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Journal articles on the topic 'Methodology of synthesis'

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Published: 26 September 2023

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1

Shea, Kalyn M., Laurent Jaquinod, and Kevin M. Smith. "Dihydroporphyrin Synthesis: New Methodology†." Journal of Organic Chemistry 63, no. 20 (October 1998): 7013–21. http://dx.doi.org/10.1021/jo980965p.

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2

Chikhradze, Nikoloz, Merab Nadirashvili, Tamar Iashvili, Akaki Gigineishvili, and Giorgi Beinashvili. "The Improvement of Picric Acid Synthesis Methodology." IOP Conference Series: Earth and Environmental Science 906, no. 1 (November 1, 2021): 012132. http://dx.doi.org/10.1088/1755-1315/906/1/012132.

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Abstract Explosives have the greatest importance in human practical activities, not only at time of war, but at tranquility as well. Nowadays, huge amount different type of explosives is synthesized, and fabricated for military and civilian applications. Nevertheless, this fact doesn’t exclude necessity of synthesis of new explosives for optimization of their characteristics, such as prime cost, power, safety during production, storage, transfer and etc. Picric acid is a fairly strong and energetic explosive, at the same time, beside to its explosive properties, it is characterized with antibacterial nature and it is the best yellow dye, especially for dyeing animal and plant tissues. The synthesis of picric acid structural analogues, is the main purpose of the research. One of the reasons of synthesis picric acid and further preparation of its structural analogues is safe nature of substances of this group, which makes them safe to various manipulations. On the other hand, it is well known that the synthesis and production of explosives is classified as high risk and costly technology. Therefore, even a small increase of their production productivity, is interesting from the economic effect point of view. During an investigation, changing of reaction conditions (temperature, concentrations and dosage of reagents) the improved method for syntheses of picric acid was developed. As result the significant increase of practical yield of picric acid, from 46% to 86% was achieved. Synthesized picric acid was placed in steel tube and tested on initiation of detonation in explosive camera. The description of modified method, comparisons to conventional technology, as well as explosion testing results is described in the paper.
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3

Padwa, A. "Tandem methodology for heterocyclic synthesis." Pure and Applied Chemistry 76, no. 11 (January 1, 2004): 1933–52. http://dx.doi.org/10.1351/pac200476111933.

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Tandem methodology for heterocyclic synthesis represents a powerful approach for the rapid buildup of molecular complexity from potentially simple starting materials. Work from our laboratory has shown that the rhodium(II)-catalyzed cyclization cascade of alpha-diazo imides represents an effective method for the synthesis of a variety of heterocyclic systems. As an extension of these studies, we became interested in using a linked Pummerer/N-acyliminium ion cyclization sequence since we felt that this combination offers unique opportunities for the assemblage of complex target molecules. A synthetic method that combines transformations of different reaction types significantly broadens the scope of such procedures in synthetic chemistry. Alpha-thiocarbocations generated from the Pummerer reaction of beta-phenylsulfinylmethyl-alpha, beta-unsaturated amides can be intercepted by the adjacent amido group to produce transient amino-substituted furans which undergo subsequent Diels–Alder cycloadditions. Using this domino amido Pummerer/Diels–Alder cascade, we were able to assemble novel polycyclic systems in a single operation. The key step in the process involves the generation of a reactive N-acyliminium ion by fragmentation of an amino-substituted [4+2]-cycloadduct. The successful synthesis of a number of alkaloids by this sequence of reactions reveals the usefulness and importance of this unique domino cascade. Application of the process for the preparation of the stenoma alkaloid stenine was recently carried out in our laboratory.
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4

Prasad, M. V. Siva, and Ravi Gottipati. "Improve Accuracy of Intrusion Detection System Using the Synthesis Computing Classifier Methodology." Journal of Advances in Computer Networks 2, no. 4 (2014): 261–68. http://dx.doi.org/10.7763/jacn.2014.v2.123.

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5

Petrovčič, Jan, Chad Nicholas Ungarean, and David Sarlah. "Recent Chemical Methodology Advances in the Total Synthesis of Meroterpenoids." Acta Chimica Slovenica 68, no. 2 (June 15, 2021): 247–67. http://dx.doi.org/10.17344/acsi.2021.6921.

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Heterogeneity of meroterpenoids arising from their dual biosynthetic origins is constantly provoking synthetic chemists to utilize their ingenuity and revise their retrosynthetic logic. By studying recent publications on meroterpenoid synthesis,tremendous advances in the field of synthetic organic chemistry can be witnessed. This feature article covers some of the most intriguing total syntheses and synthetic studies towards the meroterpenoid class of natural products from the last five years.
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6

LI, TingTing, HongWei MA, ZhiYong WEI, Fang GUO, KaiHua SHEN, Hui NIU, and Yang LI. "Synthesis methodology of dendrigraft functional polymer." Chinese Science Bulletin 61, no. 31 (April 5, 2016): 3304–14. http://dx.doi.org/10.1360/n972015-01152.

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7

McGuigan, Christopher, and Bernadette Swords. "Synthesis of phospholipids by phosphoramidite methodology." Journal of the Chemical Society, Perkin Transactions 1, no. 3 (1990): 783. http://dx.doi.org/10.1039/p19900000783.

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8

Russi, Jumar Lus, Mrio Lcio da Silva Martins, Luciano Schuch, Jos Renes Pinheiro, and Hlio Lees Hey. "Synthesis Methodology for Multipole ZVT Converters." IEEE Transactions on Industrial Electronics 54, no. 3 (June 2007): 1783–95. http://dx.doi.org/10.1109/tie.2007.895144.

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9

SHEA, K. M., L. JAQUINOD, and K. M. SMITH. "ChemInform Abstract: Dihydroporphyrin Synthesis: New Methodology." ChemInform 30, no. 9 (June 17, 2010): no. http://dx.doi.org/10.1002/chin.199909128.

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10

Bellas, Vasilios, and Matthias Rehahn. "Universal Methodology for Block Copolymer Synthesis." Macromolecular Rapid Communications 28, no. 13 (July 2, 2007): 1415–21. http://dx.doi.org/10.1002/marc.200700127.

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11

Richetto, Katia C. S., and Cosme Roberto Moreira Silva. "Synthesis of Silicon Nitride Using Taguchi Planning Methodology." Materials Science Forum 591-593 (August 2008): 760–65. http://dx.doi.org/10.4028/www.scientific.net/msf.591-593.760.

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Silicon Nitride is considered as an important material for use in structural applications. Its performance is severely influenced by modern synthesis processes. In the present work, silicon nitride powder synthesis was performed using liquid silicon tetrachloride and gaseous ammonia, at low temperature and inert atmosphere. Diimide pyrolisis was made on temperature between 1300 and 1500 0C. A Taguchi design of experiments methodology was applied, aiming to obtain powders with appropriated characteristics for structural applications. On pyrolisis, the use of alumina based substrates resulted on SIALON phase formation, probably originated from oxygen reaction, provided from alumina. Silicon carbide substrates and alumina recovered with silicon nitride enhance synthesis of pure silicon nitride powder.
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12

Umezawa, Taiki, and Fuyuhiko Matsuda. "Recent progress toward synthesis of chlorosulfolipids: total synthesis and methodology." Tetrahedron Letters 55, no. 19 (May 2014): 3003–12. http://dx.doi.org/10.1016/j.tetlet.2014.03.082.

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13

Jurczak, Janusz, and Tomasz Bauer. "Glyoxylic acid derivatives in asymmetric synthesis." Pure and Applied Chemistry 72, no. 9 (January 1, 2000): 1589–96. http://dx.doi.org/10.1351/pac200072091589.

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Synthesis of chiral derivatives of glyoxylic acid with special emphasis on N-glyoxyloyl-(2R)-bornane-10,2-sultam is presented. Investigation of glyoxylic acid chiral derivatives in various stereocontrolled organic syntheses showed their excellent ability to provide products of high optical purity. Application of our methodology to the synthesis of natural products and their analogs is presented.
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14

Shin, Eungsoo, and D. A. Streit. "Harmonic Synthesis Design Methodology for Dynamic Spring Balancing." Journal of Dynamic Systems, Measurement, and Control 118, no. 4 (December 1, 1996): 733–40. http://dx.doi.org/10.1115/1.2802350.

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A new spring balancing technique, called a two-phase optimization method, is presented. Phase 1 uses harmonic synthesis to provide a system configuration which achieves an approximation to a desired dynamic system response. Phase 2 uses results of harmonic synthesis as initial conditions for dynamic system optimization. Optimization techniques compensate for nonlinearities in machine dynamics. Example applications to robot manipulators and to walking machine legs are presented and discussed.
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15

Vázquez, Alvaro J., Cristian Rodríguez, and N. Sbarbati Nudelman. "Convenient Methodology for the Synthesis of Trialkylhydrazines." Synthetic Communications 39, no. 22 (October 21, 2009): 3958–72. http://dx.doi.org/10.1080/00397910902738120.

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16

HU, Shanying. "Reaction path synthesis methodology for waste minimization." Science in China Series B 47, no. 3 (2004): 206. http://dx.doi.org/10.1360/03yb0204.

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17

Manabe, Shino, Akiharu Ueki, and Yukishige Ito. "Polymer-supported oligosaccharide synthesis using ultrafiltration methodology." Chemical Communications, no. 35 (2007): 3673. http://dx.doi.org/10.1039/b705324j.

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18

Klein, J. O., E. Belhaire, C. Chappert, R. Cowburn, D. Read, and D. Petit. "Synthesis methodology for magnetic domain wall logic." International Journal of Electronics 95, no. 3 (March 2008): 249–63. http://dx.doi.org/10.1080/00207210701827988.

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19

Braslau, Rebecca, Anna Tsimelzon, and Jennifer Gewandter. "Novel Methodology for the Synthesis ofN-Alkoxyamines." Organic Letters 6, no. 13 (June 2004): 2233–35. http://dx.doi.org/10.1021/ol049271v.

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20

Isobe, Minoru, and Akinari Hamajima. "Ciguatoxin: developing the methodology for total synthesis." Natural Product Reports 27, no. 8 (2010): 1204. http://dx.doi.org/10.1039/b919467n.

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21

Katritzky, Alan R., Bogumila Rachwal, Stanislaw Rachwal, and Khalil A. Abboud. "Convenient Synthesis of Julolidines Using Benzotriazole Methodology." Journal of Organic Chemistry 61, no. 9 (January 1996): 3117–26. http://dx.doi.org/10.1021/jo9519118.

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22

Leighton, J., J. Spletstoser, and M. Zacuto. "Methodology for the Synthesis of Polyketide Fragments." Synfacts 2009, no. 03 (February 19, 2009): 0301. http://dx.doi.org/10.1055/s-0028-1087752.

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23

Chessa, Gavino, and Alberto Scrivanti. "Synthesis of dendritic polypyridines using divergent methodology." Journal of Heterocyclic Chemistry 34, no. 6 (November 1997): 1851–55. http://dx.doi.org/10.1002/jhet.5570340635.

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24

Katritzky, Alan R., Delphine Semenzin, Baozhen Yang, and David P. M. Pleynet. "A novel synthesis of quinolinium saltsviabenzotriazole methodology." Journal of Heterocyclic Chemistry 35, no. 2 (March 1998): 467–70. http://dx.doi.org/10.1002/jhet.5570350234.

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25

Katritzky, Alan R., Samia Agamy, Baozhen Yang, and Guofang Qiu. "Synthesis of tetracyclic and pentacyclic phenothiazinesviabenzotriazole methodology." Journal of Heterocyclic Chemistry 36, no. 2 (March 1999): 473–76. http://dx.doi.org/10.1002/jhet.5570360223.

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26

Mahajan, Pankaj S., Jyoti P. Mahajan, and Santosh B. Mhaske. "Malonic Ester Amide Synthesis: An Efficient Methodology for Synthesis of Amides." Synthetic Communications 43, no. 18 (June 3, 2013): 2508–16. http://dx.doi.org/10.1080/00397911.2012.717671.

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27

Keck, Gary E., Eugene P. Boden, and Michael R. Wiley. "Total synthesis of (+)-colletodiol: new methodology for the synthesis of macrolactones." Journal of Organic Chemistry 54, no. 4 (February 1989): 896–906. http://dx.doi.org/10.1021/jo00265a033.

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28

Boyle, F. Thomas, Zbigniew S. Matusiak, Owen Hares, and Donald A. Whiting. "Synthesis of tricyclospirodienones via spiroannulation; methodology for synthesis of aromatase inhibitors." Journal of the Chemical Society, Chemical Communications, no. 6 (1990): 518. http://dx.doi.org/10.1039/c39900000518.

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29

Algatti, Mauricio A., Emerson Ferreira de Lucena, Élson de Campos, Rogério Pinto Mota, and Jerusa Góes Aragão Santana. "New Methodology in Modeling Ceramics." Advances in Science and Technology 63 (October 2010): 158–63. http://dx.doi.org/10.4028/www.scientific.net/ast.63.158.

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The improvement of ceramic synthesis and processing methodology based on digital image processing and analysis of ceramic samples is in its initial stage. The main reason is that the models are based on poorly obtained data from sample’s digital image processing. The lack of a solid statistical analysis and digital-imaging setup standardization make the method less useful that it should be if set in a sound basis. Therefore the importance of setting a new methodology in digital image processing for data acquisition on ceramic morphology analysis is essential for setting new models for customized ceramic synthesis and processing. The present paper shows results based on Scanning Electron Microscopy (SEM) from Al2O3 ceramics obtained by starch consolidation method. Observation of different sample’s regions allowed a more accurate description of ceramic morphology. Plots of resistance to flexion versus porosity and its correlation with the grain size and shape allowed one to choose the best model for representing ceramic’s morphology. Correlation of starch percentage with sample’s porosity and mechanical resistance allowed the best experimental conditions for customized ceramic’s performance.
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30

McGarva, J. R., and G. Mullineux. "A New Methodology for Rapid Synthesis of Function Generators." Proceedings of the Institution of Mechanical Engineers, Part C: Journal of Mechanical Engineering Science 206, no. 6 (November 1992): 391–98. http://dx.doi.org/10.1243/pime_proc_1992_206_146_02.

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This paper presents the application of a new methodology for the rapid synthesis of a single-degree-of-freedom function generating linkages. Harmonic analysis and normalization are used as a means of evaluating linkage performance. The performance information for a large number of linkage types and dimensional variants are stored in a software-based library. A means whereby this library can he searched for linkages to meet prescribed performance criteria is discussed. The use of an optimization technique to ‘fine tune’ the library selections is introduced. Finally, an example of the use of the methodology is given for the synthesis of a linkage required to reproduce a particular performance requirement.
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31

Ulakpa, Wisdom Chukwuemeke. "Optimization of Biodiesel Synthesis using Response Surface Methodology." International Journal for Research in Applied Science and Engineering Technology 9, no. 5 (May 31, 2021): 1332–39. http://dx.doi.org/10.22214/ijraset.2021.34532.

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32

Joshi, Uday, Muriel Pipelier, Sebastien Naud, and Didier Dubreuil. "Ring Contraction Methodology for the Synthesis of Pyrroles." Current Organic Chemistry 9, no. 3 (February 1, 2005): 261–88. http://dx.doi.org/10.2174/1385272053369132.

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33

Cudic, Predrag, and Maciej Stawikowski. "Pseudopeptide Synthesis via Fmoc Solid-Phase Synthetic Methodology." Mini-Reviews in Organic Chemistry 4, no. 4 (November 1, 2007): 268–80. http://dx.doi.org/10.2174/157019307782411716.

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34

Vanelle, Patrice, Pascal Rathelot, José Maldonado, and Michel P. Crozet. "Synthesis of Various Substituted Nitroisoquinolines by SRN1 Methodology." HETEROCYCLES 45, no. 8 (1997): 1519. http://dx.doi.org/10.3987/com-97-7829.

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35

Liu, Jianping, Lewis N. Mander, and Masaji Koshioka. "Methodology for the synthesis of 11,13-hydroxy gibberellins." Arkivoc 2004, no. 10 (June 11, 2004): 68–79. http://dx.doi.org/10.3998/ark.5550190.0005.a08.

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36

Mukhitdinov, Akmal, Kamoliddin Ziyaev, Janserik Omarov, and Shokhsanam Ismoilova. "Methodology of constructing driving cycles by the synthesis." E3S Web of Conferences 264 (2021): 01033. http://dx.doi.org/10.1051/e3sconf/202126401033.

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The difference in the dynamics of the development of motorization in the regions of the world, the levels of traffic organization, determines the need to develop a methodology for specific operating conditions. Improvement of the existing driving cycles and methods of their development, which characterize the real operating conditions, is of great importance. An important task is considered the implementation of targeted research to improve automobile operation efficiency of vehicles by introducing modern information technologies into the process of determining the driving cycles, modernizing the design parameters of vehicles by assessing the influence of driving conditions when rationing fuel consumption, developing methods for choosing the design parameters of vehicles and the most adapted vehicle for specific operating conditions. The article provides a systematic analysis of scientific research of methodology for constructing driving cycles, factors influencing the performance and driving modes, as well as the fuel consumption of the car. The methodology for constructing a standard driving cycle for specific urban operating conditions is given based by synthesizing on passenger car driving modes in the city.
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37

Monagheddu, M., N. Bertolino, P. Giuliani, C. Zanotti, and U. Anselmi Tamburini. "Ignition phenomena in combustion synthesis: An experimental methodology." Journal of Applied Physics 92, no. 1 (July 2002): 594–99. http://dx.doi.org/10.1063/1.1486254.

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38

Banerjee, Debasish. "A methodology for synthesis of recursive functional programs." ACM Transactions on Programming Languages and Systems 9, no. 3 (July 1987): 441–62. http://dx.doi.org/10.1145/24039.24071.

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39

Williams, David, and Liangfeng Fu. "Methodology for the Synthesis of Substituted 1,3-Oxazoles." Synlett 2010, no. 04 (February 8, 2010): 591–94. http://dx.doi.org/10.1055/s-0029-1219374.

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40

Nakabayashi, Kazuhiro. "Direct arylation polycondensation as conjugated polymer synthesis methodology." Polymer Journal 50, no. 7 (April 9, 2018): 475–83. http://dx.doi.org/10.1038/s41428-018-0039-5.

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41

Kirovski, D., and M. Potkonjak. "Local watermarks: Methodology and application to behavioral synthesis." IEEE Transactions on Computer-Aided Design of Integrated Circuits and Systems 22, no. 9 (September 2003): 1277–84. http://dx.doi.org/10.1109/tcad.2003.816208.

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42

Chowdhary, A., and R. K. Gupta. "A methodology for synthesis of data path circuits." IEEE Design & Test of Computers 19, no. 6 (November 2002): 90–100. http://dx.doi.org/10.1109/mdt.2002.1047748.

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43

BALL, HAYDN L., and PAOLO MASCAGNI. "Chemical synthesis and purification of proteins: a methodology." International Journal of Peptide and Protein Research 48, no. 1 (January 12, 2009): 31–47. http://dx.doi.org/10.1111/j.1399-3011.1996.tb01104.x.

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44

Anderson, James C., and Hilmi Namli. "Ambient Temperature Unsymmetrical Biaryl Synthesis Using Suzuki Methodology." Synlett 1995, no. 07 (July 1995): 765–66. http://dx.doi.org/10.1055/s-1995-5064.

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45

Itzhaky, Shachar, Sumit Gulwani, Neil Immerman, and Mooly Sagiv. "A simple inductive synthesis methodology and its applications." ACM SIGPLAN Notices 45, no. 10 (October 17, 2010): 36–46. http://dx.doi.org/10.1145/1932682.1869463.

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46

Fu, Zaiming, Hanglin Liu, and Nan Ren. "Methodology for digital synthesis of ultra‐narrow pulses." Electronics Letters 54, no. 16 (August 2018): 969–70. http://dx.doi.org/10.1049/el.2018.1218.

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47

Jackson, Stephen K., Avedis Karadeolian, Alex B. Driega, and Michael A. Kerr. "Stereodivergent Methodology for the Synthesis of Complex Pyrrolidines." Journal of the American Chemical Society 130, no. 12 (March 2008): 4196–201. http://dx.doi.org/10.1021/ja710289k.

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48

Williams, Craig, and Rebecca Pouwer. "Method in the Madness - Methodology from Total Synthesis." Synlett 23, no. 10 (May 29, 2012): 1446–58. http://dx.doi.org/10.1055/s-0031-1290967.

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49

Job, Andreas, Carsten F. Janeck, Wolfgang Bettray, René Peters, and Dieter Enders. "The SAMP-/RAMP-hydrazone methodology in asymmetric synthesis." Tetrahedron 58, no. 12 (March 2002): 2253–329. http://dx.doi.org/10.1016/s0040-4020(02)00080-7.

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50

Partridge, Benjamin M., Stephen P. Thomas, and Varinder K. Aggarwal. "Enantioenriched synthesis of Escitalopram using lithiation–borylation methodology." Tetrahedron 67, no. 52 (December 2011): 10082–88. http://dx.doi.org/10.1016/j.tet.2011.09.142.

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