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Journal articles on the topic 'LA-ICP-MS/MS'

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Published: 8 June 2024

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1

Gallo, Jenny M., and Jose R. Almirall. "Elemental analysis of white cotton fiber evidence using solution ICP-MS and laser ablation ICP-MS (LA-ICP-MS)." Forensic Science International 190, no. 1-3 (September 2009): 52–57. http://dx.doi.org/10.1016/j.forsciint.2009.05.011.

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2

Gäbler, Hans-Eike, Sönke Rehder, Andreas Bahr, Frank Melcher, and Simon Goldmann. "Cassiterite fingerprinting by LA-ICP-MS." Journal of Analytical Atomic Spectrometry 28, no. 8 (2013): 1247. http://dx.doi.org/10.1039/c3ja50106j.

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3

Choi, Sung Hwa, Jae Sung Kim, Ji Yeon Lee, Ji Suk Jeon, Ju Wan Kim, Richard E. Russo, Jhanis Gonzalez, et al. "Analysis of arsenic in rice grains using ICP-MS and fs LA-ICP-MS." J. Anal. At. Spectrom. 29, no. 7 (2014): 1233–37. http://dx.doi.org/10.1039/c4ja00069b.

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With rice being the main staple crop in Asian countries such as China, Korea and Japan, the detection of arsenic (As), an element known to be carcinogenic to humans, has been the topic of high public interest.

4

Brandl, Michael, and Christoph Hauzenberger. "Appendix 1. Supplementary LA-ICP-MS data." Archaeologia Austriaca 1 (2018): 550–65. http://dx.doi.org/10.1553/archaeologia102s550.

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5

Hutchinson, Robert W., and James A. Hutchinson. "Single-Cell Analysis by LA-ICP-MS." Transplantation 99, no. 11 (November 2015): 2237–38. http://dx.doi.org/10.1097/tp.0000000000000989.

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6

Pan, Zixiao, Wei Wei, and Fuhe Li. "LA ICP-MS in microelectronics failure analysis." Journal of Materials Science: Materials in Electronics 22, no. 10 (July 14, 2011): 1594–601. http://dx.doi.org/10.1007/s10854-011-0451-5.

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7

Becker, J. Sabine, M. Zoriy, Valderi L. Dressler, Bei Wu, and J. Susanne Becker. "Imaging of metals and metal-containing species in biological tissues and on gels by laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS): A new analytical strategy for applications in life sciences." Pure and Applied Chemistry 80, no. 12 (January 1, 2008): 2643–55. http://dx.doi.org/10.1351/pac200880122643.

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Laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) has become established as a very efficient and sensitive trace, ultratrace, and surface analytical technique in the life sciences. We have developed a new analytical imaging technique using LA-ICP-MS to study element distribution in biological tissues. Nowadays, LA imaging ICP-MS using double-focusing sector field (LA-ICP-SFMS) or quadrupole-based mass spectrometers (LA-ICP-QMS) can be applied as an exciting tool providing new information on the pathophysiology, pharmacology, and toxicology of elements of interest in biological systems. The quantitative determination of elements (e.g., Cu, Fe, Zn, Se, and others) in biological tissues is of growing interest especially in brain research (e.g., for studying neurodegenerative diseases such as Alzheimer's or Parkinson's disease). LA-ICP-SFMS was employed to produce images of detailed regionally specific element distributions in thin tissue sections of different sizes (such as control human or rat brain tissues or tumor regions). In addition, imaging MS using LA-ICP-QMS was applied to study the uptake and transport of nutrient and toxic elements in plant tissues.Besides the quantitative imaging of essential and toxic elements in tissues, powerful analytical techniques are also required for the determination and characterization of phosphoproteins and metal-containing proteins within a large pool of proteins, after electrophoretic separation (e.g., blue native, BN and sodium dodecyl sulfate-polyacrylamide gel electrophoresis, SDS-PAGE) into 1D and 2D gels. LA-ICP-MS was used to detect metalloproteins in protein bands of 1D gels or protein spots separated after 2D gel electrophoresis (2D-GE). In addition to elemental determination by LA-ICP-MS, matrix-assisted laser desorption/ionization (MALDI)-MS was employed to identify metal-containing proteins. Recent progress will be discussed in applying LA-ICP-MS in the life sciences, including the imaging of thin slices of tissue and applications in proteome analysis in combination with MALDI-MS to investigate phosphoproteins and metal-containing proteins.

8

Popov, Daniil V. "Short communication: On the potential use of materials with heterogeneously distributed parent and daughter isotopes as primary standards for non-U–Pb geochronological applications of laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS)." Geochronology 4, no. 1 (June 15, 2022): 399–407. http://dx.doi.org/10.5194/gchron-4-399-2022.

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Abstract. Many new geochronological applications of laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) have been proposed in recent years. One of the problems associated with this rapid growth is the lack of chemically and isotopically homogeneous matrix-matched primary standards to control elemental fractionation during LA-ICP-MS analysis. In U–Pb geochronological applications of LA-ICP-MS this problem is often addressed by utilising matrix-matched primary standards with variable chemical and isotopic compositions. Here I derive a set of equations to adopt this approach for non-U–Pb geochronological applications of LA-ICP-MS.

9

Frei, Dirk, Julie A. Hollis, Axel Gerdes, Dan Harlov, Christine Karlsson, Paulina Vasquez, Gerhard Franz, Leif Johansson, and Christian Knudsen. "Advanced in situ geochronological and trace element microanalysis by laser ablation techniques." Geological Survey of Denmark and Greenland (GEUS) Bulletin 10 (November 29, 2006): 25–28. http://dx.doi.org/10.34194/geusb.v10.4884.

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Laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) was developed in 1985 and the first commercial laser ablation systems were introduced in the mid 1990s. Since then, LA-ICP-MS has become an important analytical tool in the earth sciences. Initially, the main interest for geologists was in its ability to quantitatively determine the contents of a wide range of elements in many minerals at very low concentrations (a few ppm and below) with relatively high spatial resolution (spot diameters of typically 30–100 μm). The potential of LA-ICP-MS for rapid in situ U–Th–Pb geochronology was already realised in the early to mid 1990s. However, the full potential of LA-ICP-MS as the low-cost alternative to ion-microprobe techniques for highly precise and accurate in situ U–Th–Pb age dating was not realised until the relatively recent advances in laser technologies and the introduction of magnetic sectorfield ICP-MS (SF-ICPMS) instruments. In March 2005, the Geological Survey of Denmark and Greenland (GEUS) commissioned a new laser ablation magnetic sectorfield inductively coupled plasma mass spectrometry (LA-SF-ICP-MS) facility employing a ThermoFinnigan Element2 high resolution magnetic sectorfield ICP-MS and a Merchantek New Wave 213 nm UV laser ablation system. The new GEUS LA-SF-ICP-MS facility is widely used on Survey research projects in Denmark and Greenland, as well as in collaborative research and contract projects conducted with partners from academia and industry worldwide. Here, we present examples from some of the these ongoing studies that highlight the application of the new facility for advanced geochronological and trace element in situ microanalysis of geomaterials. The application of LASF-ICP-MS based in situ zircon geochronology to regional studies addressing the Archaean geology of southern West Greenland is presented by Hollis et al. (2006, this volume).

10

Grottoli, Andréa G., Kathryn A. Matthews, James E. Palardy, and William F. McDonough. "High resolution coral Cd measurements using LA-ICP-MS and ID-ICP-MS: Calibration and interpretation." Chemical Geology 356 (October 2013): 151–59. http://dx.doi.org/10.1016/j.chemgeo.2013.08.024.

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11

Ding, Lihua, Guang Yang, Fang Xia, Claire E. Lenehan, Gujie Qian, Aoife McFadden, Joël Brugger, Xianghua Zhang, Guorong Chen, and Allan Pring. "A LA-ICP-MS sulphide calibration standard based on a chalcogenide glass." Mineralogical Magazine 75, no. 2 (April 2011): 279–87. http://dx.doi.org/10.1180/minmag.2011.075.2.279.

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AbstractThe accurate measurement of trace element concentrations in natural sulphides by laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) has been limited by the lack of matrix-matched calibration standards. The synthesis of a standard, IMER-1, by incorporating four minor and 34 trace elements into a chalcogenide glass matrix Ge28Sb12S60is reported here. Chemical analysis by electron probe microanalysis (EPMA), LA-ICP-MS, solution ICP-MS, and inductively coupled plasma-optical emission spectroscopy (ICP-OES) confirmed the excellent homogeneity of major elements (1-σ relative standard deviation (RSD) <1% for S, Sb and Ge) and acceptable homogeneity of most trace elements (1-σ RSD <10%). The standard was validated by analysing trace-elements concentrations in three geological pyrite specimens using IMER-1 as the calibration standard and comparing the results to previously reported values also determined by LA-ICP-MS but using a different calibration standard. STDGL2b-2. The results suggest that IMER-1 may be an appropriate calibration standard for LA-ICP-MS analysis of trace elements in natural sulphides.

12

Wohlgemuth-Ueberwasser, Cora C., Jan A. Schuessler, Friedhelm von Blanckenburg, and Andreas Möller. "Matrix dependency of baddeleyite U–Pb geochronology by femtosecond-LA-ICP-MS and comparison with nanosecond-LA-ICP-MS." Journal of Analytical Atomic Spectrometry 33, no. 6 (2018): 967–74. http://dx.doi.org/10.1039/c7ja00403f.

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13

Lin, Jie, Yongsheng Liu, Yueheng Yang, and Zhaochu Hu. "Calibration and correction of LA-ICP-MS and LA-MC-ICP-MS analyses for element contents and isotopic ratios." Solid Earth Sciences 1, no. 1 (June 2016): 5–27. http://dx.doi.org/10.1016/j.sesci.2016.04.002.

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14

Zhang, Wen, Zhaochu Hu, and Yongsheng Liu. "Iso-Compass: new freeware software for isotopic data reduction of LA-MC-ICP-MS." Journal of Analytical Atomic Spectrometry 35, no. 6 (2020): 1087–96. http://dx.doi.org/10.1039/d0ja00084a.

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15

Jagielska, Agata, Anna Ruszczyńska, Ewa Bulska, and Barbara Wagner. "The impact of sample preparation on the elemental composition of soft tissues assessed by laser ablation ICP-MS." Journal of Analytical Atomic Spectrometry 35, no. 7 (2020): 1340–50. http://dx.doi.org/10.1039/d0ja00115e.

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16

Herriott, Trystan M., James L. Crowley, Mark D. Schmitz, Marwan A. Wartes, and Robert J. Gillis. "Exploring the law of detrital zircon: LA-ICP-MS and CA-TIMS geochronology of Jurassic forearc strata, Cook Inlet, Alaska, USA." Geology 47, no. 11 (September 23, 2019): 1044–48. http://dx.doi.org/10.1130/g46312.1.

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Abstract Uranium-lead (U-Pb) geochronology studies commonly employ the law of detrital zircon: A sedimentary rock cannot be older than its youngest zircon. This premise permits maximum depositional ages (MDAs) to be applied in chronostratigraphy, but geochronologic dates are complicated by uncertainty. We conducted laser ablation–inductively coupled plasma–mass spectrometry (LA-ICP-MS) and chemical abrasion–thermal ionization mass spectrometry (CA-TIMS) of detrital zircon in forearc strata of southern Alaska (USA) to assess the accuracy of several MDA approaches. Six samples from Middle–Upper Jurassic units are generally replete with youthful zircon and underwent three rounds of analysis: (1) LA-ICP-MS of ∼115 grains, with one date per zircon; (2) LA-ICP-MS of the ∼15 youngest grains identified in round 1, acquiring two additional dates per zircon; and (3) CA-TIMS of the ∼5 youngest grains identified by LA-ICP-MS. The youngest single-grain LA-ICP-MS dates are all younger than—and rarely overlap at 2σ uncertainty with—the CA-TIMS MDAs. The youngest kernel density estimation modes are typically several million years older than the CA-TIMS MDAs. Weighted means of round 1 dates that define the youngest statistical populations yield the best coincidence with CA-TIMS MDAs. CA-TIMS dating of the youngest zircon identified by LA-ICP-MS is indispensable for critical MDA applications, eliminating laser-induced matrix effects, mitigating and evaluating Pb loss, and resolving complexities of interpreting lower-precision, normally distributed LA-ICP-MS dates. Finally, numerous CA-TIMS MDAs in this study are younger than Bathonian(?)–Callovian and Oxfordian faunal correlations suggest, highlighting the need for additional radioisotopic constraints—including CA-TIMS MDAs—for the Middle–Late Jurassic geologic time scale.

17

Košler, Jan, Simon E. Jackson, Zhaoping Yang, and Richard Wirth. "Effect of oxygen in sample carrier gas on laser-induced elemental fractionation in U–Th–Pb zircon dating by laser ablation ICP-MS." J. Anal. At. Spectrom. 29, no. 5 (2014): 832–40. http://dx.doi.org/10.1039/c3ja50386k.

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18

Hogmalm, K. Johan, Isabell Dahlgren, Irma Fridolfsson, and Thomas Zack. "First in situ Re-Os dating of molybdenite by LA-ICP-MS/MS." Mineralium Deposita 54, no. 6 (May 25, 2019): 821–28. http://dx.doi.org/10.1007/s00126-019-00889-1.

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19

Brandl, Michael, Christoph Hauzenberger, Maria M. Martinez, Peter Filzmoser, and Dagmara H. Werra. "Appendix A. Supplementary LA-ICP-MS data - ONLINE." Archaeologia Austriaca 1 (2016): 1190. http://dx.doi.org/10.1553/archaeologia100s1190.

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20

Neff, Christoph, Pascal Becker, Bodo Hattendorf, and Detlef Günther. "LA-ICP-MS using a nitrogen plasma source." Journal of Analytical Atomic Spectrometry 36, no. 8 (2021): 1750–57. http://dx.doi.org/10.1039/d1ja00205h.

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21

Chew, David M., Ray A. Donelick, Margaret B. Donelick, Balz S. Kamber, and Michael J. Stock. "Apatite Chlorine Concentration Measurements by LA-ICP-MS." Geostandards and Geoanalytical Research 38, no. 1 (June 21, 2013): 23–35. http://dx.doi.org/10.1111/j.1751-908x.2013.00246.x.

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22

Fernández, Beatriz. "Elemental and molecular imaging by LA-ICP-MS." Analytical and Bioanalytical Chemistry 411, no. 3 (December 12, 2018): 547–48. http://dx.doi.org/10.1007/s00216-018-1523-7.

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23

Stehrer, T., J. Heitz, J. D. Pedarnig, N. Huber, B. Aeschlimann, D. Günther, H. Scherndl, T. Linsmeyer, H. Wolfmeir, and E. Arenholz. "LA-ICP-MS analysis of waste polymer materials." Analytical and Bioanalytical Chemistry 398, no. 1 (July 11, 2010): 415–24. http://dx.doi.org/10.1007/s00216-010-3963-6.

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24

Wohlgemuth-Ueberwasser, Cora C., Chris Ballhaus, Thomas Meisel, and Jasper Berndt. "PGE-sulfide standard synthesis for LA-ICP-MS." Geochimica et Cosmochimica Acta 70, no. 18 (August 2006): A706. http://dx.doi.org/10.1016/j.gca.2006.06.1531.

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25

Almirall, José R., and Tatiana Trejos. "Applications of LA–ICP–MS to Forensic Science." Elements 12, no. 5 (October 2016): 335–40. http://dx.doi.org/10.2113/gselements.12.5.335.

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26

Pullen, Alex, Mauricio Ibáñez-Mejía, George E. Gehrels, Juan C. Ibáñez-Mejía, and Mark Pecha. "What happens when n= 1000? Creating large-n geochronological datasets with LA-ICP-MS for geologic investigations." J. Anal. At. Spectrom. 29, no. 6 (2014): 971–80. http://dx.doi.org/10.1039/c4ja00024b.

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27

Steenstra, E. S., J. Berndt, S. Klemme, W. van Westrenen, E. S. Bullock, and A. Shahar. "Addressing matrix effects for 193 nm excimer LA-ICP-MS analyses of Fe-rich sulfides and a new predictive model." Journal of Analytical Atomic Spectrometry 35, no. 3 (2020): 498–509. http://dx.doi.org/10.1039/c9ja00391f.

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Matrix effects during ns-LA-ICP-MS analyses of Fe-rich sulfides were quantified for many trace elements by comparison of elemental concentrations obtained by LA-ICP-MS and electron microprobe (EPMA) for many synthetic sulfides.

28

Dadiego, Danielle L., Alyssa Gelinas, and Tsim D. Schneider. "Unpacking the Bead: Exploring a Glass Bead Assemblage from Mission Santa Cruz, California, Using LA–ICP–MS." American Antiquity 86, no. 2 (February 15, 2021): 413–24. http://dx.doi.org/10.1017/aaq.2020.110.

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This report focuses on the morphometric and elemental analysis of glass beads collected from an adobe structure (CA-SCR-217H-T) at Mission Santa Cruz, which operated between 1791 and the 1830s in the colonial province of Alta (upper) California. Previous chemical research established a chronological framework for opacified beads collected from sites in Canada, the Great Lakes region, and the southeastern United States. Testing the viability of this chronological framework for California, we analyzed 100 white glass beads using a conventional typology and laser ablation-inductively coupled plasma-mass spectrometry (LA-ICP-MS)—the first application of LA-ICP-MS to a California mission. We present the results of the LA-ICP-MS study and then briefly comment on the potential for LA-ICP-MS to refine chronologies associated with colonial missions and other postcontact sites.

29

Weyrauch, Mona, Martin Oeser, Annika Brüske, and Stefan Weyer. "In situ high-precision Ni isotope analysis of metals by femtosecond-LA-MC-ICP-MS." Journal of Analytical Atomic Spectrometry 32, no. 7 (2017): 1312–19. http://dx.doi.org/10.1039/c7ja00147a.

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30

Kaufmann, A. B., M. Lazarov, S. Kiefer, J. Majzlan, and S. Weyer. "In situ determination of antimony isotope ratios in Sb minerals by femtosecond LA-MC-ICP-MS." Journal of Analytical Atomic Spectrometry 36, no. 7 (2021): 1554–67. http://dx.doi.org/10.1039/d1ja00089f.

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31

Tavares Jr., Armando Dias, Mauro César Geraldes, Márcio C. Inácio, William Murussi Canto Jr., and Luiz Pinheiro Cordovil da Silva. "Preliminary Results in Gold Provenance Characterization using LA ICP MS." Revista Brasileira de Geografia Física 11, no. 3 (2018): 934–47. http://dx.doi.org/10.26848/rbgf.v10.6.p934-947.

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32

Tavares Jr., Armando Dias, Mauro César Geraldes, Márcio C. Inácio, William Murussi Canto Jr., and Luiz Pinheiro Cordovil da Silva. "Preliminary Results in Gold Provenance Characterization using LA ICP MS." Revista Brasileira de Geografia Física 11, no. 3 (2018): 934–47. http://dx.doi.org/10.26848/rbgf.v11.3.p934-947.

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33

Bolea-Fernandez, Eduardo, Stijn J. M. Van Malderen, Lieve Balcaen, Martín Resano, and Frank Vanhaecke. "Laser ablation-tandem ICP-mass spectrometry (LA-ICP-MS/MS) for direct Sr isotopic analysis of solid samples with high Rb/Sr ratios." Journal of Analytical Atomic Spectrometry 31, no. 2 (2016): 464–72. http://dx.doi.org/10.1039/c5ja00404g.

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34

Norris, C. Ashley, Leonid Danyushevsky, Paul Olin, and Nicholas R. West. "Elimination of aliasing in LA-ICP-MS by alignment of laser and mass spectrometer." Journal of Analytical Atomic Spectrometry 36, no. 4 (2021): 733–39. http://dx.doi.org/10.1039/d0ja00488j.

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We have developed a device that fires the laser in alignment with the measurement cycle of sequential ICP-MS instruments, allowing quadrupole LA-ICP-MS analysis to be performed using fast response ablation cells.

35

Santamaria-Fernandez, Rebeca, Ruth Hearn, and Jean-Claude Wolff. "Detection of counterfeit tablets of an antiviral drug using δ34S measurements by MC-ICP-MS and confirmation by LA-MC-ICP-MS and HPLC-MC-ICP-MS." Journal of Analytical Atomic Spectrometry 23, no. 9 (2008): 1294. http://dx.doi.org/10.1039/b802890g.

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36

Abdullin, Fanis, Luigi A. Solari, Jesús Solé, and Carlos Ortega-Obregón. "Technical note: LA–ICP-MS U–Pb dating of unetched and etched apatites." Geochronology 3, no. 1 (January 20, 2021): 59–65. http://dx.doi.org/10.5194/gchron-3-59-2021.

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Abstract. The same unetched and chemically etched apatite crystals from five rock samples were dated by the U–Pb method via laser ablation inductively coupled plasma mass spectrometry (LA–ICP-MS). The objective of this study is to test whether chemical etching required for apatite fission track analysis impacts the precision and accuracy of apatite U–Pb geochronology. The results of this experiment suggest that etching has insignificant effects on the accuracy of apatite U–Pb ages obtained by LA–ICP-MS. Therefore, LA–ICP-MS is reliable for U–Pb analysis as part of apatite fission track and U–Pb double dating.

37

Balaram, V. "Inductively Coupled Plasma-Tandem Mass Spectrometry (ICP-MS/MS) and Its Applications." Journal of ISAS 1, no. 1 (July 31, 2022): 1–26. http://dx.doi.org/10.59143/isas.jisas.1.1.cnyr8764.

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During the last about 10 years, the inductively coupled plasma tandem quadrupole mass spectrometry (ICP-MS/MS) technique with reaction cell is being utilized for the analyses of several trace elements/isotopes at very low concentration levels in a variety of matrices including geological, environmental, biological, medical, nuclear, agriculture, food, material and metallurgical sciences. Both solution nebulization, as well as direct analysis of samples by laser ablation (LA-ICP-MS/MS), are utilized for sample introduction. In fact, ICP-MS/MS technique with collision reaction cells eliminated the need for laborious chemical separations using methods such as ion-exchange or solvent extraction procedures to eliminate/minimize spectral and matrix interference effects as these interferences are removed using online chemical reactions within the instrument itself (chemical resolution). In addition, the technique is hyphenated with chromatographic techniques such as GC and HPLCfor a variety of applications. The detection limits for several elements in the periodic table lie in the pg/ml-fg/ml range, and the technique compares favourably with the expensive, complex, and superior high resolution-ICP-MS (HR-ICP-MS), both in terms of the detection limits as well as the ability to remove the most complex interferences. Thus, the ICP MS/MS made the determinations of elemental as well as isotopic concentrations very simple andeasy even in complex materials with several novel quantification approaches. This article provides an overview of these new developments during the last decade along with several applications in all areas of science and technology.

38

Balaram, V. "Inductively Coupled Plasma-Tandem Mass Spectrometry (ICP-MS/MS) and Its Applications." Journal of ISAS 1, no. 1 (July 31, 2022): 1–26. http://dx.doi.org/10.59143/isas.jisas.1.1.lhbp9335.

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During the last about 10 years, the inductively coupled plasma tandem quadrupole mass spectrometry (ICP-MS/MS) technique with reaction cell is being utilized for the analyses of several trace elements/isotopes at very low concentration levels in a variety of matrices including geological, environmental, biological, medical, nuclear, agriculture, food, material and metallurgical sciences. Both solution nebulization, as well as direct analysis of samples by laser ablation (LA-ICP-MS/MS), are utilized for sample introduction. In fact, ICP-MS/MS technique with collision reaction cells eliminated the need for laborious chemical separations using methods such as ion-exchange or solvent extraction procedures to eliminate/minimize spectral and matrix interference effects as these interferences are removed using online chemical reactions within the instrument itself (chemical resolution). In addition, the technique is hyphenated with chromatographic techniques such as GC and HPLCfor a variety of applications. The detection limits for several elements in the periodic table lie in the pg/ml-fg/ml range, and the technique compares favourably with the expensive, complex, and superior high resolution-ICP-MS (HR-ICP-MS), both in terms of the detection limits as well as the ability to remove the most complex interferences. Thus, the ICP MS/MS made the determinations of elemental as well as isotopic concentrations very simple andeasy even in complex materials with several novel quantification approaches. This article provides an overview of these new developments during the last decade along with several applications in all areas of science and technology.

39

Dustin, Megan K., Elizabeth C. Koeman, Antonio Simonetti, Zachary Torrano, and Peter C. Burns. "Comparative Investigation between In Situ Laser Ablation Versus Bulk Sample (Solution Mode) Inductively Coupled Plasma Mass Spectrometry (ICP-MS) Analysis of Trinitite Post-Detonation Materials." Applied Spectroscopy 70, no. 9 (August 26, 2016): 1446–55. http://dx.doi.org/10.1177/0003702816662597.

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In the event of the interception of illicit nuclear materials or detonation of a nuclear device, timely and accurate deciphering of the chemical and isotopic composition of pertinent samples is pivotal in enhancing both nuclear security and source attribution. This study reports the results from a first time (to our knowledge), detailed comparative investigation conducted of Trinitite post-detonation materials using both solution mode (SM) and laser ablation (LA) inductively coupled plasma mass spectrometry (ICP-MS) techniques. Trace element abundances determined for bulk Trinitite samples subsequent to digestion and preparation for SM-ICP-MS analysis compare favorably to calculated median concentrations based on LA-ICP-MS analyses for the identical samples. The trace element concentrations obtained by individual LA-ICP-MS analyses indicate a large scatter compared to the corresponding bulk sample SM-ICP-MS results for the same sample; this feature can be attributed to the incorporation into the blast melt of specific, precursor accessory minerals (minerals in small quantities, such as carbonates, sulfates, chlorites, clay, and mafic minerals) present at ground zero. The favorable comparison reported here validates and confirms the use of the LA-ICP-MS technique in obtaining accurate forensic information at high spatial resolution in nuclear materials for source attribution purposes. This investigation also reports device-like 240Pu/239Pu ratios (∼0.022) for Pu-rich regions of the blast melt that are also characterized by higher Ca and U contents, which is consistent with results from previous studies.

40

Kukusamude, Chunyapuk, Supalak Kongsri, Ratchadawan Tamklang, and Sutthinun Taebunpakul. "Feasibility of Matrix-Matched Material for Determining Elements in Rice Flour by SN-ICP-MS and LA-ICP-MS." Foods 13, no. 11 (May 22, 2024): 1604. http://dx.doi.org/10.3390/foods13111604.

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Abstract:

The preparation of matrix-matched material for elemental quantitative analysis in rice flour matrix is proposed here for the first time as part of a feasibility study using the SN-ICP-MS and LA-ICP-MS methods. It was prepared via the spiking process in colloidal solution of rice flour with different levels of arsenic (As), cadmium (Cd) and lead (Pb), followed by drying in a climatic chamber. Comparative studies of the results on external calibration and gravimetric standard addition ICP-MS approaches through the use of calibration standard solutions were discussed. Method bias from the external calibration method was investigated, demonstrating the systematic effect arising from the sample matrix. Characterizing the concentration of measurands was then reasonably proposed using the gravimetric standard addition ICP-MS. Using powdered rice matrix reference material for ICP-MS calibration following acid digestion, the study showed a good agreement of recovery studies. A feasibility study of the LA-ICP-MS method as a direct solid analysis performed on the matrix-matched standard was then discussed. In the study, large fluctuation of signals was found for constructing calibration curve, generating poor linearity, especially for As and Pb, although yttrium (Y) as internal standard was applied. This might be ascribed to a limited microscale of homogeneity, and particularly laser-induced preferential evaporation of volatile elements. Using a number of measured data points, the mean and median were statistically recommended to improve precision. An attempt to use of similar matrix in both standard and sample is a critical point to consider to minimize the elemental fractionation effect. The proposed approach to prepare matrix-matched material could be a potential means for achieving elemental quantitation.

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Sylvester, Paul J. "Trends in Analytical Developments and Earth Science Applications in LA-ICP-MS and LA-MC-ICP-MS for 2004 and 2005." Geostandards and Geoanalytical Research 30, no. 3 (November 2006): 197–207. http://dx.doi.org/10.1111/j.1751-908x.2006.tb01062.x.

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Xie, Lie-Wen, Noreen J. Evans, Yue-Heng Yang, Chao Huang, and Jin-Hui Yang. "U–Th–Pb geochronology and simultaneous analysis of multiple isotope systems in geological samples by LA-MC-ICP-MS." Journal of Analytical Atomic Spectrometry 33, no. 10 (2018): 1600–1615. http://dx.doi.org/10.1039/c8ja00157j.

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This is a critical review that: (i) provides an overview of LA-MC-ICP-MS dating techniques; (ii) highlights the benefits of using ICs and summarizes recent improvements in ultra-high spatial resolution dating; (iii) summarizes the range of minerals utilized for LA-MC-ICP-MS geochronology and LASS.

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Gong, Gelian, Saijun Sun, Jibin Zhou, Congyin Li, Xu Liang, Xiaodong Fang, Libing You, Hongyun Xu, and Weidong Sun. "Nanosecond laser ablation tandem inductively coupled plasma mass and optical emission spectrometry for micro-chemical elemental analysis." Journal of Analytical Atomic Spectrometry 32, no. 11 (2017): 2246–53. http://dx.doi.org/10.1039/c7ja00223h.

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44

Gilbert, S. E., L. V. Danyushevsky, K. Goemann, and D. Death. "Fractionation of sulphur relative to iron during laser ablation-ICP-MS analyses of sulphide minerals: implications for quantification." J. Anal. At. Spectrom. 29, no. 6 (2014): 1024–33. http://dx.doi.org/10.1039/c4ja00012a.

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Abstract:

In this study we investigate the effect that the mineral composition has on the quantification of sulphur by Laser Ablation ICP-MS (LA-ICP-MS) between a range of sulphide minerals: pyrite, pyrrhotite, bornite, chalcopyrite, sphalerite, pentlandite and tetrahedrite.

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Scheffler, G. L., and D. Pozebon. "Advantages, drawbacks and applications of mixed Ar–N2 sources in inductively coupled plasma-based techniques: an overview." Anal. Methods 6, no. 16 (2014): 6170–82. http://dx.doi.org/10.1039/c4ay00178h.

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This review deals with mixed gas Ar–N₂ plasmas, highlighting advantages, limitations and applications of them in inductively coupled plasma optical emission spectrometry (ICP OES), inductively coupled plasma mass spectrometry (ICP-MS) and laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) techniques, covering publications in the last three decades.

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Becker, J. Sabine, Hagit Sela, Justina Dobrowolska, Miroslav Zoriy, and J. Susanne Becker. "Recent applications on isotope ratio measurements by ICP-MS and LA-ICP-MS on biological samples and single particles." International Journal of Mass Spectrometry 270, no. 1-2 (February 2008): 1–7. http://dx.doi.org/10.1016/j.ijms.2007.10.008.

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Ishii, Chihiro, Shouta M. M. Nakayama, Andrew Kataba, Yoshinori Ikenaka, Keisuke Saito, Yukiko Watanabe, Yoshiki Makino, et al. "Characterization and imaging of lead distribution in bones of lead-exposed birds by ICP-MS and LA-ICP-MS." Chemosphere 212 (December 2018): 994–1001. http://dx.doi.org/10.1016/j.chemosphere.2018.08.149.

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Garbe-Schönberg, Dieter, and Samuel Müller. "Nano-particulate pressed powder tablets for LA-ICP-MS." J. Anal. At. Spectrom. 29, no. 6 (2014): 990–1000. http://dx.doi.org/10.1039/c4ja00007b.

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Wohlgemuth-Ueberwasser, Cora C., and Klaus Peter Jochum. "Capability of fs-LA-ICP-MS for sulfide analysis in comparison to ns-LA-ICP-MS: reduction of laser induced matrix effects?" Journal of Analytical Atomic Spectrometry 30, no. 12 (2015): 2469–80. http://dx.doi.org/10.1039/c5ja00251f.

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Mouchi, Vincent, Camille Godbillot, Catherine Dupont, Marc-Antoine Vella, Vianney Forest, Alexey Ulianov, Franck Lartaud, Marc de Rafélis, Laurent Emmanuel, and Eric P. Verrecchia. "Provenance study of oyster shells by LA-ICP-MS." Journal of Archaeological Science 132 (August 2021): 105418. http://dx.doi.org/10.1016/j.jas.2021.105418.

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