Academic literature on the topic 'HSQC experiments'
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Journal articles on the topic "HSQC experiments"
Krishnamurthy, V. V. "Sensitivity-Enhanced 3D HSQC-TOCSY Experiments." Journal of Magnetic Resonance, Series B 106, no. 2 (February 1995): 170–77. http://dx.doi.org/10.1006/jmrb.1995.1028.
Full textXia, Youlin, Kong Hung Sze, Ning Li, Pang Chui Shaw, and Guang Zhu. "Protein Dynamics Measurements by 3D HNCO Based NMR Experiments." Spectroscopy 16, no. 1 (2002): 1–13. http://dx.doi.org/10.1155/2002/828353.
Full textWeitzel, Alexander, Claudia Samol, Peter J. Oefner, and Wolfram Gronwald. "Robust Metabolite Quantification from J-Compensated 2D 1H-13C-HSQC Experiments." Metabolites 10, no. 11 (November 7, 2020): 449. http://dx.doi.org/10.3390/metabo10110449.
Full textRouger, Laetitia, Serge Akoka, and Patrick Giraudeau. "Optimized decoupling schemes in ultrafast HSQC experiments." Journal of Magnetic Resonance 283 (October 2017): 89–95. http://dx.doi.org/10.1016/j.jmr.2017.08.015.
Full textYang, Linyao, Jiangchao Du, Rongtao Li, Fei Yu, and Jindong Zhong. "Bodiniosides S–Y, Seven New Triterpenoid Saponins from Elsholtzia bodinieri and Their Anti-Influenza Activities." Molecules 26, no. 21 (October 29, 2021): 6535. http://dx.doi.org/10.3390/molecules26216535.
Full textKiraly, Peter, Mathias Nilsson, and Gareth A. Morris. "Practical aspects of real-time pure shift HSQC experiments." Magnetic Resonance in Chemistry 56, no. 10 (January 12, 2018): 993–1005. http://dx.doi.org/10.1002/mrc.4704.
Full textGschwind, Ruth M., Xiulan Xie, and Pattuparambil R. Rajamohanan. "Gs-HSQC-NOESY versus gs-NOESY-HSQC experiments: signal attenuation due to diffusion; application to symmetrical molecules." Magnetic Resonance in Chemistry 42, no. 3 (February 12, 2004): 308–12. http://dx.doi.org/10.1002/mrc.1344.
Full textHu, Haitao, and Krish Krishnamurthy. "Doubly compensated multiplicity-edited HSQC experiments utilizing broadband inversion pulses." Magnetic Resonance in Chemistry 46, no. 7 (2008): 683–89. http://dx.doi.org/10.1002/mrc.2221.
Full textCharlier, Cyril, Neil Cox, Sophie Martine Prud'homme, Alain Geffard, Jean-Marc Nuzillard, Burkhard Luy, and Guy Lippens. "Virtual decoupling to break the simplification versus resolution trade-off in nuclear magnetic resonance of complex metabolic mixtures." Magnetic Resonance 2, no. 2 (August 10, 2021): 619–27. http://dx.doi.org/10.5194/mr-2-619-2021.
Full textNolis, Pau, Kumar Motiram-Corral, Míriam Pérez-Trujillo, and Teodor Parella. "Broadband homodecoupled time-shared 1H-13C and 1H-15N HSQC experiments." Journal of Magnetic Resonance 298 (January 2019): 23–30. http://dx.doi.org/10.1016/j.jmr.2018.11.005.
Full textDissertations / Theses on the topic "HSQC experiments"
Castañar, Acedo Laura. "Development and application of modern pure shift NMR techniques and improved HSQC/HSQMBC experiments." Doctoral thesis, Universitat Autònoma de Barcelona, 2015. http://hdl.handle.net/10803/300751.
Full textThe present doctoral thesis is framed within the Nuclear Magnetic Resonance (NMR) spectroscopy field, more specifically in the design of modern NMR methodologies. The research work carried out is focused on the design and application of new and modern NMR methodologies (i) to perform efficient broadband 1H homodecoupling in 1D/2D NMR experiments and (ii) to accurately determine homo- and heteronuclear coupling constants in isotropic and anisotropic conditions through improved HSQC and HSQMBC-type experiments. The thesis is presented as a compendium of publications, which have been published in prestigious peer-reviewed international scientific journals. Therefore, all the results here exposed have been previously evaluated by expert researchers in the fields of the NMR spectroscopy and chemistry. Several 1H homodecoupled NMR experiments have been developed along this doctoral thesis. Most of them are based on the Homodecoupled Band-Selective (HOBS) experiment through which it is possible to obtain homodecoupled NMR spectra with full sensitivity. HOBS methods offer a powerful and simple way to obtain high-resolved 1D and 2D NMR spectra, as efficiently demonstrated for the accurate, simple and direct measurement of T1/T2 relaxation times in overlapped regions, the determination of heteronuclear coupling constants from simplified multiplets, the determination of very small chemical shift differences with success application in enantiodifferentation studies or the analysis of highly complex mixtures. In addition, the concept of ultra-high-resolution NMR spectroscopy has been tested by combining several resolution-enhanced techniques into a single NMR experiment. On the other hand, for many years the measurement and practical use of coupling constants have been a timely topic but there are still a number of unresolved issues. Along this doctoral thesis a suite of robust HSQC and HSQMBC experiments have been developed which provide accurate and precise measurements of couplings constants through simple and direct analysis of cross-peaks without involving complex post-processing data manipulation.
Plensa, Nebot Isabel. "Hiperplasia suprarrenal congénita por defecto en la enzima 21-hidroxilasa: caracterización por el sistema HLA y aportación de la biología molecular, La." Doctoral thesis, Universitat de Barcelona, 2003. http://hdl.handle.net/10803/2982.
Full textEsta enfermedad presenta un espectro muy amplio de manifestaciones clínicas; desde formas severas que se presentan al nacimiento, en las que la virilización puede ir o no acompañada de un síndrome pierde sal, hasta formas más leves en que los signos de virilización se presentan más tardíamente. La incidencia de las formas clásicas de este déficit, oscila alrededor de 1:10.000-15.000 nacimientos, mientras la de las formas no clásicas se ha estimado en 1:1.000 en la población blanca, con marcadas variaciones étnicas.
El objetivo ha sido la caracterización clínica, biológica y genética de la HSC por déficit en 21-hidroxilasa de una población de la Comunitat Autònoma de Catalunya, con el fin de poder realizar un diagnóstico etiológico concluyente y establecer el consejo genético familiar completo.
Han colaborado 53 familias (106 cromosomas no emparentados) con al menos un hijo diagnosticado de HSC por déficit en 21-hidroxilasa, siendo el total de individuos estudiados de 214. De este total, 71 son pacientes que según los síntomas clínicos fueron clasificados en: 13 SW; 5 SV y 53 NC; 102 son progenitores y 41 son hermanos de dichos pacientes, ninguno de ellos clínicamente afecto.
Para la determinación de la función hormonal se practicó una prueba de estimulación con corticotropina (test de ACTH), con valoración de las concentraciones plasmáticas de 17-hidroxiprogesterona antes y tras 30 minutos de la inyección. La determinación de los antígenos de Clase I y Clase II del Sistema HLA, se realizó mediante la técnica de Microlinfocitotoxicidad. El análisis genético consistió en la detección de grandes reordenamientos mediante la técnica de "Southern blot", y la detección de nueve de las mutaciones puntuales más comunes mediante el diseño de una nueva metodología en la que se emplean dos estrategias según la mutación a detectar: ganancia o pérdida de al menos una diana de restricción en el producto de PCR amplificado a partir de DNA genómico o creación de una diana de restricción por amplificación (ACRS-PCR) y posterior digestión con una enzima de restricción apropiada.
El test de ACTH se confirma como fiable, ya que no se observaron falsos positivos ni falsos negativos en los valores obtenidos de 17-hidroxiprogesterona post estimulación. El nomograma de 17-hidroxiprogesterona proporciona un patrón hormonal que facilita, en la mayoría de los casos, el diagnóstico de las distintas formas de presentación clínica del déficit. No se observó la presencia del antígeno HLA-Bw47 en ninguno de los grupos analizados. Las formas no clásicas se encuentran significativamente asociadas al haplotipo HLA-B14-DR1, mientras que las formas clásicas al antígeno HLA-B5(w51).
La metodología utilizada para el análisis molecular del gen ha permitido detectar la mutación causal en el 89,62% de los cromosomas afectos, evaluados globalmente, consolidándose ésta como altamente efectiva en el diagnóstico de esta patología. Las mutaciones más frecuentes observadas han sido: Intrón 2 (50%) en SW; Intrón 2 (50%) y I172N (16,6%) en SV y V281L (61,5%) en NC. El análisis de los pedigrees ha permitido diagnosticar veintiséis formas crípticas y revelar en dos casos la presencia de mutaciones originadas de novo. La concordancia hallada entre el genotipo y el fenotipo ha sido del 97,2%, de ahí, que las predicciones desde el genotipo han de ser hechas todavía con gran cautela.
Veleba, Ondřej. "Studium vlivu složení na mechanické vlastnosti vysokohodnotného betonu." Master's thesis, Vysoké učení technické v Brně. Fakulta chemická, 2008. http://www.nusl.cz/ntk/nusl-216217.
Full textPortolés, Flaj José Manuel. "Estudio experimental y numérico de soportes tubulares circulares de acero esbeltos rellenos de hormigón de alta resistencia." Doctoral thesis, Universitat Jaume I, 2010. http://hdl.handle.net/10803/669145.
Full textBook chapters on the topic "HSQC experiments"
Longin, Teresa. "Using the HSQC Experiment to Teach 2D NMR Spectroscopy in Physical Chemistry." In ACS Symposium Series, 175–89. Washington, DC: American Chemical Society, 2021. http://dx.doi.org/10.1021/bk-2021-1376.ch012.
Full textNik, Sara, Joshua T. Weinreb, and Teresa V. Bowman. "Developmental HSC Microenvironments: Lessons from Zebrafish." In Advances in Experimental Medicine and Biology, 33–53. Cham: Springer International Publishing, 2017. http://dx.doi.org/10.1007/978-3-319-69194-7_4.
Full textBouzid, Haytham, Benferhat Rabia, and Tahar Hassaine Daouadji. "Curvature Ductility of Confined HSC Columns." In Lecture Notes in Civil Engineering, 253–62. Singapore: Springer Nature Singapore, 2023. http://dx.doi.org/10.1007/978-981-99-1748-8_21.
Full textRatajczak, Mariusz Z., Marcin Wysoczynski, Ryan Reca, Wu Wan, Ewa K. Zuba-Surma, Magda Kucia, and Janina Ratajczak. "A Pivotal Role of Activation of Complement Cascade (CC) in Mobilization of Hematopoietic Stem/Progenitor Cells (HSPC)." In Advances in Experimental Medicine and Biology, 45–58. New York, NY: Springer US, 2008. http://dx.doi.org/10.1007/978-0-387-78952-1_4.
Full textNagasawa, Takashi. "The Chemokine CXCL12 and Regulation of Hsc and B Lymphocyte Development in the Bone Marrow Niche." In Advances in Experimental Medicine and Biology, 69–75. Boston, MA: Springer US, 2007. http://dx.doi.org/10.1007/978-0-387-72009-8_9.
Full textGuthrie, Roderick I. L., and Mihaiela Isac. "Computational Fluid Dynamics and Experimental Results for the Horizontal Single Belt Casting (HSBC) of Aluminum Alloy Strips." In PRICM, 2859–66. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2013. http://dx.doi.org/10.1002/9781118792148.ch354.
Full textGuthrie, Roderick I. L., and Mihaiela Isac. "Computational Fluid Dynamics and Experimental Results for the Horizontal Single Belt Casting (HSBC) of Aluminum Alloy Strips." In Proceedings of the 8th Pacific Rim International Congress on Advanced Materials and Processing, 2859–66. Cham: Springer International Publishing, 2013. http://dx.doi.org/10.1007/978-3-319-48764-9_354.
Full textCastañar, Laura, and Teodor Parella. "Recent Advances in Small Molecule NMR: Improved HSQC and HSQMBC Experiments." In Annual Reports on NMR Spectroscopy, 163–232. Elsevier, 2015. http://dx.doi.org/10.1016/bs.arnmr.2014.10.004.
Full textConference papers on the topic "HSQC experiments"
Zhang, Changqing, Yeqinq Liu, Yue Liu, Qinghua Hu, Xinwang Liu, and Pengfei Zhu. "FISH-MML: Fisher-HSIC Multi-View Metric Learning." In Twenty-Seventh International Joint Conference on Artificial Intelligence {IJCAI-18}. California: International Joint Conferences on Artificial Intelligence Organization, 2018. http://dx.doi.org/10.24963/ijcai.2018/424.
Full textWang, Xinguo, David Moulton, and Mirjam Fürth. "The Development of a Planning Boat Model and Environmental Measurements for Free Running Model Tests." In SNAME 14th International Marine Design Conference. SNAME, 2022. http://dx.doi.org/10.5957/imdc-2022-266.
Full textWang, Xinguo, Omar Sallam, David Moulton, Jared Richardson, Rory Sunderland, Benjamin McKeig, and Mirjam Furth. "High-Speed Craft Model Design, Data Acquisition and Environment Monitoring for Free-Running Tests." In SNAME Maritime Convention. SNAME, 2022. http://dx.doi.org/10.5957/smc-2022-085.
Full textHamada, Ahmed A., Omar Khaled Sallam, Colton R. Bonnaure, Patricia Itzel Rodriguez, Jack Stason, and Mirjam Furth. "Design of a Free Running High Speed Craft Model for Testing Off the Coast of Galveston." In SNAME 26th Offshore Symposium. SNAME, 2021. http://dx.doi.org/10.5957/tos-2021-20.
Full textLi, Changyong, Zhaofei Chen, Xinxin Ding, and Shunbo Zhao. "Experimental Study on Crack Width of Reinforced HSC-on-SFRFLC Superposed Beams." In 2015 International Conference on Architectural, Civil and Hydraulics Engineering. Paris, France: Atlantis Press, 2015. http://dx.doi.org/10.2991/icache-15.2015.3.
Full textLi, Hongxia, Charles C. Okaeme, Weilin Yang, and TieJun Zhang. "Effect of Surface Wettability and Gas/Liquid Velocity Ratio on Microscale Two-Phase Flow Patterns." In ASME 2016 5th International Conference on Micro/Nanoscale Heat and Mass Transfer. American Society of Mechanical Engineers, 2016. http://dx.doi.org/10.1115/mnhmt2016-6383.
Full textWang, Jing, Feng Tian, Xiao Wang, Hongchuan Yu, Chang Hong Liu, and Liang Yang. "Multi-Component Nonnegative Matrix Factorization." In Twenty-Sixth International Joint Conference on Artificial Intelligence. California: International Joint Conferences on Artificial Intelligence Organization, 2017. http://dx.doi.org/10.24963/ijcai.2017/407.
Full textOguchi, Noritake, Junichi Sakai, Hiroyuki Inoue, and Shigeru Komukai. "Critical Hardness for HSC in Deposit Welding on Steel Line Pipes Under Cathodic Protection." In 2006 International Pipeline Conference. ASMEDC, 2006. http://dx.doi.org/10.1115/ipc2006-10227.
Full textKOWALSKI, D. "Nonlinear Analysis of Beams made of High Strength Concrete Prestressed with Unbonded Tendons." In Terotechnology XII. Materials Research Forum LLC, 2022. http://dx.doi.org/10.21741/9781644902059-12.
Full textSantos, Erick de Matos, Thayse Batista Moreira, Ana Luiza de Freitas Magalhães Gomes, Ana Paula Alvares Ramos, Fábio Ribeiro Queiroz, Paulo Guilherme de Oliveira Salles, and Letícia Conceição Braga. "STANDARDIZATION OF THE FICOLL GRADIENT TECHNIQUE FOR THE ISOLATION OF MONONUCLEAR CELLS FROM PERIPHERAL BLOOD." In Brazilian Breast Cancer Symposium 2022. Mastology, 2022. http://dx.doi.org/10.29289/259453942022v32s2030.
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