of this project is to understand the details of the electronic transport in low dimensional carbon structures at low temperatures as well as high magnetic fields. The emphasis is on the quasi-2 dimensional thin grain boundary regions of nanodiamond films and one dimensional carbon nanotubes. As such nitrogen “doped” and undoped nanodiamond films were synthesized by the hot filament chemical vapor deposition method (HFCVD). The films were micro-structurally and electrically characterized using several techniques such as Raman spectroscopy, scanning electron microscopy, transmission electron microscopy, atomic force microscopy and magnetoresistance (MR) measurements. The electronic transport properties were compared to the films deposited by microwave plasma enhanced chemical vapour deposition (MWCVD). The conductivity revealed a typical semiconducting and semi-metallic behavior for the HFCVD films depending on the nitrogen percentage in the chamber. The dephasing time of the electronic wave function was found to be weakly temperature dependant i.e. τ T-p with p < 1, a behavior reported in artificial superlattices. These results show potential application of these materials in novel nano-electronic devices. Previously the transport mechanism in nanodiamond films has been attributed to hopping conduction in the grain boundaries which is predominately disordered sp2 phases. Our studies on nanodiamond films have however shown different mechanisms in these films. We observed very little contribution from hopping and pronounced weak localization contributions in nanodiamond films. We thus establish the significance of tunneling transport in nanodiamond films. We also studied the electronic transport in films of metal filled multiwalled carbon nanotubes which show significant contribution from the hopping mechanism and a negative magnetoresistance at low fields that crosses over into positive MR at high magnetic fields.
Zhang, Yu-Wei, and 張育維. "I. The Functionalization And Application of Nanodiamond II. The Synthesis of Iressa Analoques." Thesis, 2012. http://ndltd.ncl.edu.tw/handle/mw2t8r.
Full text國立東華大學
化學系
100
In this thesis presents the use of chemical method to modify the surface of nano-diamond by covalent bond. The functional groups of nano-diamond surface were analyzed by TGA-MS. The functional groups number on the surface of nano-diamond was evaluated by GC-MS. In addition the anticancer drug ─ Iressa, was modified and connect with Paclitaxel. The anti-cancer ability in under investigation.
Hsieh, Yi-Han, and 謝邑函. "I. The Functionalization And Application of Nanodiamond II. Synthesis of Chiral Bipyridine Ligand." Thesis, 2010. http://ndltd.ncl.edu.tw/handle/12557592684650598700.
Full text國立東華大學
化學系
99
We have developed a method to monitor the degree of functionalization of nanodiamond by subsequent esterification and hydrolysis. The efforts have been taken to increase the degree of functionalization under microwave condition. In the two different attempts of oxidation; by ozone as well as treatment with conc. HNO3; earlier method found to be superior over later. Better degree of functionalization has been observed with alkylation by short side chain over nanodiamond under microwave condition than alkylation with long side chain. Higher cell activeness is evident by paclitaxel modified nanodiamond under microwave condition. We have synthesized structurally similar derivatives 1-20, 1-3 of well-known anticancer drug Iressa. The derivative 1-20 showed higher cytotoxicity than Iressa, on the other hand 1-3 failed. Adopting strategy reported by Trost et al., 2, 2’-bipyridine ligand was modified by introducing phosphine moity to it, but unfortunately all attempts have been failed to isolate ligand 2-30. on the other hand, we also designed the ligand 2-A, which contains functionalities such as amine, amide, triazole group. But it has been proved inefficient to impart an asymmetric induction to the substrates as postulated.