Relevant bibliographies by topics / Nanocrystals composite material

Academic literature on the topic 'Nanocrystals composite material'

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Published: 11 March 2023

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Journal articles on the topic "Nanocrystals composite material"

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Ramires, Elaine C., Jackson D. Megiatto, Alain Dufresne, and Elisabete Frollini. "Cellulose Nanocrystals versus Microcrystalline Cellulose as Reinforcement of Lignopolyurethane Matrix." Fibers 8, no. 4 (March 29, 2020): 21. http://dx.doi.org/10.3390/fib8040021.

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Cellulose nanocrystals (CNC) exhibit remarkable properties such as being lightweight, renewability, nanoscale dimension, raw material availability, and a unique morphology. They have been widely used in film-forming composites, but the literature is scarce concerning bulky-composites (i.e., non-filmogenic). Microcrystalline cellulose (MCC) is widely available and has emerged as an important material for the reinforcement of composites. This investigation focuses on the preparation of non-filmogenic composites prepared from a polyurethane-type matrix, based on modified lignosulfonate and castor oil, reinforced with CNC or MCC, aiming to compare their reinforcing capacity. CNC was obtained through the acid hydrolysis of MCC. Sodium lignosulfonate was chemically modified using glutaraldehyde to increase its reactivity towards isocyanate groups in the synthesis of lignopolyurethane. The results show that adding CNC or MCC led to materials with improved impact strength, flexural properties, and storage modulus compared to pristine lignopolyurethane. With the exception of the flexural modulus, which was higher for the CNC-reinforced composite compared to the MCC-reinforced composite, all other properties were similar. The set of results indicates that CNC and MCC are promising for the reinforcement of polyurethane-type matrices. Bulky materials with good properties and prepared from high renewable raw material contents were obtained, meeting current expectations concerning sustainable development.
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Wijaya, Christian J., Felycia E. Soetaredjo, Suryadi Ismadji, and Setiyo Gunawan. "Synthesis of Cellulose Nanocrystals/HKUST-1 Composites and Their Applications: Crystal Violet Removal and Doxorubicin Loading." Polymers 14, no. 22 (November 18, 2022): 4991. http://dx.doi.org/10.3390/polym14224991.

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This study developed a novel composite material containing cellulose nanocrystals (CNCs) and HKUST-1. Here, the addition of CNCs was used to enhance the characteristics of HKUST-1 in terms of surface area, adsorption ability, and functional groups. Here, the fabrication of CNCs@HKUST-1 composites was carried out by adding CNCs into the fabrication process of HKUST-1. The addition of CNCs provides additional functional groups on the surface of composite material which can be used to attach other organic compounds, such as in waste management and drug delivery systems. Here, CNCs@HKUST-1 composites were tested as a material for crystal violet (CV) removal and doxorubicin (DOX) loading. The removal capacity of CNCs@HKUST-1 composite towards CV molecules reached 1182.25 ± 27.74 mg/g, while the loading capacity for DOX drugs was around 1514.94 ± 11.67 mg/g. Both applications showed that CNCs@HKUST-1 composite had higher adsorption capacity and ability compared to its precursor materials, i.e., CNCs and HKUST-1.
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Prokešová, Pavla, Nikolay Petkov, Jiří Čejka, Svetlana Mintova, and Thomas Bein. "Micro/Mesoporous Composites Based on Colloidal Zeolite Grown in Mesoporous Matrix." Collection of Czechoslovak Chemical Communications 70, no. 11 (2005): 1829–47. http://dx.doi.org/10.1135/cccc20051829.

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Composite materials containing micro- and mesopores are prepared under instantaneous hydrothermal treatment of initial solutions generally used for zeolite Beta and precursor solutions for mesoporous Al-MCM-41 material. The resulting composites are compared with pure, highly crystalline colloidal microporous Beta zeolite and hexagonally ordered mesostructured samples. The porosity and morphological features of the composite materials are influenced by the conditions of hydrothermal synthesis of the initial colloidal solutions used for the preparation of Beta seeds, as well as by the conditions of the synchronized crystallization of the final composites. The embedding of Beta seeds in the mesoporous silica matrix is possible via immediate heating of mesoporous precursor solutions with Beta seeds primarily formed. The composite materials contain either microcrystalline Beta nanodomains with sizes of about 5-10 nm surrounded by mesoporous material or defined Beta nanocrystals (20-40 nm), and at the same time connected with mesostructured material. The presence of highly crosslinked silicate framework walls and tetrahedrally coordinated aluminum in the composite material are confirmed by solid-state 29Si and 27Al MAS NMR spectroscopy. The concentration of Brønsted acid sites in the micro/mesoporous composites is increased substantially in comparison with pure mesoporous Al-MCM-41 material proven by FTIR acetonitrile-d3 adsorption study.
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Craievich, A. F., O. L. Alves, and L. C. Barbosa. "Formation and Growth of Semiconductor PbTe Nanocrystals in a Borosilicate Glass Matrix." Journal of Applied Crystallography 30, no. 5 (October 1, 1997): 623–27. http://dx.doi.org/10.1107/s0021889897001799.

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Pb- and Te-doped borosilicate glasses are transformed by appropriate heat treatment into a composite material consisting of a vitreous matrix in which semiconductor PbTe nanocrystals are embedded. This composite exhibits interesting non-linear optical properties in the infrared region, in the range 10–20 000 Å. The shape and size distribution of the nanocrystals and the kinetics of their growth were studied by small-angle X-ray scattering (SAXS) during in situ isothermal treatment at 923 K. The experimental results indicate that nanocrystals are nearly spherical and have an average radius increasing from 16 to 33 Å after 2 h at 923 K, the relative size dispersion being time-invariant and approximately equal to 8%. This investigation demonstrates that the kinetics of nanocrystal growth are governed by the classic mechanism of atomic diffusion. The radius of nanocrystals, deduced by applying the simple Efros & Efros [Sov. Phys. Semicond. (1982), 16, 772–775] model using the energy values corresponding to the exciton peaks of optical absorption spectra, does not agree with the average radius determined by SAXS.
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Zhu, Chunxia, Shuyu Pang, Zhaoxia Chen, Lehua Bi, Shuangfei Wang, Chen Liang, and Chengrong Qin. "Synthesis of Covalent Organic Frameworks (COFs)-Nanocellulose Composite and Its Thermal Degradation Studied by TGA/FTIR." Polymers 14, no. 15 (August 2, 2022): 3158. http://dx.doi.org/10.3390/polym14153158.

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At present, the synthesis methods of crystalline porous materials often involve powder products, which not only affects the practical application but also has complex synthesis operations and limited scale. Based on the mechanochemical method, we choose COF-TpPa-1, preparing TpPa-1-DANC composites. Covalent organic frameworks (COFs) are a kind of crystalline material formed by covalent bonds of light elements. COFs possess well pore structure and high thermal stability. However, the state of synthesized powders limits their application. Cellulose nanocrystals (CNCs) are promising renewable micron materials with abundant hydroxyl groups on their surface. It is possible to prepare high-strength materials such as film, water, and aerogel. Firstly, the nanocellulose was oxidized by the sodium periodate method to obtain aldehyde cellulose nanocrystals (DANC). TpPa-1-DANC not only had the crystal characteristic peak of COFs at 2θ ≈ 5° but also had a BET surface area of 247 m2/g. The chemical bonds between COFs and DANC formed by Schiff base reaction appeared in FTIR and XPS. The pyrolysis behavior of the composite was characterized by TG-IR, which showed that the composite had good thermal stability. With the advantages of nanocellulose as a material in every dimension, we believe that this method can be conducive to the large-scale synthesis of COFs composites, and has the possibility of multi-form synthesis of COFs.
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Cherevkov, Sergei, Ruslan Azizov, Anastasiia Sokolova, Valeriia Nautran, Mikhail Miruschenko, Irina Arefina, Mikhail Baranov, et al. "Interface Chemical Modification between All-Inorganic Perovskite Nanocrystals and Porous Silica Microspheres for Composite Materials with Improved Emission." Nanomaterials 11, no. 1 (January 7, 2021): 119. http://dx.doi.org/10.3390/nano11010119.

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In recent years, there has been rapid progress in the development of photonic devices based on lead halide perovskite nanocrystals since they possess a set of unique optical and charge transport properties. However, the main limiting factor for their subsequent application is poor stability against exposure to adverse environmental conditions. In this work, a study of a composite material based on perovskite CsPbBr3 nanocrystals embedded in porous silica microspheres is presented. We developed two different approaches to change the interface between nanocrystals and the surface of the microsphere pores: surface treatment of (i) nanocrystals or (ii) microspheres. The surface modification with tetraethylorthosilicate molecules not only increased stability but also improved the optical responses of the composite material. The position of the emission band remained almost unchanged, but its lifetime increased significantly compared to the initial value. The improvement of the optical performance via surface modification with tetraethylorthosilicate molecules also works for the lead-free Bi-doped Cs2AgInCl6 double perovskite nanocrystals leading to increased stability of their optical responses at ambient conditions. These results clearly demonstrate the advantage of a composite material that can be used in novel photonic devices with improved performance.
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Petrella, A., M. Tamborra, P. D. Cozzoli, M. L. Curri, M. Striccoli, P. Cosma, G. M. Farinola, F. Babudri, F. Naso, and A. Agostiano. "TiO2 nanocrystals – MEH-PPV composite thin films as photoactive material." Thin Solid Films 451-452 (March 2004): 64–68. http://dx.doi.org/10.1016/j.tsf.2003.10.106.

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Huo, Ying, Yingying Liu, Mingfeng Xia, Hong Du, Zhaoyun Lin, Bin Li, and Hongbin Liu. "Nanocellulose-Based Composite Materials Used in Drug Delivery Systems." Polymers 14, no. 13 (June 29, 2022): 2648. http://dx.doi.org/10.3390/polym14132648.

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Nanocellulose has lately emerged as one of the most promising “green” materials due to its unique properties. Nanocellulose can be mainly divided into three types, i.e., cellulose nanocrystals (CNCs), cellulose nanofibrils (CNFs), and bacterial cellulose (BC). With the rapid development of technology, nanocellulose has been designed into multidimensional structures, including 1D (nanofibers, microparticles), 2D (films), and 3D (hydrogels, aerogels) materials. Due to its adaptable surface chemistry, high surface area, biocompatibility, and biodegradability, nanocellulose-based composite materials can be further transformed as drug delivery carriers. Herein, nanocellulose-based composite material used for drug delivery was reviewed. The typical drug release behaviors and the drug release mechanisms of nanocellulose-based composite materials were further summarized, and the potential application of nanocellulose-based composite materials was prospected as well.
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Liu, Sichen, Yanbo Yu, Kelu Ni, Tongda Liu, Min Gu, Yingchen Wu, Guanben Du, and Xin Ran. "Construction of a novel electrochemical sensor based on biomass material nanocellulose and its detection of acetaminophen." RSC Advances 12, no. 43 (2022): 27736–45. http://dx.doi.org/10.1039/d2ra04125a.

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Ozola, Zanda U., Rudite Vesere, Silvija N. Kalnins, and Dagnija Blumberga. "Paper Waste Recycling. Circular Economy Aspects." Environmental and Climate Technologies 23, no. 3 (December 1, 2019): 260–73. http://dx.doi.org/10.2478/rtuect-2019-0094.

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Abstract Paper waste is a raw material for a lot of products with different added value. The engineering, economic and environmental aspects of paper waste recycling are analysed for production of composite material, cellulose nanofibers and nanocrystals, bricks with paper components, porous carbon, film of biopolymer, enzymatic sugar and bioenergy: bioethanol, hydrogen and biofuel. Through multicriteria analysis, it was possible to determine the most feasible paper waste recycling product in case of four product groups: egg packaging boxes, cardboard, reused paper, cellulose nanomaterials (nanofibers and nanocrystals). The production of cellulose nanofibres and cellulose nanocrystals has an advantage over egg packaging and cardboard production as well as reusable paper.
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Dissertations / Theses on the topic "Nanocrystals composite material"

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Cozzarini, Luca. "Nanomaterials based on II-VI Semiconductors." Doctoral thesis, Università degli studi di Trieste, 2012. http://hdl.handle.net/10077/7359.

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2010/2011
This thesis describes: (i) synthesis and characterization of colloidal nanocrystals of II-VI semiconductor compounds; (II) development of two novel materials using such nanocrystals as “building blocks”: (IIa) a nanocrystals/polymer composite, to be used as phosphor in LED-based lighting devices; (IIb) an inorganic, nano-structured multiphase material, showing a promising geometry as an electronic intermediate band material. Different typologies of nanocrystals (single-phase, alloyed or core-shells) were successfully synthesized using air-stable, safe reagents. Their optical properties (absorption spectrum, fluorescence wavelength and fluorescence quantum yield) were mapped as function of different parameters. Good results in engineering optical properties were achieved by: (a) changing size and/or composition in single-phase nanocrystals; (b) tuning shell composition and thickness and/or mutually diffusing one material into the other in multi-phase nanocrystals. The influence of different surface ligands on optical properties and on solubility in different media was also studied. Nanocrystal/polymer composite lenses were obtained from nanocrystals with desired fluorescence wavelength and quantum yield, mixed in an appropriate solvent with polymer pellets. The mixture was drop casted or tape casted on a solid substrate, obtaining solid, transparent lenses after solvent evaporation. A nano-structured, all-inorganic material (composed of semiconducor nanocrystals embedded into a wider bandgap semiconductor) was obtained through self-assembly and densification of colloidal core-shells nanocrystals. The realization of this composite supracrystal was achieved via a multi-step process: (i) colloidal synthesis of core-shell nanocrystals; (ii) surface ligands exchange; (iii) assembly; (iv) heat treatment. Evolution of the optical properties during heat treatment suggests that it is possible to sinter the shell material without altering the internal nano-heterostructure, if temperature and time of the treatment are controlled properly.
In questa tesi sono descritti: (I) la sintesi colloidale e la caratterizzazione di nanocristalli di semiconduttori II-VI; (II) lo sviluppo, utilizzando i suddetti nanocristalli quali “unità da costruzione”, di due materiali innovativi: (IIa) un composito nanocristalli/polimero, da usare come fosforo in dispositivi per illuminazione basati su LED; (IIb) un materiale inorganico nano-strutturato multifase, con una geometria promettente quale materiale a banda elettronica intermedia. Differenti semiconduttori II-VI sono stati sintetizzati in forma di nanocristalli (monofasici, in forma di lega o in struttura di tipo “core-shell”) usando reagenti sicuri e stabili in atmosfera. Le loro proprietà ottiche (spettro di assorbimento, lunghezza d’onda di fluorescenze e resa quantica di fluorescenza) sono state mappate in funzione di numerosi parametri. Sono stati raggiunti ottimi risultati nel controllo delle proprietà ottiche sia in nanocristalli a fase singola (modificandone le dimensioni o la composizione chimica) che in nanocristalli multifase (regolandone la composizione e lo spessore della “shell”, nonché mutualmente diffondendo un materiale nell’altro). È stata anche studiata l’influenza di differenti leganti superficiali sulle proprietà ottiche e sulla solubilità dei nanocristalli in differenti solventi. Lenti composite di nanocristalli/polimero sono state ottenute a partire da nanocristalli aventi la lunghezza d’onda e la resa quantica di fluorescenza desiderate, mescolandoli con pellet di polimero in solventi appropriati. La miscela è stata depositata su un supporto, tramite drop casting o tape casting, ottenendo lenti solide trasparenti dopo l’evaporazione del solvente. Un materiale inorganico nano strutturato (costituito da nanocristalli di semiconduttore racchiusi all’interno di un secondo materiale semiconduttore a bandgap maggiore) è stato ottenuto tramite l’autoassemblaggio e la densificazione di nanocristalli core-shell sintetizzati con procedure di chimica colloidale. La realizzazione di suddetto sovra-cristallo si è svolta in più fasi: (i) sintesi colloidale; (ii) sostituzione dei leganti superficiali; (iii) assemblaggio; (iv) trattamento termico. I risultati derivanti dallo studio dell’evoluzione delle proprietà ottiche durante il trattamento termico suggeriscono che sia possibile sinterizzare il materiale della shell senza alterare la nano-eterostruttura interna, se la temperatura e il tempo del trattamento sono scelti opportunamente.
XXIV Ciclo
1983
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Lee, Jinwook 1966. "Semiconductor nanocrystal composite materials and devices." Thesis, Massachusetts Institute of Technology, 2002. http://hdl.handle.net/1721.1/8039.

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Thesis (Ph.D.)--Massachusetts Institute of Technology, Dept. of Materials Science and Engineering, 2002.
Includes bibliographical references.
This thesis describes the synthesis and characterization of semiconductor nanocrystal (quantum dot, QD) embedded composite materials and possible device applications of the resulting luminescent materials. Chemically synthesized ZnS overcoated CdSe, (CdSe)ZnS, QDs are incorporated into a polymer host material. The main challenge in the preparation of QD-polymer composites is the prevention of both phase separation and aggregation of the QDs within the polymer host material, while sustaining the original quantum efficiency of the QDs in their growth solution. Possible ways to incorporate QDs into an optically clear polymer matrix are considered. A guideline for a successful QD-polymer composite is discussed for various polymer systems: ligand polymers, ligand monomer and covalent bonding to a polymer matrix, and in-situ polymerization. The best composite system is based on incorporation of QDs into a poly(laurylmethacrylate) matrix during in-situ polymerization in the presence of TOP ligands. The successful incorporation of QDs into a polymer host material demonstrates the ability to form QD-polymer composite light emitting materials. The emission spans nearly the entire region of saturated and mixed colors with narrow emission profiles. The light emission spectra of QD-polymer composites excited by a blue diode light are also simulated by Monte Carlo methods and compared to the measured spectra from actual devices. The synthesis and characterization of QD-microspheres, which can be used as active fluorescent building blocks, are also described.
(cont.) In order to enhance the stability and compatibility of QDs in a polymer microsphere, the QDs are treated with polymerizable phosphine ligands, small oligomeric phosphine methacrylate (SOPM), and the following homogeneous solution polymerization is investigated to form monodisperse QD-microspheres. The QD-microspheres can store optical information assigned by embedded QDs in multiple codes. The surface functionalization of these capsules could provide a means for attaching capsules to surfaces and allow capsules to assemble into 3D structures.
by Jinwook Lee.
Ph.D.
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Way, Amanda E. "Stimuli-Responsive Nanofiber Composite Materials: From Functionalized Cellulose Nanocrystals to Guanosine Hydrogels." Case Western Reserve University School of Graduate Studies / OhioLINK, 2014. http://rave.ohiolink.edu/etdc/view?acc_num=case1390388160.

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Seregin, Vladimir Victor. "Part I, Fabrication and surface modification of composite biomaterials based on silicon and calcium disilicide Part II, Synthesis and characterization of erbium doped silicon nanocrystals encapsulated by aluminum and zinc oxides /." Fort Worth, Tex. : Texas Christian University, 2006. http://etd.tcu.edu/etdfiles/available/etd-04252006-145309/unrestricted/seregin.pdf.

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Berkowitz, Kyle Matthew. "Characterization and Analysis of Shape Memory Polymer Composites With Cellulose Nanocrystal Fillers." Case Western Reserve University School of Graduate Studies / OhioLINK, 2014. http://rave.ohiolink.edu/etdc/view?acc_num=case1396526722.

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Angellier, Hélène. "Nanocristaux d'amidon de maïs cireux pour applications composites." Phd thesis, Université Joseph Fourier (Grenoble), 2005. http://tel.archives-ouvertes.fr/tel-00010699.

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Une suspension aqueuse de nanocristaux d'amidon de maïs cireux est obtenue par hydrolyse acide de grains d'amidon (longueur:40-60nm, largeur:15-30nm, épaisseur:5-7nm). Le premier objectif de la thèse est l'optimisation de la préparation de ces nanocristaux par la mise en place d'un plan d'expériences. Leur structure moléculaire est ensuite étudiée par dégradation enzymatique, et leur modification chimique de surface est envisagée. Le deuxième objectif est l'utilisation de ces nanocristaux comme charge de renfort dans une matrice polymère. Deux polymères naturels ont été choisis: le latex de caoutchouc naturel et l'amidon thermopalstique. Les nanocomposites, mis en oeuvre par casting, sont caractérisés en termes de propriétés morphologiques, structurales, barrière et mécaniques.
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Kehrle, Julian [Verfasser], Bernhard [Akademischer Betreuer] Rieger, Johann Peter [Gutachter] Plank, and Bernhard [Gutachter] Rieger. "Surface Hydrosilylation: The Key to Silicon Nanocrystal Hybrid and Composite Materials / Julian Kehrle ; Gutachter: Johann Peter Plank, Bernhard Rieger ; Betreuer: Bernhard Rieger." München : Universitätsbibliothek der TU München, 2018. http://d-nb.info/1170321615/34.

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Sonseca, Olalla Agueda. "DEVELOPMENT OF SHAPE-MEMORY COMPOSITES BASED ON A BIODEGRADABLE POLYESTER ELASTOMER." Doctoral thesis, Universitat Politècnica de València, 2019. http://hdl.handle.net/10251/54129.

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[EN] The current PhD thesis deals with the development and characterization of novel nanocomposites based on biodegradable poly(mannitol sebacate) (PMS) matrices with tailored properties and shape-memory capabilities for biomedical applications. Two types of fillers -cellulose nanocrystals (CNC) and electrospun poly(lactic acid) nanofibers (NF-PLA)- were used as reinforcement in order to induce and/or enhance the shape-memory properties of PMS matrices. Also, different crosslinking profiles and stoichiometric ratios between mannitol and sebacic acid (1:1 and 1:2) were studied and evaluated to obtain samples with low and high degrees of crosslinking. An appropriate combination of the crosslinking profile and the monomer ratio for PMS matrix, as well as the addition of low content of CNC, allowed the development of PMS/CNC nanocomposites with a wide range of mechanical properties and degradation profiles. On the other hand, highly oriented poly(lactic acid) (PLA) nanofiber mats obtained by electrospinning were embedded in the PMS matrices. An enhancement of up to 53-fold in the Young's modulus was observed for PMS/NF-PLA nanocomposites filled with 15 wt% of PLA nanofibers. The incorporation of fillers (CNC and NF-PLA) allowed the development of thermally active shape-memory nanocomposites with an enhancement of parameters such as recovery stress and shape fixity. The electrospun PLA-reinforced nanocomposites, offered the best balance of mechanical and thermal properties, as well as a greater control of the transition temperature for switching the change of shape, within a useful range of temperatures. Owing to that, these materials may be of interest as smart responsive systems in long-term biomedical applications.
[ES] La presente tesis doctoral, se centra en el desarrollo y caracterización de nuevos nanocompuestos biodegradables, a partir de matrices de poli(mannitol sebacato) (PMS) con propiedades a medida y capacidades de memoria de forma para aplicaciones biomédicas. Dos tipos de cargas -nanocristales de celulosa (CNC) y nanofibras de ácido poliláctico (NF-PLA) obtenidas mediante electrospinning- se han utilizado como refuerzo, con la finalidad de inducir y/o mejorar las propiedades de memoria de forma en matrices de PMS. Se han estudiado y evaluado diferentes tratamientos de curado y ratios de reacción entre el mannitol y ácido sebácico (1:1 y 1:2), con la finalidad de obtener muestras con bajo y alto grado de reticulación. Una combinación adecuada del tratamiento de curado y el ratio entre monómeros del PMS, así como la adición de bajos contenidos de CNC, permitió desarrollar nanocompuestos de PMS/CNC con un amplio rango de propiedades mecánicas y perfiles de degradación. Por otro lado, se han producido mats de nanofibras de ácido poliláctico (PLA) con alta orientación mediante la técnica de electrospinning, para embeberse en matrices de PMS, observándose una mejora de hasta 53 veces en el módulo de Young para nanocompuestos de PMS/NF-PLA con un 15% en peso de nanofibras. La incorporación de cargas (CNC y NF-PLA) permitió el desarrollo de nanocompuestos con memoria de forma activada térmicamente, con una mejora de parámetros tales como la fuerza de recuperación y la capacidad de fijación. Los nanocompuestos reforzados con NF-PLA obtenidas por electrospinning, ofrecieron el mejor balance de propiedades mecánicas y térmicas, así como un mayor control de la temperatura de transición para la activación del cambio de forma en un intervalo útil de temperaturas. Por todo ello, estos materiales pueden resultar de interés como sistemas activos en aplicaciones biomédicas de larga duración.
[CAT] La present tesi doctoral se centra en el desenvolupament i caracterització de nous nanocompostos biodegradables a partir de matrius de poli(mannitol sebacato) (PMS) amb propietats a mesura i capacitats de memòria de forma per a aplicacions biomèdiques. Dos tipus de càrregues -nanocristals de cel·lulosa (CNC) i nanofibres d'àcid polilàctic (NF-PLA) obtingudes mitjançant electrospinning- s'han utilitzat com a reforç amb la finalitat d'induir i/o millorar les propietats de memòria de forma en matrius de PMS. S'han estudiat i avaluat diferents tractaments de curat i ràtios de reacció entre el mannitol i àcid sebàcic (1:1 i 1:2) amb la finalitat d'obtenir mostres amb baix i alt grau de reticulació. Una combinació adequada del tractament de curat i el ràtio entre monòmers del PMS, així com l'addició de baixos continguts de CNC, va permetre desenvolupar nanocompostos de PMS/CNC amb un ampli rang de propietats mecàniques i perfils de degradació. D'altra banda, s'han produït mats de nanofibres d'àcid polilàctic (PLA) amb alta orientació mitjançant la tècnica de electrospinning, per embeure's en matrius de PMS, observant-se una millora de fins a 53 vegades en el mòdul de Young per nanocompostos de PMS/NF-PLA amb un 15% en pes de nanofibres. La incorporació de càrregues (CNC i NF-PLA) va permetre el desenvolupament de nanocompostos amb memòria de forma activada tèrmicament, amb una millora de paràmetres tals com la força de recuperació i la capacitat de fixació. Els nanocompostos reforçats amb NF-PLA obtingudes per electrospinning, van oferir el millor balanç de propietats mecàniques i tèrmiques, així com un major control de la temperatura de transició per a l'activació del canvi de forma en un interval útil de temperatures. Per tot això, aquests materials poden resultar d'interés com a sistemes actius en aplicacions biomèdiques de llarga durada.
Sonseca Olalla, A. (2015). DEVELOPMENT OF SHAPE-MEMORY COMPOSITES BASED ON A BIODEGRADABLE POLYESTER ELASTOMER [Tesis doctoral no publicada]. Universitat Politècnica de València. https://doi.org/10.4995/Thesis/10251/54129
TESIS
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Wang, Qi. "Electrochemical synthesis of CeO2 and CeO2/montmorillonite nanocomposites." Thesis, University of North Texas, 2003. https://digital.library.unt.edu/ark:/67531/metadc4378/.

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Nanocrystalline cerium oxide thin films on metal and semiconductor substrates have been fabricated with a novel electrodeposition approach - anodic oxidation. X-ray diffraction analysis indicated that as-produced cerium oxide films are characteristic face-centered cubic fluorite structure with 5 ~ 20 nm crystal sizes. X-ray photoelectron spectroscopy study probes the non-stoichiometry property of as-produced films. Raman spectroscopy and Scanning Electron Microscopy have been applied to analyze the films as well. Deposition mode, current density, reaction temperature and pH have also been investigated and the deposition condition has been optimized for preferred oriented film formation: galvanostatic deposition with current density of -0.06 mA/cm2, T > 50oC and 7 < pH < 10. Generally, potentiostatic deposition results in random structured cerium oxide films. Sintering of potentiostatic deposited cerium oxide films leads to crystal growth and reach nearly full density at 1100oC. It is demonstrated that in-air heating favors the 1:2 stoichiometry of CeO2. Nanocrystalline cerium oxide powders (4 ~ 10 nm) have been produced with anodic electrochemical synthesis. X-ray diffraction and Raman spectroscopy were employed to investigate lattice expansion phenomenon related to the nanoscale cerium oxide particles. The pH of reaction solution plays an important role in electrochemical synthesis of cerium oxide films and powder. Cyclic voltammetry and rotation disk electrode voltammetry have been used to study the reaction mechanisms. The results indicate that the film deposition and powder formation follow different reaction schemes. Ce(III)-L complexation is a reversible process, Ce3+ at medium basic pH region (7~10) is electrochemically oxidized to and then CeO2 film is deposited on the substrate. CE mechanism is suggested to be involved in the formation of films, free Ce3+ species is coordinated with OH- at high basic pH region (>10) to Ce2O3 immediately prior to electrochemically oxidation Ce2O3 to CeO2. CeO2 / montmorillonite nanocomposites were electrochemically produced. X-ray diffraction and Raman spectroscopy illustrate the retaining of FCC structure for cerium oxide. Fourier Transform Infrared Spectroscopy and Differential Scanning Calorimetry of composites indicate the insertion of montmorillonite platelets into the structural matrix of cerium oxide. Sintering study of the nanocomposites demonstrates that low concentration of montmorillonite platelet coordination into cerium oxide matrix increases crystal growth rate whereas high concentration of montmoillonite in nanocomposites retards the increase of crystallite size during the densification process.
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Guidetti, Giulia. "Cellulose photonics : designing functionality and optical appearance of natural materials." Thesis, University of Cambridge, 2018. https://www.repository.cam.ac.uk/handle/1810/277918.

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Cellulose is the most abundant biopolymer on Earth as it is found in every plant cell wall; therefore, it represents one of the most promising natural resources for the fabrication of sustainable materials. In plants, cellulose is mainly used for structural integrity, however, some species organise cellulose in helicoidal nano-architectures generating strong iridescent colours. Recent research has shown that cellulose nanocrystals, CNCs, isolated from natural fibres, can spontaneously self-assemble into architectures that resemble the one producing colouration in plants. Therefore, CNCs are an ideal candidate for the development of new photonic materials that can find use to substitute conventional pigments, which are often harmful to humans and to the environment. However, various obstacles still prevent a widespread use of cellulose-based photonic structures. For instance, while the CNC films can display a wide range of colours, a precise control of the optical appearance is still difficult to achieve. The intrinsic low thermal stability and brittleness of cellulose-based films strongly limit their use as photonic pigments at the industrial scale. Moreover, it is challenging to integrate them into composites to obtain further functionality while preserving their optical response. In this thesis, I present a series of research contributions that make progress towards addressing these challenges. First, I use an external magnetic field to tune the CNC films scattering response. Then, I demonstrate how it is possible to tailor the optical appearance and the mechanical properties of the films as well as to enhance their functionality, by combining CNCs with other polymers. Finally, I study the thermal properties of CNC films to improve the retention of the helicoidal arrangement at high temperatures and to explore the potential use of this material in industrial fabrication processes, such as hot-melt extrusion.
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Books on the topic "Nanocrystals composite material"

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Kumar, Dinesh. Nanocellulose and Its Composites for Water Treatment Applications. Taylor & Francis Group, 2021.

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Kumar, Dinesh. Nanocellulose and Its Composites for Water Treatment Applications. Taylor & Francis Group, 2021.

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Kumar, Dinesh. Nanocellulose and Its Composites for Water Treatment Applications. Taylor & Francis Group, 2021.

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Nanocellulose and Its Composites for Water Treatment Applications. Taylor & Francis Group, 2021.

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Book chapters on the topic "Nanocrystals composite material"

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Thiyagarajan, P., M. Kottaisamy, and M. S. Ramachandra Rao. "Synthesis and Characterization of ZnO-Based Phosphors and Related Phosphor Composites in Bulk, Thin Film and Nano Form." In ZnO Nanocrystals and Allied Materials, 247–68. New Delhi: Springer India, 2013. http://dx.doi.org/10.1007/978-81-322-1160-0_12.

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Striccoli, M., M. L. Curri, and R. Comparelli. "Nanocrystal-Based Polymer Composites as Novel Functional Materials." In Toward Functional Nanomaterials, 173–92. New York, NY: Springer US, 2009. http://dx.doi.org/10.1007/978-0-387-77717-7_4.

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Pakzad, Anahita, and Reza S. Yassar. "Mechanics of Cellulose Nanocrystals and their Polymer Composites." In New Frontiers of Nanoparticles and Nanocomposite Materials, 233–63. Berlin, Heidelberg: Springer Berlin Heidelberg, 2010. http://dx.doi.org/10.1007/8611_2010_38.

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Dunlop, Matthew J., Bishnu Acharya, and Rabin Bissessur. "Effect of Cellulose Nanocrystals on the Mechanical Properties of Polymeric Composites." In Biocomposite Materials, 77–95. Singapore: Springer Singapore, 2021. http://dx.doi.org/10.1007/978-981-33-4091-6_4.

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Mondal, Kona, Neha Mulchandani, Somashree Mondal, and Vimal Katiyar. "Development of Biomass-Derived Cellulose Nanocrystals and its Composites." In Materials Horizons: From Nature to Nanomaterials, 237–69. Singapore: Springer Singapore, 2020. http://dx.doi.org/10.1007/978-981-15-1251-3_11.

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Zhong, Linxin, and Xinwen Peng. "Biorenewable Nanofiber and Nanocrystal: Renewable Nanomaterials for Constructing Novel Nanocomposites." In Handbook of Composites from Renewable Materials, 155–226. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2017. http://dx.doi.org/10.1002/9781119441632.ch130.

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Yuan, Quan, Xiao Dong Guo, Qi Xin Zheng, Ming Zhao, Zheng Qi Pan, Shun Guang Chen, and Da Ping Quan. "Bioinspired Growth of Hydroxyapatite Nanocrystals on PLGA- (PEG- ASP)n Scaffolds Modified with Oligopeptide Derived from BMP-2." In Advances in Composite Materials and Structures, 1261–64. Stafa: Trans Tech Publications Ltd., 2007. http://dx.doi.org/10.4028/0-87849-427-8.1261.

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Chen, Nan Chun, and Dong Chen. "From Kaolins (with Addition of Al2O3) to Mullite Composite Nanocrystals: Experiments and Analysis." In Key Engineering Materials, 2264–66. Stafa: Trans Tech Publications Ltd., 2007. http://dx.doi.org/10.4028/0-87849-410-3.2264.

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Rahimi, Shahab Kashani, and Joshua U. Otaigbe. "Green hybrid composites from cellulose nanocrystal." In Hybrid Polymer Composite Materials, 65–99. Elsevier, 2017. http://dx.doi.org/10.1016/b978-0-08-100791-4.00004-5.

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Soosaimanickam, Ananthakumar, Pedro J. Rodríguez-Cantó, Juan P. Martínez-Pastor, and Rafael Abargues. "Preparation and processing of nanocomposites of all-inorganic lead halide perovskite nanocrystals." In Hybrid Perovskite Composite Materials, 19–93. Elsevier, 2021. http://dx.doi.org/10.1016/b978-0-12-819977-0.00002-0.

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Conference papers on the topic "Nanocrystals composite material"

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Shao, Wenyao, and Mengwen Yan. "Solvothermal synthesis of cobalt oxides nanocrystals." In 2ND INTERNATIONAL CONFERENCE ON COMPOSITE MATERIALS AND MATERIAL ENGINEERING (ICCMME 2017). Author(s), 2017. http://dx.doi.org/10.1063/1.4983602.

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Illera, Danny, Victor Fontalvo, and Humberto Gomez. "Cellulose Nanocrystals Assisted Preparation of Electrochemical Energy Storage Electrodes." In ASME 2017 International Mechanical Engineering Congress and Exposition. American Society of Mechanical Engineers, 2017. http://dx.doi.org/10.1115/imece2017-71495.

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Renewable energy sources demands sustainable energy storage technologies through the incorporation of low-cost and environment-friendly materials. In this regard, cellulose nanocrystals (CN), which are needle-shaped nanostructure derived from cellulose-rich resources, are extracted by sulfuric acid hydrolysis of biomass and used as both template and binder for the construction of electrochemical capacitors electrodes. A composite material is synthetized comprising CN and a conjugated electroactive polymer (CEP) to overcome the electrical insulating properties of cellulose as well as to exploit enhanced electrochemical activity by increased electrode surface-area. A one-step in-situ film synthesis protocol is evaluated by performing simultaneous polymerization and film deposition. The effect of proportion of starting components are evaluated through statistical Response Surface Methodology towards optimizing the electrochemical performance. Depending on the mass proportion of the starting components, a conducting network could be created by surface coating of the CEP on the whiskers during polymerization. Electrochemical measurements suggest an increase in specific surface area by at least a factor of two relative to bare CEP as a consequence of the template role of cellulose. Therefore, adjustment of the proposed one-step synthesis parameters allows tuning the material properties to meet specific application requirements regarding electrochemical performance.
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ZHANG, Meng, Jing WANG, Shi CHEN, and Feng WU. "Electrospun Composite of Fe3O4/Cu Nanocrystals Encapsulated in Carbon Fibers as an Anode Material with High Rate Capability for Lithium Ion Batteries." In 3rd International Conference on Material Engineering and Application (ICMEA 2016). Paris, France: Atlantis Press, 2016. http://dx.doi.org/10.2991/icmea-16.2016.63.

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Roberts, N. A., D. G. Walker, and D. Y. Li. "Molecular Dynamics Simulation of Thermal Conductivity of Nanocrystalline Composite Films." In ASME/JSME 2007 Thermal Engineering Heat Transfer Summer Conference collocated with the ASME 2007 InterPACK Conference. ASMEDC, 2007. http://dx.doi.org/10.1115/ht2007-32520.

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The effectiveness of a thermoelectric device is measured by the figure of merit ZT, which is inversely proportional to the thermal conductivity. Superlattice materials often have a reduced thermal conductivity because of the introduction of interface scattering and, therfore, improved performance. The present work is focused on the effective thermal conductivity of nanocomposite films. This configuration could also improve ZT because of phonon-interface scattering introduced by the nanocrystals. The effects of crystal size and mass fraction is studied numerically using a molecular dynamics simulation. Results indicate that a reduction in the effective thermal conductivity can be achieved with the addition of a nanocrystal.
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Kumar, D., N. Sudhir, S. Yarmolenko, Q. Wei, J. Sankar, J. Narayan, and S. J. Pennycook. "Synthesis and Characterization of Metal-Ceramic Thin Film Nanocomposites With Improved Mechanical Properties." In ASME 2002 International Mechanical Engineering Congress and Exposition. ASMEDC, 2002. http://dx.doi.org/10.1115/imece2002-39370.

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Thin films composite materials consisting of metallic nanocrystals embedded in an insulator host have been synthesized using alternating-target pulsed laser deposition of Fe/Ni and Al2O3. The evaluation of structural quality of the thin film composites using high resolution transmission electron microscopy and scanning transmission electron microscopy with atomic number contrast has revealed the formation of a biphase system with thermodynamically driven segregation of Ni and alumina during pulsed laser deposition. The best hardness values of the thin film composites, measured using nanoindentation techniques, was found to 20–30% larger than pure alumina films fabricated under identical conditions. The improvement in values of hardness of Al2O3 thin films by embedding metal nanocrystals is related to the evolution of a microstructure which efficiently hinders the manipulation and movement of dislocation and the growth of microcracks, which in turn, is achieved by grain boundary hardening.
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Sheveleva, Irina V., Veniamin V. Zheleznov, Svetlana Yu Bratskaya, Valery G. Kuryavyi, and Valentin A. Avramenko. "Adsorption of Cesium Radionuclides by the Composite Sorbents Carbon Fiber/Transition Metals Ferrocyanides." In ASME 2011 14th International Conference on Environmental Remediation and Radioactive Waste Management. ASMEDC, 2011. http://dx.doi.org/10.1115/icem2011-59255.

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Among various methods of cesium removal from aqueous solutions, sorption using transition metals ferrocyanides is the most efficient method due to extremely high affinity of cesium ions to ferrocyanides. The efficiency of transition metals ferrocyanides application is known to depend on the crystal size being the highest for nanocrystals. Although nanocrystals are difficult to handle in direct application, they can be used in composite materials. In this case two main problems arise: how to control the crystal size of transition metals ferrocyanides and fix them reliably in the supporting matrix. Here we suggest a new route to preparation of composite materials selective to cesium ions using transition metals ferrocyanides stabilized by siloxane-acrylate latexes. The size of transition metals ferrocyanides is controlled by the size of latex particles and their stability is determined by ionization of polyacrylic acid carboxylic groups on the functionalized latex surface. These functionalized particles can be used as precursors in preparation of composite materials by sedimentation and polymerization of latexes on the solid surface of porous matrix, e.g. carbon fibers. Several routes of preparation of carbon fiber based composite materials using functionalized latexes and sorption properties of the obtained materials are discussed. The effect of preparation conditions (method used, carbon fiber polarization potential, concentration of latexes functionalized with transition metals ferrocyanides) on cesium uptake by composite sorbents from solutions of various salinity is reported.
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Kim, Jaehwan, Lindong Zhai, Seongcheol Mun, Hyun-U. Ko, and Young-Min Yun. "Cellulose nanocrystals, nanofibers, and their composites as renewable smart materials." In SPIE Smart Structures and Materials + Nondestructive Evaluation and Health Monitoring, edited by Vijay K. Varadan. SPIE, 2015. http://dx.doi.org/10.1117/12.2084996.

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Yang, Jun-Song, and Fu-Zhi Shen. "Preparation and Ferromagnetic Behavior of Fe3O4-Graphene Oxide Composite Nanocrystals." In 2016 International Conference on Mechanics and Materials Science (MMS2016). WORLD SCIENTIFIC, 2017. http://dx.doi.org/10.1142/9789813228177_0098.

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Ghosh, Subhabrata, and B. N. Shivakiran Bhaktha. "Eu-doped on-chip blue-light emitting glass-ceramic waveguides." In JSAP-OSA Joint Symposia. Washington, D.C.: Optica Publishing Group, 2017. http://dx.doi.org/10.1364/jsap.2017.8a_pb2_2.

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Rare-earth (RE) activated glass-ceramics are two phase composite materials consisting of nanocrystals embedded in amorphous matrix, combining the advantages of optical glasses with the crystal-like environment for RE-ions [1, 2]. Hence, RE-doped transparent glass-ceramic waveguides are widely adopted for integrated optic applications such as on-chip lasers, optical amplifiers etc. [3, 4] because of their narrow and intense emission from 4f-intrashell transition.
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Fortunati, E., and L. Torre. "Cellulose nanocrystals in nanocomposite approach: Green and high-performance materials for industrial, biomedical and agricultural applications." In VIII INTERNATIONAL CONFERENCE ON “TIMES OF POLYMERS AND COMPOSITES”: From Aerospace to Nanotechnology. Author(s), 2016. http://dx.doi.org/10.1063/1.4949586.

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