Relevant bibliographies by topics / Metal-arene compounds

Academic literature on the topic 'Metal-arene compounds'

Author: Grafiati
Published: 10 December 2022
Last updated: 28 January 2023

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Journal articles on the topic "Metal-arene compounds"

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Harris, Ronald L. "Bis(arene)metal compounds." Journal of Organometallic Chemistry 299, no. 1 (January 1986): 105–10. http://dx.doi.org/10.1016/0022-328x(86)84037-2.

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Pekachaki, Henrik Margharian, Saeed Taghvaei-Ganjali, Fereshteh Motiee, and Mandana Saber-Tehrani. "APPLICATION OF CALIXARENE DERIVATIVES AS TACKIFIER RESIN IN RUBBER COMPOUNDS FOR TIRE APPLICATIONS." Rubber Chemistry and Technology 92, no. 3 (July 1, 2019): 467–80. http://dx.doi.org/10.5254/rct.19.81510.

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ABSTRACT The effect of p-tert-Butylcalix[4]arene on rubber-nylon-6 fabric and rubber-metal bead wire adhesion strength was quantified. For this purpose, two typically used rubber compounds were employed for two reinforcing motorcycle tire components: ply and bead. The standard pull-out tests of rubber–fabric and rubber–metal showed improvements in adhesion strength by incorporating p-tert-Butylcalix[4]arene into rubber compounds. However, the maximum values of adhesion force to pull the polyamide fabrics and brass-coated metal wires out of the rubber compounds were observed when only 1.0 phr of p-tert-Butylcalix[4]arene was used. The adhesion performance of both fabric and metal wire decreased with higher loading amounts of p-tert-Butylcalix[4]arene. The effect of a commercial phenolic tackifying resin was also evaluated in bead compound. Very similar adhesion results to p-tert-Butylcalix[4]arene were obtained when using 1.0 phr phenolic resin.
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Hansen, Valerie M., Jonathan L. Male, and Roland K. Pomeroy. "Arene–manganese and arene–rhenium compounds of formula (arene)M(CO)2(SiCl3)." Canadian Journal of Chemistry 75, no. 5 (May 1, 1997): 531–35. http://dx.doi.org/10.1139/v97-062.

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Derivatives of formula (arene)M(CO)2(SiCl3) (M = Mn, Re) have been prepared in moderate to good yield by the reaction of M(CO)5(SiCl3) and the appropriate arene (with heptane in those cases where the arene was a solid) in an evacuated sealed tube at 230–260 °C for 12–24 h, depending on the arene and the metal. Carefully purified reagents were necessary to obtain satisfactory yields. The (η6-1,4-C6H4tBu2)M(CO)2(SiCl3) complexes in solution exhibit free rotation of the arene ring about the metal atom to −120 °C as ascertained by 1H NMR spectroscopy. The manganese compound did show the onset of decoalescence of two of the signals due to the arene ligand in the 13C{1H} NMR spectrum in CD2Cl2, solution below −90 °C. This, however, is interpreted in terms of restricted rotation of the tert-butyl substituent rather than restricted rotation of the arene ring. Keywords: arene, manganese, rhenium, restricted rotation.
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Wang, Jie, Hongyu Guan, Chunhua Ge, Ping Fan, Xijuan Xing, and Yunshan Shang. "Azocalix[4]arene with three distal ethyl ester residues as a highly selective chromogenic sensor for Ca2+ ions." Heterocyclic Communications 24, no. 3 (June 27, 2018): 147–50. http://dx.doi.org/10.1515/hc-2017-0239.

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AbstractThree azocalix[4]arenes with distal ethyl ester residues, 5-phenylazo-25,26,27-tris[(ethoxycarbonyl)methoxy]-28-hydroxycalix[4]arene (2), 5-(o-methylphenyl)azo-25,26,27-tris[(ethoxycarbonyl)methoxy]-28-hydroxycalix[4]arene (3), 5-(p-Methylphenyl)azo-25,26,27-tris[(ethoxycarbonyl)methoxy]-28-hydroxycalix[4]arene (4), were synthesized and their binding properties with metal ions were investigated by ultraviolet (UV)/visible spectroscopy. The chromogenic behavior of these compounds upon metal ion complexation indicates a specific selectivity toward Ca2+ ion in the presence of other cations tested. The stoichiometry of 3 to Ca2+ ion in the complex is 1:1 and the stability constant of the complex is 1.28×104m−1.
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Zhi, Sanjun, Hongjun Yao, and Wei Zhang. "Difunctionalization of Dienes, Enynes and Related Compounds via Sequential Radical Addition and Cyclization Reactions." Molecules 28, no. 3 (January 23, 2023): 1145. http://dx.doi.org/10.3390/molecules28031145.

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Radical reactions are powerful in creating carbon–carbon and carbon–heteroatom bonds. Designing one-pot radical reactions with cascade transformations to assemble the cyclic skeletons with two new functional groups is both synthetically and operationally efficient. Summarized in this paper is the recent development of reactions involving radical addition and cyclization of dienes, diynes, enynes, as well as arene-bridged and arene-terminated compounds for the preparation of difunctionalization cyclic compounds. Reactions carried out with radical initiators, transition metal-catalysis, photoredox, and electrochemical conditions are included.
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Schneider, Jörg J., and Dirk Wolf. "Mechanistische Untersuchungen zum reversiblen Gleichgewicht von metallorganischen Tripeldecker- und Sandwichkomplexen des Typs [Bis{(η5-CpR)Co}-μ-{η4:η4-aren}] und [(η5-CpR)Co(η6-aren)] / Mechanistic Studies towards the Reversible Equilibrium between Metal Organic Triple Decker and Sandwich Complexes [Bis{(η5 -CpR)Co}-μ-{η4 :η4-arene}] and [{(η5-CpR)Co(η6-arene)]." Zeitschrift für Naturforschung B 53, no. 11 (November 1, 1998): 1267–72. http://dx.doi.org/10.1515/znb-1998-1105.

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The arene ligand exchange mechanism of slipped arene triple deckers [Bis{(η5-CpR)Co}-μ-{η4:η4-arene}] (R = Me5, 1,2,4 tri-tert butyl, arene = benzene, toluene) 1 was studied by 1H-NMR spectroscopy for different concentrations and solvents. It has been found that triple deckers of type 1 decompose slowly in solution. A unique equilibrium, between these triple deckers and the mixed sandwich complexes [(η6-arene)Co(η5-CpR)] and 14 e [(η5-Cp)Co]solv fragments generated in situ by decomposition o f 1 exists. In addition to this equilibrium arene lability of the thus formed mixed sandwich complex type has been detected by NMR making slipped triple deckers 1 ideal single source compounds for the generation of two [(η5-Cp)Co] fragments in one reaction step. Such fragments are valuable metal ligand components with high synthetic utility in organometallic chemistry.
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Küppers, Luca, and Walter Frank. "Investigation of mesitylene-solvated group 13 mixed-metal halides: syntheses and crystal structures of bis(1,3,5-trimethylbenzene)gallium(I) tetrachlorido- and tetrabromidoaluminate(III) and (1,3,5-trimethylbenzene)gallium(I) tetraiodidoaluminate(III). Variation of the gallium-π-arene bond strength." Zeitschrift für Naturforschung B 74, no. 10 (October 25, 2019): 773–82. http://dx.doi.org/10.1515/znb-2019-0139.

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AbstractBis(1,3,5-trimethylbenzene)gallium(I) tetra­chloridoaluminate(III), [(1,3,5-(CH3)3C6H3)2Ga][AlCl4] (1), bis(1,3,5-trimethylbenzene)gallium(I) tetrabromido­aluminate(III), [(1,3,5-(CH3)3C6H3)2Ga][AlBr4] (2) and (1,3,5-trimethylbenzene)gallium(I) tetraiodidoaluminate(III), [1,3,5-(CH3)3C6H3Ga][AlI4] (3) were synthesized from the corresponding subvalent GaI/AlIII mixed metal halides and characterized via C,H analysis, Raman spectroscopy, X-ray powder diffraction and X-ray single crystal diffraction. Compound 1 crystallizes in the noncentrosymmetric monoclinic space group Cc isotypic to [(1,3,5-(CH3)3C6H3)2Ga][GaCl4]. For 2 and 3 the monoclinic space group P21/n is found, however, they are neither isotypic nor homotypic. While 2 is isotypic to [(1,3,5-(CH3)3C6H3)2In][InBr4], 3 establishes a new structure type. In the solids of all three title compounds coordination polymeric chains are found, in 1 and 2 built up from bis(arene)-coordinated, in 3 from mono(arene)-coordinated Ga+ ions and the corresponding AlX4− anions in a 1κCl:2κCl′ (1), 1κCl,Cl′:2κCl″ (2) or 1κCl,Cl′:2κCl″:3κCl‴ (3) bridging mode. Taking into account the weaker coordinating character of the AlCl4− as compared to the AlBr4− anion, in line with expectations the number of gallium halogen contacts is increased and the strength of the π-arene bonding is reduced in the bromide 2 as compared to the chloride 1. Finally, with the even more strongly coordinating AlI4− anion the arene coordination is limited to one molecule. Considering mesitylene complexes of gallium, the formation of a mono(arene) complex is unprecedented and even considering group 13 elements in general, the formation of a mono(mesitylene) complex like 3 is unusual. Furthermore, compound 3 is the first structurally characterized arene solvate of a main group metal tetraiodidometallate.
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Preda, Ana-Maria, Małgorzata Krasowska, Lydia Wrobel, Philipp Kitschke, Phil C. Andrews, Jonathan G. MacLellan, Lutz Mertens, et al. "Evaluation of dispersion type metal···π arene interaction in arylbismuth compounds – an experimental and theoretical study." Beilstein Journal of Organic Chemistry 14 (August 15, 2018): 2125–45. http://dx.doi.org/10.3762/bjoc.14.187.

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The dispersion type Bi···π arene interaction is one of the important structural features in the assembly process of arylbismuth compounds. Several triarylbismuth compounds and polymorphs are discussed and compared based on the analysis of single crystal X-ray diffraction data and computational studies. First, the crystal structures of polymorphs of Ph3Bi (1) are described emphasizing on the description of London dispersion type bismuth···π arene interactions and other van der Waals interactions in the solid state and the effect of it on polymorphism. For comparison we have chosen the substituted arylbismuth compounds (C6H4-CH═CH2-4)3Bi (2), (C6H4-OMe-4)3Bi (3), (C6H3-t-Bu2-3,5)3Bi (4) and (C6H3-t-Bu2-3,5)2BiCl (5). The structural analyses revealed that only two of them show London dispersion type bismuth···π arene interactions. One of them is the styryl derivative 2, for which two polymorphs were isolated. Polymorph 2a crystallizes in the orthorhombic space group P212121, while polymorph 2b exhibits the monoclinic space group P21/c. The general structure of 2a is similar to the monoclinic C2/c modification of Ph3Bi (1a), which leads to the formation of zig-zag Bi–arenecentroid ribbons formed as a result of bismuth···π arene interactions and π···π intermolecular contacts. In the crystal structures of the polymorph 2b as well as for 4 bismuth···π arene interactions are not observed, but both compounds revealed C–HPh···π intermolecular contacts, as likewise observed in all of the three described polymorphs of Ph3Bi. For compound 3 intermolecular contacts as a result of coordination of the methoxy group to neighboring bismuth atoms are observed overruling Bi···π arene contacts. Compound 5 shows a combination of donor acceptor Bi···Cl and Bi···π arene interactions, resulting in an intermolecular pincer-type coordination at the bismuth atom. A detailed analysis of three polymorphs of Ph3Bi (1), which were chosen as model systems, at the DFT-D level of theory supported by DLPNO-CCSD(T) calculations reveals how van der Waals interactions between different structural features balance in order to stabilize molecular arrangements present in the crystal structure. Furthermore, the computational results allow to group this class of compounds into the range of heavy main group element compounds which have been characterized as dispersion energy donors in previous work.
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Hanif, Muhammad, Patricia Schaaf, Wolfgang Kandioller, Michaela Hejl, Michael A. Jakupec, Alexander Roller, Bernhard K. Keppler, and Christian G. Hartinger. "Influence of the Arene Ligand and the Leaving Group on the Anticancer Activity of (Thio)maltol Ruthenium(II)–(η6-Arene) Complexes." Australian Journal of Chemistry 63, no. 11 (2010): 1521. http://dx.doi.org/10.1071/ch10232.

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Maltol and its metal complexes have shown promising applications in medicinal chemistry. We report here the synthesis and characterization of Ru(η6-arene)(halido) coordination compounds bearing maltol or thiomaltol ligands and studies on their behaviour in aqueous solution, their reactions with the DNA model guanosine 5′-monophosphate (5′-GMP) and their in vitro anticancer activity in human tumour cell lines. The compounds hydrolyze rapidly and quantitatively to the respective aqua species by exchange of the halido ligand. With pKa values of >8, such species would also be present in biological media and they proved reactive to 5′-GMP. The thiomaltol compounds show promising in vitro activity with IC50 values (50% inhibitory concentration) in the low micromolar range, whereas activity of the maltol complexes is marginal. Variation of the arene ligand (benzene, toluene, p-cymene or biphenyl) resulted only in minor changes in activity.
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Profilet, Robert D., Arlene P. Rothwell, and Ian P. Rothwell. "Surface-supported group 5 metal organometallic compounds for catalytic arene hydrogenation." Journal of the Chemical Society, Chemical Communications, no. 1 (1993): 42. http://dx.doi.org/10.1039/c39930000042.

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Dissertations / Theses on the topic "Metal-arene compounds"

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Mobbs, B. E. "Arene transition metal complexes in synthesis." Thesis, University of Oxford, 1985. http://ora.ox.ac.uk/objects/uuid:4c7030d4-297e-4af8-a622-d5b4963fc0a3.

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This thesis deals with the applications of organopalladium and organochromium chemistry to the functionalisation of the benzopyran ring system, at a variety of oxidation levels. Section I demonstrates the functionalisation of 3-, 6-, and 8-bromochromones via palladium (0) insertion into the C-Br bond. The resultant arylpalladium species are shown to undergo addition to the least substituted end of a variety of olefins including methyl acrylate, acrylonitrile and styrene. Subsequent palladium-hydride elimination leads to overall palladium catalysed vinylation of the chromone and the synthesis of a number of novel compounds. Vinylation occurs regiospecifically at the site of chromone bromination and is shown to allow clean substituent introduction into each of the three sites. The palladium catalysed reaction of 3,6-dibromo-chromone with methyl acrylate leads to vinylation at both the C3 and C6 positions. Carbonylation of the 6-bromochromone in ethanol or butanol leads to the 6-ethyl or 6-butyl esters respectively. The palladium catalysed vinylation of the 6-bromochromone with ethyl vinyl ether leads to a mixture of products from addition of the chromone to either end of the olefin. With p-bromophenol or p-bromo-N,N-dimethylaniline the reaction gives exclusively the acetylated product arising from addition to the more substituted end of the olefin. This change in orientation is rationalised by considering the polarisation of the olefin and the arylpalladium species. Section II demonstrates the functionalisation of chroman and 4-chromanol via coordination to the Cr(CO)3 moiety. (η6-Chroman)Cr(CO)3 is synthesised and is shown to undergo regiospecific ring deprotonation at C8 under kinetic conditions or regiospecific benzylic deprotonation at C4 under thermodynamic conditions. The resultant anions are quenched with alkyl halides, aldehydes, Eschenmoser's salt and methyl disulphide resulting in selective functionalisation of either site. No mixed products are observed. The uncomplexed arene is shown to be totally unreactive under identical conditions. (η6-4-Chromanol)Cr(CO)3 is synthesised and is shown to undergo regiospecific C8 ring deprotonation by comparison with authentic samples of the C5 and C8 methylated alcohols. Protection of the hydroxyl group as its methyl, t-butyldimethylsilyl or methoxymethyl ethers is found not to alter the regiochemistry of deprotonation. The 4-chromanol t-butyldimethylsilyl and tri-i-propylsilyl ethers are synthesised and coordinated to the metal unit. Cleavage of the silyl ethers is shown to proceed with loss of stereochemistry, indicating C-0 bond cleavage.
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Ismail, Ashraf A. "Chalcocarbonyl chemistry : application in hormonal receptor determination, metalloporphyrins and metal-arene bond activation." Thesis, McGill University, 1985. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=72063.

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The reaction of ((eta)-Arene)Cr(CO)(,2)(CX) (X = S, Se) complexes with excess (RO)(,3)P (R = Me, Et, n-Bu, Ph) yields Cr(CO)(,2)(CX) (RO)(,3)P (,3), predominantly as the mer I isomer, in which a phosphite ligand is trans to CX. Arene displacement from ((eta)-C(,6)H(,6))Cr(CO)(,2)(CX) by tridentate phosphine ligands L-L-L L-L-L = (Me)C(CH(,2)P(Ph)(,2))(,3), (Ph(,2)PCH(,2)CH(,2))(,2)PhP gives fac-(L-L-L)Cr(CO)(,2)(CX) products. The molecular structures of Cr(CO)(,2)(CX) (MeO)(,3)P (,3) have been determined by single crystal X-ray diffraction. Intramolecular isomerization of these complexes as well as their tricarbonyl analogue has been demonstrated and activation parameters have been calculated for the rearrangement processes. Two-dimensional ('31)P NMR spectroscopy has provided evidence that isomerization occurs via trigonal prismatic intermediates. Kinetic investigations of the reaction of ((eta)-C(,6)H(,6))Cr(CO)(,2)(CX) with (MeO)(,3)P have established a first-order rate dependence on both the complex and the entering ligand. The faster reaction rate of the selenocarbonyl derivative relative to its thiocarbonyl analogue originates in a lower entropy of activation in the former case. The effect on the reaction rate of variation in the nature of the arene and of the entering ligand has been investigated.
An approach to hormonal receptor assay involving the detection by FT-IR spectroscopy of Cr(CO)(,3)-labelled modified estradiol bound to estrogen receptors in target tissue is reported.
The FT-IR spectra of FeTPP(CX) FeTPP = (5,10,15,20-tetraphenyl-porphinato)Fe(II); X = S, Se and FeTPP(CX)L (X = S, Se; L = pyridine, ethanol) have been obtained. Some changes in the porphyrin spectrum were observed with variation or removal of L, but not with variation of X.
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Escárcega, Bobadilla Martha Verónica. "Organometallic compounds and metal nanoparticles as catalysts in low environmental impact solvents." Doctoral thesis, Universitat Rovira i Virgili, 2011. http://hdl.handle.net/10803/9114.

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Durant les darreres dècades, el disseny de processos en el marc de la química sostenible ha anat creixent de forma exponencial. La recerca constant de processos mes benignes amb el medi ambient ha implicat un gran esforç per obtenir millors rendiments mitjançant l'activació de llocs específics, i possant especial èmfasi amb el control de la quimio-, la regio- i la enantioselectivitat, punts crucials per a l'economia atómica. En aquest sentit, els dissolvents juguen un paper crític, i com podrà veure's al llarg d'aquesta memòria..
Aquesta Tesi s'enfoca en l'ús de mitjans de reacció alternatius i sostenibles, com són els líquids iònics (ILs), el diòxid de carboni supercrític (scCO2) i la barreja de ambdós dissolvents, amb l'objectiu de disminuir l'ús de dissolvents orgànics convencionals i la seva aplicació en els següents processos catalítics: hidrogenació asimètrica, reacció de Suzuki d'acoblament creuat C-C, reacció d'alquilació al·lílica asimètrica i la hidrogenació de arens.
In the last decades, the design of processes in the framework of the sustainable chemistry has been exponentially growing. The constant searching of cleaner processes has led to a lot of effort to obtain higher yields by activation of specific sites, and improving chemo-, regio- and enantio-selectivities, which are crucial from a point of view of an atom economy strategy. In this sense, solvents play a critical role.
This PhD thesis focuses on the use of alternative sustainable reaction media such as ionic liquids (ILs), supercritical carbon dioxide (scCO2) and mixtures of both solvents in different catalytic processes, with the aim of decreasing the use of conventional organic solvents applied in the following catalytic reactions: homogeneous and supported rhodium catalysed asymmetric hydrogenation, biphasic palladium catalysed Suzuki C-C cross-coupling, homogeneous palladium catalysed asymmetric allylic alkylation, and ruthenium and rhodium nanoparticles catalysed arene hydrogenation were tested.
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SEMRA, ASSIA. "Substitutions nucleophiles en serie arenetricarbonylchrome." Paris 6, 1987. http://www.theses.fr/1987PA066622.

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Books on the topic "Metal-arene compounds"

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Peter, Kündig E., and Böttcher A, eds. Transition metal arene [pi]-complexes in organic synthesis and catalysis. Berlin: Springer-Verlag, 2004.

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Kündig, E. Peter. Transition Metal Arene ? -Complexes in Organic Synthesis and Catalysis. Springer, 2013.

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Book chapters on the topic "Metal-arene compounds"

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Wilkinson, G., and F. A. Cotton. "Cyclopentadienyl and Arene Metal Compounds." In Progress in Inorganic Chemistry, 1–124. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470166024.ch1.

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Mashima, K., and A. Nakamura. "Metal–Arene Complexes." In Compounds of Groups 7-3 (Mn..., Cr..., V..., Ti..., Sc..., La..., Ac...), 1. Georg Thieme Verlag KG, 2003. http://dx.doi.org/10.1055/sos-sd-002-00508.

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Negishi, E. i., and T. Takahashi. "Metal–η-Arene and –η-Arene Complexes." In Compounds of Groups 7-3 (Mn..., Cr..., V..., Ti..., Sc..., La..., Ac...), 1. Georg Thieme Verlag KG, 2003. http://dx.doi.org/10.1055/sos-sd-002-00798.

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Negishi, E. i., and T. Takahashi. "Metal–η-Arene Complexes." In Compounds of Groups 7-3 (Mn..., Cr..., V..., Ti..., Sc..., La..., Ac...), 1. Georg Thieme Verlag KG, 2003. http://dx.doi.org/10.1055/sos-sd-002-00805.

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Kündig, E. P., and S. H. Pache. "Direct Synthesis of Metal–Bis(arene) Complexes via Metal Evaporation." In Compounds of Groups 7-3 (Mn..., Cr..., V..., Ti..., Sc..., La..., Ac...), 1. Georg Thieme Verlag KG, 2003. http://dx.doi.org/10.1055/sos-sd-002-00216.

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Kündig, E. P., and S. H. Pache. "Synthesis of Metal–Bis(arene) Complexes by Arene Exchange, by Arene Transformation Reactions, and by Cyclic Condensation Reactions." In Compounds of Groups 7-3 (Mn..., Cr..., V..., Ti..., Sc..., La..., Ac...), 1. Georg Thieme Verlag KG, 2003. http://dx.doi.org/10.1055/sos-sd-002-00218.

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Kündig, E. P., and S. H. Pache. "Synthesis of Tricarbonylmetal--Arene Complexes from Metal–Carbonyls." In Compounds of Groups 7-3 (Mn..., Cr..., V..., Ti..., Sc..., La..., Ac...), 1. Georg Thieme Verlag KG, 2003. http://dx.doi.org/10.1055/sos-sd-002-00219.

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Kündig, E. P., and S. H. Pache. "Synthesis of Metal–Bis(arene) Complexes by Reductive Methods." In Compounds of Groups 7-3 (Mn..., Cr..., V..., Ti..., Sc..., La..., Ac...), 1. Georg Thieme Verlag KG, 2003. http://dx.doi.org/10.1055/sos-sd-002-00217.

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Theopold, K. H., A. Mommertz, and B. A. Salisbury. "Synthesis of Metal–Cyclodienyl Complexes from Metal–Arene or –Cycloheptatriene Complexes by Nucleophilic Addition." In Compounds of Groups 7-3 (Mn..., Cr..., V..., Ti..., Sc..., La..., Ac...), 1. Georg Thieme Verlag KG, 2003. http://dx.doi.org/10.1055/sos-sd-002-00269.

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Ojima, I., A. T. Vu, and D. Bonafoux. "Rhodium–Arene Complexes." In Compounds with Transition Metal-Carbon pi-Bonds and Compounds of Groups 10-8 (Ni, Pd, Pt, Co, Rh, Ir, Fe, Ru, Os), 1. Georg Thieme Verlag KG, 2001. http://dx.doi.org/10.1055/sos-sd-001-00400.

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Reports on the topic "Metal-arene compounds"

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Rothwell, I. P. Catalytic arene hydrogenation using early transition metal hydride compounds. Office of Scientific and Technical Information (OSTI), March 1993. http://dx.doi.org/10.2172/6443562.

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Rothwell, I. P. Catalytic arene hydrogenation using early transition metal hydride compounds. Progress report. Office of Scientific and Technical Information (OSTI), March 1993. http://dx.doi.org/10.2172/10159596.

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