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Journal articles on the topic 'Mesoporous silicates'

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Author: Grafiati

Published: 10 December 2022

Last updated: 28 January 2023

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1

E. Sangok, Faustina, Sabrina M. Yahaya, Izza Taib Nurul, Siti Zaleha Sa'ad, and Nor Fazila Rasaruddin. "Comparison Study of Amino-Functionalized and Mercaptopropyl-Functionalized Mesoporous Silica MCM-41." Advanced Materials Research 550-553 (July 2012): 1603–6. http://dx.doi.org/10.4028/www.scientific.net/amr.550-553.1603.

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The ability to decorate silicate surface with different organoalkoxysilanes creates powerful new capabilities for catalyst, adsorbents and chemical separation. Mesopororus silica, MCM-41 was modified by grafting of amino and mercaptopropyl functional group. The structures of these materials were characterized by using Fourier Transform Infrared Spectroscopy (FT-IR), and X-Ray diffraction (XRD). The samples were found to exhibit structural properties similar to those reported earlier. Significant functional groups of the modified mesoporous silicates were found in the spectrum of FT-IR. Standard structure of mesoporous silicates were found to be preserved at planar [100] of XRD difractogram of mesoporous silicates. Adsorption of Cu (II) ions were done under different temperatures, initial concentrations and pH. Adsorption process also was determined from kinetic point of view and was found to be better fitted to pseudo second order of kinetic model.

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2

Macquarrie, Duncan J., Dominic B. Jackson, James E. G. Mdoe, and James H. Clark. "Organomodified hexagonal mesoporous silicates." New Journal of Chemistry 23, no. 5 (1999): 539–44. http://dx.doi.org/10.1039/a900839j.

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3

Hudson, Sarah, Jakki Cooney, and Edmond Magner. "Proteins in Mesoporous Silicates." Angewandte Chemie International Edition 47, no. 45 (October 27, 2008): 8582–94. http://dx.doi.org/10.1002/anie.200705238.

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4

Liu, Guozhen, Nicholas M. K. Tse, Matthew R. Hill, Danielle F. Kennedy, and Calum J. Drummond. "Disordered Mesoporous Gadolinosilicate Nanoparticles Prepared Using Gadolinium Based Ionic Liquid Emulsions: Potential as Magnetic Resonance Imaging Contrast Agents." Australian Journal of Chemistry 64, no. 5 (2011): 617. http://dx.doi.org/10.1071/ch11064.

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Gadolinium doped mesoporous silica (gadolinosilicate) nanoparticles were synthesized using a novel approach aimed at incorporating Gd ions into a porous silica network. The ionic liquid, gadolinium (Z)-octadec-9-enoate (Gd Oleate) was utilized in a dual role, as a soft template to generate porous silica and also to act as a gadolinium source for incorporation into the silicate. The generated silicate materials were characterized for size, structure and composition, confirming that gadolinium was successfully doped into the silicate network in a mesoporous nanoparticulate form. Proton relaxivity results indicated that the gadolinium doped silicates had slightly lower longitudinal relaxivity and much higher transverse relaxivity than the commercial contrast agent Magnevist®, suggesting that the mesoporous nanoparticulate materials have potential as contrast agents for magnetic resonance imaging.

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5

Srinivasan, U., I. Homma, C. M. Chun, D. M. Dabbs, D. A. Hajduk, S. M. Gruner, and I. A. Aksay. "Nanocomposite processing via infiltration of mesoporous silica." Proceedings, annual meeting, Electron Microscopy Society of America 53 (August 13, 1995): 212–13. http://dx.doi.org/10.1017/s0424820100137434.

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Synthesis of materials with nanoscale (1~100 nm) organization is important in various applications. Recently, scientists at Mobil described a new family of mesoporous molecular sieves. These materials have regular arrays of uniform pore channels ranging from 1.6~10 nm in diameter in contrast to other mesoporous solids such as amorphous silicas and modified layered clays and silicates. A surfactantsilicate co-assembly model has been proposed to explain the formation of these materials. According to this pathway, the matching of the charge density at the organic-inorganic interface controls the assembly of the mesophases and four distinct silica mesophases have been observed, lamellae, hexagonally packed tubes, and two bicontinuous structures of cubic symmetry. Different phases are constructed by varying the synthesis parameters such as the surfactant/silicate ratio and the acidity. Here, we report the synthesis of a new amorphous mesoporous phase with short range order and with no long range crystallinity. Due to its interpenetrating network structure, this amorphous mesoporous silica can be used as a matrix for nanocomposite processing. Here, we use it as a host to process ruby glass.

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6

Kouznetsova, T. F., A. I. Ivanets, and V. S. Komarov. "Low-temperature synthesis of mesoporous M41S metal-silicates and their adsorption and capillary-condensation properties." Proceedings of the National Academy of Sciences of Belarus, Chemical Series 55, no. 3 (September 13, 2019): 338–44. http://dx.doi.org/10.29235/1561-8331-2019-55-3-338-344.

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Low-temperature synthesis of the mesoporous silicates containing d-metals is carried out. The measured isotherms of low-temperature nitrogen adsorption-desorption by chrome, vanadium and zirconium silicate adsorbents belong to Type IV (b) of sorption isotherms on IUPAC classification. Such isothermal curves are inherent in mesoporous systems with the M41S type of ordering of the making elements. Increasing рН of sedimentation and metal content lead to amorphization of samples and distortion of a supramolecular lattice with uniform regular geometry and a long-range ordering.

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7

Wan, Ying, Dieqing Zhang, Na Hao, and Dongyuan Zhao. "Organic groups functionalised mesoporous silicates." International Journal of Nanotechnology 4, no. 1/2 (2007): 66. http://dx.doi.org/10.1504/ijnt.2007.012316.

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8

Hudson, Sarah P., Robert F. Padera, Robert Langer, and Daniel S. Kohane. "The biocompatibility of mesoporous silicates." Biomaterials 29, no. 30 (October 2008): 4045–55. http://dx.doi.org/10.1016/j.biomaterials.2008.07.007.

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9

Ukmar, Tina, and Odon Planinšek. "Ordered mesoporous silicates as matrices for controlled release of drugs." Acta Pharmaceutica 60, no. 4 (December 1, 2010): 373–85. http://dx.doi.org/10.2478/v1007-010-0037-4.

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Ordered mesoporous silicates as matrices for controlled release of drugs Interest in and thereby also development of ordered mesoporous silicates as drug delivery devices have grown immensely over the past few years. On hand selected cases from the literature, the power of such systems as delivery devices has been established. Specifically, it is shown how it is possible to enhance the release kinetics of poorly soluble drugs by embedding them in mesoporous silicates. Further critical factors governing the structure and release of the model drug itraconazole incorporated in an SBA-15 matrix are briefly reviewed. The possibility of functionalizing the surface of mesoporous matrices also under harsher conditions offers a broad platform for the design of stimuli-responsive drug release, including pH responsive systems and systems which respond to the presence of specific ions, reducing agents, magnetic field or UV light, whose efficiency and biocompatibility has been established in vitro.

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10

García, Hermenegildo. "Photoresponsive porous organosilicas." Pure and Applied Chemistry 75, no. 8 (January 1, 2003): 1085–90. http://dx.doi.org/10.1351/pac200375081085.

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Novel structured functional hybrid materials can be obtained by incorporating photoresponsive organic components into the silicate walls of periodic mesoporous silicates. Two such materials are described, containing either viologens or stilbene analogs. Thermal or photochemical activation of viologen units generates the corresponding radical cations, whose lifetime can vary from months to milliseconds, depending on the surfactant content of the solid. In a second example, the porosity and tortuosity of the silicate can be modulated by irradiation of an organosilica containing a stilbene-like moiety.

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11

Crudden, C., K. McEleney, D. Allen, and A. Holliday. "Mesoporous Silicates as Grubbs Catalyst Scavengers." Synfacts 2006, no. 9 (September 2006): 0962. http://dx.doi.org/10.1055/s-2006-949251.

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12

Alam, Nurul, and Robert Mokaya. "Crystalline mesoporous silicates from layered precursors." Journal of Materials Chemistry 18, no. 12 (2008): 1383. http://dx.doi.org/10.1039/b717273g.

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13

Kimura, Tatsuo, and Kazuyuki Kuroda. "Ordered Mesoporous Silica Derived from Layered Silicates." Advanced Functional Materials 19, no. 4 (February 24, 2009): 511–27. http://dx.doi.org/10.1002/adfm.200800647.

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14

Gounder, Rajamani. "Hydrophobic microporous and mesoporous oxides as Brønsted and Lewis acid catalysts for biomass conversion in liquid water." Catal. Sci. Technol. 4, no. 9 (2014): 2877–86. http://dx.doi.org/10.1039/c4cy00712c.

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15

Widmer, Susanne, Michael J. Reber, Patrick Müller, Catherine E. Housecroft, Edwin C. Constable, René M. Rossi, Dominik Brühwiler, Lukas J. Scherer, and Luciano F. Boesel. "Incorporation of a FRET dye pair into mesoporous materials: a comparison of fluorescence spectra, FRET activity and dye accessibility." Analyst 140, no. 15 (2015): 5324–34. http://dx.doi.org/10.1039/c5an00850f.

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16

Malhis, Abeer A., Sharif H. Arar, Manar K. Fayyad, and Hamdallah A. Hodali. "Amino- and thiol-modified microporous silicalite-1 and mesoporous MCM-48 materials as potential effective adsorbents for Pb(II) in polluted aquatic systems." Adsorption Science & Technology 36, no. 1-2 (January 25, 2017): 270–86. http://dx.doi.org/10.1177/0263617416689270.

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Aluminum-free zeolite silicalite-1 and the ordered mesoporous silicates Mobile Crystalline Material No. 48 (MCM-48) were prepared and functionalized with 3-aminopropyltriethoxysilane (APTES) and 3-mercaptopropyltrimethoxysilane (MPTMS) for the enhancement of adsorption capacity. Functionalization via post synthesis grafting method was adopted and the functionalized silicate systems were denoted as silicalite-1-NH2, silcalite-1-SH, MCM-48-NH2 and MCM-48-SH. Functionalization, that was confirmed by XRD, FT-IR and surface area measurements, indicated no structural changes on the silicate materials. The adsorption of Pb(II) ions into these modified silicates was investigated in aqueous solutions with optimized pH at 5.5 where adsorption influencing factors including contact time, adsorbent dose and metal ion initial concentration were studied. Adsorption experimental data for silicalite-1-NH2, MCM-48-NH2 and MCM-48-SH showed satisfactory correlation with Langmuir and Freundlich models. According to Langmuir isotherm, the maximum capacities for the above three modified silicate systems, for 100 ppm Pb(II) dose, are 43.5, 75.2 and 31.2 mg/g and with Kf constant values of 16.9, 44.4 and 12.0 L/mg from Freundlich isotherm, respectively. The three modified silicate systems exhibited complete sequestration of Pb(II) ion concentrations in the range 0.48–1.7 ppm from samples collected from Zarqa River in four seasons of the year 2013.

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17

Landmesser, H. "Interior surface hydroxyl groups in ordered mesoporous silicates." Solid State Ionics 101-103, no. 1-2 (November 1997): 271–77. http://dx.doi.org/10.1016/s0167-2738(97)00189-6.

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18

LANDMESSER, H. "Interior surface hydroxyl groups in ordered mesoporous silicates." Solid State Ionics 101-103 (November 1997): 271–77. http://dx.doi.org/10.1016/s0167-2738(97)84042-8.

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19

Lin, Hong-Ping, Yah-Ru Cheng, and Chung-Yuan Mou. "Hierarchical Order in Hollow Spheres of Mesoporous Silicates." Chemistry of Materials 10, no. 12 (December 1998): 3772–76. http://dx.doi.org/10.1021/cm980493v.

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20

O'Brien, Stephen, Julian M. Keates, Stephen Barlow, Mark J. Drewitt, Benjamin R. Payne, and Dermot O'Hare. "Synthesis and Characterization of Ferrocenyl-Modified Mesoporous Silicates." Chemistry of Materials 10, no. 12 (December 1998): 4088–99. http://dx.doi.org/10.1021/cm980510g.

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21

Gaffney, Darragh, Jakki Cooney, and Edmond Magner. "Modification of Mesoporous Silicates for Immobilization of Enzymes." Topics in Catalysis 55, no. 16-18 (September 29, 2012): 1101–6. http://dx.doi.org/10.1007/s11244-012-9899-7.

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22

Lu, Yi, Junlin Zheng, Jinku Liu, and Jin Mu. "Fe-containing mesoporous silicates with macro-lamellar morphology." Microporous and Mesoporous Materials 106, no. 1-3 (November 2007): 28–34. http://dx.doi.org/10.1016/j.micromeso.2007.02.017.

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23

Kim, Seok, Sung Goo Lee, and Soo Jin Park. "Ion Conducting Behaviors of Polymeric Composite Electrolytes Containing Mesoporous Silicates." Solid State Phenomena 119 (January 2007): 51–54. http://dx.doi.org/10.4028/www.scientific.net/ssp.119.51.

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Polymeric composite electrolytes (PCE) based on poly(ethylene oxide) (PEO) and mesoporous silicates as a filler material were fabricated, and investigated for understanding the effects of filler addition into the polymer matrix on the ionic conductivity. For a lithium battery application, it is necessary to increase ion conductivity of PCE by modification of microstructure. The ionic conductivity was enhanced with increasing MCM-41 contents due to the decreased crystallinity of PEO. Furthermore, the regular mesoporous structure could be functioned as an ion transfer channel for high ion mobility.

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24

Sun, Xinzhi, and Fanglin Du. "Synthesis, Characterization and Catalytic Properties of Monometal/SiO2 and Bimetal/SiO2 Hollow Spheres with Mesoporous Structure." Nano 12, no. 12 (December 2017): 1750148. http://dx.doi.org/10.1142/s179329201750148x.

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Monometallic M1(M[Formula: see text] Ni/Cu/Fe/Co) silicates and bimetallic Ni–M2(M[Formula: see text] Cu/Fe/Co) silicates hollow spheres with mesoporous structure and the controllable morphology have been synthesized successfully via one-step sacrificial template method under hydrothermal conditions. The catalysts were obtained by reducing the corresponding silicates in situ under the hydrogen atmosphere at a certain temperature. All the silicates and the catalysts M1/SiO2 and Ni–M2/SiO2 hollow spheres have been characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Brunauer–Emmett–Teller (BET) and temperature-programmed reduction (TPR) thoroughly and systematically. The morphology and reaction conditions of bimetallic Ni–M2 silicates hollow spheres depend on the second metal M2, which has been verified by SEM, TEM and XRD. From the results, it can be concluded that bimetallic silicates possess better physical properties in favor of the catalytic activity. Bimetallic Ni–M2/SiO2 hollow spheres had higher catalytic property than the monometallic M1/SiO2 and the conversion of nitrobenzene could reach 100% within 3[Formula: see text]h using Ni–Cu/SiO2 and Ni–Fe/SiO2 hollow spheres as catalysts.

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25

Li, Yunping, Wei Xiong, Chun Wang, Bo Song, and Guolin Zhang. "Synthesis of hexagonal mesoporous silicates functionalized with amino groups in the pore channels by a co-condensation approach." RSC Advances 6, no. 59 (2016): 53991–4000. http://dx.doi.org/10.1039/c5ra24597d.

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Mesoporous silicates functionalized with amino groups in the pore channels have been made by the co-condensation of tetraethoxyl siloxide (TEOS) with precursors of P–Si through a triblock copolymer-templated sol–gel process under acidic conditions.

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26

Patiparn, P., and S. Takizawa. "Effect of surface functional group on adsorption of organic pollutants on hexagonal mesoporous silicate." Water Supply 6, no. 3 (July 1, 2006): 17–25. http://dx.doi.org/10.2166/ws.2006.742.

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Hexagonal mesoporous silicates (HMSs) are synthetic silicate materials that have uniform mesopores, comparatively large surface areas, and uniform surface functional groups, which lead to higher adsorption selectivity. Selective adsorption characteristics of HMSs for six types of organic pollutants (2,4-d, mecoprop, 4-chlorophenol, toluene, dichloroacetic acid, and thioflavin T) from synthetic wastewater were investigated. Five different types of HMSs were synthesized by surfactant-templating methods, and three of them were subsequently grafted with organic surface functional groups, i,e. n-octyldimethyl-, 3-aminopropyltriethoxy-, and 3-mercaptopropyl-groups. Titanium-substituted HMS was also made in the same way as pristine HMS. Increasing hydrophobicity of HMSs did not always enhance adsorption of hydrophobic adsorbates, such as toluene. Grafted organic functional groups changed surface charge, which enhanced electrostatic force between HMSs and ionic pollutants. Negatively charged contaminants, i.e. 2,4-d, mecoprop and dichloroacetic acid, were more readily adsorbed on positively charged AM-HMS by electrostatic interaction. Hydrogen bonding and van der Waals interaction between adsorbents and adsorbates, as well as combination of these forces, also enhanced the adsorption capacities of HMSs. In addition to the electrostatic interaction, a cationic dye, thioflavin T, was adsorbed on the surfaces due to hydrogen bonding and van der Waals interaction for hydrophilic surfaces and hydrophobic surfaces, respectively.

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27

Ramanathan, Anand, and Bala Subramaniam. "Metal-Incorporated Mesoporous Silicates: Tunable Catalytic Properties and Applications." Molecules 23, no. 2 (January 29, 2018): 263. http://dx.doi.org/10.3390/molecules23020263.

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28

Gao, Xun, Hassnain Asgar, Ivan Kuzmenko, and Greeshma Gadikota. "Architected mesoporous crystalline magnesium silicates with ordered pore structures." Microporous and Mesoporous Materials 327 (November 2021): 111381. http://dx.doi.org/10.1016/j.micromeso.2021.111381.

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29

Urbán, Mónika, Zoltán Kónya, Dóra Méhn, Ji Zhu, and Imre Kiricsi. "Mesoporous silicates as nanoreactors for synthesis of carbon nanotubes." PhysChemComm 5, no. 20 (2002): 138–41. http://dx.doi.org/10.1039/b203767j.

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30

Pai, R. A. "Mesoporous Silicates Prepared Using Preorganized Templates in Supercritical Fluids." Science 303, no. 5657 (January 23, 2004): 507–10. http://dx.doi.org/10.1126/science.1092627.

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31

Nandiwale, Kakasaheb Y., Andrew M. Danby, Anand Ramanathan, Raghunath V. Chaudhari, and Bala Subramaniam. "Zirconium-Incorporated Mesoporous Silicates Show Remarkable Lignin Depolymerization Activity." ACS Sustainable Chemistry & Engineering 5, no. 8 (July 13, 2017): 7155–64. http://dx.doi.org/10.1021/acssuschemeng.7b01344.

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32

Wan, Ying, and Zhao. "On the Controllable Soft-Templating Approach to Mesoporous Silicates." Chemical Reviews 107, no. 7 (July 2007): 2821–60. http://dx.doi.org/10.1021/cr068020s.

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33

Nguyen-Phan, Thuy-Duong, Chae Young Lee, Jin Suk Chung, and Eun Woo Shin. "Adsorption of benzene onto mesoporous silicates modified by titanium." Research on Chemical Intermediates 34, no. 8-9 (August 2008): 743–53. http://dx.doi.org/10.1007/bf03036933.

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34

Kiricsi, I. "Thermal stability of platinum particles embedded in mesoporous silicates." Journal of Thermal Analysis and Calorimetry 79, no. 3 (February 2005): 573–77. http://dx.doi.org/10.1007/s10973-005-0581-1.

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35

Ambrogi, Valeria, Luana Perioli, Fabio Marmottini, Oriana Accorsi, Cinzia Pagano, Maurizio Ricci, and Carlo Rossi. "Role of mesoporous silicates on carbamazepine dissolution rate enhancement." Microporous and Mesoporous Materials 113, no. 1-3 (August 2008): 445–52. http://dx.doi.org/10.1016/j.micromeso.2007.12.003.

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36

KATO, Katsuya, Roxana IRIMESCU, Takao SAITO, Yoshiyuki YOKOGAWA, and Haruo TAKAHASHI. "Catalytic Properties of Lipases Immobilized on Various Mesoporous Silicates." Bioscience, Biotechnology, and Biochemistry 67, no. 1 (January 2003): 203–6. http://dx.doi.org/10.1271/bbb.67.203.

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37

Sepehrian, Hamid, Syed Waqif-Husain, Javad Fasihi, and Mohamad Khayatzadeh Mahani. "Adsorption Behavior of Molybdenum on Modified Mesoporous Zirconium Silicates." Separation Science and Technology 45, no. 3 (February 19, 2010): 421–26. http://dx.doi.org/10.1080/01496390903423519.

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38

Deere, J., E. Magner, J. G. Wall, and B. K. Hodnett. "Adsorption and activity of cytochrome c on mesoporous silicates." Chemical Communications, no. 5 (2001): 465. http://dx.doi.org/10.1039/b009478l.

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39

Sayari, Abdelhamid, Michal Kruk, Mietek Jaroniec, and Igor L. Moudrakovski. "New Approaches to Pore Size Engineering of Mesoporous Silicates." Advanced Materials 10, no. 16 (November 1998): 1376–79. http://dx.doi.org/10.1002/(sici)1521-4095(199811)10:16<1376::aid-adma1376>3.0.co;2-b.

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40

Kimura, Tatsuo, and Kazuyuki Kuroda. "ChemInform Abstract: Ordered Mesoporous Silica Derived from Layered Silicates." ChemInform 41, no. 11 (February 19, 2010): no. http://dx.doi.org/10.1002/chin.201011212.

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41

Shin, E. W., H. S. Choi, T. D. Nguyen-Phan, J. S. Chung, and E. J. Kim. "Interaction of Pb2+ ions with surfactant-containing mesoporous silicates." Journal of Industrial and Engineering Chemistry 14, no. 4 (July 2008): 510–14. http://dx.doi.org/10.1016/j.jiec.2008.01.015.

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42

Goto, Yasutomo, Yoshiaki Fukushima, Yoshihiro Kubota, and Yoshihiro Sugi. "Mesoporous materials from leached calcium silicates with hollow structure." Journal of Porous Materials 13, no. 2 (April 2006): 147–52. http://dx.doi.org/10.1007/s10934-006-7018-5.

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43

Okamura, Junji, Satoru Nishiyama, Shigeru Tsuruya, and Mitsuo Masai. "Formation of Cu-supported mesoporous silicates and aluminosilicates and liquid-phase oxidation of benzene catalyzed by the Cu-mesoporous silicates and aluminosilicates." Journal of Molecular Catalysis A: Chemical 135, no. 2 (October 1998): 133–42. http://dx.doi.org/10.1016/s1381-1169(97)00298-7.

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44

Alam, Nurul, and Robert Mokaya. "Strongly acidic mesoporous aluminosilicates prepared via hydrothermal restructuring of a crystalline layered silicate." Journal of Materials Chemistry A 3, no. 15 (2015): 7799–809. http://dx.doi.org/10.1039/c5ta00548e.

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45

Figueras, François, Hafedh Kochkar, and Stefano Caldarelli. "Crystallization of hydrophobic mesoporous titano-silicates useful as epoxidation catalysts." Microporous and Mesoporous Materials 39, no. 1-2 (September 2000): 249–56. http://dx.doi.org/10.1016/s1387-1811(00)00200-6.

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46

Urbán, Mónika, Dóra Méhn, Zoltán Kónya, and Imre Kiricsi. "Production of carbon nanotubes inside the pores of mesoporous silicates." Chemical Physics Letters 359, no. 1-2 (June 2002): 95–100. http://dx.doi.org/10.1016/s0009-2614(02)00656-5.

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47

Imran, Gaffar, and Rajamanickam Maheswari. "Mn-incorporated SBA-1 cubic mesoporous silicates: Synthesis and characterization." Materials Chemistry and Physics 161 (July 2015): 237–42. http://dx.doi.org/10.1016/j.matchemphys.2015.05.043.

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48

Qian, H., P. Li, M. Malac, H. Yang, S. Mutyala, H. Furukawa, and M. Kawasaki. "Methods for location of palladium catalyst nanoparticles in mesoporous silicates." Microscopy and Microanalysis 14, S2 (August 2008): 180–81. http://dx.doi.org/10.1017/s1431927608084110.

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49

Parvulescu, V., L. Buhoci, G. Roman, B. Albu, and G. Popescu. "Composite membranes with micro- or mesoporous silicates and organic polymers." Separation and Purification Technology 25, no. 1-3 (October 2001): 25–32. http://dx.doi.org/10.1016/s1383-5866(01)00087-9.

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50

Batista, Luciano N., Thiago L. Vasconcelos, Carlos A. Senna, Braúlio S. Archanjo, Eduardo Miguez, Rosane A S San Gil, and Maria Inês B. Tavares. "Impact of nanoconfinement on acetylacetone Equilibria in Ordered Mesoporous Silicates." Nanotechnology 31, no. 35 (June 17, 2020): 355706. http://dx.doi.org/10.1088/1361-6528/ab94db.

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