Relevant bibliographies by topics / Hydroxy selenide

Academic literature on the topic 'Hydroxy selenide'

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Published: 10 December 2022
Last updated: 29 January 2023

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Journal articles on the topic "Hydroxy selenide"

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Kadu, Rahul, Monojit Batabyal, Heena Kadyan, Apurba Lal Koner, and Sangit Kumar. "An efficient copper-catalyzed synthesis of symmetrical bis(N-arylbenzamide) selenides and their conversion to hypervalent spirodiazaselenuranes and hydroxy congeners." Dalton Transactions 48, no. 21 (2019): 7249–60. http://dx.doi.org/10.1039/c8dt04832k.

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Eom, Taejun, and Anzar Khan. "Selenium-Epoxy ‘Click’ Reaction and Se-Alkylation—Efficient Access to Organo-Selenium and Selenonium Compounds." Chemistry 2, no. 4 (October 5, 2020): 827–36. http://dx.doi.org/10.3390/chemistry2040054.

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This work establishes the ‘click’ nature of the base-catalyzed oxirane ring opening reaction by the selenolate nucleophile. The ‘click’-generated ß-hydroxy selenide can be alkylated to afford cationic selenium species. Hemolytic studies suggest that selenonium cations do not lyse red blood cells even at high concentrations. Overall, these results indicate the future applicability of the developed organo-selenium chemistry in the preparation of a new class of cationic materials based on the seleno-ether motif.
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Eom, Taejun, and Anzar Khan. "Selenonium Polyelectrolyte Synthesis through Post-Polymerization Modifications of Poly (Glycidyl Methacrylate) Scaffolds." Polymers 12, no. 11 (November 13, 2020): 2685. http://dx.doi.org/10.3390/polym12112685.

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Atom transfer radical polymerization of glycidyl methacrylate monomer with poly(ethylene glycol)-based macroinitiators leads to the formation of reactive block copolymers. The epoxide side-chains of these polymers can be subjected to a regiospecific base-catalyzed nucleophilic ring-opening reaction with benzeneselenol under ambient conditions. The ß-hydroxy selenide linkages thus formed can be alkylated to access polyselenonium salts. 77Se-NMR indicates the formation of diastereomers upon alkylation. In such a manner, sequential post-polymerization modifications of poly(glycidyl methacrylate) scaffolds via selenium-epoxy and selenoether alkylation reactions furnish practical access to poly(ethylene glycol)-based cationic organoselenium copolymers.
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Tanini, Damiano, Alessandro Degl'Innocenti, and Antonella Capperucci. "Bis(trimethylsilyl)selenide in the Selective Synthesis of β-Hydroxy, β-Mercapto, and β-Amino Diorganyl Diselenides and Selenides Through Ring Opening of Strained Heterocycles." European Journal of Organic Chemistry 2015, no. 2 (November 21, 2014): 357–69. http://dx.doi.org/10.1002/ejoc.201403015.

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Tanini, Damiano, Alessandro Degl'Innocenti, and Antonella Capperucci. "ChemInform Abstract: Bis(trimethylsilyl)selenide in the Selective Synthesis of β-Hydroxy, β-Mercapto, and β-Amino Diorganyl Diselenides and Selenides Through Ring Opening of Strained Heterocycles." ChemInform 46, no. 22 (May 15, 2015): no. http://dx.doi.org/10.1002/chin.201522234.

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ABE, Hitoshi, Akira YAMASAKI, and Takashi HARAYAMA. "Direct Conversion of a Benzylic Hydroxy Group into a Selenenyl Group Using the Phenyl Trimethylsilyl Selenide-Aluminum Bromide Combination." CHEMICAL & PHARMACEUTICAL BULLETIN 46, no. 8 (1998): 1311–13. http://dx.doi.org/10.1248/cpb.46.1311.

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Wang, Hongwei, Hongchen Li, Guoqi Yu, Yun-Bing Zhou, Yalong Bai, Yanling Hei, and Junwei Chen. "Synthesis of β-Hydroxy Aryl Selenides via Transition-Metal-Free Three-Component Reaction of Arylamines, Elemental Selenium, and Epoxides." Synthesis 53, no. 19 (May 5, 2021): 3621–29. http://dx.doi.org/10.1055/a-1499-8742.

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AbstractAn efficient protocol for the construction of valuable β-hydroxy aryl selenides from easily available arylamines, elemental selenium, and epoxides through a transition-metal-free radical process is described. A wide variety of β-hydroxy aryl selenides were obtained in good to excellent yields with excellent stereo- and regioselectivity. In this reaction, two C–Se bonds can be built along with the cleavage of a C–N and C–O bond, demonstrating the high step economy and efficiency of this approach.
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ABE, H., A. YAMASAKI, and T. HARAYAMA. "ChemInform Abstract: Direct Conversion of a Benzylic Hydroxy Group into a Selenenyl Group Using the Phenyl Trimethylsilyl Selenide-Aluminum Bromide Combination." ChemInform 30, no. 5 (June 17, 2010): no. http://dx.doi.org/10.1002/chin.199905150.

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Lipinski, Boguslaw. "Redox-Active Selenium in Health and Disease: A Conceptual Review." Mini-Reviews in Medicinal Chemistry 19, no. 9 (May 6, 2019): 720–26. http://dx.doi.org/10.2174/1389557517666161104125022.

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Although it is generally accepted that selenium (Se) is important for life, it is not well known which forms of organic and/or inorganic Se compound are the most biologically active. In nature Se exists mostly in two forms, namely as selenite with fourvalent and selenate with sixvalent cations, from which all other inorganic and organic species are derived. Despite a small difference in their electronic structure, these two inorganic parent compounds differ significantly in their redox properties. Hence, only selenite can act as an oxidant, particularly in the reaction with free and/or protein- bound sulhydryl (SH) groups. For example, selenite was shown to inhibit the hydroxyl radicalinduced reduction and scrambled reoxidation of disulfides in human fibrinogen thus preventing the formation of highly hydrophobic polymer, termed parafibrin. Such a polymer, when deposited within peripheral and/or cerebral circulation, may cause irreversible damage resulting in the development of cardiovascular, neurological and other degenerative diseases. In addition, parafibrin deposited around tumor cells produces a protease-resistant coat protecting them against immune recognition and elimination. On the other hand, parafibrin generated by Ebola’s protein disulfide isomerase can form a hydrophobic ‘spike’ that facilitates virus attachment and entry to the host cell. In view of these specific properties of selenite this compound is a potential candidate as an inexpensive and readily available food supplement in the prevention and/or treatment of cardiovascular, neoplastic, neurological and infectious diseases.
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Jin, Li Ming, Chen Zhuang, Chun Shan Quan, Xiao Jing Zhao, and Sheng Di Fan. "Synthesis of Chitooligosaccharide-Selenium and its Antioxidant Activity In Vitro." Advanced Materials Research 680 (April 2013): 149–53. http://dx.doi.org/10.4028/www.scientific.net/amr.680.149.

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The objective of this study was to synthesize a new organic selenium compound, chitooligosaccharide-selenium (COSSe), and evaluate its antioxidant abilities on hydroxyl radicals, super oxide radicals and DPPH in vitro. Sodium selenite and chitooligosaccharide (COS) were used to synthesize COSSe by chemical method. The yield was 37.26% and the content of selenium (Se) was 9.02mg/g. COSSe was characterized by ultraviolet (UV) and infrared (IR) techniques. The results proved the successful synthesis of COSSe. The antioxidant activities on hydroxyl radicals, super oxide radicals and DPPH of COSSe were investigated. The results showed that antioxidant activities were concentration related in the setting concentration range and the antioxidant effects of COSSe were totally better than that of COS. The scavenging rates on hydroxyl radicals, superoxide radicals and DPPH of 2.5mg/mL COSSe were 71.19%, 64.54% and 69.78%, respectively. This research provides a possible application of COSSe as a low toxic and effective organic Se-enriched healthy product.
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Dissertations / Theses on the topic "Hydroxy selenide"

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Redon, Sébastien. "Reactivité des composés carbonyles α-selenies α, β-insatures : préparation et valorisation de motifs dieniques, cyclopropaniques et dihydropyraniques." Rouen, 2008. http://www.theses.fr/2008ROUES012.

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Dans le premier chapitre, une synthèse de diènes séléniés à partir d’énals a-séléniés a été développée par réaction de Wittig ou Wadsworth﷓Horner﷓Emmons. Une étude par RMN 77Se a permis de déterminer les proportions et la configuration des isomères formés. La position vinylique et allylique du groupement sélénié de ces diènes, permet leur réarrangement sigmatropique en hydroxyallène. L’addition d’ylures de phosphore non-stabilisés sur des énones a-séléniées ne conduit pas aux diènes attendus mais à des cyclopropanes et dihydrofuranes par une addition de Michael suivie d’une cyclisation. La stéréochimie et les proportions de chacun des diastéréomères des cyclopropanes ont été déterminées par RMN 77Se et par des expériences NOESY. Enfin, l’utilisation des haute-pressions nous a permis de développer des réactions d’hétéro-Diels﷓Alder à demande inverse donnant des dihydropyranes. Lorsque ces dihydropyranes séléniés sont oxydés, ceux-ci se réarrangent pour donner des alkoxy furan-2-ones
In the first chapter, the synthesis of selenylated dienes from a-selenylated enals was developed by Wittig or Wadsworth﷓Horner﷓Emmons réactions on selenylated enals. A 77Se NMR study allowed us to determine the proportions and the configuration of the isomers. The both vinylic and allylic position of the selenyl group of these dienes, allows a sigmatropic rearrangement in hydroxyallenes. The addition of non-stabilized phosphore ylides on a-selenylated enones does not give the selenylated dienes awaited but new cyclopropanes and dihydrofuranes according to an addition Michael followed by a cyclization. The stereochemistry of the cyclopropanes and the proportions of each of the diastereomers were determined by 77Se NMR and by NOESY experiences. The use of the high pressures allowed us to develop reactions of hetero-Diels﷓Alder at inverse demand to access to new dihydropyrans. When these dihydropyranes are subjected to oxidizing conditions, they rearrangent into alkoxy furan-2-ones
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Castro, Liérson Borges de. "Estudo da Reatividade de Fenilcalcogenolatos de Índio(III)." Universidade Federal de Santa Maria, 2011. http://repositorio.ufsm.br/handle/1/4205.

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Conselho Nacional de Desenvolvimento Científico e Tecnológico
Indium(III) benzenechalcogenolates (chalcogen = sulfur, selenium) prepared from elemental indium and diphenyl dichalcogenide provide an alternative synthetic route to produce carbon-chalcogen bonds. These compounds promote the regioselective hydrochalcogenation of terminal aminoalkynes to produce the Markovnikov adducts; provide a pratical method to prepare organyl phenyl chalcogenides from organyl halides; and their reaction with vinylarenes in aqueous media produces the respectives β-hydroxy selenides. Ditellurides present a different performance compared to others studied dichalcogenides. Indium(I) salts react with tellurium compounds and through extrusion of one tellurium atom produce diaryl tellurides. This work presents new synthetic methodologies and discusses the general aspects and limitations of indium chalcogenolates in the different systems investigated.
Fenilcalcogenolatos de índio(III) (calcogênio = enxofre e selênio), preparados a partir de índio metálico e difenil dicalcogenetos, são uma alternativa em síntese para geração de ligações carbono-calcogênio. Estes compostos promovem a hidrocalcogenação Markovnikov de alquinilaminas terminais com rigorosa regiosseletividade; conduzem, de modo prático, ao preparo de organil fenilcalcogenetos frente a haletos orgânicos; e na reação com estirenos possibilitam a síntese de β-hidroxisselenetos em meio aquoso. Já os diteluretos empregados apresentam comportamento diferenciado em relação aos demais dicalcogenetos estudados. A reação de sais de índio(I) com os compostos de telúrio conduzem a extrusão de telúrio e a obtenção de diaril teluretos. O trabalho desenvolvido, além de apresentar novas metodologias sintéticas, discute as generalidades e limitações dos calcogenolatos de índio nos diferentes sistemas investigados.
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Ward, Virginia R. "Aspects of organoselenium chemistry." Thesis, 2013. http://hdl.handle.net/2440/81756.

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A range of β-amidoalkyl phenylselenides were prepared in order to explore their cyclisation via oxidation of the selenium moiety to the selenone followed by intramolecular displacement. At first, the β-amidoalkyl phenylselenides were prepared in one-step from the alkenes. However, the one-step preparation was complicated by side-reactions and a two-step method was found to give clean reactions and higher yields of a wide range of the desired amido selenides. Along with the expected oxazolines, isomeric N-acylaziridines were obtained from the cyclisation reaction. Formation of N-acylaziridines by cyclisation of amides is unusual, and variation of the conditions was explored in order to optimise this novel aziridine-forming reaction. It was found that conducting the oxidation reaction at low temperature favoured the aziridine products. In this way, the aziridines derived from all prepared β-amido selenides were obtained in good to excellent yield. From some substrates, the aziridine was obtained as the exclusive product. The low temperature generation of a selenone from the corresponding selenide had not been reported previously. Experiments were carried out which provided evidence for the supposition that the intermediate in the cyclisation reaction was the selenone. The preparation of β-amido selenides was also investigated using silver ion to sequester the halide of the selenium reagent, rendering the selenium species more electrophilic and its addition to the alkene to give a seleniranium ion, irreversible. The seleniranium ion was generated in the presence of nitrile to allow attack by the weak nitrile nucleophile upon the seleniranium ion, giving a nitrilium ion. With addition of water to the nitrilium ion, β-amido selenides were formed in moderate yield. Thus, it was shown that the β-amido selenides could be prepared without the use of strong acid. Addition of azide to the nitrilium ion gave a tetrazole, which demonstrated that this methodology could provide access to selenides substituted at the β-position with groups other than the amido group. β-Benzamidocyclohexyl phenyl selenoxide and β-benzamidocyclohexyl phenyl selenone were prepared, and hydrogen bonding in the two compounds was examined spectroscopically. An X-ray crystal structure of the selenoxide showed intermolecular hydrogen bonding between the amide hydrogen and the seleninyl oxygen, in contrast to proposals in the literature that analogous selenoxides were stabilised by intramolecular hydrogen bonding in the solid state. Three β-hydroxy selenides were prepared and their low-temperature oxidation and cyclisation was explored with a view to obtaining the corresponding oxetanes. The low-temperature procedure did not translate successfully to the cyclisation of ϒ- hydroxy selenides to oxetanes, instead giving complex mixtures. However, with reference to literature conditions for the preparation of methoxy-substituted oxetanes, the ϒ-hydroxy selenides were cyclised to the corresponding oxetanes by oxidation in methanol at room temperature, demonstrating that the scope of this method could be widened to a more generalised preparation of oxetanes.
Thesis (Ph.D.) -- University of Adelaide, School of Chemistry & Physics, 2013
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Wu, Chih-Chung, and 吳致中. "The copper indium selenide precursor synthesized by microwave-assisted hydro-/solvo-thermal method and its film fabricated by electrophoresis deposition." Thesis, 2008. http://ndltd.ncl.edu.tw/handle/24414721488942660708.

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碩士
國立臺灣科技大學
化學工程系
96
The objective of the presented study is to fabricate uniform, dense CuInSe2 thin film for next-generation solar cells by employing electrophoresis deposition technique (EPD). The study can be divided into two parts, including synthesis of CuInSe2 particles and preparation of CuInSe2 thin films by using EPD technique. First, the viability of microwave-assisted solvo- and hydro-thermal method in the preparation of CuInSe2 materials is investigated. For microwave-assisted solvo-thermal method, pure chalcopyrite structure of the materials was achieved within 30 min with ethylenediamine as solvent, indicating the success in synthesis of CuInSe2 materials. The results showed great improvement for synthesis of CuInSe2 since materials can only be synthesized with at least 20-fold time with conventional heating. The morphologies of the synthesized CuInSe2 materials can be controlled with appropriate pretreatment, however, it is not suitable for the subsequent EPD technique. Therefore, low cost and environmental friendly microwave-assisted hydrothermal method was employed instead of solvothermal one for possible use in thin film fabrication by EPD. It was found that stoichiometric CuInSe2 precursors are able to be synthesized with uniform morphology at the condition of 180 oC for 30 mins. Reduction of the process time is also observed as well. Further the chalcopyrite CuInSe2 particles can be obtained by the post reduction process at 500℃ in H2. On the other hand, deposition of the CuInSe2 thin film by EPD technique was performed with the hydrothermal-derived CuInSe2 precursors. The technique possesses the characteristics of short processing time and precise control in film thickness. Nevertheless, the prepared thin films are porous even after reduction at 600 oC. The fact may result from the loss of oxygen during reduction process as well as the originally porous nature for the precursor thin film. The behavior can be the guide for the future improvement. Besides, the reduced CuInSe2 thin film was analyzed by Raman and XPS, in which only chalcopyrite structure was shown without any impurities.
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Hraníček, Jakub. "Konstrukce miniaturních průtokových cel pro elektrochemické generování těkavých sloučenin." Doctoral thesis, 2011. http://www.nusl.cz/ntk/nusl-312116.

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(EN) The presented dissertation thesis summarizes the new results of electrochemical generation of volatile compounds usable in atomic spectral methods. The main aim of this work is to develop and to characterize new types of electrolytic flow-through cells and to examine their possibilities of determination of arsenic, selenium and antimony by using the electrochemical hydride generation technique coupled with atomic absorption spectrometry with a quartz tube atomizer. Individual electrolytic cells were designed and constructed to comply with two important requirements. The cathode chamber of the electrolytic cell should have a minimal volume and a high efficiency of analyte conversion to the volatile hydride. Constructed electrolytic cells are divided into the construction groups and described in the experimental part. Selenium was chosen as the first analyte. The relevant working parameters (such as type, concentration and flow rate of electrolytes, generation current and carrier gas flow rate) were optimized for each newly constructed electrolytic cell. Under the optimal working parameters, the basic characteristics of selenium determination were found out by using electrochemical hydride generation. The electrolytic cells were compared to each other and with the classical electrolytic cell...
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Book chapters on the topic "Hydroxy selenide"

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Kirsch, G., E. Perspicace, and S. Hesse. "Synthesis and Transformations of 2- and 3-hydroxy-Selenophenes and 2- and 3-Amino-Selenophenes." In Selenium and Tellurium Chemistry, 239–50. Berlin, Heidelberg: Springer Berlin Heidelberg, 2011. http://dx.doi.org/10.1007/978-3-642-20699-3_10.

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Bhumbla, D. K., S. S. Dhaliwal, K. S. Sajwan, and B. S. Sekhon. "Selenium and Molybdenum Adsorption on Kaolinite Clay Mineral Coated with Hydrous Oxides of Iron and Aluminum." In Chemistry of Trace Elements in Fly Ash, 237–49. Boston, MA: Springer US, 2003. http://dx.doi.org/10.1007/978-1-4757-4757-7_16.

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Hodgson, D. M., and P. G. Humphreys. "Elimination of β-Hydroxy Selenides." In Alcohols, 1. Georg Thieme Verlag KG, 2008. http://dx.doi.org/10.1055/sos-sd-036-00498.

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Yudin, A. K., and A. Caiazzo. "Synthesis from Vicinal Hydroxy Sulfides and Selenides." In Ethers, 1. Georg Thieme Verlag KG, 2008. http://dx.doi.org/10.1055/sos-sd-037-00244.

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Drabowicz, J., J. Lewkowski, W. Kudelska, and T. Girek. "Base-Catalyzed Elimination Reaction of β-Hydroxy Sulfones." In Sulfur, Selenium, and Tellurium, 1. Georg Thieme Verlag KG, 2008. http://dx.doi.org/10.1055/sos-sd-039-00216.

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Drabowicz, J., and J. Lewkowski. "Reaction of Sulfuryl Chloride with β-Hydroxy Sulfoxides." In Sulfur, Selenium, and Tellurium, 1. Georg Thieme Verlag KG, 2008. http://dx.doi.org/10.1055/sos-sd-039-00880.

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Margaretha, P. "Replacement of an Alcoholic Hydroxy Group with Selenium Tetrachloride." In Chlorine, Bromine, and Iodine, 1. Georg Thieme Verlag KG, 2007. http://dx.doi.org/10.1055/sos-sd-035-00074.

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Taber, Douglass F. "Best Synthetic Methods: Functional Group Transformations." In Organic Synthesis. Oxford University Press, 2013. http://dx.doi.org/10.1093/oso/9780199965724.003.0003.

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Vinyl glycine 2 is a useful precursor to a variety of amino acids. Timothy E. Long of the University of Georgia found (Tetrahedron Lett. 2009, 50, 5067) that the o-nitrophenyl sulfoxide 1 eliminated smoothly in refluxing toluene. Alicia Boto and Rosendo Hernández of IPNA La Laguna observed (Tetrahedron Lett. 2009, 50, 3974) that a related selenoxide elimination proceeded to give the single regioisomer 4. Avelino Corma of the Universidad Politécnica de Valencia developed ( Chemical Commun. 2009, 4947) a gold catalyst for the selective hydroboration of alkynes over alkenes. Eiji Shirakawa and Tamio Hayashi of Kyoto University devised (Chemical Commun. 2009, 5088) a Ru catalyst for the conversion of an alkenyl triflate such as 8 to the corresponding bromide. Tristan H. Lambert of Columbia University found (J. Am. Chem. Soc. 2009, 131, 13930) that the dichloride 11 smoothly converted a variety of alcohols into the corresponding chlorides. Crown ethers have been used to promote SN2 reactivity by solubilizing the metal cation. Sungyul Lee of Kyunghee University, Dae Yoon Chi of Sogang University, and Choong Eui Song of Sungkyunkwan University demonstrated (Angew. Chem. Int. Ed. 2009, 48, 7683) that the inexpensive polyethylene glycols were also effective. Mugio Nishizawa of Tokushima Bunri University devised (Synlett 2009, 1175) conditions for the rapid regioselective hydration of hydroxy alkynes such as 15. Jaume Vilarrasa of the Universitat de Barcelona developed (Organic Lett. 2009, 11, 4414) a mild alternative protocol for the Nef reaction, converting a nitroalkane such as 17 into the corresponding ketone under neutral conditions. Clément Mazet of the University of Geneva optimized (Tetrahedron Lett. 2009, 50, 4141) the Ir-catalyzed conversion of an allylic alcohol 19 into the saturated aldehyde. Jonathan M. J. Williams of the University of Bath established (Angew. Chem. Int. Ed. 2009, 48, 7375) that under Ir-catalyzed “borrowing hydrogen” conditions, alkyl amines could donate alkyl groups to anilines such as 21. Danfeng Huang and Yulai Hu of Northwest Normal University devised (Organic Lett. 2009, 11, 4474) a simple protocol for conversion of an acid 23 to the Weinreb amide 24. of the Universitat
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Conference papers on the topic "Hydroxy selenide"

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Juniper, D. T., C. Rymer, M. Briens, M. De Marco, J. Barbi, and G. Fontinhas. "Hydroxy-selenomethionine is an effective selenium source for pregnant heifers and their calf." In 6th EAAP International Symposium on Energy and Protein Metabolism and Nutrition. The Netherlands: Wageningen Academic Publishers, 2019. http://dx.doi.org/10.3920/978-90-8686-891-9_38.

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