Dissertations / Theses on the topic 'Materials Testing System'
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Dekany, Justin. "Cryostat System for Spacecraft Materials Testing." DigitalCommons@USU, 2016. https://digitalcommons.usu.edu/etd/5014.
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The main cause of spacecraft failures is due to the harsh space environment; therefore, rigorous testing of materials used in modern spacecraft is imperative to ensure proper operation during the life span of the mission. Enhancing the capabilities of ground-based test facilities allows for more accurate measurements to be taken as it better simulates the environment to which spacecraft will be exposed. The range of temperature measurements has been significantly extended for an existing space environment simulation test chamber used in the study of electron emission, sample charging and discharge, electrostatic discharge and arcing, electron transport, and luminescence of spacecraft materials. This was accomplished by incorporating a new two-stage, closed-cycle helium cryostat, which has an extended sample temperature range from 450 K, with long-term controlled stability of -7Pa) that can simulate diverse space environments. These existing capabilities include controllable vacuum and ambient neutral gases conditions (< 10-7 to 10-1 Pa), electron fluxes (5 eV to 30 KeV monoenergetic, focused, pulsed sources ranging from 10-4 to 1010 nA-cm-2), ion fluxes (<0.1 to 5keV monoenergetic sources for inert and reactive gases with pulsing capabilities), and photon irradiation (numerous continuous and pulsed monochromatic and broadband IR/VIS/UV [0.5 to 7 eV] sources). The original sample mount accommodates one to four samples of 1 cm to 2.5 cm diameter in a low-temperature carousel, which allows rapid sample exchange and controlled exposure of the individual samples. Multiple additional sample mounts have been added to allow for standalone use for constant voltage measurements, radiation induced and conductivity tests, as well as extended capabilities for electron-induced luminescent measurements to be conducted using various material sample thickness in the original existing space environment simulation test chamber.
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Hussain, Hyder. "Torsion fatigue system for mechanical characterization of materials." Ohio : Ohio University, 2000. http://www.ohiolink.edu/etd/view.cgi?ohiou1172002877.
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Brown, Andrew M. "Design, construction and analysis of a chaotic vibratory system." Thesis, Georgia Institute of Technology, 1985. http://hdl.handle.net/1853/18172.
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Stahlberg, Martin. "Acoustic monitoring and control system to determine the properties of damping materials." Thesis, Nelson Mandela Metropolitan University, 2012.
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Experience shows that the noise and sound quality in vehicles are often a recurring criticism. The bodies of modern vehicles consist predominantly of thin sheets of metal. It is hard to prevent the excitation of bending vibrations and the subsequent emission of disturbing noise while driving. The noise spectrum in a car that can be heard by the driver is from ”latent roar” to ”chattering” noise of the body and engine. In automotive vehicles damped materials, especially plastics or materials made from sheet metal and surface damping treatments, are used. Those have high internal energy losses and damp sound oscillatory systems found in the body or interior of cars. A further advantage of such treated components is that they are applied to existing components working over wide temperature and frequency ranges. Many companies provide such ”sound-absorbing compounds”. The requirements for these damping materials are high temperature-resistance, water repellence, fuel and oil-resistance and good adhesion to the base material [17]. The acoustic properties, especially the damping of the plate vibrations through rubber are of interest. the question arises how can the damping coeficient of coated metal sheets can be measured and secondly, by how much the road noise is reduced when built-in sheets are coated with a known damped material. With the Oberst Bar Test Method (named after Dr. H. Oberst) the properties are determined of the internal damping materials that can be used to simulate mechanical constructions to determine damping of larger surfaces. This method describes a laboratory test procedure for measuring the mechanical properties of damped materials. A block diagram of the test system consisting of a damped material bonded to a vibrating cantilever steel bar is shown in figure 2.1. This method is useful for testing materials such as metals, enamels, ceramics, rubbers, plastics, reinforced epoxy matrices and wood. In addition to damping measurement, the test allows for the determination of the Young’s modulus E of the material. E is calculated from the resonance frequency of a given mode and from the physical constants of the bar. By associating the damping factor with the Young’s modulus, a complex quantity is defined which is called the Complex Modulus of Elasticity. Measurements of dynamic mechanical properties are also useful in the research on the molecular structure of materials.
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Srinivaas, Sujith. "Testing and Analysis of Innovative High-Speed Automotive Fastening System for Multi Materials." The Ohio State University, 2020. http://rave.ohiolink.edu/etdc/view?acc_num=osu1587397193415362.
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Bettinger, David Darwin. "Microprocessor-based system for the detection and characterization of acoustic emissions for materials testing." Thesis, This resource online, 1992. http://scholar.lib.vt.edu/theses/available/etd-09192009-040239/.
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de, Vaulx Thomas. "Determination of the first damage criterion of a glass/epoxy composite material using an in-situ test system." Thesis, Georgia Institute of Technology, 1999. http://hdl.handle.net/1853/17608.
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Mohammedshah, Juzer Mohsin. "System identification of adaptive composites." Thesis, Virginia Tech, 1990. http://hdl.handle.net/10919/41935.
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de, Caussin Dylan Robert. "Design and Testing of a Top Mask Projection Ceramic Stereolithography System for Ceramic Part Manufacturing." DigitalCommons@CalPoly, 2016. https://digitalcommons.calpoly.edu/theses/1625.
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Ceramic manufacturing is an expensive process with long lead times between
the initial design and final manufactured part. This limits the use of ceramic as a viable material unless there is a large project budget or high production volume associated with the part. Ceramic stereolithography is an alternative to producing low cost parts through the mixing of a photo curable resin and ceramic particles. This is an additive manufacturing process in which each layer is built upon the previous to produce a green body that can be sintered for a fully dense ceramic part.
This thesis introduces a new approach to ceramic stereolithography with a top mask projection light source which is much more economical compared to current vector scanning methods. The research goes through the design and development of a stereolithography printer prototype capable of handling ceramics and the testing of different mixtures to provide the best printing results with varying viscosities. The initial testing of this printer has created a starting point for top mask projection as an economical alternative to current ceramic manufacturing techniques.
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Couval, Romain. "Scale up of a test fluid for testing the fuel system robustness against soft particles in biodiesels." Thesis, Luleå tekniska universitet, Institutionen för teknikvetenskap och matematik, 2021. http://urn.kb.se/resolve?urn=urn:nbn:se:ltu:diva-85745.
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The future of fuels will most probably be a mixture of different fuels, called drop-in fuels. It is already known that these drop-in fuels will lead to solubility issues, with creation of deposit on crucial fuel system parts, due to the formation of soft particles. The fuel system of the future should be robust against any type of soft particles. Today, there is no scaled up test fluid existing for testing full scale fuel systems. The objective of this thesis was to develop a scaled up test fluid which is a key element to the development of a test method to enhance the fuel system robustness against soft particles. A test fluid was achieved by a concentrate of calcium soap diluted two thousand times to reach a volume of 1000 litres with a concentration of 1,4 ppm. The concentration was measured by gas chromatography mass spectroscopy method following a derivatisation as sample preparation. The formation of the concentrate was established by changing the type of fuel, the level of aging, the amount of calcium and other counterions and eventually by addition of third elements. The concentrate was made of aged B100, calcium oxide powder and water. The test fluid was made by diluting the concentrate with fresh B7 and a protocol to characterise the stability of this test fluid was developed. This test fluid was tested under real condition in a filter rig giving homogeneous concentration all along the experiment, which confirmed the stability of the test fluid.
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Esmaeeli, Roja. "DIRECT TESTING OF TIRE TREAD COMPOUNDS AT HIGH FREQUENCIES USING A NEWLY DEVELOPED DYNAMIC MECHANICAL ANALYSIS (DMA) SYSTEM." University of Akron / OhioLINK, 2020. http://rave.ohiolink.edu/etdc/view?acc_num=akron1591741751909052.
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Johnson, Jason R. "Developing the Axisymmetric Expanding Ring: A High Strain-Rate Materials Characterization Test." The Ohio State University, 2014. http://rave.ohiolink.edu/etdc/view?acc_num=osu1387807565.
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Bulnes, Kevin, Diego Paredes, and Leonardo Vinces. "An Automatic Biodiesel Decanting System for the Optimization of Glycerin Separation Time by Applying Electric Field and Temperature." Universidad Peruana de Ciencias Aplicadas (UPC), 2021. http://hdl.handle.net/10757/653784.
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El texto completo de este trabajo no está disponible en el Repositorio Académico UPC por restricciones de la casa editorial donde ha sido publicado.During biodiesel production, crude biodiesel and glycerin are separated in resting tanks due to gravity and differences in density, glycerin accumulates at the base of the contender; such operation is called decantation. The decantation stage, within the production of biodiesel based on recycled oil, takes from 8 to 24 h to complete. Therefore, the development of an automatic biodiesel decanting system is presented in order to optimize the production time in the line of this bio-fuel. The process consists of applying an electric field through two electrodes at 9 kV and simultaneously applying temperature. The results of the implementation showed that the production time was reduced by up to 99% without affecting the quality of biodiesel, according to the parameters of the American Society for Testing and Materials (ASTM).
Revisión por pares
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Gurav, Neelam. "Biocompatibility testing of resorbable materials using improved in-vitro techniques." Thesis, University College London (University of London), 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.286360.
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Zhang, Peihong. "Amplitude correction for reduced axis scanning of layered materials." Access citation, abstract and download form; downloadable file 5.49 Mb, 2004. http://wwwlib.umi.com/dissertations/fullcit/3131705.
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Martin, Allen. "Cooking system interactions: compatibility of energy source and container material." Thesis, Virginia Tech, 1988. http://hdl.handle.net/10919/45903.
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A laboratory experiment was performed to investigate the interaction between container material and energy source. The energy sources used include: conventional electric coil, gas flame, induction, solid element, and electric resistance coil under glass-ceramic. The container materials investigated include: thin gauge aluminum, heavy gauge aluminum, glass-ceramic, thin gauge porcelain-on-steel, and heavy gauge stainless steel with thick aluminum heat core. Crepes were prepared to determine the browning pattern for each cooking system (combination of energy source and container material). Water was used as a test medium for both speed of heating and retained heat tests. Duncan Multiple Range Tests were performed to determine significant differences between systems, and a General Linear Models Procedure was used to assess the contribution made by each variable on variances between systems.
When speed of heating, and retained heat are desired, the important variable was the cooktop. The induction, gas flame, and conventional electric coil boiled water more quickly, and the solid element and the electric resistance coil under glass-ceramic retained the most heat. When even browning is desired, the choice of cookware is important. Heavy gauge aluminum and heavy gauge stainless steel with a thick aluminum heat core produced the most even browning. Systems that performed all tests well include the conventional electric coil paired with heavy gauge aluminum or heavy gauge stainless steel with thick aluminum heat core cookware.
Master of Science
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Neelakantan, Vijay. "Modeling, design, testing and control of a two-stage actuation mechanism using piezoelectric actuators for automotive applications." The Ohio State University, 2005. http://rave.ohiolink.edu/etdc/view?acc_num=osu1127236489.
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LI, BO. "UV-LIGA COMPATIBLE ELECTROFORMED NANO-STRUCTURED MATERIALS FOR MICRO MECHANICAL SYSTEMS." Doctoral diss., University of Central Florida, 2005. http://digital.library.ucf.edu/cdm/ref/collection/ETD/id/2269.
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UV-LIGA is a microfabrication process realzed by material deposition through microfabricated molds. UV photolithography is conducted to pattern precise thick micro molds using UV light sensitive materials, mostly SU-8, and electroforming is performed to fabricate micro metallic structures defined by the micro molds. Therefore, UV-LIGA is a bottom-up in situ material-addition process. UV-LIGA has received broad attention recently than LIGA – a micro molding fabrication process using X-ray to pattern the micro molds. LIGA is an expansive and is limited in access. In comparing to LIGA, the UV-LIGA is a cost effective process, and is widely accessible and safe. Therefore, it has been extensively used for the fabrication of metallic micro-electro-mechanical-systems (MEMS). The motivation of this research was to study micro mechanical systems fabricated with nano-structured metallic materials via UV-LIGA process. Various micro mechanical systems with high-aspect-ratio and thick metallic structures have been developed and are presented in this desertation. A novel micro mechanical valve has been developed with nano-structured nickel realized with UV-LIGA fabrication technique. Robust compact valves are crucial for space applications where payload and rubstaness are critically concerned. Two types of large flow rate robust passive micro check valve arrays have been designed, fabricated and tested for robust hydraulic actuators. The first such micro valve developed employs nanostructured nickel as the valve flap and single-crystal silicon as the substrates to house inlet and outlet channels. The Nano-structured nickel valve flap was fabricated using the UV-LIGA process developed and the microchannels were fabricated by deep reactive etching (DRIE) method. The valves were designed to operate under a high pressure (>10MPa), able to operate at high frequencies (>10kHz) in cooperating with the PZT actuator to produce large flow rates (>10 cc/s). The fabricated microvalves weigh 0.2 gram, after packing with a novel designated valve stopper. The tested results showed that the micro valve was able to operate at up to 14kHz. This is a great difference in comparison to traditional mechanical valves whose operations are limited to 500 Hz or less. The advantages of micro machined valves attribute to the scaling laws. The second type of micro mechanical valves developed is a in situ assembled solid metallic (nickel) valves. Both the valve substrates for inlet and outlet channels and the valve flap, as well as the valve stopper were made by nickel through a UV-LIGA fabrication process developed. Continuous multiple micro molds fabrication and molding processes were performed. Final micro mechanical valves were received after removing the micro molds used to define the strutures. There is no any additional machining process, such as cutting or packaging. The alignment for laminated fabrication was realized under microscope, therefore it is a highly precise in situ fabrication process. Testing results show the valve has a forward flow rate of19 cc/s under a pressure difference of 90 psi. The backward flow rate of 0.023 cc/s, which is negligible (0.13%). Nano-structured nickel has also been used to develop laminated (sandwiched) micro cryogenic heater exchanger with the UV-LIGA process. Even though nickel is apparently not a good thermal conductor at room temperature, it is a good conductor at cryogentic temerpature since its thermal conductivity increases to 1250 W/k·m at 77K. Micro patterned SU-8 molds and electroformed nickel have been developed to realize the sandwiched heat exchanger. The SU-8 mold (200mm x 200mm x50mm) array was successfully removed after completing the nickel electroforming. The second layer of patterned SU-8 layer (200mm x 200mm x50mm, as a thermal insulating layer) was patterned and aligned on the top of the electroformed nickel structure to form the laminated (sandwiched) micro heat exchanger. The fabricated sandwiched structure can withstand cryogenic temperature (77K) without any damages (cracks or delaminations). A study on nanocomposite for micro mechanical systems using UV-LIGA compatible electroforming process has been performed. Single-walled carbon nanotubes (SWNTs) have been proven excellent mechanical properties and thermal conductive properties, such as high strength and elastic modulus, negative coefficient of thermal expansion (CTE) and a high thermal conductivity. These properties make SWNT an excellent reinforcement in nanocomposite for various applications. However, there has been a challenge of utilizing SWNTs for engineering applications due to difficulties in quality control and handling – too small (1-2nm in diameter). A novel copper/SWNT nanocomposite has been developed during this dissertational research. The goal of this research was to develop a heat spreader for high power electronics (HPE). Semiconductors for HPE, such as AlGaN/GaN high electron mobility transistors grown on SiC dies have a typical CTE about 4~6x10-6/k while most metallic heat spreaders such as copper have a CTE of more than 10x10-6/k. The SWNTs were successfully dispersed in the copper matrix to form the SWNT/Cu nano composite. The tested composite density is about 7.54 g/cm3, which indicating the SWNT volumetric fraction of 18%. SEM pictures show copper univformly coated on SWNT (worm-shaped structure). The measured CTE of the nanocomposite is 4.7 x 10-6/°C, perfectly matching that of SiC die (3.8 x 10-6/°C). The thermal conductivity derived by Wiedemann-Franz law after measuring composit's electrical conductivity, is 588 W/m-K, which is 40% better than that of pure copper. These properties are extremely important for the heat spreader/exchanger to remove the heat from HPE devices (SiC dies). Meanwhile, the matched CTE will reduce the resulted stress in the interface to prevent delaminations. Therefore, the naocomposite developed will be an excellent replacement material for the CuMo currently used in high power radar, and other HPE devices under developing. The mechanical performance and reliability of micro mechanical devices are critical for their application. In order to validate the design & simulation results, a direct (tensile) test method was developed to test the mechanical properties of the materials involved in this research, including nickel and SU-8. Micro machined specimens were fabricated and tested on a MTS Tytron Micro Force Tester with specially designed gripers. The tested fracture strength of nanostructured nickel is 900±70 MPa and of 50MPa for SU-8, resepctively which are much higher than published values.Ph.D.
Department of Mechanical, Materials and Aerospace Engineering;
Engineering and Computer Science
Mechanical Engineering
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İnce, Umut Güden Mustafa. "A case study of material testing for corrosion in low temperature geothermal systems/." [s.l.]: [s.n.], 2005. http://library.iyte.edu.tr/tezler/master/malzemebilimivemuh/T000387.pdf.
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Yilmaz, Tuba. "Characterization of tissue mimicking materials for testing of implantable and on body antennas." Master's thesis, Mississippi State : Mississippi State University, 2009. http://library.msstate.edu/etd/show.asp?etd=etd-05282009-120047.
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Lansing, Eric. "Verification of Polymeric Material Change in the Air Intake System." Thesis, KTH, Skolan för kemivetenskap (CHE), 2017. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-213012.
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The air intake manifold is an integral part of modern internal combustion engines. Currently manufactured in glass fibre reinforced PA66, inquiries have been raised regarding a change of material to glass fibre reinforced PP. A new engine project is the purpose for which this proposed material is evaluated. The thermochemical environment in the air intake system puts high demands on the material. Ageing treatments and tensile testing was conducted on samples of the new material, as well as on the currently used PA66 to evaluate mechanical response of each material to treatments made to simulate the air intake environment. Furthermore, understanding of the chemical setup is lacking and needs to be studied. Experiments was performed to study the chemistry of the intake environment. Results indicated that PP can retain sufficient mechanical rigidity and strength when subjected to parameters made to simulate the air intake. Moreover, results regarding the chemical environment in the air intake system provided limited information.
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Zhao, Lei. "Bench scale apparatus measurement uncertainty and uncertainty effects on measurement of fire characteristics of material systems." Link to electronic thesis, 2005. http://www.wpi.edu/Pubs/ETD/Available/etd-050105-182456/.
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Teh, Kuen Tat. "Impact damage resistance and tolerance of advanced composite material systems." Diss., This resource online, 1993. http://scholar.lib.vt.edu/theses/available/etd-06062008-170512/.
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Li, S. "Experimental testing and numerical investigation of materials with embedded systems during indentation and complex loading conditions." Thesis, Liverpool John Moores University, 2018. http://researchonline.ljmu.ac.uk/8981/.
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In this work, parametric FE (Finite Element) modelling has been developed and used to study the deformation of soft materials with different embedded systems under indentation and more complex conditions. The deformation of a soft material with an embedded stiffer layer under cylindrical flat indenter was investigated through FE modelling. A practical approach in modelling embedded system is evaluated and presented. The FE results are correlated with an analytical solution for homogenous materials and results from a mathematical approach for embedded systems in a half space. The influence of auxeticity on the indentation stiffness ratio and the de-formation of the embedded system under different conditions (indenter size, thickness and embedment depth of the embedded layer) was established and key mechanisms of the Poisson’s ratio effect are highlighted. The results show that the auxeticity of the matrix has a direct influence on the indentation stiffness of the system with an embedded layer. The enhancement of indentation resistance due to embedment increases, as the matrix Poisson’s ratio is decreased to zero and to negative values. The indentation stiffness could be increased by over 30% with a thin inextensible shell on top of a negative Poisson’s ratio matrix. The deformation of the embedded layer is found to be significantly influenced by the auxeticity of the matrix. Selected case studies show that the modelling approach developed is effective in simulating piezoelectrical sensors, and force sensitive resistor, as well as investigating the deformation and embedded auxetic meshes. A full scale parametric FE foot model is developed to simulate the deformation of the human foot under different conditions including soles with embedded shells and negative Poisson’s ratio. The models used a full bone structure and effective embedded structure method to increase the modelling efficiency. A hexahedral dominated meshing scheme was applied on the surface of the foot bones and skin. An explicit solver (Abaqus/Explicit) was used to simulate the transient landing process. Navicular drop tests have been performed and the displacement of the Navicular bone is measured using a 3D image analysing system. The experimental results show a good agreement with the numerical models and published data. The detailed deformation of the Navicular bone and factors affecting the Navicular bone displacement and measurement is discussed. The stress level and rate of stress increase in the Metatarsals and the injury risk in the foot between forefoot strike (FS) and rearfoot (RS) is evaluated and discussed. A detailed full parametric FE foot model is developed and validated. The deformation and internal energy of the foot and stresses in the metatarsals are comparatively investigated. The results for forefoot strike tests showed an overall higher average stress level in the metatarsals during the entire landing cycle than that for rearfoot strike. The increased rate of the metatarsal stress from the 0.5 body weight (BW) to 2 BW load point is 30.76% for forefoot strike and 21.39% for rearfoot strike. The maximum rate of stress increase among the five metatarsals is observed on the 1st metatarsal in both landing modes. The results indicate that high stress level during forefoot landing phase may increase potential of metatarsal injuries. The FE was used to evaluate the effect of embedded shell and auxetic materials on the foot-shoe sole interaction influencing both the contact area and the pressure. The work suggests that application of the auxetic matrix with embedded shell can reinforce the indentation resistance without changing the elastic modulus of the material which can optimise the wearing experience as well as providing enough support for wearers. . Potential approaches of using auxetic structures and randomly distributed 2D inclusion embedded in a soft matrix for footwear application is discussed. The design and modelling of foot prosthetic, which resembles the human foot structure with a rigid structure embedded in soft matrix is also presented and discussed.
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McKinnie, Douglas J. "Objective selection of critical material for subjective testing of low bit-rate audio coding systems." Thesis, McGill University, 1996. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=29771.
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Perceptual low bit-rate audio coding schemes cannot be evaluated with the traditional method of measuring the difference between input signal and output signal. A valid measure is the severity of differences between input and output that are audible to human listeners, measurement of which requires well-conducted subjective testing. Test sensitivity is improved through the use of "critical" audio program. Selection of such audio material has in the past been done by subjective listening. An objective method of selecting critical material could offer many advantages, including faster and simpler selection of new materials, the ability to evaluate a much larger number of potential materials, and the potential of much better critical materials as a larger portion of available music is explored. The use of perceptual models for selection of critical materials has been investigated. Prediction of criticality was found to be inadequate with the models used.
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Burger, A. F. "Rheology of polymer modified binders : a comparative study of three binders and three binder/filler systems." Thesis, Stellenbosch : Stellenbosch University, 2001. http://hdl.handle.net/10019.1/52438.
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Thesis (MEng)--University of Stellenbosch, 2001.ENGLISH ABSTRACT: The use of polymer modified binders have increased drastically over the past twenty years. It is generally accepted that current empirical specification tests do not adequately characterise the improvement in binder properties when bitumen is modified with polymers. At the University of Stellenbosch, a programme was initiated to relate binder properties to asphalt mix performance. This study forms part of that programme. This study focuses on three binders and is an attempt to characterise binder properties fundamentally. The binders that were tested are: • 60/70 penetration grade bitumen • SBS modified 60/70 bitumen • Bitumen-Rubber Two rheometers were used to characterise the binder properties: • Sliding Plate Rheometer (SPR) • Dynamic Shear Rheometer (DSR) The Sliding Plate Rheometer was modified to allow testing at elevated temperatures. The modification is described in this thesis. Three types of testing were used to test the binders: • Creep tests (SPR and DSR) • Dynamic tests (Strain and Frequency Sweeps - DSR) • Flow tests (high temperature viscosity tests - DSR) The results of the tests were used to characterise differences between the binders. Shear susceptibility lines were plotted and viscosities calculated from the creep test results; Master Curves and Black Diagrams were plotted from frequency sweep results; flow test results were used to characterise high temperature behaviour. A further development in the asphalt industry is the move towards the development of performance based specifications. A programme has been initiated in this regard and this study forms part of the programme. As a step towards the development of performance based specifications filler was included in this study. BinderlFiller systems were subjected to the same test programme the binders were, to characterise the influence on binder properties of filler addition. Some of the conclusions that were drawn at the end of the study are: • Polymer modification improves binder properties related to rutting. • Filler addition does not affect binder properties negatively. • Shear rate is very important during production of asphalt mixes and construction of asphalt layers containing polymer modified binders.
AFRIKAANSE OPSOMMING: Die gebruik van polimeer gemodifiseerde bitumen het drasties toegeneem oor die afgelope twintig jaar. Dit word algemeen aanvaar dat die huidige empiriese spesifikasie toetse nie die verbetering in bindmiddeleienskappe van polimeer modifisering aanvaarbaar karakteriseer nie. 'n Program is geïnisieer by die Universiteit van Stellenbosch om 'n verband te vind tussen bindmiddeleienskappe en asfaltmengseleienskappe. Hierdie studie vorm deel van die program. Hierdie werk fokus op drie bindmiddels en is 'n poging om die bindmiddeleienskappe fundamenteel te karakteriseer. Die bindmiddels wat gebruik is in hierdie werk, is: • 60/70 penetrasiegraad bitumen • SBS gemodifiseerde 60/70 bittimen • Bitumen-Rubber Twee reometers is gebruik om bindmiddeleienskappe te karakteriseer: • Glyplaat Reometer (SPR) • Dinamiese SkuifReometer (DSR) Die glyplaat reometer is aangepas om toetse by hoër temperature te doen en die aanpassing wat gemaak is word in die tesis beskryf. Drie tipes toetse is uitgevoer om die bindmiddels mee te toets: • Kruiptoetse (SPR en DSR) • Dinamiese toetse (DSR) • Vloei toetse (DSR) Die resultate van die toetse is gebruik om die verksille tussen die bindmiddels te kwalifiseer. Verskillende grafieke en figure is getrek van die resultate om die onderskeie bindmiddels te karakteriseer. Die beweging weg van empmese spesifikasies na werkverrigting gebaseerde spesifikasies in die asfalt industrie is 'n verder nuwe ontwikkeling. 'n Program is geïnisïeer ten opsigte hiervan en hierdie werk vorm deel van die program. As 'n stap in die ontwikkeling van die werkverrigting gebaseerde spesifikasies is 'n vuIler ingesluit in die toetsprogram. Bindmiddel/vuIler stelsels is onderwerp aan dieselfde toetse waaraan die bindmiddels onderwerp is om die invloed van die vuIler op die bindmiddels te karakteriseer. Sommige van die gevolgtrekkings waartoe gekom is aan die einde van die tesis, is: • Polimeer modifisering verbeter bindmiddeleienskappe met betrekking tot wielsporing. • Die toevoeging van vuIler affekteer nie die bindmiddeleienskappe negatiefnie. • Die vervormingstempo is van groot belang wanneer asfaltmengsels gemeng en lae gebou word van mengsels wat polimeer gemodifiseerde bitumen bevat.
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Maniglia, Jeffrey J. Jr. "Design, Fabrication, and Testing of an EMR Based Orbital Debris Impact Testing Platform." DigitalCommons@CalPoly, 2013. https://digitalcommons.calpoly.edu/theses/956.
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This paper describes the changes made from Cal Poly’s initial railgun system, the Mk. 1 railgun, to the Mk. 1.1 system, as well as the design, fabrication, and testing of a newer and larger Mk. 2 railgun system. The Mk. 1.1 system is developed as a more efficient alteration of the original Mk. 1 system, but is found to be defective due to hardware deficiencies and failure, as well as unforeseen efficiency losses. A Mk. 2 system is developed and built around donated hardware from the Naval Postgraduate School. The Mk. 2 system strove to implement an efficient, augmented, electromagnetic railgun and projectile system capable of firing an approximate 1g aluminum projectile to speeds exceeding 2 km/s. A novel three part projectile is proposed to mitigate rail and projectile degradation. Projectile and sabot system kinematic equations are derived and the projectile is designed and tested along with Mk. 2 barrel. A numerical electromechanical model is developed to predict the performance of the Mk. 2 system and projectile assembly, and predicts a final velocity for the fabricated system exceeding 3.5 km/s and an efficiency as high as 24%. Testing of the Mk. 2 system showed catastrophic failure of the projectile during initial acceleration, resulting in very short acceleration times and distance, low velocity projectiles, and low efficiencies. During further testing of various projectile configurations, the barrel structure failed due to a large internal arc. Future work for the Mk. 2 system is discussed, a revised external barrel structure suggested, and a solid, more conventional solid chevron projectile design suggested.
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Speicher, Matthew S. "Cyclic testing and assessment of shape memory alloy recentering systems." Diss., Georgia Institute of Technology, 2009. http://hdl.handle.net/1853/33834.
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In an effort to mitigate damage caused by earthquakes to the built environment, civil engineers have been commissioned to research, design, and build increasingly robust and resilient structural systems. Innovative means to accomplish this task have emerged, such as integrating Shape Memory Alloys (SMAs) into structural systems. SMAs are a unique class of materials that have the ability to spontaneously recover strain of up to 8%. With proper placement in a structural system, SMAs can act as superelastic "structural fuses", absorbing large deformations, dissipating energy, and recentering the structure after a loading event. Though few applications have made it into practice, the potential for widespread use has never been better due to improvements in material behavior and reductions in cost. In this research, three different SMA-based structural applications are developed and tested. The first is a tension/compression damper that utilizes nickel-titanium (NiTi) Belleville washers. The second is a partially restrained beam-column connection utilizing NiTi bars. The third is an articulated quadrilateral bracing system utilizing NiTi wire bundles in parallel with c-shape dampers. Each system was uniquely designed to allow a structure to undergo large drift demands and dissipate energy while retaining strength and recentering ability. This exploratory work highlights the potential for SMA-based structural applications to enhance seismic structural performance and community resilience.
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Cranford, Alexander Davis. "Clinical comparison of two indirect bonding systems on retention rates of orthodontic brackets chemical cured custom base vs. light-cured non-custom base /." Thesis, Birmingham, Ala. : University of Alabama at Birmingham, 2009. https://www.mhsl.uab.edu/dt/2009m/cranford.pdf.
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Caccialupi, Alessandro. "Systems development for high temperature, high strain rate material testing of hard steels for plasticity behavior modeling." Thesis, Available online, Georgia Institute of Technology, 2004:, 2003. http://etd.gatech.edu/theses/available/etd-04082004-180051/unrestricted/caccialupi%5Falessandro%5F200312%5Fms.pdf.
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Hosca, Erhan. "Numerical analyses of the effectiveness of secondary tailgate support systems : a stability approach /." Thesis, This resource online, 1995. http://scholar.lib.vt.edu/theses/available/etd-03042009-040821/.
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Brown, Bryan. "Unmanned Aerial Systems for Emergency Response." University of Cincinnati / OhioLINK, 2016. http://rave.ohiolink.edu/etdc/view?acc_num=ucin1460729457.
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Lizarralde, Jon Mikel. "Non-destructive testing of thin strip material : Implementation of the 3MA technique at a steel producing company." Thesis, Högskolan i Gävle, Avdelningen för bygg- energi- och miljöteknik, 2017. http://urn.kb.se/resolve?urn=urn:nbn:se:hig:diva-24256.
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This study is an initial attempt to investigate the possibility of substituting conventional laboratory destructive testing techniques at Sandvik's strip steel production facilities with the 3MA (Micro-magnetic Multi-parameter Microstructure and Stress Analysis) NDT (nondestructive testing) technique. The interest for the research comes from various problems with the actual destructive testing method. Sandvik manufactures thin strip steel (among other products) and controls the quality of its product by taking samples from the ends of the strip and measuring the sample's material properties in a separate laboratory. Hence, the sample preparation process is time and material consuming, and the results obtained from the laboratory measurements are not always representative of the real values along the whole length of the strip (usually several kilometers). Therefore, the present project involves the correlation between three material properties (Vickers hardness, tensile strength and carbide density) and a selection of micro-magnetic parameters measured with the 3MA-II equipment manufactured by the Fraunhofer IZFP institute. The 3MA-II system is based on four measuring techniques (harmonic analysis, magnetic Barkhausen noise, incremental permeability and Eddy current testing) and is capable of recording up to 41 micro-magnetic parameters. Samples of two different steel grades (composition) were used in the study. The results for hardness and tensile strength (average relative errors of 1.04% and 0.78%, respectively) corroborated the applicability of the 3MA technique to steel strip inspection. Thus, the implementation of this technique would lead to an improvement in the company's energy efficiency and sustainability. However, finding a good correlation between micromagnetic parameters and material properties is not always possible and, in the case of carbide density, no reliable correlation was achieved. So, further experiments are proposed for future studies regarding carbide density and other material properties.
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Song, Peng [Verfasser]. "Influence of material and testing parameters on the lifetime of TBC systems with MCrAlY and NiPtAl bondcoats / Peng Song." Aachen : Hochschulbibliothek der Rheinisch-Westfälischen Technischen Hochschule Aachen, 2012. http://d-nb.info/1020857609/34.
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Lee, Hsing-Juin. "Determination of the complex modulus of a solid propellant and random vibration analysis of the layered viscoelastic cylinders with finite element method." Diss., Virginia Polytechnic Institute and State University, 1987. http://hdl.handle.net/10919/77816.
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Aeronautical structures, such as aircraft or missiles, are usually highly sophisticated systems often subjected to random vibration environment. Thus, in various design, development, and production stages, laboratory random vibration testing of sampled solid rocket motors on electromagnetic or hydraulic shakers are routinely performed as an important experiment-oriented quality control strategy. Nevertheless, it is crucial to understand the dynamic structural behavior of these layered viscoelastic cylinders such as solid rocket motors under random vibration tests analytically.
In this study, a methodology has been developed to deal with the random vibration of a general class of composite structures with frequency-dependent viscoelastic material properties as represented by the example of solid rocket motors. The method combines the finite element method, structural dynamics, strain energy approach, and random vibration analysis concepts. The method is a more powerful technique capable of treating sophisticated random vibration problems with complicated geometry, nonhomogeneous materials, and frequency-dependent stiffness and damping properties.
Before the random vibration analysis could proceed, a microcomputer-based dynamic mechanical analyzer system was used together with time-temperature superposition principle to obtain the frequency-dependent dynamic viscoelastic properties of the solid propellant. The strain energy approach has been used to calculate the frequency-dependent equivalent viscoelastic damping which is in turn judiciously represented by a combination of viscous damping and structural damping to accommodate this frequency dependent material property.
Modal analysis data together with half power band width calculated at each natural frequency are highly useful guides in the harmonic analysis to achieve computational efficiency. On one hand, the technique used in this study has a hybrid taste in the sense that it makes use of best features and capabilities of both modal analysis and harmonic analysis to achieve the goal of random vibration analysis in addition to the power of finite element technique. The displacement, acceleration and stress power spectra have been obtained for significant points on the rocket model together with their root mean square values. These data can be used for various analyses, testing, design, and other purposes as discussed in later sections of this study.Ph. D.
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Silva, Marcos Valério Gebra da 1971. "Determinação das dimensões espaciais de corpos sólidos por técnicas ópticas de moiré." [s.n.], 2011. http://repositorio.unicamp.br/jspui/handle/REPOSIP/256864.
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Orientadores: Inacio Maria Dal Fabbro, Celina de almeidaDissertação (mestrado) - Universidade Estadual de Campinas, Faculdade de Engenharia Agrícola
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Resumo: A medição de sólidos tridimensionais tem recebido uma grande atenção da comunidade científica, devido à sua ampla gama de aplicações. Como por exemplo, no controle de qualidade industrial, na medição do corpo humano para aplicações de ergonomia, e muitas outras áreas. Porém existem diversos métodos e técnicas para se obter tais medições, este trabalho demonstra a técnica de moiré que é uma técnica sem contato e não destrutiva, com um rápido processo de digitalização cujos fenômenos de Franjas de Moiré são o resultado da subtração da projeção de grades sobre um certo objeto com relação as grades projetadas em um plano referencial. Possui medição precisa comparável com a de outros sistemas. Demonstra também a exatidão das técnicas de moiré, sendo dado maior enfoque na técnica de moiré de projeção com deslocamento de fase, e pela utilização de dois tipos de grades a de Ronchi e senoidal, onde são observados os possíveis erros das diversas técnicas de moiré e por outros métodos metrológicos. Neste trabalho foi comprovado o melhor desempenho dos tipos e variação da frequência de grades incluindo vários exemplos práticos da sua aplicação em sólidos regulares e irregulares (frutos), comparação com outras técnicas em vários problemas em engenharia agrícola e determinação volumétrica de sólidos regulares e irregulares. Emprego de "softwares" gratuitos o qual também foi uma preocupação para disseminação da técnica, tais como ImageJ, RisingSun Moiré, SCILAB/SIP e rotinas
Abstract: Measurement of three-dimensional solids has received great attention from the scientific community due to its wide range of applications. As examples in can be mentioned industrial quality control, human body measurement applied to ergonomics and many other areas. The pertinent literature discloses several methods and techniques to carry three dimensional measurements. Moiré technique is a group of non-contact and non-destructive methods based on the more phenomena which fringes are the result of the subtraction of the grid projected onto the surface under study and the grid projected onto a reference plane. Moiré methods are yield accurate measurements if compared to other measuring systems. This work was foccused on the projection moiré technique with phase shift, and the use of two types of grids named Ronchi and sinusoidal one. Metrological errors of various techniques as compared with the moiré method have been determined as well. This work demonstrated the best performance of grid frequency variation through several practical applied to regular and irregular solids (fruits). Body dimensions were compared with convention techniques as water immersion and calypper. The application of free software such as ImageJ, RisingSun Moire, Scilab / SIP and routines was considered very useful to reach the final results
Mestrado
Maquinas Agricolas
Mestre em Engenharia Agrícola
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Wa, Kasongo Kasongo. "An investigation into the feasibility of incorporating didanosine into innovative solid lipid nanocarriers." Thesis, Rhodes University, 2010. http://hdl.handle.net/10962/d1003278.
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The research undertaken in these studies aimed to investigate the feasibility of developing and manufacturing innovative solid lipid carriers, such as solid lipid nanoparticles (SLN) and/or nanostructured lipid carriers (NLC) using a hot high pressure homogenization method, for didanosine(DDI). In addition, studies using in vitro differential protein adsorption were undertaken to establish whether the SLN and/or NLC have the potential to deliver DDI to the central nervous system (CNS). Prior to initiating pre-formulation, formulation development and optimization studies of DDI-Ioaded SLN and/or NLC, it was necessary to develop and validate an analytical method for the in vitro quantitation and analysis of DDI. An accurate, precise and sensitive RP-HPLC method with UV detection set at 248 nm was developed, optimized and validated for the quantitative in vitro analysis of DDI in formulations. Pre-formulation studies were designed to evaluate the thermal stability of DDI and to select and characterize lipid excipients that may be used for the manufacture of the nanocarriers. It was established that DDI is thermostable at temperatures not exceeding 163°C and therefore a hot high pressure homogenization technique could be used to manufacture DDI-loaded SLN and/or NLC. Lipid screening studies revealed that DDI is poorly soluble in both solid and liquid lipids. A combination of Precirol® ATO 5 and Transcutol® HP was found to have the best solubilizing-potential for DDI of all lipids investigated. The inclusion of Transcutol® HP into Precirol® ATO 5 changed the polymorphic form of the solid lipid from the stable 13-modification to a material that exhibited the co-existence between α- and β-polymorphic forms. The relatively high solubility of DDI in Transcutol® HP compared to Precirol® ATO 5 was an indication that a solid lipid matrix prepared from a binary mixture of Precirol® ATO 5 and Transcutol® HP was likely to have a higher loading capacity and encapsulation efficiency for DDI than a matrix consisting of Precirol® ATO 5 alone. Furthermore, the potential for the solid lipid matrix to exist in the α- and/or β-modifications when Transcutol® HP was added to Precirol® ATO 5 suggested that expulsion of DDI from a solid lipid matrix during prolonged storage periods was likely to be minimal. Therefore it was considered logical to investigate the feasibility of incorporating DDI into NLC and not in SLN. However, due to the limited solubility of DDI in lipids, formulation development of DDI-loaded NLC commenced using small quantities of DDI. Formulation development and optimization studies of DDI-loaded NLC were initially aimed at selecting a surfactant system that was capable of stabilizing NLC in an aqueous environment. Solutol® HS alone or a ternary mixture consisting of Solutol® HS, Tween® 80 and Lutrol® F68 was found to stabilize the nanoparticles in terms of particle size and the polydispersity index. The use of the ternary mixture as the surfactant system was preferred to using Solutol® HS alone as Lutrol® F68 and especially Tween® 80 have been successfully used to target the delivery of API to the brain. Aqueous DDI-free and DDI-Ioaded NLC containing increasing amounts of DDI were manufactured using hot high pressure homogenization at 800 bar for three cycles. The NLC formulations were characterized in terms of particle size, polydispersity index, zeta potential, and polymorphism, degree of crystallinity, encapsulation efficiency (EE), shape and surface morphology. The mean particle size for all formulations was below 250 nm with narrow polydispersity indices, indicating that narrow particle size distribution had been achieved. The d99% values for all formulations tested, were generated using laser diffractometry, and were below 400 nm, with span values ranging from 0.84 - 1.19 also suggesting that a narrow particle size distribution had been achieved. The zeta potential values measured in double distilled water with the conductivity adjusted to 50 μS/cm ranged from -18.4 to -11.4 mV. In addition, all the formulations showed a decrease in the degree of crystallinity as compared to the bulk lipid material and WAXS shows that the formulations existed in a single β-modification form. Furthermore DDI that had been incorporated into the NLC appeared to be molecularly dispersed in the lipid matrices. These parameters remained unaffected for most formulations following storage for two months at 25°C. In addition these formulations contained a mixture of spherical and non-spherical particles irrespective of the amount of DDI that was added during the manufacture of the formulations. These studies showed that it was feasible to develop and incorporate small amounts of DDI into NLC. However in order to use these delivery systems for oral administration of DDI to paediatric patients, strategies to improve the amount of DDI that could be loaded into the particles and to achieve high encapsulation efficiencies had to be developed. The limited solubility of DDI in lipid media was identified as a major factor that affected the loading capacity and encapsulation efficiency of DDI in the NLC. Therefore, a novel strategy aimed at increasing the saturation solubility of DDI in the lipid by attempting to increase the dissolution velocity of the drug in the lipid using a particle size reduction approach, was designed and investigated. DDI was dispersed in Transcutol® HP and the particle size of DDI in the liquid lipid medium was reduced gradually using hot high pressure homogenization and the product obtained from these studies was used to manufacture DDI-loaded NLC using a cold high pressure homogenization procedure. Although the encapsulation efficiency and drug loading following use of this approach was relatively high, the particles were large and showed a tendency to grow in size leading to the formation of microparticles after storage for two months at 25°C. In addition, the degree of crystallinity of the nanoparticles increased rapidly over the same storage period which led to expulsion of DDI nanoparticles for the NLC, despite the DDI loading in NLC being unaffected. It was clearly evident that this new approach of manufacturing solid lipid nanocarriers could be used as a platform not only for enhancing the loading capacity of DDI in solid lipid nanocarriers but also for other hydrophilic drugs. Differential protein adsorption patterns of DDI-loaded NLC were generated in vitro using two-dimensional polyacrylamide gel electrophoresis (2-D PAGE) in order to establish the potential for these systems to deliver DDI to the CNS. NLC formulations containing small amounts of DDI were used as these formulations showed a better stability profile than the formulation with a higher encapsulation efficiency and drug loading capacity. Furthermore, the encapsulation efficiency and drug loading of DDI were considered sufficient for use in 2-D PAGE studies. Data obtained from 2-D PAGE analysis reveal that DDI-loaded NLC preferentially adsorb proteins in vitro that are responsible for specific brain targeting in vivo. More importantly, these studies reveal that in addition to Tween® 80 that has already been shown to have the potential to target CDDS to the brain, Solutol® HS 15 has the potential to achieve a similar objective. Consequently, DDI-loaded NLC have the potential to deliver DDI to the brain and these results may be used as a platform for conducting in vivo studies to establish whether DDI can cross the blood brain barrier and enter the CNS when administered in NLC which may in turn lead to a major breakthrough in the management of HIV/AIDS and Aids Dementia Complex (ADC).
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MARQUES, ROGERIO A. "Estudo da resistência à corrosão do aço inoxidável ferrítico AISI 444 para aplicação como biomaterial." reponame:Repositório Institucional do IPEN, 2014. http://repositorio.ipen.br:8080/xmlui/handle/123456789/26397.
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Tese (Doutorado em Tecnologia Nuclear)
IPEN/T
Instituto de Pesquisas Energeticas e Nucleares - IPEN-CNEN/SP
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Pegonen, Reijo. "Development of an Improved Thermal-Hydraulic Modeling of the Jules Horowitz Reactor." Doctoral thesis, KTH, Reaktorteknologi, 2017. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-197712.
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The newest European high performance material testing reactor, the Jules Horowitz Reactor, is under construction at CEA Cadarache research center in France. The reactor will support existing and future nuclear reactor technologies, with the first criticality expected at the end of this decade. The current/reference CEA methodology for simulating the thermalhydraulic behavior of the reactor gives reliable results. The CATHARE2 code simulates the full reactor circuit with a simplified approach for the core. The results of this model are used as boundary conditions in a three-dimensional FLICA4 core simulation. However this procedure needs further improvement and simplification to shorten the computational requirements and give more accurate core level data. The reactor’s high performance (e.g. high neutron fluxes, high power densities) and its design (e.g. narrow flow channels in the core) render the reactor modeling challenging compared to more conventional designs. It is possible via thermal-hydraulic or solely hydraulic Computational Fluid Dynamics (CFD) simulations to achieve a better insight of the flow and thermal aspects of the reactor’s performance. This approach is utilized to assess the initial modeling assumptions and to detect if more accurate modeling is necessary. There were no CFD thermal-hydraulic publications available on the JHR prior to the current PhD thesis project. The improvement process is split into five steps. In the first step, the state-of-the-art CEA methodology for thermal-hydraulic modeling of the reactor using the system code CATHARE2 and the core analysis code FLICA4 is described. In the second and third steps, a CFD thermal-hydraulic simulations of the reactor’s hot fuel element are undertaken with the code STAR-CCM+. Moreover, a conjugate heat transfer analysis is performed for the hot channel. The knowledge of the flow and temperature fields between different channels is important for performing safety analyses and for accurate modeling. In the fourth step, the flow field of the full reactor vessel is investigated by conducting CFD hydraulic simulations in order to identify the mass flow split between the 36 fuel elements and to describe the flow field in the upper and lower plenums. As a side study a thermal-hydraulic calculation, similar to those performed in previous steps is undertaken utilizing the outcome of the hydraulic calculation as an input. The final step culminates by producing an improved, more realistic, purely CATHARE2 based, JHR model, incorporating all the new knowledge acquired from the previous steps. The primary outcome of this four year PhD research project is the improved, more realistic, CATHARE2 model of the JHR with two approaches for the hot fuel element. Furthermore, the project has led to improved thermal-hydraulic knowledge of the complex reactor (including the hot fuel element), with the most prominent findings presented.QC 20161208
DEMO-JHR
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Patabendige, Chami N. K. "Material characterisation, phase transitions, electrochemical properties and possible fuel cell applications of Nd₂₋ₓPrₓCuO₄ and Nd2-x-y LayPrₓCuO₄ systems." Thesis, University of St Andrews, 2012. http://hdl.handle.net/10023/3181.
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The well-known lanthanide cuprates exist in two principal forms, T and T´, which behave as p-type and n-type conductors, respectively. In order to understand the structural properties and crystal chemistry from the T to T´ phase, the Nd₁.₈₋ₓLaₓPr₀.₂CuO₄ (NLPCO) system was studied varying the La substitution ratio (0≤x≤1.8) and then characterised using high temperature X-ray powder diffraction. From analysis of the X-ray diffraction patterns obtained at room temperature, there are clearly five distinguishable regions for the NLPCO system. They are, (1) monophasic T´ solid–solution (2) two phase mixture T´ + T´´ (3) monophasic T´´solid–solution (4) two phase mixture T´´ + O and finally (5) monophasic O phase solid–solution. The T´´ form has previously been suggested as an ordered form of T´; however here we show via high temperature X-ray diffraction studies that it is a non-transformable metastable phase formed on quenching of the T phase via an orthorhombically distorted variant. Also neutron diffraction and selected area electron diffraction (SAED) studies confirmed that the T ´´phase is 4- fold Cu coordinated. The structural, magnetic and electrical properties of this NLPCO series have been investigated for the selected compositions using X-ray diffraction, magnetization measurements, thermal analysis and conductivity measurements. The aim of the second half of this work was to discover the basic high temperature electrical characteristics of Nd₂₋ₓPrₓCuO₄ and investigate how this matches with those required for components on the SOFC cathode side to identify which dopant level shows highest conductivity and whether it is stable at different temperatures. The idea was to make a new concept in SOFC cathodes and current collector development, using n-type conductors instead of p- type conductors and to try to produce a high conductivity material which is stable under the chemical and thermal stresses that exist while under load that can be used in cathode or current collector applications. The Nd₂₋ₓPrₓCuO₄ (NPCO) series has been studied over a range of dopant levels (x=0.15 - 0.25) and maximum conductivity of 86.7 Scm⁻¹ has been obtained for the composition where x = 0.25. Also NPCO shows n-type semiconductor behaviour which gives operational advantages when operating at mild oxygen deficiency. AC impedance studies have been carried out on symmetrical cells to investigate the performance of NPCO as a cathode material. These studies mainly focused on polarization resistance and the activation energies of the cells. Low Rp values and low activation energies are obtained for a composite cathode compared to pure cathode material. Two configurations of NPCO as cathode materials were tested, pre-fired and in-siu fired. Pre-fired NPCO exhibited better performance than in-situ fired NPCO. Both in-situ and pre-fired current collecting NPCO still showed lowest activation energies which suggest good catalytic activity. From all of these studies, it is evident that the praseodymium doped neodymium cuprate material shows considerable promise as a potential cathode material for solid oxide fuel cell applications.
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Farjoud, Alireza. "Physics-based Modeling Techniques for Analysis and Design of Advanced Suspension Systems with Experimental Validation." Diss., Virginia Tech, 2011. http://hdl.handle.net/10919/77354.
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This research undertakes the problem of vibration control of vehicular and structural systems using intelligent materials and controllable devices. Advanced modeling tools validated with experimental test data are developed to help with understanding the fundamentals as well as advanced and novel applications of smart and conventional suspension systems.
The project can be divided into two major parts. The first part is focused on development of novel smart suspensions using Magneto-Rheological (MR) fluids in unique configurations in order to improve efficiency, controllability, and safety of today's vehicles. In this part of the research, attention is paid to fundamentals as well as advanced applications of MR technology. Extensive rheological studies, both theoretical and experimental, are performed to understand the basic behaviors of MR fluids as complex non-Newtonian fluids in novel applications. Using the knowledge obtained from fundamental studies of MR fluids, unique application concepts are investigated that lead to design, development, and experimental testing of two new classes of smart devices: MR Hybrid Dampers and MR Squeeze Mounts. Multiple generations of these devices are built and tested as proof of concept prototypes. Advanced physics-based mathematical models are developed for these devices. Experimental test data are used to validate the models and great agreement is obtained. The models are used as design tools at preliminary as well as detailed design stages of device development. The significant finding in this part of the research is that MR fluids can deliver a much larger window of controllable force in squeeze mode compared to shear and valve modes which can be used in various applications.
The second part of the research is devoted to the development of innovative design tools for suspension design and tuning. Various components of suspension systems are studied and modeled using a new physics-based modeling approach. The component of main interest is the shim stack assembly in hydraulic dampers which is modeled using energy and variational methods. A major finding is that the shims should be modeled individually in order to represent the sliding effects properly when the shim stack is deflected. Next, the individual component models are integrated into a full suspension model. This model is then used as a tool for suspension design, synthesis, and tuning. Using this design tool, suspension engineers in manufacturing companies and other industrial sections can easily perform parametric studies without the need to carry out time consuming and expensive field and laboratory tests.Ph. D.
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Hobdell, Stephen Barry. "Thermally stimulated current and electrokinetic investigations of HV cable models." Thesis, Bangor University, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.311421.
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Snyder, Nicholas B. "DESIGN, VALIDATION, AND VERIFICATION OF THE CAL POLY EDUCATIONAL CUBESAT KIT STRUCTURE." DigitalCommons@CalPoly, 2020. https://digitalcommons.calpoly.edu/theses/2148.
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In this thesis, the development of a structure for use in an educational CubeSat kit is explored. The potential uses of this kit include augmenting existing curricula with aspects of hands on learning, developing new ways of training students on proper space systems engineering practices, and overall contributing to academic capacity building at Cal Poly and its collaborators. The design improves on existing CubeSat kit structures by increasing accessibility to internal components by implementing a modular backplane system, as well as adding the ability to be environmentally tested. Manufacturing of the structure is completed with both additive (Fused Deposition Modeling with ABS polymer and Selective Laser Melting with AlSi10Mg metal) and subtractive (milling with Al-6061) technologies. Modal, harmonic, and random vibration analyses and tests are done to ensure the structure passes vibration testing qualification loads, as outlined by the National Aeronautics and Space Administration’s General Environmental Standards. Successful testing of the structure, defined as deforming less than 0.5 millimeters and maintaining a factor of safety above 2, is achieved with all materials of interest. Thus, the structure becomes the first publicly available CubeSat kit designed to survive environmental testing. Achieving this goal with a structure made of the cheap, widely available material ABS showcases the potential usability of 3D-printed polymers in CubeSat structures.
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Twagirimana, Emmanuel. "Evaluation of adhesion properties in bitumen-aggregate systems for winter surfacing seals using the bitumen bond strength test." Thesis, Stellenbosch : Stellenbosch University, 2014. http://hdl.handle.net/10019.1/95953.
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Thesis (MEng)--Stellenbosch University, 2014.ENGLISH ABSTRACT: Flexible pavement designers have a choice of two wearing course: either asphalt concrete or surfacing seals. The latter have been widely used by several countries as their preferred wearing course over other methods, especially countries with a limited number of average inhabitants per square kilometre. Moreover, the surfacing seals were identified as an efficient cost effective road preventive maintenance technique. Surfacing seals in New Zealand, South Africa and Australia cover about 65%, 80% and 90% of their surfaced road networks respectively. The preference of surfacing seals is due to their competitive initial cost and ease of construction. In South Africa, the life expectancy of surfacing seals varies between 8 and 12 years with an average of 10 years. This has not been the case in a number of surfacing seals constructed in winter, especially when the night recorded temperature is below 10oC. The dominant failure mechanism is ravelling (chip loss) soon after construction due to traffic loading. This chip loss is linked to the poor adhesion bond development rate in the bitumen-aggregate system during winter adverse conditions. In order to address the issue of premature chip loss the need for the development of a robust adhesion test method was identified. For that purpose, recently, researchers in the bitumen industry developed the Bitumen Bond Strength test method. This method was used in this study. This study intends to contribute to the understanding of binder-aggregate adhesion bond development for winter surfacing seals using the BBS test. Binder type, precoat type and conditioning, aggregate type and curing time are amongst the factors influencing winter seals adhesion bond performance. An experimental matrix involving three types of binder, two types of aggregate, four different precoating fluids, two precoat conditionings and two binder-curing times were then developed and investigated. Winter weather parameters affecting adhesion properties were also taken into consideration during the course of the investigation. Throughout the test, the procedure described in AASHTO TP 91-11 was followed. However, in order to enhance the control of the binder application temperature, a new method for hot applied binder sample preparation was developed as part of this study. The findings show that there is a significant difference between adhesion properties of the hot applied binders (70/100 and S-E1) and the emulsion (SC-E1). In most of the cases, the hot applied binders performed better than the emulsion. The failure mode observed was found to be linked to the condition of the precoating. The influence of the precoat type and conditioning, and effect of binder curing time were significantly highlighted. The use of a dry precoat benefited the adhesion bond strength up to around 50% relatively to the corresponding non-precoated combination. However, a decrement in the bond strength due to precoating of up to 28.7% was also observed. A statistical analysis using ANOVA did not illustrate any statistical significant effect of the aggregate type. The interaction effects analysis using ANOVA revealed the aggregate type interacting with precoat type to be the most influential interaction at level two. The precoat conditioning implication to the adhesion development rate, which influences the time for opening to traffic after construction, was illustrated. Insightful aspects on the compatibility between the binder type and precoat type and conditioning during the aggregate precoating practices and on the time for opening to traffic are highlighted. Finally, the repeatability analysis proved the BBS test to be a repeatable testing method with caution. Recommendations for further studies that could support the conclusions drawn in this study were provided.
AFRIKAANSE OPSOMMING: Buigbare plaveiselontwerpers het 'n keuse van twee deklae: óf Asfalt of oppervlak seëls. Laasgenoemde word algemeen gebruik deur verskeie lande as hul voorkeur deklaag, veral die lande met beperkte aantal gemiddelde inwoners per vierkante kilometer. Verder, is die seëls geïdentifiseer as 'n doeltreffende koste-effektiewe deklaag tegniek. Oppervlakseëls in Nieu-Seeland, Suid-Afrika en Australië dek ongeveer 65%, 80% en 90% van hul padnetwerke onderskeidelik. Die seëls se voorkeur is te danke aan hul mededingende aanvanklike koste en eenvoudige vorm van die konstruksie. In Suid-Afrika wissel die seël se lewensverwagting tussen 8 en 12 jaar met 'n gemiddeld van 10 jaar. Dit is egter nie die geval van 'n aantal seëls wat in die winter gebou word nie, veral wanneer die aangetekende nagtemperatuur onder 10o C daal nie. Die dominante swigtingsmeganisme is stroping (klipverlies) kort na konstruksie. Hierdie klipverlies is gekoppel aan die power kleef-ontwikkeling van bitumen gedurende die winter. Ten einde die probleem van voortydige klipverlies aan te spreek het die behoefte vir die ontwikkeling van 'n robuuste toetsmetode ontstaan. Om hierdie rede het navorsers onlangs in die bitumenbedryf die “BBS toetsmetode” ontwikkel en is dié toetsmetode in hierdie studie gebruik. Hierdie studie beoog om by te dra tot die begrip van bindmiddel-klip kleefontwikkeling vir die winter seëls dmv die BBS toets. Die faktore, insluitend maar nie beperk tot bindmiddeltipe, voorafdekking (“PRECOAT”) -tipe en kondisionering, aggregaattipe en kuurtyd beïnvloed winter seëls se kleefeienskappe. 'n Eksperimentele matriks met drie tipes bindmiddels, twee tipes aggregate, vier verskillende voorafdekking-vloeistowwe, twee voorafdekking kondisionering en twee bindmiddel kuurtye is toe ontwikkel en ondersoek. Winter weer parameters wat kleefeienskappe beïnvloed is ook in ag geneem tydens die verloop van die ondersoek. Regdeur die studie is die prosedure AASHTO TP 91-11 gevolg, maar ten einde die beheer van die bindmiddel spuittemperatuur te verbeter, is ‘n nuwe metode vir warmspuit-bindmonsters voorbereiding ontwikkel as deel van hierdie studie. Die bevindinge toon dat daar 'n beduidende verskil tussen die kleefeienskappe van die warm aangewende bindmiddels (70/100 en S-E1) en die emulsie (SC-E1) is. In die meeste van die gevalle het die warmspuit-bindmiddels beter as emulsie gevaar. Daar is gevind dat die swigtingsmeganisme verbind word met die toestand van die voorafdekking. Die invloed van voorafdekkingtipe, kondisionering, en die effek van bindmiddelkuurtyd is duidelik uitgelig. Die gebruik van droë voorafdekking het die kleefkrag tot sowat 50% verhoog relatief tot die ooreenstemmende onbedekte klipkombinasie. Daar is egter ook ‘n verlaging van die kleefkrag weens voorafdekking gevind van tot so hoog soos 28,7 persent. Die statistiese ontleding met behulp van ANOVA het geen statisties beduidende effek van die verksillende aggregaattipe te vore gebring nie. Die interaksie-effek analise, met behulp van ANOVA, het wel die interaksie met voorafdekkingtipe met aggregaat die mees invloedryke bevestig. Die voorafdekking kondisioneering het ver rykende kleefkrag implikasies bloot gelê, wat die tyd vir die opening van die verkeer na konstruksie beïnvloed. Insigwekkende aspekte oor die versoenbaarheid tussen die bindmiddeltipe, voorafdekkingtipe, kondisionering, voorafdekkingpraktyk en tyd tot opening vir verkeer word uitgelig. Ten slotte, die herhaalbaarheidsanalise het die BBS toets as 'n herhaalbare toetsmetode met omsigtigheid bewys. Daar is aanbevelings tot verdere studies, wat uit die gevolgtrekking gekom het, gemaak.
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Howard, Dawne E. "The Finding Aid Container List Optimization Survey: Recommendations for Web Usability." Thesis, School of Information and Library Science, 2006. http://hdl.handle.net/1901/340.
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This paper examines the results of a usability study for finding aids from the Special Collections Research Center at North Carolina State University. In 2005, the Special Collections Research Center reformatted its finding aids so that the container information, typically located on the left-hand side of the document, moved to the right-hand side of the document. The study tested the effectiveness of this change, and determined that traditional finding aids performed better. The analysis of the study’s results is followed by a discussion about Web usability guidelines for online finding aids.
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Juratovac, Joseph M. "Strain Rate Sensitivity of Ti-6Al-4V and Inconel 718 and its Interaction with Fatigue Performance at Different Speeds." Ohio University / OhioLINK, 2020. http://rave.ohiolink.edu/etdc/view?acc_num=ohiou1605875502029283.
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Kerr, Justin Hamilton. "Ground based impact testing of Orbiter thermal protection system materials in support of the Columbia accident investigation." Thesis, 2005. http://hdl.handle.net/1911/18771.
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On January 16, 2003, the Space Shuttle Columbia (OV-102) was launched for a nominal 16-day mission of microgravity research. Fifteen days and 20 hours after launch, and just 16 minutes before its scheduled landing, the OV-102 vehicle disintegrated during its descent. The entire crew was lost. Film and video cameras located around the launch complex captured images of the vehicle during its ascent. Of note were data that showed a piece of debris strike the port wing at approximately 82 sec after lift-off (T+82). As resulting analysis would show, the source of the debris was the left bipod ramp of the Shuttle external tank. This foam debris struck the Orbiter leading edge at sufficient velocity to breech the thermal protection system (TPS). During reentry at the end of the mission, the hot plasma impinged inside the Orbiter wing and aerodynamic forces ultimately failed the wing structure.
This thesis documents the activities conducted to evaluate the effects of foam impact on Orbiter TPS. These efforts were focused on, to the greatest extent practical, replicating the impact event during the STS-107 mission ascent. This thesis fully documents the test program development, methodology, results, analysis, and conclusions to the degree that future investigators can reproduce the tests and understand the basis for decisions made during the development of the tests.
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LEE, KUANG_YI, and 李光益. "An Application of Grey System Theory in Forecasting and Management for Semiconductor Packaging and Testing on Materials." Thesis, 2018. http://ndltd.ncl.edu.tw/handle/6cz4z3.
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碩士明新科技大學
管理研究所碩士在職專班
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This study proposes Grey System models (GM) for the top 1 material ( Gold wire) usage forecasting semiconductor packaging and testing. The MAPE, MSE and Theil’U inequality coefficient were being used to evaluate the predictive errors of the models proposed. The time series data is obtained from SAP System. The empirical results show that Data during 2013 to 2015, NGBM model has a better predictive performance than GM(1,1) model and Arima model. In this research, we confirmed that the prediction error rate of the GM is less than 15%, therefore, that it can be applicable to medium-term time service data forecasting.
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Maisano, Paul Angelo. "Puncture resistance of geotextiles and evaluation of the g-rating classification system." Thesis, 1995. https://vuir.vu.edu.au/18189/.
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The puncture resistance of geotextiles in Australia is measured in terms of the G-Rating,
which is the product of CBR and drop cone puncture test results.
CBR and drop cone puncture tests were conducted on 24 geotextiles to provide up-to-
date results, and to evaluate the G-Rating. CBR puncture tests using modified
plungers were also conducted to assess the accuracy of shape factors quoted in the
literature- 3.0 for angular aggregate and 0.8 for rounded aggregate. Wide strip
tensile tests were also conducted to compare with CBR puncture test results.
The results of the testing program show no relationship between wide strip tensile
test results and CBR puncture test results. The modified plunger CBR puncture test
results show that shape factors are not only shape dependent, but are fabric
dependent as well, with the results somewhat different from those commonly
quoted. The exponent used to calculate the G-Rating varies for the same fabric
tested at different drop heights in the drop cone puncture test. Also, the restriction
of elongation in CBR puncture tests to 80 per cent by the G-Rating classification
system, was found unnecessary for all the geotextiles tested, as elongation at failure
in all cases did not exceed 80 per cent.
A Rupture Index classification is proposed, being the product of failure load and
vertical plunger displacement at failure in a CBR puncture test. It is considered to
be simpler than the G-Rating as it relies on the results of only one test. The
Rupture Index calculated for a given fabric will not vary by more than the inherent
variability of the specimens tested. However, G-Rating values were shown to vary
considerably for the same fabric tested at different drop heights in the drop cone
puncture test.
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"Thermal Actuation and Fluidic Characterization of a Fluorescence-Based Multiplexed Detection System." Master's thesis, 2018. http://hdl.handle.net/2286/R.I.50454.
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abstract: This work describes efforts made toward the development of a compact, quantitative fluorescence-based multiplexed detection platform for point-of-care diagnostics. This includes the development of a microfluidic delivery and actuation system for multistep detection assays. Early detection of infectious diseases requires high sensitivity dependent on the precise actuation of fluids.
Methods of fluid actuation were explored to allow delayed delivery of fluidic reagents in multistep detection lateral flow assays (LFAs). Certain hydrophobic materials such as wax were successfully implemented in the LFA with the use of precision dispensed valves. Sublimating materials such as naphthalene were also characterized along with the implementation of a heating system for precision printing of the valves.
Various techniques of blood fractionation were also investigated and this work demonstrates successful blood fractionation in an LFA. The fluid flow of reagents was also characterized and validated with the use of mathematical models and multiphysics modeling software. Lastly intuitive, user-friendly mobile and desktop applications were developed to interface the underlying Arduino software. The work advances the development of a system which successfully integrates all components of fluid separation and delivery along with highly sensitive detection and a user-friendly interface; the system will ultimately provide clinically significant diagnostics in a of point-of-care device.Dissertation/Thesis
Masters Thesis Biomedical Engineering 2018