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Journal articles on the topic 'Nanocarbons syntheses'

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Author: Grafiati

Published: 10 March 2023

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1

Kecsenovity, Egon, Balazs Endrodi, and Csaba Janáky. "(Invited) Rationally Designed Semiconductor/Nanocarbon Photoelectrodes for Solar Fuel Generation." ECS Meeting Abstracts MA2018-01, no. 31 (April 13, 2018): 1880. http://dx.doi.org/10.1149/ma2018-01/31/1880.

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Given that CO2 is a greenhouse gas, using the energy of sunlight to convert CO2 to transportation fuels (such as methanol or methane) represents a value-added approach to the simultaneous generation of alternative fuels and environmental remediation of carbon emissions. Electrochemistry and photoelectrochemistry have been proven to be a useful avenue for solar water splitting. CO2 reduction, however, is multi-electron in nature (e.g., 6 e- to methanol) with considerable kinetic barriers to electron transfer. It therefore requires the use of carefully designed electrode surfaces to accelerate e- transfer rates to levels that make practical sense. In this talk I will present hybrid photoelectrodes leading to enhanced efficiency, selectivity, and stability. First, I will present the use of electrosynthetic (and photoelectrosynthetic) methods for preparing semiconductors on nanocarbon-modified electrode surfaces. Composites of nanocarbons with both inorganic and organic semiconductors represent an interesting class of new functional materials. Therefore, I will show how electrodeposition can be used to tune composition, crystal structure, and morphology of the nanocomposites for targeted applications. In the second part of my talk, selected examples will be given for how these electrosynthesized hybrid assemblies can be deployed in various photoelectrochemical application schemes, most importantly CO2 conversion. I will present the controlled synthesis and photoelectrochemical behavior of Cu2O/CNT and Cu2O/graphene composites. A carefully designed, multiple-step electrodeposition protocol was developed that ensured homogeneous coating of the CNTs with the Cu2O nanocrystals. TiO2/ graphene nanocomposites were also obtained in a similar manner. This enhanced charge transport property for the hybrids resulted in a drastic increase in the photocurrents measured for the CO2 reduction. In addition to this superior performance, long term photoelectrolysis measurements proved that the Cu2O/nanocarbon hybrids were more stable than the oxide alone. Taking these observations together as a whole, a general model will be presented on the role of the nanocarbon scaffold. Acknowledgements This research was partially supported by the “Széchenyi 2020” program in the framework of GINOP-2.3.2-15-2016-00013 “Intelligent materials based on functional surfaces – from syntheses to applications” project.

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2

Nakanishi, Yusuke, Shinpei Furusawa, Zheng Liu, Yuta Sato, Yohei Yomogida, Kazuhiro Yanagi, Kazu Suenaga, and Yasumitsu Miyata. "(Invited, Digital Presentation) Atomically Precise Synthesis of One-Dimensional Transition Metal Chalcogenides Using Nano-Test-Tubes." ECS Meeting Abstracts MA2022-01, no. 10 (July 7, 2022): 769. http://dx.doi.org/10.1149/ma2022-0110769mtgabs.

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Since the discovery of fullerenes in 1985, nanocarbon materials have played a crucial role in materials science. Over the past decade, significant efforts have been directed towards exploring post nanocarbons. Two-dimensional (2D) layers of transition metal chalcogenides (TMCs) have been widely recognized as ‘beyond graphene’ due to their versatile chemistry. On the other hand, their 1D counterparts (nanowires, nanoribbons, and nanotubes) could exhibit the unique electronic properties, significantly distinct from the 2D layers as well as 1D nanocarbons (Fig. 1a).[1] However, exploring their potentials has been hampered by their limited availability. Although these materials have been prepared by using chemical and lithographic methods,[2] the reliable production of well-defined 1D TMCs remains a significant challenge. Here we report atomically precise fabrication of 1D TMCs by using carbon/boron-nitride nanotubes (CNTs/BNNTs) as a template. Chemically and mechanically robust CNTs/BNNTs have increasingly been employed to promote and stabilize the bottom-up growth of 1D materials, allowing their facile handling and characterization. Isolation of a single MoTe/WTe nanowires inside CNTs enabled us to observe their dynamic torsions, which are not seen in the bulk (Fig. 1b).[3] Furthermore, we have utilized hollow spaces and external surfaces of BNNTs to produce a variety of 1D MX2 structures including single-walled MoS2NTs with the small diameter of ~1 nm. Electrically and optically insulating BNNTs can serve as an ideal ‘nano-test-tubes’ for precisely studying electronic properties of guest materials. The successful syntheses of 1D TMCs using CNTs/BNNTs might open up the possibilities for exploring unprecedented physics and potential applications. Reference: [1] a) G. Seifert et al. Phys. Rev. Lett. 1999, 85, 146. b) Y. Li et al. J. Am. Chem. Soc. 2008, 130, 16739. c) I. Popov et al. Nano Lett. 2008, 8, 4093. [2] (a) J. Kibsgaard et al. Nano Lett. 2008, 8, 3928. (b) X. Liu et al. Nat. Commun. 2013, 4, 1776. (c) P. Chithaiah et al. ACS Nano 2020, 14, 3004 [3] (a) M. Nagata et al. Nano Lett. 2019, 19, 4845. (b) N. Kanda et al. Nanoscale 2020, 12, 17185. Figure 1

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3

Itami, Kenichiro. "(Invited, Digital Presentation) Molecular Nanocarbon Synthesis and Beyond." ECS Meeting Abstracts MA2022-01, no. 10 (July 7, 2022): 789. http://dx.doi.org/10.1149/ma2022-0110789mtgabs.

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Our goal is the creation of super molecules, innovative functional molecules with significant properties and/or beautiful molecules. To this end, we have focused on catalyst-enabling synthetic chemistry with broad directions, including applications in molecular nanocarbons, pharmaceuticals, and plant/animal chemical biology, and the development of rapid molecule-assembly methods using unique catalysts. In particular, we have pioneered molecular nanocarbon science by the bottom-up synthesis of structurally uniform nanocarbons of fundamental and practical importance. Representative achievements include: (1) the development of single-step aromatic π-extension (APEX) methods for the rapid and programmable synthesis of nanocarbon molecules (Science 2018, Nature Commun. 2015, Nature Chem. 2015, Nature Commun. 2021); (2) the synthesis of carbon nanorings, nanobelts and pure nanotubes (ACIE 2009, Science 2017, Nature Chem. 2013, Nature Commun. 2018, Nature Commun. 2019, Nature Chem. 2021); and (3) the synthesis of topologically unique nanocarbons such as warped nanographenes, carbon nanocages, all-benzene catenanes, and trefoil knots (Science 2019, Nature Chem. 2013, Nature Catal. 2020). In this talk, most recent beautiful molecular nanocarbons will be presented. We will also describe about our exciting interdisciplinary research conducted at the Institute of Transformative Bio-Molecules (ITbM) in Nagoya University and Institute of Chemistry in Academia Sinica, Taiwan, where we aim at developing game-changing molecules for nanocarbon-based chemical biology. By using our original rapid molecule-assembling catalysts, a number of lead compounds were rapidly discovered.

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4

Isobe, Hiroyuki. "(Invited) A Versatile Strategy for the Synthesis of Nanocarbon Molecules." ECS Meeting Abstracts MA2022-01, no. 10 (July 7, 2022): 790. http://dx.doi.org/10.1149/ma2022-0110790mtgabs.

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Synthesis of molecules with large, curved π-systems attracts much interest, because of high expectations to deepen our understanding of nanocarbons. Many "nanocarbon molecules" are being synthesized via elaborate synthesis. However, due to challenging nature of the synthesis, the methods tend to be one-off and specific for one molecule. Herein we show our recent explorations of a versatile synthetic method adopting "phenine", which covers various shapes of large nanocarbon molecules. Synthesis of gigantic, 7-kDa nanocarbon molecules, defective nanotubes, bowls, saddles and hemispheres will be shown at the presentation.

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Chen, Xing-Yu, Ji-Kun Li, and Xiao-Ye Wang. "Recent Advances in the Syntheses of Helicene-Based Molecular Nanocarbons via the Scholl Reaction." Chinese Journal of Organic Chemistry 41, no. 11 (2021): 4105. http://dx.doi.org/10.6023/cjoc202107063.

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6

Zhou, Yang, and Yuta Nishina. "Bottom-up synthesis of nitrogen-doped nanocarbons by a combination of metal catalysis and a solution plasma process." Nanoscale Advances 2, no. 10 (2020): 4417–20. http://dx.doi.org/10.1039/d0na00327a.

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We developed a bottom-up synthesis of nanocarbons with specific functions from molecules without leaving groups, by employing a metal catalyst under solution plasma irradiation. Using pyridine, the nitrogen-doped nanocarbon was synthesized by this method.

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7

Vidick, Deborah, Xiaoxing Ke, Michel Devillers, Claude Poleunis, Arnaud Delcorte, Pietro Moggi, Gustaaf Van Tendeloo, and Sophie Hermans. "Heterometal nanoparticles from Ru-based molecular clusters covalently anchored onto functionalized carbon nanotubes and nanofibers." Beilstein Journal of Nanotechnology 6 (June 10, 2015): 1287–97. http://dx.doi.org/10.3762/bjnano.6.133.

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Heterometal clusters containing Ru and Au, Co and/or Pt are anchored onto carbon nanotubes and nanofibers functionalized with chelating phosphine groups. The cluster anchoring yield is related to the amount of phosphine groups available on the nanocarbon surface. The ligands of the anchored molecular species are then removed by gentle thermal treatment in order to form nanoparticles. In the case of Au-containing clusters, removal of gold atoms from the clusters and agglomeration leads to a bimodal distribution of nanoparticles at the nanocarbon surface. In the case of Ru–Pt species, anchoring occurs without reorganization through a ligand exchange mechanism. After thermal treatment, ultrasmall (1–3 nm) bimetal Ru–Pt nanoparticles are formed on the surface of the nanocarbons. Characterization by high resolution transmission electron microscopy (HRTEM) and high angle annular dark field scanning transmission electron microscopy (HAADF-STEM) confirms their bimetal nature on the nanoscale. The obtained bimetal nanoparticles supported on nanocarbon were tested as catalysts in ammonia synthesis and are shown to be active at low temperature and atmospheric pressure with very low Ru loading.

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Tichit, Didier, and Mayra G. Álvarez. "Layered Double Hydroxide/Nanocarbon Composites as Heterogeneous Catalysts: A Review." ChemEngineering 6, no. 4 (June 22, 2022): 45. http://dx.doi.org/10.3390/chemengineering6040045.

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The synthesis and applications of composites based on layered double hydroxides (LDHs) and nanocarbons have recently seen great development. On the one hand, LDHs are versatile 2D compounds that present a plethora of applications, from medicine to energy conversion, environmental remediation, and heterogeneous catalysis. On the other, nanocarbons present unique physical and chemical properties owing to their low-dimensional structure and sp2 hybridization of carbon atoms, which endows them with excellent charge carrier mobility, outstanding mechanical strength, and high thermal conductivity. Many reviews described the applications of LDH/nanocarbon composites in the areas of energy and photo- and electro-catalysis, but there is still scarce literature on their latest applications as heterogeneous catalysts in chemical synthesis and conversion, which is the object of this review. First, the properties of the LDHs and of the different types of carbon materials involved as building blocks of the composites are summarized. Then, the synthesis methods of the composites are described, emphasizing the parameters allowing their properties to be controlled. This highlights their great adaptability and easier implementation. Afterwards, the application of LDH/carbon composites as catalysts for C–C bond formation, higher alcohol synthesis (HAS), oxidation, and hydrogenation reactions is reported and discussed in depth.

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9

Koshikawa, Yusuke, Ryo Miyashita, Takuya Yonehara, Kyoka Komaba, Reiji Kumai, and Hiromasa Goto. "Conducting Polymer Metallic Emerald: Magnetic Measurements of Nanocarbons/Polyaniline and Preparation of Plastic Composites." C 8, no. 4 (November 4, 2022): 60. http://dx.doi.org/10.3390/c8040060.

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Synthesis of polyaniline in the presence of fullerene nanotubes (nanocarbons) in water was carried out with oxidative polymerization. The surface of the sample showed metallic emerald green color in bulk like the brilliance of encrusted gemstones. The composite showed unique magnetic behavior, such as microwave power-dependent magnetic resonance as magnetic spin behavior and macroscopic paramagnetism with a maximum χ value at room temperature evaluated with superconductor interference device. Surface structure of the composite was observed with optical microscopy, circular polarized differential interference contrast optical microscopy, scanning electron microscopy, and electron probe micro analyzer. Polymer blends consisting of polyaniline, nano-carbons, and hydroxypropylcellulose or acryl resin with both conducting polymer and carbon characters were prepared, which can be applied for electrical conducting plastics. The combination of conducting polymer and nano-carbon materials can produce new electro-magneto-active soft materials by forming a composite. This paper reports evaluation of magnetic properties as a new point of nanocarbon and conducting polymer composite.

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10

LIU, LIHONG. "SINGLE-STEP SYNTHESIS OF COBALT-OXIDE SHELLED NANOCARBONS." International Journal of Nanoscience 04, no. 04 (August 2005): 591–98. http://dx.doi.org/10.1142/s0219581x05003255.

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In this paper, we report a simple solid-state method for fabricating cobalt-oxide–carbon core-shell nanostructures. With this technique, various forms of nanocarbons such as nanotubes, polyhedrons and onions can be generated via pyrolyzing cobalt–complex xerogels at 150 ~ 340°C. The thus-formed nanocarbons can be protected by cobalt-oxide matrix up to 1000°C in air atmosphere. Cobalt-oxide shelled or unshelled nanocarbons can be controlled by choosing a suitable complexing agent for the xerogel precursors. In particular, glycine has been proven to be a good complexing agent for low-temperature formation of unshelled nanocarbons and high-temperature generation of shelled nanocarbons.

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11

Kumanek, Bogumiła, Grzegorz Stando, Paweł S. Wróbel, and Dawid Janas. "Impact of Synthesis Parameters of Multi-Walled Carbon Nanotubes on their Thermoelectric Properties." Materials 12, no. 21 (October 30, 2019): 3567. http://dx.doi.org/10.3390/ma12213567.

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Carbon nanotubes have been intensively researched for many years because of a wide array of promising properties that they have. In this paper, we present the impact of synthesis parameters on thermoelectric properties of nanocarbon material. We conducted a number of syntheses of multi-walled carbon nanotubes (MWCNTs) at different temperatures (800 and 900 °C) using various amounts of catalyst (2%, 5.5%, and 9.6%) to facilitate the process. We also tested the influence of injection rate of precursor and the necessity of material purification on thermoelectric properties of MWCNTs. The electrical conductivity, thermal conductivity, and Seebeck coefficient were measurement for all samples. Based on these parameters, the values of Power Factor and Figure of Merit were calculated. The results show that the most important parameter in the context of thermoelectric properties is purity of employed MWCNTs. To obtain appropriate material for this purpose optimum synthesis temperature and appropriate content of the catalyst must be selected. The study also reveals that post-synthetic purification of nanocarbon is essential to produce an attractive material for thermoelectrics.

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12

Huczko, A., H. Lange, G. Cota-Sanchez, and Gervais Soucy. "PLASMA SYNTHESIS OF NANOCARBONS." High Temperature Material Processes (An International Quarterly of High-Technology Plasma Processes) 6, no. 3 (2002): 16. http://dx.doi.org/10.1615/hightempmatproc.v6.i3.100.

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13

Shang, Sensen, Wen Dai, Lianyue Wang, Ying Lv, and Shuang Gao. "Metal-free catalysis of nitrogen-doped nanocarbons for the ammoxidation of alcohols to nitriles." Chemical Communications 53, no. 6 (2017): 1048–51. http://dx.doi.org/10.1039/c6cc09151b.

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14

González Miera, Greco, Satoshi Matsubara, Hideya Kono, Kei Murakami, and Kenichiro Itami. "Synthesis of octagon-containing molecular nanocarbons." Chemical Science 13, no. 7 (2022): 1848–68. http://dx.doi.org/10.1039/d1sc05586k.

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15

Nguyen, Duong Nguyen, Uk Sim, and Jung Kyu Kim. "Biopolymer-Inspired N-Doped Nanocarbon Using Carbonized Polydopamine: A High-Performance Electrocatalyst for Hydrogen-Evolution Reaction." Polymers 12, no. 4 (April 15, 2020): 912. http://dx.doi.org/10.3390/polym12040912.

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Hydrogen-evolution reaction (HER) is a promising technology for renewable energy conversion and storage. Electrochemical HER can provide a cost-effective method for the clean production of hydrogen. In this study, a biomimetic eco-friendly approach to fabricate nitrogen-doped carbon nanosheets, exhibiting a high HER performance, and using a carbonized polydopamine (C-PDA), is described. As a biopolymer, polydopamine (PDA) exhibits high biocompatibility and can be easily obtained by an environmentally benign green synthesis with dopamine. Inspired by the polymerization of dopamine, we have devised the facile synthesis of nitrogen-doped nanocarbons using a carbonized polydopamine for the HER in acidic media. The N-doped nanocarbons exhibit excellent performance for H2 generation. The required overpotential at 5 mA/cm2 is 130 mV, and the Tafel slope is 45 mV/decade. Experimental characterizations confirm that the excellent performance of the N-doped nanocarbons can be attributed to the multisite nitrogen doping, while theoretical computations indicate the promotion effect of tertiary/aromatic nitrogen doping in enhancing the spin density of the doped samples and consequently in forming highly electroactive sites for HER applications.

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Pérez-Mayoral, E., V. Calvino-Casilda, and E. Soriano. "Metal-supported carbon-based materials: opportunities and challenges in the synthesis of valuable products." Catalysis Science & Technology 6, no. 5 (2016): 1265–91. http://dx.doi.org/10.1039/c5cy01437a.

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17

Bettini, Simona, and Gabriele Giancane. "Synthesis, Functionalization and Applications of Nanocarbons." Nanomaterials 12, no. 16 (August 10, 2022): 2738. http://dx.doi.org/10.3390/nano12162738.

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The Special Issue “Synthesis, Functionalization and Applications of Nanocarbons” starts from the growing interest of the scientific community in carbon-based materials and the various applications of these versatile compounds [...]

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18

Higuchi, Mai, Mizuri Yaguchi, Miru Yoshida-Hirahara, Hitoshi Ogihara, and Hideki Kurokawa. "Facile synthesis of nanostructured perovskites by precursor accumulation on nanocarbons." RSC Advances 12, no. 10 (2022): 6186–91. http://dx.doi.org/10.1039/d1ra08357k.

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Various nano-perovskites are synthesized by dropping a precursor solution of metal salts into nanocarbon, followed by drying and calcination in air. The accumulation of precursors on the surface of nanocarbon is the key step.

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19

Wang, Hailiang. "Hybrid material design for energy applications: impact of graphene and carbon nanotubes." Pure and Applied Chemistry 86, no. 1 (January 22, 2014): 39–52. http://dx.doi.org/10.1515/pac-2014-5013.

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Abstract This article reviews the origin and progress of inorganic/nanocarbon hybrid material research in my Ph.D. career. Building chemical bonds between inorganic active materials and nanocarbon substrates is the key to controlled hybrid material synthesis that allows for controlling the size and morphology of the materials and enhancing electron transport within the electrodes. Our inorganic/nanocarbon hybrid materials manifest superior electrochemical performance for asymmetrical supercapacitors, ultrafast nickel-iron batteries, lithium ion batteries, lithium-sulfur batteries, and electrocatalysis of oxygen reduction and evolution reactions. X-ray absorption near edge structure (XANES) spectroscopy has been utilized to characterize the chemical bonding and charge transfer at the interface of inorganic nanocrystals and nanocarbon substrates. Probing the physical and chemical states of the hybrid materials under electrochemical reaction conditions is an important future direction in this area.

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Liu, Yujing, Xuan Wang, Xiaohui Jiang, Xia Li, and Liangmin Yu. "Shape-controlled synthesis of porous carbons for flexible asymmetric supercapacitors." Nanoscale 10, no. 48 (2018): 22848–60. http://dx.doi.org/10.1039/c8nr06966b.

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21

Ariga, Katsuhiko, Michio Matsumoto, Taizo Mori, and Lok Kumar Shrestha. "Materials nanoarchitectonics at two-dimensional liquid interfaces." Beilstein Journal of Nanotechnology 10 (July 30, 2019): 1559–87. http://dx.doi.org/10.3762/bjnano.10.153.

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Much attention has been paid to the synthesis of low-dimensional materials from small units such as functional molecules. Bottom-up approaches to create new low-dimensional materials with various functional units can be realized with the emerging concept of nanoarchitectonics. In this review article, we overview recent research progresses on materials nanoarchitectonics at two-dimensional liquid interfaces, which are dimensionally restricted media with some freedoms of molecular motion. Specific characteristics of molecular interactions and functions at liquid interfaces are briefly explained in the first parts. The following sections overview several topics on materials nanoarchitectonics at liquid interfaces, such as the preparation of two-dimensional metal-organic frameworks and covalent organic frameworks, and the fabrication of low-dimensional and specifically structured nanocarbons and their assemblies at liquid–liquid interfaces. Finally, interfacial nanoarchitectonics of biomaterials including the regulation of orientation and differentiation of living cells are explained. In the recent examples described in this review, various materials such as molecular machines, molecular receptors, block-copolymer, DNA origami, nanocarbon, phages, and stem cells were assembled at liquid interfaces by using various useful techniques. This review overviews techniques such as conventional Langmuir–Blodgett method, vortex Langmuir–Blodgett method, liquid–liquid interfacial precipitation, instructed assembly, and layer-by-layer assembly to give low-dimensional materials including nanowires, nanowhiskers, nanosheets, cubic objects, molecular patterns, supramolecular polymers, metal-organic frameworks and covalent organic frameworks. The nanoarchitecture materials can be used for various applications such as molecular recognition, sensors, photodetectors, supercapacitors, supramolecular differentiation, enzyme reactors, cell differentiation control, and hemodialysis.

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22

Guan, Shuzhe, Xuanchi Liu, and Wumanjiang Eli. "The synthesis of nanocarbon-poly(ricinoleic acid) composite as a lubricant additive with improved dispersity and anti-wear properties." RSC Advances 11, no. 30 (2021): 18171–78. http://dx.doi.org/10.1039/d1ra01720a.

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23

Zhang, Lu-Hua, Wen-Cui Li, Lei Tang, Quan-Gao Wang, Qing-Tao Hu, Yu Zhang, and An-Hui Lu. "Primary amine modulated synthesis of two-dimensional porous nanocarbons with tunable ultramicropores." Journal of Materials Chemistry A 6, no. 47 (2018): 24285–90. http://dx.doi.org/10.1039/c8ta09545k.

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24

Segawa, Yasutomo, Motonobu Kuwayama, Yuh Hijikata, Masako Fushimi, Taishi Nishihara, Jenny Pirillo, Junya Shirasaki, Natsumi Kubota, and Kenichiro Itami. "Topological molecular nanocarbons: All-benzene catenane and trefoil knot." Science 365, no. 6450 (July 18, 2019): 272–76. http://dx.doi.org/10.1126/science.aav5021.

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The generation of topologically complex nanocarbons can spur developments in science and technology. However, conventional synthetic routes to interlocked molecules require heteroatoms. We report the synthesis of catenanes and a molecular trefoil knot consisting solely of para-connected benzene rings. Characteristic fluorescence of a heterocatenane associated with fast energy transfer between two rings was observed, and the topological chirality of the all-benzene knot was confirmed by enantiomer separation and circular dichroism spectroscopy. The seemingly rigid all-benzene knot has rapid vortex-like motion in solution even at –95°C, resulting in averaged nuclear magnetic resonance signals for all hydrogen atoms. This interesting dynamic behavior of the knot was theoretically predicted and could stimulate deeper understanding and applications of these previously untapped classes of topological molecular nanocarbons.

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Lehmann, K., O. Yurchenko, and G. Urban. "Effect of the aromatic precursor flow rate on the morphology and properties of carbon nanostructures in plasma enhanced chemical vapor deposition." RSC Advances 6, no. 39 (2016): 32779–88. http://dx.doi.org/10.1039/c6ra02999j.

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Kausar, Ayesha, Ishaq Ahmad, Malik Maaza, M. H. Eisa, and Patrizia Bocchetta. "Cutting-Edge Green Polymer/Nanocarbon Nanocomposite for Supercapacitor—State-of-the-Art." Journal of Composites Science 6, no. 12 (December 6, 2022): 376. http://dx.doi.org/10.3390/jcs6120376.

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Supercapacitors have attained a special stance among energy storage devices such as capacitors, batteries, fuel cell, and so forth. In this state-of-the-art overview on green synthesis approaches and green materials for supercapacitors, the cutting-edge green polymer/nanocarbon nanocomposite systems were explored by focusing on the design and related essential features. In this regard, various polymers were reconnoitered including conjugated polymers, thermosetting matrices, and green-cellulose-based matrices. Nanocarbon nanomaterials have also expanded research thoughtfulness for green-technology-based energy storage devices. Consequently, green polymer/nanocarbon nanocomposites have publicized fine electron conduction pathways to promote the charge storage, specific capacitance, energy density, and other essential features of supercapacitors. Future research directions must focus on the design of novel high performance green nanocomposites for energy storage applications.

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Zhang, Xinyu, and Sanjeev K. Manohar. "Microwave synthesis of nanocarbons from conducting polymers." Chemical Communications, no. 23 (2006): 2477. http://dx.doi.org/10.1039/b603925a.

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Schaub, Tobias A. "Bottom‐Up Synthesis of Discrete Conical Nanocarbons." Angewandte Chemie International Edition 59, no. 12 (January 29, 2020): 4620–22. http://dx.doi.org/10.1002/anie.201914830.

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29

Hatakeyama, Rikizo, Toshiaki Kato, Yongfeng Li, and Toshiro Kaneko. "Plasma Processing Based Synthesis of Functional Nanocarbons." Plasma Chemistry and Plasma Processing 34, no. 3 (March 29, 2014): 377–402. http://dx.doi.org/10.1007/s11090-014-9547-z.

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Kharlamova, Marianna V., Maria G. Burdanova, Maksim I. Paukov, and Christian Kramberger. "Synthesis, Sorting, and Applications of Single-Chirality Single-Walled Carbon Nanotubes." Materials 15, no. 17 (August 26, 2022): 5898. http://dx.doi.org/10.3390/ma15175898.

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The synthesis of high-quality chirality-pure single-walled carbon nanotubes (SWCNTs) is vital for their applications. It is of high importance to modernize the synthesis processes to decrease the synthesis temperature and improve the quality and yield of SWCNTs. This review is dedicated to the chirality-selective synthesis, sorting of SWCNTs, and applications of chirality-pure SWCNTs. The review begins with a description of growth mechanisms of carbon nanotubes. Then, we discuss the synthesis methods of semiconducting and metallic conductivity-type and single-chirality SWCNTs, such as the epitaxial growth method of SWCNT (“cloning”) using nanocarbon seeds, the growth method using nanocarbon segments obtained by organic synthesis, and the catalyst-mediated chemical vapor deposition synthesis. Then, we discuss the separation methods of SWCNTs by conductivity type, such as electrophoresis (dielectrophoresis), density gradient ultracentrifugation (DGC), low-speed DGC, ultrahigh DGC, chromatography, two-phase separation, selective solubilization, and selective reaction methods and techniques for single-chirality separation of SWCNTs, including density gradient centrifugation, two-phase separation, and chromatography methods. Finally, the applications of separated SWCNTs, such as field-effect transistors (FETs), sensors, light emitters and photodetectors, transparent electrodes, photovoltaics (solar cells), batteries, bioimaging, and other applications, are presented.

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Voznyakovskii, Aleksandr Petrovich, Anatoliy Petrovich Karmanov, Anna Yur'yevna Neverovskaya, Aleksey Aleksandrovich Voznyakovskii, Lyudmila Sergeyevna Kocheva, and Sergey Viktorovich Kidalov. "BIOMASS OF SOSNOWSKYI'S HOGWEED AS RAW MATERIAL FOR 2D THE CARBONIC NANOSTRUCTURES OBTAINING." chemistry of plant raw material, no. 4 (December 21, 2020): 83–92. http://dx.doi.org/10.14258/jcprm.2020047739.

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The possibility of the carbonization of the Sosnowskyi's hogweed (Heracléum sosnówskyi) biomass for obtaining the carbonic nanmaterials was studied. The characteristic of component composition is given and the parameters of the superficially-porous structure of plant biomass are established. The isotherms of adsorption and desorption of nitrogen on the surface are studied and it is shown that they relate to the type II according to the IUPAC classification. The distribution of times according to the sizes is investigated and it is established that the basic portion of the pore space of the vegetable raw material forms the mezopors with an average width 3.5 of nm. The specific surface area according to Brunauer-Emmet-Teller is determined, which composed 16.4 m2/g. Using a method of the carbonization of organic materials under the effect of local extremely high temperatures and oxidizers the synthesis of nanocarbonic powders, which are formed under the conditions of the self-propagating high-temperature synthesis (SHS method), was carried out. By the methods of spectral analysis (Raman spectroscopy, X-ray diffractometry) and electron microscopy it is shown that from their morphometric parameters the particles of the obtained carbonized product correspond to 2D nanocarbon in the form of grafenic nanoplates. The low-defect planar surface and the presence of the oxygen-containing terminal groups are the characteristic properties of new product. The specific surface area, which composed 179.1 m2/g, is determined. The specific surface area, which composed 179.1 m2/g, is determined. It is established that the micropores introduce the basic contribution to the specific surface area of nanomaterial on the basis of the Sosnowskyi's hogweed biomass.

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32

Mansurov, Z. A. "Recent Achievements and Future Challenges in Nanoscience and Nanotechnology." Eurasian Chemico-Technological Journal 22, no. 4 (December 30, 2020): 241. http://dx.doi.org/10.18321/ectj994.

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The article presents the investigation results of the formation and synthesis of nanosized materials which were obtained at the Institute of Combustion Problems, many works have been brought to practical use. Investigations of low-temperature soot formation become the basis of nanomaterial synthesis methods, developed at the Institute for Combustion Problems since 1985. Flame can be considered as a chemical reactor to produce target products. The main feature of the processes based on technological combustion is that the target product is formed as a result of the combustion reaction, occurring spontaneously at high temperatures with a high speed without consuming external energy, i.e. due to its own heat. With the development of nanotechnology, new challenges have emerged in the synthesis of nanomaterials under combustion synthesis conditions. Below is a list of works on nanomaterials synthesis carried out at the Institute: complete scheme of soot formation; energy intensive nanocarbon materials; development and study of perovskite photocatalysts for hydrogen evolution; obtaining carbon fibers by the method of electrospinning; obtaining of biologically soluble membranes based on polymeric nanofibres and hydroxyapatite of calcium; synthesis of nanocarbon sorbents for purification of water from heavy metal ions.

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33

Islam, Md Zahidul, Anyarat Watthanaphanit, Sangwoo Chae, and Nagahiro Saito. "Li–air battery and ORR activity of nanocarbons produced with good synthesis rate by solution plasma process." Materials Advances 2, no. 8 (2021): 2636–41. http://dx.doi.org/10.1039/d0ma00926a.

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Lee, SeungHyo, YongKang Heo, Maria Antoaneta Bratescu, Tomonaga Ueno, and Nagahiro Saito. "Solution plasma synthesis of a boron–carbon–nitrogen catalyst with a controllable bond structure." Physical Chemistry Chemical Physics 19, no. 23 (2017): 15264–72. http://dx.doi.org/10.1039/c6cp06063c.

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Synthesis of boron–carbon–nitrogen (BCN) nanocarbon with a controllable bond structure for enhanced oxygen reduction reaction (ORR) activity and durability was performed using a new method of discharge in organic solution mixtures named the ‘Solution Plasma Process’.

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35

Huczko, Andrzej, Agnieszka Dąbrowska, Michał Bystrzejewski, P. Baranowski, Santosh K. Tiwari, Łukasz Dobrzycki, Maciej Fronczak, et al. "Novel nanocarbons via facile one-pot combustion synthesis." Diamond and Related Materials 121 (January 2022): 108746. http://dx.doi.org/10.1016/j.diamond.2021.108746.

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36

Kudiyarov, Viktor N., Roman R. Elman, and Nikita E. Kurdyumov. "The Effect of High-Energy Ball Milling Conditions on Microstructure and Hydrogen Desorption Properties of Magnesium Hydride and Single-Walled Carbon Nanotubes." Metals 11, no. 9 (September 6, 2021): 1409. http://dx.doi.org/10.3390/met11091409.

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Magnesium hydride is considered to be one of the most promising hydrogen storage materials, although it nevertheless has some problems, such as the high value of the activation energy of hydrogen desorption. To solve this problem, some scientists have proposed adding nanocarbon materials, in particular carbon nanotubes, to magnesium hydride. Currently, a detailed understanding of the mechanisms of obtaining composites based on magnesium hydride and carbon nanotubes is lacking, as is our understanding of the effect of nanocarbon additives on the activation energy and temperature of hydrogen desorption depending on the parameters of the composite synthesis. In addition, the data obtained at various values of milling parameters are very different, and in some works the effect of carbon nanomaterials on the hydrogen properties of magnesium hydride was not confirmed at all. Thus, it is important to determine the effect of nanocarbon additives on the properties of hydrogen storage of magnesium hydride under various milling parameters. This work is devoted to the study of the effect of nanocarbon additives on magnesium hydride and the determination of the dependences of the hydrogen desorption temperature and activation energy on the synthesis parameters. Composite powders containing MgH2 with 5 wt.% single-walled carbon nanotubes (SWCNT) were prepared using a planetary ball mill. The milling was carried out at various milling speeds, namely 300, 660, and 900 rpm. Results suggested that the structure of the nanotubes is preserved with prolonged grinding of magnesium hydride and SWCNT in a ball mill for 180 min at a relatively low grinding speed of 300 rpm. The composite obtained with these parameters has the lowest temperature of hydrogen desorption and an activation energy of H2 desorption of 162 ± 1 kJ/mol H2, which is 15% lower than that of the magnesium hydride MgH2 (189 ± 1 kJ/mol H2).

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37

James, Anthonette Anak, Md Rezaur Rahman, Durul Huda, Faisal M. Aqlan, Mohammed Mahbubul Matin, Muhammad Khusairy Bin Bakri, Kuok King Kuok, and Mohammed Muzibur Rahman. "Synthesis and characterization of novel nano-carbon mixture from Dabai (Canarium odontophyllum) nutshell." BioResources 17, no. 3 (June 3, 2022): 4452–69. http://dx.doi.org/10.15376/biores.17.3.4452-4469.

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The nanocarbon-based mixture was shown to be an effective adsorbent for removing dyes and heavy metals from wastewater via adsorption. The goal of this research was to prepare and investigate the properties of a bio-carbon mixture made from Dabai (Canarium odontophyllum) nutshell with the addition of titanium dioxide (TiO2) and montmorillonite (MMT) clay. Fourier transform infrared (FTIR) spectroscopy was used to determine the functional groups of raw carbon and potassium hydroxide (KOH)-activated carbon (AC). The FTIR analysis of the active carbon revealed that the active carbon had more surface chemistry than the non-AC. Scanning electron microscopy (SEM) analysis was used to compare the raw and AC morphologies and the developed nanocarbon. The results were confirmed using energy dispersive X-ray (EDX) analysis to verify the elements in the studied sample. The SEM analysis revealed that the structure of both the carbon samples was irregular, granular, and porous. BET analysis showed that nano-activated carbon had higher surface area compared to activated carbon itself. Response surface methodology (RSM) was used in Design-Expert 13.0 software for the sample composition development to achieve the best performance of the developed nanocarbon as an adsorbent.

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38

Mansurov, Zulkhair A. "Obtaining of Nanomaterials in Combustion Processes." Advanced Materials Research 486 (March 2012): 134–39. http://dx.doi.org/10.4028/www.scientific.net/amr.486.134.

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An experimental study has been conducted in premixed and counterflow diffusion flames in order to obtain the nanocarbon materials. In this paper the synthesis of fullerenes, carbon nanotubes and superhydrophobic soot surface in the regime of hydrocarbon flames were studied. The original results in the field of synthesis of fullerenes, carbon nanotubes and syperhydrophobic soot in hydrocarbon flames were carried out for the last years at the Institute of Combustion Problems.

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39

Zollo, G., and F. Gala. "Atomistic Modeling of Gas Adsorption in Nanocarbons." Journal of Nanomaterials 2012 (2012): 1–32. http://dx.doi.org/10.1155/2012/152489.

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Carbon nanostructures are currently under investigation as possible ideal media for gas storage and mesoporous materials for gas sensors. The recent scientific literature concerning gas adsorption in nanocarbons, however, is affected by a significant variation in the experimental data, mainly due to the different characteristics of the investigated samples arising from the variety of the synthesis techniques used and their reproducibility. Atomistic simulations have turned out to be sometimes crucial to study the properties of these systems in order to support the experiments, to indicate the physical limits inherent in the investigated structures, and to suggest possible new routes for application purposes. In consideration of the extent of the theme, we have chosen to treat in this paper the results obtained within some of the most popular atomistic theoretical frameworks without any purpose of completeness. A significant part of this paper is dedicated to the hydrogen adsorption on C-based nanostructures for its obvious importance and the exceptional efforts devoted to it by the scientific community.

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40

Teng, Tun-Ping, Li Lin, and Chao-Chieh Yu. "Preparation and Characterization of Carbon Nanofluids by Using a Revised Water-Assisted Synthesis Method." Journal of Nanomaterials 2013 (2013): 1–12. http://dx.doi.org/10.1155/2013/582304.

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A revised water-assisted synthesis system (RWAS) was used to fabricate carbon/water nanofluids (CWNFs). The CWNFs were manufactured by heating graphite rods at different temperatures (700, 800, 900, and 1000°C). Aspects of the CWNFs and suspended nanocarbon, such as the morphology, structure, optical characteristics, and production rate, were fully characterized. Furthermore, the suspension performance of the CWNFs was controlled by adding a dispersant (water-soluble chitosan) at different concentrations. Finally, the CWNFs were determined to assess the influence of both the heating temperature of the graphite rod module (process temperature) and the dispersant concentration on the fundamental characteristics of the CWNFs. The results showed that the nanocarbon was a mixture of nanocrystalline graphite and amorphous carbon. Heating the graphite rod module at higher process temperatures resulted in a higher production rate and a greater nanocarbon particle size. Furthermore, adding dispersant could improve the suspension performance; increase the viscosity, density, and specific heat; and reduce the thermal conductivity of the CWNFs. The optimal combination of the process temperature range and dispersant concentration was 800 to 900°C and 0.2 wt.%, respectively, based on the production rate, suspension performance, and other fundamental properties of the CWNFs.

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Vesel, Alenka, Rok Zaplotnik, Gregor Primc, Luka Pirker, and Miran Mozetič. "One-Step Plasma Synthesis of Nitrogen-Doped Carbon Nanomesh." Nanomaterials 11, no. 4 (March 25, 2021): 837. http://dx.doi.org/10.3390/nano11040837.

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A one-step method for plasma synthesis of nitrogen-doped carbon nanomesh is presented. The method involves a molten polymer, which is a source of carbon, and inductively coupled nitrogen plasma, which is a source of highly reactive nitrogen species. The method enables the deposition of the nanocarbon layer at a rate of almost 0.1 µm/s. The deposited nanocarbon is in the form of randomly oriented multilayer graphene nanosheets or nanoflakes with a thickness of several nm and an area of the order of 1000 nm2. The concentration of chemically bonded nitrogen on the surface of the film increases with deposition time and saturates at approximately 15 at.%. Initially, the oxygen concentration is up to approximately 10 at.% but decreases with treatment time and finally saturates at approximately 2 at.%. Nitrogen is bonded in various configurations, including graphitic, pyridinic, and pyrrolic nitrogen.

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42

Liang, Xiayi, Wenhao Zhang, Mengqi Zhang, Guanhua Qiu, Yuhong Zhang, Tao Luo, and Cunqing Kong. "Facile synthesis of nitrogen-doped graphene quantum dots as nanocarbon emitters for sensitive detection of catechol." RSC Advances 12, no. 39 (2022): 25778–85. http://dx.doi.org/10.1039/d2ra04209f.

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Itami, Kenichiro. "Toward controlled synthesis of carbon nanotubes and graphenes." Pure and Applied Chemistry 84, no. 4 (March 13, 2012): 907–16. http://dx.doi.org/10.1351/pac-con-11-11-15.

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A bottom-up synthesis of structurally uniform carbon nanotubes (CNTs) and graphenes is recognized as one of the greatest challenges of primary importance in nanocarbon science. This paper highlights our efforts to address these challenges since 2005. These endeavors have led to (i) modular, size-selective, and scalable synthesis of [n]cycloparapheneylenes (CPPs), the shortest segment of armchair CNTs, (ii) design and synthesis of the shortest segment of chiral CNTs, and (iii) efficient synthesis of carbon nanosheets through catalytic C–H bond arylation of polycyclic aromatic hydrocarbons (PAHs). We consider these works as a possible first step toward a controlled synthesis of structurally uniform CNTs and nanographenes.

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44

Sarno, Maria, Adolfo Senatore, Davide Scarpa, and Claudia Cirillo. "“Green” Synthesis of Nanocarbons for Reduced Friction and Wear." Lubricants 8, no. 2 (February 2, 2020): 13. http://dx.doi.org/10.3390/lubricants8020013.

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In the following study, green carbon nanotubes and green few-layer reduced graphene oxide (rGO) were synthesized through simple, sustainable, and scalable processes starting from recycled plastic and charcoal, respectively, and with the highest number of steps involving non-harmful substances. After an extensive physicochemical characterization, which evidenced that both nano-carbons exhibit structures comparable with that of materials produced through more traditional methods and from pure sources, the samples were dispersed in two types of conventional base oils, in particular group I and group III, in order to carry out, for the first time on these green nanomaterials, an accurate study on their tribological performance. Tribological tests evidenced a remarkable reduction of coefficient of friction and wear scar diameter, especially for the green rGO dispersed at 0.1 wt% in the group III oil along with SDBS-Tween 80 surfactants mixture: 18% and 15% at ambient temperature, 12% and 13% at 80 °C, respectively. Furthermore, the tribological performance of the synthesized samples in both oils remained high for 160 min of investigation. A comparison with the same material obtained with a traditional synthesis revealed the absence of fouling phenomena in the lubrication chambers in our case, confirming the higher tribological performances of the green rGO sample, probably, as a consequence of its less ordered nature.

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45

Su, D. S., A. Rinaldi, W. Frandsen, and G. Weinberg. "Nanocarbons: efficient synthesis using natural lava as supported catalyst." physica status solidi (b) 244, no. 11 (November 2007): 3916–19. http://dx.doi.org/10.1002/pssb.200776140.

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46

Olchowski, Rafał, and Ryszard Dobrowolski. "Synthesis, properties and applications of CMK-3-type ordered mesoporous carbons." Annales Universitatis Mariae Curie-Sklodowska, sectio AA – Chemia 73, no. 1 (November 6, 2019): 11. http://dx.doi.org/10.17951/aa.2018.73.1.11-30.

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For the last two decades the CMK-3-type carbon was the subject of study by researchers from all over the world for wide range of applications: adsorptive, catalytic, magnetic and electric. Changing of modification strategies resulted in obtaining carbonaceous materials with interesting properties. In this review the synthesis, properties and applications of the CMK-3-type nanocarbon are described.

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47

Ott, Alexander, Simone Rogg, Stefan Lauterbach, Hans-Joachim Kleebe, Christian Hess, and Gabriela Mera. "Novel 0D-nanocarbon-silica ceramic composites: sol–gel synthesis and high-temperature evolution." Dalton Transactions 49, no. 21 (2020): 7144–54. http://dx.doi.org/10.1039/d0dt01016b.

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Novel mesoporous, high specific surface area (up to 562 m² g⁻¹) 0D-nanocarbon-based silicon-containing ceramic composites were produced by a straightforward sol–gel method followed by polymer-to-ceramic transformation.

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48

Mansurov, Zulkhair. "Combustion Synthesis of Nanomaterials." Advanced Materials Research 699 (May 2013): 138–43. http://dx.doi.org/10.4028/www.scientific.net/amr.699.138.

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An experimental study has been conducted in premixed and counterflow diffusion flames in order to obtain the nanocarbon materials. The original results in the field of synthesis of fullerenes, carbon nanotubes, syperhydrophobic soot,grapheme and nickel oxide nanoparticles in hydrocarbon flames were carried out for the last years at the Institute of Combustion Problems. Nanoparticles of nickel oxides contribute to the efficient absorption of light energy. Surfacing on the surface of a silicon solar cell of led to an increase in solar cell efficiency by 3%.

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49

Pérez-Villar, Sofía, and Javier Carretero-González. "Electrochemical synthesis of Fe oxide-based catalysts for the growth of nanocarbons." RSC Adv. 4, no. 104 (2014): 59862–68. http://dx.doi.org/10.1039/c4ra09803j.

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Liu, Sijie, Liting Cui, Zhiyao Peng, Jingjing Wang, Yajing Hu, Ao Yu, Haining Wang, Ping Peng, and Fang-Fang Li. "Eco-friendly synthesis of N,S co-doped hierarchical nanocarbon as a highly efficient metal-free catalyst for the reduction of nitroarenes." Nanoscale 10, no. 46 (2018): 21764–71. http://dx.doi.org/10.1039/c8nr07083k.

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