Dissertations / Theses: 'Herbicides'

1

Marchesan, Eli Danieli. "Eficiência agronômica e comportamento de formulações de atrazina com taxas distintas de liberação em latossolo vermelho distroférrico." Universidade Tecnológica Federal do Paraná, 2011. http://repositorio.utfpr.edu.br/jspui/handle/1/235.

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CNPQ
A atrazina (2-cloro-4-etilamino-6-isopropilamino-striazina) é um herbicida mundialmente utilizado no controle de plantas daninhas, com potencial para contaminar águas subterrâneas e prejudicar culturas sensíveis em sucessão. O uso de formulações de liberação lenta de atrazina poderia se constituir estratégia mitigadora do impacto ambiental e contribuir para a melhoria da eficiência de controle de plantas daninhas. Com o objetivo de determinar o comportamento ambiental e a eficiência agronômica de formulação de atrazina com liberação lenta (xerogel), comparando-a com formulação comercial, foram realizados um experimento a campo e três bioensaios em casa de vegetação. O experimento a campo foi implantado com a cultura do milho, utilizando-se o delineamento de blocos ao acaso, em parcelas subdivididas, em um esquema (2 x 6) + 4. Nas parcelas principais foram locadas as formulações (atrazina WG e atrazina xerogel), e nas subparcelas as concentrações de atrazina (0, 3200, 3600, 4200, 5400 e 8000 g ha-1), com acréscimo de quatro parcelas testemunha capinadas. Amostras de solo foram coletadas nas parcelas com 8000 g ha-1 para realização de bioensaios em casa de vegetação para avaliação da persistência e lixiviação das formulações. Nos bioensaios, o delineamento experimental foi inteiramente casualizado. No experimento a campo, avaliou-se a densidade e o controle visual de plantas daninhas e o rendimento de grãos de milho. Nos bioensaios, as principais variáveis avaliadas foram estatura, fitotoxicidade, massas de planta verde e seca. No primeiro bioensaio, selecionou-se a espécie cultivada mais adequada para utilização em testes para determinação da lixiviação e persistência das formulações de atrazina. No experimento a campo, a formulação WG exerceu maior controle de B. plantaginea que xerogel nas avaliações de mais precoces, mas nas avaliações mais tardias a atrazina xerogel foi mais eficiente. Não ocorreram diferenças de rendimento de grãos de milho entre as formulações e doses testadas. O grau de sensibilidade à atrazina variou de acordo com a espécie: quiabo e ervilha apresentaram pequena sensibilidade; aveia e trigo apresentaram nível intermediário e tomate e rabanete o mais alto nível de sensibilidade à presença de atrazina no solo. A biodisponibilização de atrazina ao solo variou em função do tempo e da formulação: até 5 dias após a aplicação, a disponibilização com a formulação xerogel foi maior; no período entre 14 e 28 dias, a biodisponibilização por atrazina WG foi superior à por xerogel; aos 35 dias após a aplicação, xerogel proporcionou maior atrazina ao solo do que WG. A meia vida foi de 30 e 38 dias, para atrazina WG e atrazina xerogel, respectivamente. Maior concentração de atrazina foi encontrada na superfície do solo (0 a 4 cm), nas duas formulações. Porém, a quantificação de atrazina por bioensaio indicou maior concentração da formulação WG entre 2 e 4 cm, em contraste com o resultado da análise cromatográfica, que indicou maior concentração da formulação xerogel.
Atrazine (2-chloro-4-ethylamine-6-isopropylamine-striazina) is an herbicide used worldwide to control weeds with potential to contaminate groundwater and harm sensitive crops in succession. The use of controlled release formulations of atrazine could be a strategy to mitigate environmental impact and contribute to improving the efficiency of weed control with atrazine. Aiming to determine the environmental performance and agronomic efficiency of atrazine formulation of controlled release (xerogel), compared with the commercial formulation were conducted one experiment in the field and three bioassays in greenhouse. The field experiment was implemented with the corn, using randomized blocks design, with split plots in a scheme (2 x 6) + 4. In the main plots were located formulations (atrazine xerogel and WG), and in sub-plots the atrazine concentrations (0, 3200, 3600, 4200, 5400 and 8000 g ha-1), with four additional control plots weeded. Soil samples were collected from each plot with 8000 g ha-1 for bioassays in the greenhouse to evaluate the persistence and leaching of the formulations. The experimental designs of bioassays were completely randomized. In the field experiment, we evaluated the density and visual control of weeds and yield of maize. In bioassays, the main variables were height, phytotoxicity, green and dry plant mass. In the first bioassay was selected cultivated species most suitable for use in tests to determine the persistence and leaching of atrazine formulations. In the field experiment, the formulation WG produced greater control of B. plantaginea than xerogel in earlier assessments, but in later assessments atrazine xerogel was more effective. There were no differences in grain yield of maize between the formulations and doses tested. The degree of sensitivity to atrazine varied according to species: okra and peas showed little sensitivity; oats and wheat had an intermediate; radish and tomato had the highest level of sensitivity to the presence of atrazine in soil. The bioavailability of atrazine to soil varied depending on the time and formulation: until 5 days after application, atrazine disponibility by xerogel formulation was higher and in period between 14 and 28 days, the bioavailability of atrazine by WG was higher than by xerogel; 35 days after application, atrazine xerogel showed higher disponibility than the WG. The half-life was 30 and 38 days for atrazine WG and xerogel, respectively. Higher concentrations of atrazine were found in surface soil (0-4 cm) in two formulations. However, the quantification of atrazine by bioassay indicated a greater concentration of WG formulation between 2 and 4 cm, in contrast with the results of chromatographic analysis, which indicated a greater concentration of the xerogel formulation.

2

Tofoli, Gustavo Radomille [UNESP]. "Efeito do tamanho do alvo e condições operacionais sobre a uniformidade de deposição de pulverizações em pré-emergência." Universidade Estadual Paulista (UNESP), 2001. http://hdl.handle.net/11449/97245.

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Este trabalho teve como objetivo estudar o efeito do tamanho do alvo e condições operacionais sobre a uniformidade de deposição de pulverizações em pré-emergência. Duas barras pulverizadoras de mesmo modelo (12 m e espaçamento entre bicos de 0,5 m) sendo uma para cada tipo de bico.Dois tipos de bicos (jato cônico modelo JA- 1,5 e jato plano modelo API 110-02) testados com uma mesma velocidade de aplicação (4km/h). Para o preparo das caldas de pulverização foram utilizados: água, nitrato de potássio, nitrato de cálcio, sulfato de cobre e sulfato de zinco. Os alvos foram construídos de chapa de fórmica, que foram cortadas em placas quadradas com tamanho de 13 x 13 cm. Ao centro de 602 placas foram feitos orifícios de diversos tamanhos de diâmetro: 10,16 cm, 5,8 cm, 2,54 cm, 1,27 cm, 0,63 cm e 0,32 cm. Para cada tamanho de orifício foram feitas 117 repetições. Totalizando 702 placas. Os alvos foram posicionados no piso do terreno de maneira aleatória. Depois da pulverização, estes foram lavados com 25 ml de água deionizada, dando origem as amostras. Estas, depois de filtradas, foram analisadas em espectrofotômetro de plasma. As leituras de concentrações foram transformadas em volume ( l), e este divido pela área de cada círculo correspondente, resultando em dados de depósito em l/cm2. Os dados de depósitos foram transformados em % da média, e realizado os cálculos de freqüências acumuladas para cada tamanho de alvo. O modelo de Gompertz (y = e **(a-e**(-b-c*x))) foi utilizado para ajustar os dados e efetuar as análises de regressão, obtendo os valores de R2 (0,985 a 0,997) e um novo valor de freqüência acumulada para cada curva. Calculou-se os valores de média, mediana, moda, os percentis 1, 2, 5, 10, 20, 40, 60, 80, 90, 95, 98 e 99.e os coeficientes de variação para todos os diferentes tamanhos de alvo para os respectivos bicos... .
It were studied two types of nozzles. The first one is a conic jet nozzle model JÁ 1,5. The second type is a flat fan nozzle model API 110-02. The application speed was 4km/h. It were used two similar sprayers set with boons 12 m wide and nozzles spaced by 0,5m. The spray solution for the fan jet nozzle was prepared with water, potassium nitrate and copper sulfate. For the conic jet nozzle theses salts were replaced by calcium nitrate and zinc sulfate. The targets were made of formica foils cut into square plates of 13 cm x 13 cm. One hundred of these plates were used to estimate the drift. In all the other 702 plates (117 replications for each type of target) it were made central circular holes of different diameters: 10,16 cm, 5,8 cm, 2,54 cm, 1,27 cm, 0,63 cm and 0,32 cm. The targets were randomly arranged on the ground. After spraying and drying the spray solution, each target was washed with 25 ml of de-ionized water. These water samples were filtered and analyzed in plasma spectrophotometer. The concentrations of the tracers in the final volume of 25 mL allowed to calculate the deposits of both spray solutions (in L/cmø) in each target. These data were converted in to percent of the means for each nozzle type and target size. Frequency distribution curves were fitted to the data. The Gompertz (y=e**(a-e**(-b-c*x))) model provided the highest determination coefficients, ranging from 0,985 and 0,997. In addition to the Relative Standard Deviation (RSD%) it were estimated the values of the mean, the median, the mode and the 1, 2, 5, 10, 20, 40, 60, 80, 90, 95, 98 and 99 percents, using the frequency distribution curves. Among the central tendency measures, the mode, the median and the 1, 2, 5, 10, 20, 40, 60, 80, 90, 95, 98 and 99 percents allowed more precise comparisons of spray deposits of different nozzles in targets of several sizes; the mean is very sensitive... (Complete abstract, click electronic address below).

3

Oliveira, Jefferson Anthony Gabriel de [UNESP]. "Matéria seca, teores de macronutrientes e produtividade de soja transgênica e não transgênica com diferentes manejos de plantas daninhas." Universidade Estadual Paulista (UNESP), 2011. http://hdl.handle.net/11449/98743.

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No contexto das grandes culturas produtoras de grãos, a soja foi a que mais cresceu em termos percentuais nos últimos 37 anos, tanto no Brasil quanto em nível mundial. O presente trabalho teve por objetivo verificar se há diferença entre variedades de soja transgênica e não transgênica quanto ao desenvolvimento vegetativo e reprodutivo através do acúmulo de matéria seca na parte aérea e dos teores de macronutrientes na matéria seca produzida, quando estas são submetidas à presença de herbicidas específicos para o controle de plantas daninhas. O experimento foi realizado na Fazenda de Ensino, Pesquisa e Extensão da Faculdade de Engenharia/UNESP - Campus de Ilha Solteira, localizada no município de Selvíria – MS. Os tratamentos foram compostos de duas variedades de soja transgênica (BRS Valiosa RR e BRS Favorita RR) e duas variedades convencionais (MGBR 46 – Conquista e MGBR 68 – Vencedora), com controle de plantas daninhas através de uso de herbicidas ou capinas. A semeadura da soja ocorreu no dia 20/11/2009, em um espaçamento de 0,45 m entrelinhas e 15 sementes por metro de sulco. O delineamento experimental utilizado foi o em blocos casualizados com 4 repetições, apresentando as parcelas, 7 linhas com 50 m de comprimento. Avaliaram-se as características agronômicas como: altura de inserção da primeira vagem; altura de plantas; número de ramos por planta; número de vagens por planta; população de plantas; produtividade de grãos; massa de 1000 grãos no estádio R8 da cultura. Também foi avaliado em amostragens quinzenais a partir do 21o dias após a germinação, a matéria seca de folhas, caules, vagens e grãos e o teor de macronutrientes nesta e o estado nutricional das plantas, através de amostragem foliar, no florescimento pleno. Os resultados obtidos perm itiram concluir que: aos 81 dias após emergência, quando as plantas encontram -se no...
In the context of major grain-producing crops, soybean was grown the most in percentage terms over the past 37 years, both in Brazil and worldw ide. This study aimed to observe the differences between varieties of GM and non GM soya on the vegetative and reproductive development through the dry matter accumulation in shoots and macronutrient content in dry matter yield when they are subjected to t he presence of herbicides for weed control. The experiment was conducted at Faculdade de Engenharia/UNESP – Ilha Solteira, located in Selvíria county. The treatments consisted of two transgenic soybeans varieties (BRS Favorita and BRS Valiosa) and two conventional varieties (MGBR 46 - Conquista and MGBR 68 - Vencedora), with control of weeds through the use of herbicides or weeding. The sowing of soybean was performed in 11/20/2009, at a spacing of 0.45 m between rows and 15 seeds per meter of furrow. The experimental design was a randomized block with 4 replicates, with plots at seven lines to fifty meter long. We evaluated the agronomic characteristics such as height of first pod, plant height, number of branches per plant, number of pods per plant, plant population, yield, 1000 grain weight of the R8 stage of culture. Was also assessed in biweekly samples from the 21 th day after germination, the dry matter of leaves, stems, pods and grains and content of macronutrients and nutritional status of this plant, by sampling leaves in full bloom. The results showed that: at 81 days after emergence, when plants are in the initial stage R5, it is gotten the highest total dry matter in transgenic and conventional varieties of soybeans, there is a greater concentration of N, P and K in the grains as they are approaching maturity, contrary to that observed for stems, leaves and pods, there is a significant... (Complete abstract click electronic access below)

4

Tofoli, Gustavo Radomille. "Efeito do tamanho do alvo e condições operacionais sobre a uniformidade de deposição de pulverizações em pré-emergência /." Botucatu : [s.n.], 2001. http://hdl.handle.net/11449/97245.

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Orientador: Edivaldo Domingues Velini
Banca: Carlos Gilberto Raetano
Banca: Dagoberto Martins
Resumo: Este trabalho teve como objetivo estudar o efeito do tamanho do alvo e condições operacionais sobre a uniformidade de deposição de pulverizações em pré-emergência. Duas barras pulverizadoras de mesmo modelo (12 m e espaçamento entre bicos de 0,5 m) sendo uma para cada tipo de bico.Dois tipos de bicos (jato cônico modelo JA- 1,5 e jato plano modelo API 110-02) testados com uma mesma velocidade de aplicação (4km/h). Para o preparo das caldas de pulverização foram utilizados: água, nitrato de potássio, nitrato de cálcio, sulfato de cobre e sulfato de zinco. Os alvos foram construídos de chapa de fórmica, que foram cortadas em placas quadradas com tamanho de 13 x 13 cm. Ao centro de 602 placas foram feitos orifícios de diversos tamanhos de diâmetro: 10,16 cm, 5,8 cm, 2,54 cm, 1,27 cm, 0,63 cm e 0,32 cm. Para cada tamanho de orifício foram feitas 117 repetições. Totalizando 702 placas. Os alvos foram posicionados no piso do terreno de maneira aleatória. Depois da pulverização, estes foram lavados com 25 ml de água deionizada, dando origem as amostras. Estas, depois de filtradas, foram analisadas em espectrofotômetro de plasma. As leituras de concentrações foram transformadas em volume ( l), e este divido pela área de cada círculo correspondente, resultando em dados de depósito em l/cm2. Os dados de depósitos foram transformados em % da média, e realizado os cálculos de freqüências acumuladas para cada tamanho de alvo. O modelo de Gompertz (y = e **(a-e**(-b-c*x))) foi utilizado para ajustar os dados e efetuar as análises de regressão, obtendo os valores de R2 (0,985 a 0,997) e um novo valor de freqüência acumulada para cada curva. Calculou-se os valores de média, mediana, moda, os percentis 1, 2, 5, 10, 20, 40, 60, 80, 90, 95, 98 e 99.e os coeficientes de variação para todos os diferentes tamanhos de alvo para os respectivos bicos... (Resumo completo, clicar acesso eletrônico abaixo).
Abstract: It were studied two types of nozzles. The first one is a conic jet nozzle model JÁ 1,5. The second type is a flat fan nozzle model API 110-02. The application speed was 4km/h. It were used two similar sprayers set with boons 12 m wide and nozzles spaced by 0,5m. The spray solution for the fan jet nozzle was prepared with water, potassium nitrate and copper sulfate. For the conic jet nozzle theses salts were replaced by calcium nitrate and zinc sulfate. The targets were made of formica foils cut into square plates of 13 cm x 13 cm. One hundred of these plates were used to estimate the drift. In all the other 702 plates (117 replications for each type of target) it were made central circular holes of different diameters: 10,16 cm, 5,8 cm, 2,54 cm, 1,27 cm, 0,63 cm and 0,32 cm. The targets were randomly arranged on the ground. After spraying and drying the spray solution, each target was washed with 25 ml of de-ionized water. These water samples were filtered and analyzed in plasma spectrophotometer. The concentrations of the tracers in the final volume of 25 mL allowed to calculate the deposits of both spray solutions (in L/cmø) in each target. These data were converted in to percent of the means for each nozzle type and target size. Frequency distribution curves were fitted to the data. The Gompertz (y=e**(a-e**(-b-c*x))) model provided the highest determination coefficients, ranging from 0,985 and 0,997. In addition to the Relative Standard Deviation (RSD%) it were estimated the values of the mean, the median, the mode and the 1, 2, 5, 10, 20, 40, 60, 80, 90, 95, 98 and 99 percents, using the frequency distribution curves. Among the central tendency measures, the mode, the median and the 1, 2, 5, 10, 20, 40, 60, 80, 90, 95, 98 and 99 percents allowed more precise comparisons of spray deposits of different nozzles in targets of several sizes; the mean is very sensitive... (Complete abstract, click electronic address below).
Mestre

5

Oliveira, Jefferson Anthony Gabriel de. "Matéria seca, teores de macronutrientes e produtividade de soja transgênica e não transgênica com diferentes manejos de plantas daninhas /." Ilha Solteira : [s.n.], 2011. http://hdl.handle.net/11449/98743.

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Orientador: Edson Lazarini
Banca: Salatiér Buzetti
Banca: Luiz Carlos Ferreira de Souza
Resumo: No contexto das grandes culturas produtoras de grãos, a soja foi a que mais cresceu em termos percentuais nos últimos 37 anos, tanto no Brasil quanto em nível mundial. O presente trabalho teve por objetivo verificar se há diferença entre variedades de soja transgênica e não transgênica quanto ao desenvolvimento vegetativo e reprodutivo através do acúmulo de matéria seca na parte aérea e dos teores de macronutrientes na matéria seca produzida, quando estas são submetidas à presença de herbicidas específicos para o controle de plantas daninhas. O experimento foi realizado na Fazenda de Ensino, Pesquisa e Extensão da Faculdade de Engenharia/UNESP - Campus de Ilha Solteira, localizada no município de Selvíria - MS. Os tratamentos foram compostos de duas variedades de soja transgênica (BRS Valiosa RR e BRS Favorita RR) e duas variedades convencionais (MGBR 46 - Conquista e MGBR 68 - Vencedora), com controle de plantas daninhas através de uso de herbicidas ou capinas. A semeadura da soja ocorreu no dia 20/11/2009, em um espaçamento de 0,45 m entrelinhas e 15 sementes por metro de sulco. O delineamento experimental utilizado foi o em blocos casualizados com 4 repetições, apresentando as parcelas, 7 linhas com 50 m de comprimento. Avaliaram-se as características agronômicas como: altura de inserção da primeira vagem; altura de plantas; número de ramos por planta; número de vagens por planta; população de plantas; produtividade de grãos; massa de 1000 grãos no estádio R8 da cultura. Também foi avaliado em amostragens quinzenais a partir do 21o dias após a germinação, a matéria seca de folhas, caules, vagens e grãos e o teor de macronutrientes nesta e o estado nutricional das plantas, através de amostragem foliar, no florescimento pleno. Os resultados obtidos perm itiram concluir que: aos 81 dias após emergência, quando as plantas encontram -se no... (Resumo completo, clicar acesso eletrônico abaixo)
Abstract: In the context of major grain-producing crops, soybean was grown the most in percentage terms over the past 37 years, both in Brazil and worldw ide. This study aimed to observe the differences between varieties of GM and non GM soya on the vegetative and reproductive development through the dry matter accumulation in shoots and macronutrient content in dry matter yield when they are subjected to t he presence of herbicides for weed control. The experiment was conducted at Faculdade de Engenharia/UNESP - Ilha Solteira, located in Selvíria county. The treatments consisted of two transgenic soybeans varieties (BRS Favorita and BRS Valiosa) and two conventional varieties (MGBR 46 - Conquista and MGBR 68 - Vencedora), with control of weeds through the use of herbicides or weeding. The sowing of soybean was performed in 11/20/2009, at a spacing of 0.45 m between rows and 15 seeds per meter of furrow. The experimental design was a randomized block with 4 replicates, with plots at seven lines to fifty meter long. We evaluated the agronomic characteristics such as height of first pod, plant height, number of branches per plant, number of pods per plant, plant population, yield, 1000 grain weight of the R8 stage of culture. Was also assessed in biweekly samples from the 21 th day after germination, the dry matter of leaves, stems, pods and grains and content of macronutrients and nutritional status of this plant, by sampling leaves in full bloom. The results showed that: at 81 days after emergence, when plants are in the initial stage R5, it is gotten the highest total dry matter in transgenic and conventional varieties of soybeans, there is a greater concentration of N, P and K in the grains as they are approaching maturity, contrary to that observed for stems, leaves and pods, there is a significant... (Complete abstract click electronic access below)
Mestre

6

Perim, Lucas [UNESP]. "Efeitos de óleos nas características físicas e químicas da calda de aplicação e na ação da atrazina." Universidade Estadual Paulista (UNESP), 2011. http://hdl.handle.net/11449/86377.

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Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
O uso de adjuvantes é adotado em todo o mundo, a fim de melhorar a eficácia das formulações de defensivos agrícolas, independente do tipo de alvo. Existem duas maneiras principais em que adjuvantes podem melhorar o desempenho final do produto. Em primeiro lugar, aumentando a quantidade de ingrediente ativo retido pelo alvo e, por outro, melhorando a sua absorção. O objetivo do presente trabalho foi avaliar os efeitos de óleos minerais e vegetais nas características físicas e químicas da calda de aplicação e na ação do herbicida atrazina (Gesaprim 500® SC). Os tratamentos estudados foram: atrazina, atrazina + Natur’l Óleo®; atrazina + Agr’Óleo®; atrazina + Assist® e testemunhas. Todos os adjuvantes foram acionados na proporção de 0.5% do volume da calda aplicada. As plantas indicadoras utilizadas nos estudos sobre os efeitos dos adjuvantes sobre a ação da atrazina foram: Ipomoea grandifolia,Brachiaria plantaginea, Merremia cissoides e Euphorbia heterophylla. Os parâmetros estudados foram: tensão superficial, pH, efeito do tempo de preparo da calda e do pH sobre a tensão superficial, evaporação da calda, tamanho de gotas, eficácia de controle de plantas daninhas, influência da chuva no controle da atrazina e a velocidade de absorção da atrazina com o uso do fluorômetro. O delineamento experimental utilizado foi em bloco casualizados, com quatro repetições. Portanto com os resultados obtidos pode-se concluir que uso de óleos vegetais ou minerais influenciou positivamente nas características físicas e químicas da calda de aplicação agindo diretamente na ação de herbicidas apresentando uma alta eficiência de controle das espécies estudadas
The adjuvants are used all over the world in order to improve the effectiveness of the herbicides formulations, independent of target. There are two main ways in which adjuvants can improve the performance of the final product. First, increasing the amount of active ingredient retained by the target and secondly, promoting its absorption. The objective of this study was to evaluate the effects of mineral and vegetable oils in physical and chemical characteristics of the application and action of the herbicide Gesaprim 500® (atrazine). The treatments studied were: atrazine; atrazine + Natur'l Óleo®; atrazine + Agr'Óleo®; atrazine + Assist® and check. All adjuvants were used at a rate of 0.5% of the volume of spray applied. The indicator plants used in studies on the effects of adjuvants on the action of atrazine were: Ipomoea grandifolia, Brachiaria plantaginea, Merremia cissoides and Euphorbia heterophylla. The parameters studied were: surface tension, pH, effect of time preparing the solutions and pH on surface tension, evaporation of the solution, droplet size, effective weed control, rain influence in weed control, the active ingredient absorption velocity using the fluorometer method. The experimental design was randomized blocks with four replications. So with the results we can conclude that the use of vegetable or mineral oils had a positive influence on physical and chemical characteristics and at the application acts the treatments showed a highly efficient control of the studied species

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Lucio, Felipe Ridolfo. "Ocorrência de espécies do gênero Digitaria em canaviais do centro oeste paulista e susceptibilidade de alguns acessos à herbicidas /." Jaboticabal : [s.n.], 2011. http://hdl.handle.net/11449/96817.

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Orientador: Robinson Antonio Pitelli
Banca: Ricardo Victória Filho
Banca: Roberto Estevão Bragion de Toledo
Resumo: O capim-colchão possui ampla colonização e distribuição geográfica, apresentando crescimento vigoroso mesmo em condições de estiagem e sua eficácia de controle não tem sido consistente, especialmente com herbicidas inibidores do Fotossistema II. As razões desta falta de consistência de controle são muitas, no entanto a existência de diferentes espécies pode ser considerada uma das principais. Tendo por base os relatos acima, o presente trabalho teve por objetivo identificar as diferentes espécies do complexo Digitaria spp e avaliar as respostas a ação de diferentes herbicidas inibidores de fotossíntese e associação com inibidores de carotenóides em estudos de curvas de dose resposta. Os herbicidas foram aplicados em pré-emergência com quatro repetições avaliando o controle até 60 DAA. Nos resultados obtidos, pode-se observar que existe diversidade de espécies dentro do gênero Digitaria em áreas cultivadas com cana-de-açúcar. Apenas nestes estudos foram identificadas D. horizontalis, D. nuda e D. ciliaris, as quais mostraram diferença na susceptibilidade aos herbicidas testados. Também foram verificadas diferenças entre os acessos dentro das espécies D. horizontalis e D. nuda. O fato de todas as plantas serem designadas com o nome popular de capim-colchão, estudos de controle, muitas vezes, podem mudar em função da espécie, gerando divergências na eficácias biológicas dos herbicidas sobre este complexo de espécies, pois não são incomuns em que as duas ou mais ocorram na mesma área
Abstract: The crabgrass has extensive colonization and geographical distribution, with strong growth even in drought conditions and the control performance has not been consistent, especially with Photosystem II inhibiting herbicides. The reasons for this lack of control consistenc are many, but the existence of different species can be considered a major. Based on the above reports, this aimed study to identify the different species of the Digitaria spp complex and evaluate responses to the action of several photosystem - II inhibiting herbicides in studies of dose-response curves. This study was conducted evaluating the performance of six bouts of crabgrass in the sugarcane in São Paulo State to herbicides: ametryn, diuron; ametryn + clomazone, diuron + hexazinone, diuron + hexazinone + mesotrione; hexazinone; metribuzim and tebuthiuron. Herbicides were applied in pre-emergence with four replications evaluating the control until 60 DAA. The results obtained, it can be seen that there really is diversity of species within the genus Digitaria in areas cultivated with sugarcane. Only in these studies were identified D. horizontalis, D. nuda and D. ciliares, which showed differences in susceptibility to herbicides. There were also significant differences among accessions within species D. horizontalis and D. nuda. The fact that all plants are designed with the popular name of crabgrass, the results of studies of chemical control, can often change depending on the species, leading to differences in biological effectiveness of herbicides on this species complex, as there are unusual in that two or more of them occur in the same area
Mestre

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Fleitz, Nicholas J. "COMPARISON OF SOIL-APPLIED AND POSTEMERGENCE HERBICIDES WITH MULTIPLE SITES OF HERBICIDAL ACTIVITY ON TWO POPULATIONS OF HERBICIDE-RESISTANT PALMER AMARANTH IN KENTUCKY." UKnowledge, 2018. https://uknowledge.uky.edu/pss_etds/99.

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With the introduction of herbicide resistant Palmer amaranth into Kentucky during the past 10 years there has been an increasing concern for effective control measures in grain production. Field trials were performed in 2016 and 2017 near Barlow and Paris, KY to determine efficacy of chemical control programs targeting herbicide resistant Palmer amaranth. Percent visual control, effects on plant density and plant height were measured in 2016 to determine treatment effectiveness. Treatments containing four different sites of herbicide activity achieved an average of 98% control. Treatments containing only 3, 2 or 1 site of activity only achieved 64%, 45% and 33% control, respectively. Within the long-chain fatty acid inhibitors herbicides in this study, pre-emergent applied pyroxasulfone provided greater control than S-metolachlor or acetochlor. Pyroxasulfone also provided greater control than the photosystem II herbicides atrazine and metribuzin. In 2017 PRE treatments consisting of three-way mixtures of flumioxazin + pyroxasulfone + chlorimuron or S-metolachlor + metribuzin + fomesafen followed by a POST herbicide treatment provided > 90% suppression of Palmer amaranth 4 weeks after trial initiation. Post-emergence treatments containing glyphosate + dicamba or glyphosate + 2,4-D following a soil-applied pre-emergent treatment achieved the most effective season-long control of Palmer amaranth.

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Karadogan, Burhan. "Studies towards the synthesis of the herbicidins and brevioxime." Thesis, University of Sussex, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.324184.

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Alves, Elza [UNESP]. "Seletividade de herbicidas para gramíneas forrageiras tropicais aplicados em pré e pós-emergência." Universidade Estadual Paulista (UNESP), 2001. http://hdl.handle.net/11449/86467.

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O presente trabalho constou de oito estudos, que foram realizados em casa-de-vegetação, nos quais avaliou-se a seletividade de diferentes herbicidas, aplicados em pré e pós-emergência, em algumas gramíneas forrageiras tropicais: Brachiaria decumbens Stapf cv. Basilisk, Brachiaria brizantha (Hochst) Stapf cv. Marandu, Panicum maximum Jacq cv. Tanzânia e Panicum maximum Jacq cv. Mombaça. Os herbicidas e doses utilizadas, em g i.a /ha, foram: (i) aplicados em pós-emergência, imazethapyr a 50 e 100, metsulfuron-methyl a 1,0 e 2,0, chlorimuron-ethyl a 7,5 e 15, nicosulfuron a 25 e 50, bentazon a 360 e 720, diclofop-metil 140 e 280, fenoxaprop-ethyl a 30 e 60, atrazine 1.500 e 3.000 e ametryne a 625 e 1.250 e (ii) aplicados em pré-emergência, alachlor a 1.680 e 3.360, metolachlor 1.200 e 2.400, diuron a 800 e 1.600, imazaquin a 75 e 150, imazapyr a 250 e 500, imazethapyr a 50 e 100, clomazone a 450 e 900, flumetsulam a 70 e 140, ametryne a 625 e 1.250, metribuzin a 525 e 1.050 e trifluralin a 900 e 1.800, além de testemunha sem aplicação de herbicidas. Utilizou-se delineamento inteiramente casualizado com os tratamentos em seis repetições. O consumo de calda de aplicação foi de 180 L/ha e a barra de aplicação continha quatro bicos de jato plano, tipo Teejet 110.02 espaçados de 0,50 m e posicionados a 0,50 m de altura dos vasos. Avaliou-se a intoxicação das plantas com uma escala visual de notas e, no final dos estudos, a altura e massa da matéria seca de plantas. Para o P. maximum cv. Mombaça, apenas os herbicidas imazaquin, na menor dose, imazethapyr e flumetsulam aplicados em pré-emergência, foram seletivos; os herbicidas metsulfuron-methyl, chlorimuron-ethyl, nicosulfuron, diclofop-methil, atrazine e ametryne aplicados em pós-emergência, foram visualmente seletivos para a cultivar Mombaça. Para o P. maximum cv. Tanzânia, os herbicidas... .
This research was accomplished in eight experiments, carried out in green house with the aim of to avaluating the selectivity of different herbicides, applied at pre and post-emergence, in the following tropical grass forages: Brachiaria decumbens Stapf cv. Basilisk, Brachiaria brizantha (Hochst) Stapf cv. Marandu, Panicum maximum Jacq cv. Tanzânia and Panicum maximum Jacq cv. Mombaça. The herbicides and doses (g a.e. /ha) acessed were (i) pulverized in post-emergence imazethapyr at 50 and 100, metsulfuron-methyl at 1,0 and 2,0, chlorimuron-ethyl at 7,5 and 15, nicosulfuron at 25 and 50, bentazon at 360 and 720, diclofop-metil at 140 and 280, fenoxaprop-ethyl at 30 and 60, atrazine at 1.500 and 3.000 and ametryne at 625 and 1.250, (ii) in pre-emegency, alachlor at 1.680 and 3.360, metolachlor at 1.200 and 2.400, diuron at 800 and 1.600, imazaquin at 75 and 150, imazapyr at 250 and 500, imazethapyr at 50 and 100, clomazone at 450 and 900, flumetsulam at 70 and 140, ametryne at 625 and 1.250, metribuzin at 525 and 1.050, trifluralin at 900 and 1.800, and a control plot. The experimental design was totally randomized, with the trataments with six replications. The application solution consumed was 180 L/ha and the application bar had four TEEJET 110.02 plain jet nozzle, at 0,5 m height from each other and at 0,5 m from the pulverized pots. The plants intoxication was evaluated by a visual grade scale. At the end of the study plant height and dry matter weight were evaluated. To P. maximum cv. Mombaça, only imazaquin at the lower dose, imazethapyr and flumetsulam applied in preemergency acted selectively. The post-emergence herbicides, metsulfuron-methyl, chlorimuron-ethyl, nicosulfuron, diclofop-methil, atrazine and ametryne were visually selectives to Mombaça cultivar. To P. maximum cv. Tanzânia, the post-emergence herbicides... (Complete abstract, click electronic address below).

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Maciel, Cleber Daniel de Goes [UNESP]. "Simulação do caminhamento de herbicidas em diferentes tipos e quantidades de palhadas utilizadas no sistema de plantio direto." Universidade Estadual Paulista (UNESP), 2001. http://hdl.handle.net/11449/86471.

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O presente trabalho teve como objetivos a quantificação da produção de biomassa seca das principais palhadas utilizadas como cobertura morta em sistemas de plantio direto, nos Estados do Paraná e Mato Grosso do Sul, bem como a avaliação das dinâmicas de molhamento e o comportamento de um traçante (simulando herbicidas), em diferentes coberturas mortas. No levantamento de biomassa foram amostrados os resíduos culturais de cevada (Hordeum vulgare L.), azevém (Lolium multiflorum), trigo (Triticum aestivum), aveias colhida e rolada (A. strigosa Schieb), milho (Zea mays), milheto (Penisetum americanum) e capim-braquiária (Brachiaria decumbens Stapf). As frequências acumuladas dos dados originais forma adequadamente ajustados segundo modelo de Gompertz, apresentando elevada precisão (Rø > 0,9873). Os restos culturais de milho e trigo apresentaram a maior e menor uniformidades de distribuição do peso de matéria seca, respectivamente. Os estudos de dinâmica de molhamento e recuperação do corante FDC-1 foram desenvolvidos através de simulação de chuva artificial sobre 3000, 6000 e 9000 Kg de matéria seca ha elevado a -1, utilizando sete tipos de palhas. Destacam-se em, ambos os casos, o ajuste adequado dos dados originais ao modelo de Mitscherlich (Rø > 0,9064 e > 0,9758). Os resultados indicam uma tendência de uniformização na retenção da água das chuva entre os diferentes tipos de palhadas, com o aumento da quantidade de cobertura utilizada. A formação de pontos secos associados a canais preferenciais de escorrimento, induzem a menor capacidade de embebição e retenção da água das chuvas pelas palhadas. As quantidades totais do corante FDC-1 que atingiram o solo foram relativamente uniformes, após precipitações entre 10 e 20 mm, independente do tipo e quantidade de palha, indicando que ambas características pouco interferem na capacidade do traçante em transpor a cobertura morta.
The presente work had as objectives to quantify the production of dry cultural residues of the man straws used as mulches in no-till systems, in the State of Paraná and Mato Grosso do Sul, as well as, to evaluate the wetting dynamic and the behavior of a dye (simulating herbicides), in different cultural residues. In the biomass survey it were evaluated the cultural residues (Kg of dry matter ha raised -1) of barley (Hordeum vulgare L.), perennial ryegrass (Lolium multiflorum), wheat (Triticum aestivum), harvested oat (Avena strigosa Schieb), rolled oat (Avena strigosa Schieb), corn (Zea mays), millet (Penisetum americanum) and braquiária grass (Brachiaria decumbens Stapf). The acumullated frequencies of the original data fitted well to the Gompertz model (Rø > 0,9064 e > 0,9758). The most and least uniform distribution of the cultural residues in the field were observed for corn and wheat respectivelly. The studies of the wetting dynamic and recovery of the dye FDC-1 were developed through simulation of artificial rain on 3000, 6000 and 9000 Kg of dry matter ha raised -1 of seven types of straws. The data fitted well to the Mitscherlich (Rø > 0,9064 and > 0,9758). The results indicated an uniformity tendency in the retention of the rain water among the different types of straws, with the increase of th amont of mulch. The formation fo dry points associated to preferential channels of running off, reduces the capacity of absorption and retention of the rain water by the straws. The total amounts of the dye FDC-1 that reached the soil were relatively uniform, after precipitations between 10 and 20 mm, independt of the type and amount of straw, indicating that both characteristics have minimum efects in the capacity of the dye in transporting the straw.

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Oliveira, Régis de Campos. "Respostas fotossintéticas de macroalgas lóticas do filo Chlorophyta submetidas à herbicidas à base de glifosato /." Rio Claro, 2018. http://hdl.handle.net/11449/152782.

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Orientador: Ciro Cesar Zanini Branco
Coorientador: Ciro Cesar Zanini Branco
Banca: Anna Isabel Nassar Bautista
Banca: Orlando Necchi Junior
Banca: Jorge Laço Portinho
Banca: Celia Leite Sant'Anna
Resumo: Herbicidas podem atingir ambientes aquáticos em regiões agrícolas, afetando os produtores primários e, consequentemente, a teia trófica e a ciclagem de nutrientes. Neste contexto, macroalgas lóticas do filo Chlorophyta foram coletadas, cultivadas, e submetidas a três concentrações diferentes (0,28; 3,5; e 6 mg L-1) de glifosato grau técnico e da formulação comercial Roundup®, e uma concentração (0,03 mg L-1) de ácido aminometilfosfônico (AMPA), além do grupo controle (0 mg L-1), para a avalição da resposta fotossintética através da evolução do oxigênio dissolvido, da fluorescência da clorofila a, e da concentração de clorofila a, realizados após um e sete dias de exposição ao herbicida. Os resultados mostram que, no geral, o Roundup® foi o herbicida que mais afetou negativamente as respostas fotossintéticas das macroalgas testadas, gerando danos ao aparato fotossintético, provocando reduções na taxa de fotossíntese líquida, e na concentração de clorofila a. O glifosato grau técnico e o AMPA também causaram efeitos inibitórios significativos para a resposta fotossintética, ainda que em uma escala menor. Em relação às concentrações utilizadas, a concentração de 0,28 mg L-1, que corresponde ao limite permitido pela legislação brasileira para a água destinada a irrigação e consumo animal, gerou reduções efetivas na resposta fotossintética de Nitella microcarpa var. wrightii (Roundup®) Nitella subglomerata (glifosato grau técnico e Roundup®) e Desmidium grevillei (Roundup®). A con... (Resumo completo, clicar acesso eletrônico abaixo)
Abstract: Herbicides can contaminate aquatic environments in agricultural regions, affecting primary producers and, consequently, the food web and nutrient cycling. In this context, lotic macroalgae of the phylum Chlorophyta were collected and cultivated in three different concentrations (0.28; 3.5; and 6 mg L-1) of technical grade glyphosate and Roundup®, and one concentration (0.03 mg L-1) of aminomethylphosphonic acid (AMPA), in addition to the control group (0 mg L-1). Were evaluated the photosynthetic response through the oxygen evolution, chlorophyll a fluorescence, and the chlorophyll a concentration, performed with one and seven days of exposure to the herbicide. The results show that, in general, Roundup® was the herbicide most negatively affected the photosynthetic responses of macroalgae tested, causing damage to the photosynthetic apparatus, reducing the photosynthetic rates, and chlorophyll a concentration. Technical grade glyphosate and AMPA likewise caused significant inhibitory effects on the photosynthetic response, although on a smaller scale. About the concentrations used, the 0.28 mg L-1, which correspond to the limit for Brazilian law in water for irrigation and animal consumption, led to effective reductions in the photosynthetic response of Nitella microcarpa var. wrightii (Roundup®) Nitella subglomerata (glyphosate technical grade and Roundup®) and Desmidium grevillei (Roundup®). The concentration of 0.03 mg L-1 used in the AMPA treatment also inhibited the phot... (Complete abstract click electronic access below)
Doutor

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de, Souza Rodrigues Juliana. "Resposta fisiológica de alface a subdoses de maturadores utilizados em cana-de-açucar /." Jaboticabal, 2019. http://hdl.handle.net/11449/191066.

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Orientador: Pedro Luis da Costa Aguiar Alves
Resumo: É prática comum durante o cultivo da cana-de-açúcar o uso de maturadores de forma antecipar a colheita. No entanto, considerando que pode haver cultivos próximos, como o de hortaliças, é importante ressaltar os cuidados necessários quando dá aplicação destes produtos, que é realizada por via aérea, a fim de evitar a deriva. Culturas sensíveis, como a da alface, podem sofrer efeitos deletérios. Sendo assim, objetivou-se com este trabalho avaliar o efeito da deriva dos maturadores glyphosate, trinexapac-ethyl e sulfometuron comumente utilizados em cana-de-açúcar no crescimento da alface ‘Lucy Brown’ e ‘Vanda’. O experimento foi instalado em ambiente aberto do Laboratório de Plantas Daninhas (LAPDA), UNESP/FCAV nos meses de outubro e novembro. Mudas de alface foram transplantadas para vaso com capacidade para 5 L, sendo cada planta a parcela experimental. O experimento foi constituído de 15 tratamentos estabelecidos no delineamento em blocos casualizados em esquema fatorial 3x5, com cinco repetições. O primeiro fator correspondeu aos maturadores e o segundo às subdoses, de forma a simular a deriva, sendo essas de 0, 3%, 6%, 9% e 12% da dose recomendada de cada produto, sendo aplicados quando as mudas apresentavam ao início da formação da cabeça, para a cultivar Lucy Brown e o estádio de 6 a 7 folhas para a cultivar Vanda. Após aplicação, as avaliações ocorreram aos 5, 10, 15 e 20 dias após aplicação (DAA). Foram realizadas avaliações visuais, com base na escala EWRC (1964), teor... (Resumo completo, clicar acesso eletrônico abaixo)
Abstract: It is common practice during the cultivation of sugarcane to use ripeners in order to anticipate the harvest. However, considering that there may be crops nearby, such as vegetables, it is important to emphasize the necessary care when applying these products, which is carried out by air, in order to avoid drifting. Sensitive crops, such as lettuce, can suffer deleterious effects. Therefore, the aim of this work was to evaluate the effect of the glyphosate, trinexapac-ethyl and sulfometuron ripening effects commonly used in sugarcane on 'Lucy Brown' and 'Vanda' lettuce growth. The experiment was installed in an open environment at the Laboratory of Weeds (LAPDA), UNESP / FCAV in the months of October and November. Lettuce seedlings were transplanted to a 5 L pot, each plant being the experimental plot. The experiment consisted of 15 treatments established in a randomized complete block design in a 3x5 factorial scheme, with five replications. The first factor corresponded to the ripeners and the second to the subdoses, in order to simulate the drift, being 0, 3%, 6%, 9% and 12% of the recommended dose of each product, being applied when the seedlings presented at the beginning of the head formation, for the Lucy Brown cultivar and the 6 to 7 leaf stage for the Vanda cultivar. After application, the evaluations occurred at 5, 10, 15 and 20 days after application (DAA). Visual evaluations were performed based on the EWRC scale (1964), chlorophyll content, quantum efficiency of ... (Complete abstract click electronic access below)
Mestre

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Maleki, Saber Haghighati. "Degradation of atrazine by soil consortia : characterization of enzymatically active fractions from cell bound and cell free enrichment cultures." Virtual Press, 1997. http://liblink.bsu.edu/uhtbin/catkey/1048376.

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Soil samples were collected from several corn fields with history of atrazine (herbicide) application. Samples were inoculated into Erlenmeyer flasks each containing 50m1 of minimal basal salts medium amended with 100 ppm atrazine as sole nitrogen source. Flasks were shaken at 200 rpm at ambient temperature and were examined daily for one week for microbial growth and/or disappearance of atrazine. Promising consortia were subcultured for further additional enrichments before characterization of potentially active protein (enzyme)fractions. Proteins from cell-free and cellbound fractions were compared for ability to denature atrazine. Following gel permeation chromatography, isolated protein fractions were examined for atrazinefound in the cell-bound fractions capable degrading degradation. Two were found in the cell-free fractions (approx. Mol. wts. 55kDa and 180kDa) and one (55 kDa) atrazine to hydroxyatrazine. Atrazine and its breakdown products (hydroxyatrazine in particular) were detected via HPLC using C18 and C8 columns with absorbance at 229 nm.
Department of Biology

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Latorre, Débora de Oliveira [UNESP]. "Levantamento da susceptibilidade de Conyza canadensis e resistencia cruzada em Amaranthus tuberculatus em Nebraska, Estados Unidos da America." Universidade Estadual Paulista (UNESP), 2017. http://hdl.handle.net/11449/156017.

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
Os herbicidas são um dos fatores mais importantes que vem consideravelmente contribuindo no aumento na proteção das culturas, devido sua inovação no controle de plantas daninhas ao longo dos últimos 70 anos. O uso continuo de um mesmo ingrediente ativo ou modo de ação impõe uma alta pressão de seleção em uma população de plantas daninhas e a seleção de indivíduos resistentes a herbicidas pode ocorrer. A intensidade da seleção imposta pelos herbicidas e a frequência inicial de indivíduos resistentes a herbicidas dentro de uma população de plantas daninhas são fatores chave importantes no processo de evolução da resistência. Fluxo gênico via pólen, sementes e propágulos vegetativos são uma potencial fonte de distribuição de resistência a herbicidas, como previamente reportado em Conyza canadensis e Amaranthus ssp. Conyza canadensis e Amaranthus ssp são potencialmente capazes de transferir genes que conferem resistência a herbicidas via pólen e/ou sementes, por produzirem pólen que pode ser disseminado a longas distancia e grande número de sementes. Os objetivos gerais dos estudos realizados foram caracterizar o nível de resistência de duas espécies de plantas daninhas de Nebraska, Estados Unidos da América. Um primeiro estudo em casa de vegetação foi conduzido para caracterizar o nível de resistência a glyphosate de populações de buva coletadas em áreas não cultivadas foi conduzido. Experimentos de dose-resposta com 9 doses de glyphosate e 28 populações de buva foram avaliados. Um segundo estudo em casa de vegetação foi conduzido para caracterizar o nível de uma população de caruru resistente a 2,4-D a diferentes formulações de herbicidas fenóxicos. De acordo com o primeiro estudo de dose-resposta, menos de sete por cento das populações de Conyza canadensis em áreas de pastagem próximas a áreas de cultivo expressaram “resistência prática” a glyphosate (plantas sobreviventes a dose de glyphosate mais usual em Nebraska – 1,260 g ae ha-1). Baseado em nossos resultados, foi detectado baixa frequência de resistência a glyphosate em populações de Conyza canadensis em áreas de pastagem de Nebraska, indicando que indivíduos resistentes a glyphosate dispersos das áreas de cultivo não são o biótipo predominante nessas áreas. Os resultados do segundo estudo mostraram que a população de Amarantus tuberculatus resistente a 2,4-D foi significativamente mais suscetíveis às formulações dos herbicidas Dicamba DGA, Dicamba DMA, Corasil, 2,4-DP, e 2,4-DP-p, enquanto sobreviveram a altas doses dos herbicidas 2,4-D 2EHE, 2,4-D EE, 2,4-DB, MCPB, MCPA, MCPA 2EHE, CMPP e CMPP-p.
Herbicides are one of the most important factors that have contributed to protect crop yields. This is due to innovative weed control over the last 70 years. The over-reliance on a single herbicide active ingredient or mode of action impose a high selection pressure on a weed population and the selection of herbicide-resistant individual plants may occur. The intensity of selection imposed by herbicides and the initial frequency of herbicide resistant in a weed population play a major role in the herbicide resistance evolution. Gene flow by pollen, seed, and vegetative propagules have the potential to move herbicide-resistant weed species, as reported previous reported in Conyza canadensis and Amaranthus genus. Conyza canadensis and Amaranthus tuberculatus are potentially able to proliferate herbicide resistance by pollen and/or seeds due to be prolific seed producer and its pollen are capable to be disseminated for long distances. The general objectives of these studies were to characterize the herbicide resistance level of two weed species in Nebraska, United States. A greenhouse study was performed to characterize the fold of glyphosate resistance in horseweed populations from non-crop areas. Dose-response experiments with 28 horseweed populations were evaluated across nine glyphosate rates. A second greenhouse study was performed to characterize the level of a 2,4-D-resistant waterhemp population resistance to various auxinic herbicides. According to the first dose-response study, less than seven percent of the rangeland Conyza canadensis populations screened expressed “practical” resistance to glyphosate (plants surviving to most common glyphosate rate used in Nebraska of 1,260g ae ha-1). Therefore, low frequency of GR in horseweed populations was detected in Nebraska rangeland indicating that GR individuals dispersed from row crops into rangeland are not the predominant biotype in these non-row crop areas. For the second study, the results showed that 2,4-D-WR population were significantly more sensitive to Dicamba DGA, Dicamba DMA, Corasil, 2,4-DP, and 2,4-DP-p herbicides formulations, whereas survived to the higher doses of 2,4-D 2EHE, 2,4-D EE, 2,4-DB, MCPB, MCPA, MCPA 2EHE, CMPP and CMPP-p. The founds on this studied showed the 2,4-D-WR population exhibits cross-resistance to 2,4-D 2EHE, 2,4-D EE, 2,4-DB, MCPB, MCPA, MCPA 2EHE, CMPP and CMPP-p herbicides.
006860/2015-00

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Perim, Lucas 1980. "Efeitos de óleos nas características físicas e químicas da calda de aplicação e na ação da atrazina /." Botucatu : [s.n.], 2011. http://hdl.handle.net/11449/86377.

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Resumo: O uso de adjuvantes é adotado em todo o mundo, a fim de melhorar a eficácia das formulações de defensivos agrícolas, independente do tipo de alvo. Existem duas maneiras principais em que adjuvantes podem melhorar o desempenho final do produto. Em primeiro lugar, aumentando a quantidade de ingrediente ativo retido pelo alvo e, por outro, melhorando a sua absorção. O objetivo do presente trabalho foi avaliar os efeitos de óleos minerais e vegetais nas características físicas e químicas da calda de aplicação e na ação do herbicida atrazina (Gesaprim 500® SC). Os tratamentos estudados foram: atrazina, atrazina + Natur'l Óleo®; atrazina + Agr'Óleo®; atrazina + Assist® e testemunhas. Todos os adjuvantes foram acionados na proporção de 0.5% do volume da calda aplicada. As plantas indicadoras utilizadas nos estudos sobre os efeitos dos adjuvantes sobre a ação da atrazina foram: Ipomoea grandifolia,Brachiaria plantaginea, Merremia cissoides e Euphorbia heterophylla. Os parâmetros estudados foram: tensão superficial, pH, efeito do tempo de preparo da calda e do pH sobre a tensão superficial, evaporação da calda, tamanho de gotas, eficácia de controle de plantas daninhas, influência da chuva no controle da atrazina e a velocidade de absorção da atrazina com o uso do fluorômetro. O delineamento experimental utilizado foi em bloco casualizados, com quatro repetições. Portanto com os resultados obtidos pode-se concluir que uso de óleos vegetais ou minerais influenciou positivamente nas características físicas e químicas da calda de aplicação agindo diretamente na ação de herbicidas apresentando uma alta eficiência de controle das espécies estudadas
Abstract: The adjuvants are used all over the world in order to improve the effectiveness of the herbicides formulations, independent of target. There are two main ways in which adjuvants can improve the performance of the final product. First, increasing the amount of active ingredient retained by the target and secondly, promoting its absorption. The objective of this study was to evaluate the effects of mineral and vegetable oils in physical and chemical characteristics of the application and action of the herbicide Gesaprim 500® (atrazine). The treatments studied were: atrazine; atrazine + Natur'l Óleo®; atrazine + Agr'Óleo®; atrazine + Assist® and check. All adjuvants were used at a rate of 0.5% of the volume of spray applied. The indicator plants used in studies on the effects of adjuvants on the action of atrazine were: Ipomoea grandifolia, Brachiaria plantaginea, Merremia cissoides and Euphorbia heterophylla. The parameters studied were: surface tension, pH, effect of time preparing the solutions and pH on surface tension, evaporation of the solution, droplet size, effective weed control, rain influence in weed control, the active ingredient absorption velocity using the fluorometer method. The experimental design was randomized blocks with four replications. So with the results we can conclude that the use of vegetable or mineral oils had a positive influence on physical and chemical characteristics and at the application acts the treatments showed a highly efficient control of the studied species
Orientador: Edivaldo Domingues Velini
Coorientador: Eduardo Negrisoli
Banca: Augusto Guerreiro Fontoura Costa
Banca: Caio Antonio Carbonari
Mestre

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Lucio, Felipe Ridolfo [UNESP]. "Ocorrência de espécies do gênero Digitaria em canaviais do centro oeste paulista e susceptibilidade de alguns acessos à herbicidas." Universidade Estadual Paulista (UNESP), 2011. http://hdl.handle.net/11449/96817.

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
Monsanto
O capim-colchão possui ampla colonização e distribuição geográfica, apresentando crescimento vigoroso mesmo em condições de estiagem e sua eficácia de controle não tem sido consistente, especialmente com herbicidas inibidores do Fotossistema II. As razões desta falta de consistência de controle são muitas, no entanto a existência de diferentes espécies pode ser considerada uma das principais. Tendo por base os relatos acima, o presente trabalho teve por objetivo identificar as diferentes espécies do complexo Digitaria spp e avaliar as respostas a ação de diferentes herbicidas inibidores de fotossíntese e associação com inibidores de carotenóides em estudos de curvas de dose resposta. Os herbicidas foram aplicados em pré-emergência com quatro repetições avaliando o controle até 60 DAA. Nos resultados obtidos, pode-se observar que existe diversidade de espécies dentro do gênero Digitaria em áreas cultivadas com cana-de-açúcar. Apenas nestes estudos foram identificadas D. horizontalis, D. nuda e D. ciliaris, as quais mostraram diferença na susceptibilidade aos herbicidas testados. Também foram verificadas diferenças entre os acessos dentro das espécies D. horizontalis e D. nuda. O fato de todas as plantas serem designadas com o nome popular de capim-colchão, estudos de controle, muitas vezes, podem mudar em função da espécie, gerando divergências na eficácias biológicas dos herbicidas sobre este complexo de espécies, pois não são incomuns em que as duas ou mais ocorram na mesma área
The crabgrass has extensive colonization and geographical distribution, with strong growth even in drought conditions and the control performance has not been consistent, especially with Photosystem II inhibiting herbicides. The reasons for this lack of control consistenc are many, but the existence of different species can be considered a major. Based on the above reports, this aimed study to identify the different species of the Digitaria spp complex and evaluate responses to the action of several photosystem – II inhibiting herbicides in studies of dose-response curves. This study was conducted evaluating the performance of six bouts of crabgrass in the sugarcane in São Paulo State to herbicides: ametryn, diuron; ametryn + clomazone, diuron + hexazinone, diuron + hexazinone + mesotrione; hexazinone; metribuzim and tebuthiuron. Herbicides were applied in pre-emergence with four replications evaluating the control until 60 DAA. The results obtained, it can be seen that there really is diversity of species within the genus Digitaria in areas cultivated with sugarcane. Only in these studies were identified D. horizontalis, D. nuda and D. ciliares, which showed differences in susceptibility to herbicides. There were also significant differences among accessions within species D. horizontalis and D. nuda. The fact that all plants are designed with the popular name of crabgrass, the results of studies of chemical control, can often change depending on the species, leading to differences in biological effectiveness of herbicides on this species complex, as there are unusual in that two or more of them occur in the same area

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Rademacher, William Hale. "Effects of prometryn applied in irrigation water on furrow irrigated cotton and residue persistence." Thesis, The University of Arizona, 1985. http://etd.library.arizona.edu/etd/GetFileServlet?file=file:///data1/pdf/etd/azu_e9791_1985_193_sip1_w.pdf&type=application/pdf.

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Potyka, Ingrid. "Emulsion-formulation of microbial herbicides." Thesis, University of Bristol, 1995. http://hdl.handle.net/1983/618a10ab-a6e4-49c4-bf4c-1b3c343c4135.

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Development of microbial herbicides is constrained by unreliability in the field where conditions are often sub-optimal for infection. Crucially, sufficient moisture, often dew, is required to establish infection. Two model systems, Colletotrichum dematium (Pers. ex Fr. ) Grove on Chenopodium album L. and Mycocentrospora acerina (Hartig) Deighton on Viola arvensis Murr., have been investigated and formulation requirements for each system identified, principally to reduce the dew period necessary for infection. Effects of adjuvants (surfactants, stickers and humectants) on spore germination and appressorium formation were investigated in vitro. Few were toxic and then, principally, at high concentration. The surfactants Tween 40,60 and 80 were compatible with both pathogens. Similarly, the stickers acacia, ghatti, guar, karaya, locust bean and xanthan gums and low viscosity alginic acid were all non-toxic as was the humectant glycerol. Each pathogen reacted differently to the adjuvants and any potential microbial herbicide will need individual matching of adjuvants to give an effective formulation. A working formulation (rapeseed oil-in-water (1: 10 v/v) emulsion using 0.1 % v/v Tween 40 as the emulsifier) was found to reduce the dew period requirement of M. acerina from 36 to 18 hours. The formulation protected spores from desiccation for 24 hours after application, or for 16 hours following a sub-optimum dew period occurring immediately after application. Scanning electron microscopy showed that the applied spores, and the developing mycelium, were immersed in the oil deposit. Transmission electron microscopy of sections through formulation deposits on the leaf revealed that some inversion of the emulsion, to form a water-inoil deposit, had occurred, suggesting a mechanism of protection against desiccation. The oil phase infiltrated the cortical intercellular spaces only when the leaf was infected. This intercellular oil contained more water than that on the leaf surface. Emulsion-formulation applied to run-off with an 'air brush', consistently gave significantly better weed control under sub-optimal dew conditions than a formulation of surfactant only. When applied with a conventional hydraulic nozzle at 400 1 ha" the emulsion was only occasionally superior to the surfactant alone. Such interactions require further in-depth investigation. The importance of correct inoculum placement for maximum effectiveness, independent of formulation type, was highlighted. Unless all meristems are killed, survivors quickly grow, despite the death of neighbouring leaves and petioles, and the weed suffers merely a growth check. Formulation as emulsion improved diseasee stablishmenta nd diseasee xpressioni n the target weedo nly in somec ircumstancesF. urther researchin to spraya pplicationm ethodsa ndt heir interactions with formulation, host and environment is clearly necessary

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Crosswhite, Franks S., William R. Feldman, and Edwin W. Minch. "Impact of Herbicides on Cacti." University of Arizona (Tucson, AZ), 1995. http://hdl.handle.net/10150/553076.

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The effects of nine herbicides were evaluated on five species of cacti selected to be congeneric with species classified as rare, threatened or endangered. Experimental plants were monitored at monthly intervals for survival and vigor for either six or sixteen months after herbicide treatment, depending on the overall condition of the untreated controls of each species. The severity of herbicide impact varied among active ingredients from lethality to virtually no effect. Some herbicides resulted in slow decline of treated plants, while for other herbicides most damage occurred within a short time after treatment. Some treated plants were observed to recover from herbicide damage, especially with paraquat. A wide variety of factors, both environmental as well as anatomical and physiological characteristics of the test plants are important in determining how a given plant will respond to herbicide exposure.

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Azania, Carlos Alberto Mathias [UNESP]. "Comparação de métodos para determinar a seletividade de herbicidas na cultura da cana-de-açúcar." Universidade Estadual Paulista (UNESP), 2004. http://hdl.handle.net/11449/105228.

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
Este trabalho objetivou comparar a precisão experimental do delineamento em blocos casualizados convencional e blocos casualizados com tratamentos testemunhas pareadas sobre a seletividade dos herbicidas azafenidin + hexazinone, isoxaflutole, metribuzin e diuron + hexazinone, aplicados em condição de pós-emergência inicial e tardia da cana-de-açúcar nas épocas das chuvas e de estiagem. Os experimentos foram conduzidos no município de Araras, SP, após a colheita com queima prévia do canavial, em soqueira de cana-de-açúcar (cv. RB835089), de terceiro e quarto corte, durante dois anos agrícolas (safras de 2001/2002 e 2002/2003), nas épocas das chuvas e de estiagem, respectivamente. O delineamento experimental foi o de blocos casualizados com cinco tratamentos e quatro repetições, acrescido de uma testemunha capinada para cada tratamento químico, dentro de cada bloco. Os herbicidas utilizados foram diuron + hexazinone (1170 + 330 g ha-1), azafenidin + hexazinone (192,5 + 247,5 g ha-1), metribuzin (1,92 L ha-1) e isoxaflutole (127,5 g ha-1) e testemunha capinada. Os herbicidas foram aplicados com equipamento costal pressurizado (CO2), munido de barra com três bicos Teejet DG (Drift Guardian) 110.02 VS, espaçados de 0,50 cm, a uma pressão de 35 libras pol-2 em volume de calda de aproximadamente 250 L ha-1. Concluiu-se que o delineamento em blocos com testemunhas pareadas possui maior precisão experimental que o delineamento em blocos ao acaso tradicional, quando as comparações envolvem as médias de tratamentos e testemunha; para a comparação de médias constatou-se maior precisão experimental para o teste t de Student e a desvantagem do delineamento em blocos com testemunhas pareadas é o aumento da área experimental, devido ao maior número de parcelas das testemunhas...
This research aimed to evaluate the effect of additional checks on experimental precision to each treatment of a randomized complete block design when determining selectivity of azafenidin + hexazinone, isoxaflutole, metribuzin and diuron + hexazinone on sugarcane, applied early and late postemergence in rainy and dry season. Field trials were carried out at Araras-SP, Brazil using sugarcane cv. RB835089 with burn pre-harvest system, during the rainy season of 2001 and the dry season of 2002. The treatments diuron + hexazinone (1170 + 330 g ha-1), azafenidin + hexazinone (192,5 + 247,5 g ha-1), metribuzin (1,92 L ha-1) e isoxaflutole (127,5 g ha-1) and hand-weeded correspondent checks for each treatment were arranged in a randomized complete block design with four replications. Larger experimental precision was achieved when additional checks where included in statistical analysis and so, compensated the practical disadvantage of increasing experimental area. Student's t test provided the best results for mean comparisons. In the rainy season and for early applications, only isoxaflutole reduced sugarcane production and caused injuries symptoms. Meanwhile, in late postemergence, whole treatments decreased sugarcane production, all except diuron + hexazinone, affected the technological characteristics estimated but only azafenidin + hexazinone caused injuries symptoms. During the dry season, early applications performed similarly to the checks but effects for all late postemergence treatments were detected, except in the case of yield and fluorescence index (Fv/Fm) estimations for metribuzin.

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Ballaminut, Carlos Eduardo Carneiro. "Seletividade da cultura do algodoeiro aos herbicidas Diuron, Clomazone, Trifloxysulfuron-sodium e Pyrithiobac-sodium." Universidade de São Paulo, 2009. http://www.teses.usp.br/teses/disponiveis/11/11136/tde-14122009-144354/.

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A utilização de herbicidas para o manejo químico de plantas daninhas é um dos métodos mais eficientes de controle utilizados atualmente. Entretanto, herbicidas considerados seletivos às culturas podem interferir no desenvolvimento vegetativo das plantas ou na produtividade final. Dessa forma, este estudo teve como objetivo avaliar o efeito dos quatro principais herbicidas utilizados na cultura do algodoeiro atualmente, dois utilizados em pré-emergência da cultura e plantas daninhas (Clomazone e Diuron) e dois utilizados em pós-emergência da cultura e plantas daninhas (Trifloxysulfuron-sodium e Pyrithiobac-sodium) nas cultivares Fibermax 966, DeltaOpal e Aroeira, principais cultivares utilizadas comercialmente, com baixo, médio e alto vigor vegetativo, respectivamente. O delineamento experimental adotado foi de blocos casualizados, com 4 repetições. Cada um dos blocos constou de 9 sub-parcelas para cada uma das 3 cultivares, totalizando 36 sub-parcelas. Nas sub-parcelas de cada cultivar foram distribuídos oito tratamentos herbicidas, além da testemunha, sendo esta mantida livre de plantas daninhas durante todo o ciclo da cultura através de capinas manuais. Foram avaliados os principais fatores de desenvolvimento das plantas de algodoeiro como altura de plantas, Índice de Área foliar (IAF), massa seca de folha e ramos, produtividade, massa de capulhos, germinação de sementes e qualidade da fibra. Tanto para os herbicidas pré-emergentes, como para os pós-emergentes, foram verificadas injúrias nas plantas de algodoeiro, principalmente nos tratamentos com maior dosagem (Diuron na dose de 2,0 kg ia/ha, Clomazone na dose de 600 g ia/ha, Trifloxysulfuronsodium na dose de 7.5g ia g/ha e Pyrithiobac-sodium na dose de 140g ia/ha), entretanto, estas foram temporárias, desaparecendo nas avaliações posteriores. Em relação ao efeito destas injúrias no desenvolvimento vegetativo, a cultivar Fibermax 966 apresentou redução no acúmulo de massa seca e IAF, ambos na segunda avaliação para os tratamentos de pós-emergentes na maior dose, entretanto, esta diminuição de crescimento não proporcionou efeito negativo na produtividade final, massa de capulhos, germinação ou qualidade da fibra. Para as demais cultivares, os tratamentos herbicidas pós-emergentes não causaram nenhuma redução no desenvolvimento vegetativo quando comparados com a testemunha, tão pouco para as características finais como produtividade e qualidade de fibra. Para os tratamentos herbicidas em pré-emergência, o herbicida Diuron na dose de 2,0 kg ia/ha causou as maiores cloroses nas cultivares analisadas, além de levar a um menor acúmulo de massa seca e produtividade final para a cultivar Aroeira, quando comparada ao tratamento com Clomazone. Para as demais cultivares, não foram verificados quaisquer efeitos em relação ao desenvolvimento vegetativo, produtividade final ou qualidade da fibra produzida.
The use of herbicides for weed chemical management is one of the most efficient methods used nowadays. However, herbicides considered selective to the crop can cause some problems to the vegetative development or to the final yield. This way, the study aimed to evaluate the effect of four of the main herbicides used in the cotton crop, two of them used as pre-emergent of the crop and weeds (Clomazone and Diuron) and two used as post-emergent of the crop and weeds (Trifloxysulfuron-sodium e Pyrithiobac-sodium) in the varieties Fibermax 966, DeltaOpal and Aroeira, the main varieties commercially grown, with low, medium and high vegetative development. The experimental design used was the randomized blocks, with 4 replications. Each one of the blocks had 9 sup-plots to each variety, with a final number of 36 sub-plots. In the subplots of each variety there were 8 herbicides treatments plus the control treatment, this one left without weed interference along all the crop development, using manual weed control. The main features evaluated were plants height, Leaf Area Index (LAI), dry matter, yield, balls weight, seed germination and fiber quality. For both, the pre-emergent herbicide treatments, and postemergent treatments, there were injuries in the cotton plants, mainly to the treatments with highest doses (Diuron 2,0 kg ia/ha, Clomazone 600 g ia/ha, Trifloxysulfuron-sodium 7.5g ia g/ha and Pyrithiobac-sodium 140g ia/ha), however, these injuries were temporary and were not present in future evaluations. Regarding the effect of the injuries to the vegetative development, the cultivar Fibermax 966 showed Leaf Area Index and dry matter reduction in the post-emergent treatments, both in the second evaluation to the treatments in the highest dose. This decrease in plant development did not impact final yield, balls weight, seed germination or fiber quality. To the other varieties, the post-emergent herbicide treatments did not lead any vegetative development reduction when compared to the control treatment, neither to the final characteristics as yield, fiber quality and seed germination. Para os tratamentos herbicidas em pré-emergência, o herbicida Diuron na maior dose causou as maiores cloroses nas cultivares analisadas, além de levar a um menor acúmulo de massa seca e produtividade final para a cultivar Aroeira, quando comparada ao tratamento com Clomazone. Para as demais cultivares, não foram verificados quaisquer efeitos em relação ao desenvolvimento vegetativo, produtividade final ou qualidade da fibra produzida. For the pre-emergent herbicide treatments, Diuron in the highest dose caused greater damage to the different materials, leading to dry matter reduction and final yield for the cultivar Aroeira, when compared to the Clomazone treatment. For the other cultivars, the treatment did not present any effects in plants development, final yield or fiber quality.

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Dores, Eliana Freire Gaspar de Carvalho [UNESP]. "Contaminação de águas superficiais e subterrâneas por pesticidas em Primavera do Leste, Mato Grosso." Universidade Estadual Paulista (UNESP), 2004. http://hdl.handle.net/11449/105654.

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Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
Motivado pela crescente preocupação no meio científico sobre a contaminação de recursos hídricos superficiais e subterrâneos por pesticidas e considerando a inexistência de estudos abrangentes sobre a questão em Mato Grosso, o presente estudo teve por objetivo geral avaliar a contaminação por herbicidas em águas em Primavera do Leste – MT e como objetivos específicos determinar as concentrações de herbicidas em amostras de água usada para consumo humano e avaliar a exposição da população consumidora a estes herbicidas e ainda determinar a concentrações dos herbicidas em águas superficiais e subterrâneas próximas a áreas de produção de algodão, fazendo uma avaliação do cenário de risco existente neste ambiente. Esta é uma região de intensa atividade agrícola mecanizada e usuária de grandes quantidades de pesticidas. Foi realizado levantamento do uso de pesticidas no entorno da cidade de Primavera do Leste; descrição do meio físico e levantamento de dados meteorológicos, que permitiram fazer uma análise preliminar do potencial de contaminação de águas superficiais e subterrâneas por pesticidas. A partir dessa análise, selecionaram-se os princípios ativos a serem analisados em amostras de água, sendo estes: atrazina e seus metabólitos desetilatrazina e desisopropilatrazina, simazina, metribuzim, metolacloro e trifluralina. Em seguida, foi feita a adaptação e validação do método de análise destas substâncias em água, a partir dos métodos citados na literatura. Para avaliação da contaminação por herbicidas nas águas usadas para consumo humano em Primavera do Leste, amostras de água de poços tubulares e de água superficial foram coletadas em três épocas diferentes, em 1998/1999: uma no final do período de seca; uma no início das chuvas e outra no final das chuvas. Dos herbicidas analisados, a metribuzim...
The present study was motivated by the growing concern among scientists about the contamination of aquatic environments, either superficial or underground, by pesticides used in agriculture. It aimed to assess the contamination by herbicides of drinking water in Primavera do Leste, MT and of superficial and groundwater in cotton crop areas, evaluating the risk scenario in this region. This is a region of intense mechanized agriculture activity where large amounts of pesticides are used. A survey about pesticide usage in the surroundings of the city of Primavera do Leste; a description of the physical environment and a survey of climate data were carried out, which allowed a preliminary assessment of the potential for contamination by pesticides of superficial and underground waters in the region to be done. The active ingredients to be analyzed – atrazine and its metabolites desethylatrazine and desisopropylatrazine, simazine, metribuzin, metolachlor and trifluralin – were selected based on this evaluation. Sequentially, an analytical method for these substances in water was adapted from published methods and validated. Water samples were collected in three different periods, in 1998/1999: one in the end of the dry season; one in the beginning of the rainy season (planting period); other in the end of the rainy season (harvest period). Among the analyzed herbicides, metribuzin was the more frequently detected one in the three sampling periods. In the second sampling (beginning of rain) a greater number of samples contaminated with at least one of the studied substances was found. Maximum concentrations were: 0,415 μg L-1 of DEA; 0,156 μg L-1 of atrazine; 0,138 μg L-1 of simazine; 0,882 μg L-1 of metribuzin and 1,732 μg L-1 of metolachlor. None of the analyzed pesticides were detected in levels higher than the limits established by USEPA, which allowed us to conclude that the presence...(Complete abstract click electronic access below)

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Elsayed, Omniea. "Biodegradation of chloroacetanilide herbicides in wetlands." Thesis, Strasbourg, 2015. http://www.theses.fr/2015STRAJ003/document.

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Les chloroacétanilides sont une famille d'herbicides largement utilisée en agriculture, et contribuent de ce fait à la pollution environnementale. Leur devenir, y compris dans les écosystèmes rédox-dynamiques récepteurs comme les zones humides, est encore mal compris. Dans ce travail, la dégradation microbienne de chloroacétanilides (métolachlore, acétochlore et l'alachlore) a été étudiée par des approches innovantes de chimie analytique et de biologie moléculaire, à l'échelle du laboratoire en utilisant des microcosmes en colonnes, et in situ dans des zones humides construites à ciel ouvert et conçues pour traiter les intrants chimiques issus de l'agriculture.Une nouvelle méthode d’analyse isotopique composés-spécifiques a été développée. Les résultats indiquent la biodégradation des chloroacétanilides dans les zones humides, également suggérée par la détection des produits de dégradation correspondants (acides éthane sulfonique et oxanilique). Dans les expériences en microcosme de laboratoire, les chloroacétanilides ont principalement été dégradés dans les zones anoxiques de la rhizosphère, suggèrant un rôle prépondérant des processus anaérobies. L'analyse par chromatographie chirale du métolachlore a en outre révélé la dégradation préférentielle de l'énantiomère S du métolachlore, confirmant l'importance des processus biologiques dans la dissipation des chloroacétanilides. Les corrélations qui ont pu être observées entre les changements de variables hydrochimiques et de conditions hydrauliques et des différences de composition bactérienne détectées par génotypage par polymorphisme de longueur des fragments de restriction (T-RFLP) et par pyroséquençage du gène ARNr 16S confirme le potentiel de bio-indicateurs basés sur l'ADN pour suivre le fonctionnement des écosystèmes.Sur la base de ce travail, la détection et l'identification des micro-organismes et des voies biochimiques responsables de la dégradation de chloroacétanilides dans les zones humides, ainsi que l'élaboration d'indicateurs génétiques bactériens pour le suivi de la dégradation de chloroacétanilides en zones humides, émergent comme autant d’objectifs de recherche à court-terme
Chloroacetanilide herbicides are widely used in agriculture, and thereby contribute to environmental pollution. Their fate, including in redox-dynamic receptor ecosystems such as wetlands, remains poorly understood. In this work, microbial degradation of chloroacetanilides (metolachlor, acetochlor and alachlor) was investigated by emerging chemical and molecular biological approaches, at the lab-scale using microcosm columns, and in situ, in outdoor constructed wetlands designed for the treatment of chemical pollutants originating from agriculture.A novel compound-specific isotope analysis (CSIA) method was developed, and the results indicated biodegradation of chloroacetanilides in wetlands, which was also suggested by detection of ethane sulfonic acid and oxanilic acid degradation products. In lab-scale wetland microcosms, chloroacetanilides were mainly degraded in anoxic rhizosphere zones, suggesting a predominant role of anaerobic processes. Chiral chromatographic analysis of metolachlor revealed preferential degradation of the (S) enantiomer of metolachlor, and further confirmed the role of biological processes in chloroacetanilide dissipation. Changes in hydrochemical variables and hydraulic conditions correlated with differences in wetland bacterial composition detected by terminal restriction fragment length polymorphism (T-RFLP) and pyrosequencing analyses of the bacterial 16S rRNA gene, confirming the potential of DNA-based bioindicators for follow-up of ecosystem functioning.On the basis of this work, detecting and identifying the microorganisms and biochemical pathways responsible for chloroacetanilide degradation in wetlands, as well as developing bacterial gene-based indicators of wetland functioning, emerge as research objectives for the near future

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Barnwell, Philip. "Graminicide antagonism by auxin-type herbicides." Thesis, Nottingham Trent University, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.290403.

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Adu-Tutu, Kwame Owusu. "Control of Striga using sulfonylurea herbicides." Thesis, University of Reading, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.292671.

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Umeda, K., and N. Lund. "New Postemergence Herbicides Evaluation in Cantaloupes." College of Agriculture and Life Sciences, University of Arizona (Tucson, AZ), 2001. http://hdl.handle.net/10150/214924.

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Halosulfuron applied POST with an adjuvant and ammonium sulfate was effective against lambsquarters and nutsedge. Rimsulfuron, flumetsulam, and thifensulfuron were effective against the pigweeds and purslane with minimal activity against lambsquarters. Halosulfuron and rimsulfuron were safe on melons and flumetsulam and thifensulfuron were marginally safe on cantaloupes. The combinations of these products may offer broader spectrum weed control.

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Umeda, Kai. "Comparison of Preemergence Herbicides in Spinach." College of Agriculture and Life Sciences, University of Arizona (Tucson, AZ), 2004. http://hdl.handle.net/10150/215256.

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Spinach exhibited progressively increased injury and crop stand reduction with increasing rates of s-metolachlor and dimethenamid-p. At the lowest rate applied, s-metolachlor at 0.38 lb ai/A caused minimal injury at 10% and slight stand reduction compared to the untreated check. Dimethenamid-p injured spinach 25% at the lowest rate applied and significant stand reduction was observed at 0.5 lb ai/A or greater. At equivalent rates, dimethenamid-p was more injurious to spinach than s-metolachlor.

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Kopec, David M., Jeff J. Gilbert, Steve Nolan, and Mohammed Pessarakli. "Perennial Ryegrass Transition Using Selected Herbicides." College of Agriculture and Life Sciences, University of Arizona (Tucson, AZ), 2009. http://hdl.handle.net/10150/216646.

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Thirteen herbicide treatments were applied on May 8, 2006, on a golf course fairway to assess transition and turf quality effects. Initial injury to perennial ryegrass was most extreme for Tranxit GTA when applied at 1.0 oz/prod/acre and Katana applied at 2.0 oz/prod/acre. Katana resulted in the total elimination of ryegrass and resulted in a fully necrotic canopy (straw cover) within two weeks after application to July 19, 2006 (72 Days after treatment). The development and persistence of necrotic leaf tissue of perennial ryegrass (straw) had the greatest impact on decreasing overall turfgrass quality ratings. No treatment went through the summer without some loss of quality at some point, including the untreated control. Certainty had little or no effect on transition when applied once at the rate of 1.25 oz/prod/acre. Surflan was not effective in ryegrass transition. The tank mix of Transit and nicosulfuron applied at the rate of 0.25 oz/prod./A each, produced an enhanced transition with nominal quality. In similar fashion, Monument applied at 0.35 oz./A produced an enhanced transition with nominal quality. A rates used in this test, other treatments had either too slow of a transition or had poor and extended low quality turf scores from rapid development of dead ryegrass (straw) and subsequent slow bermudagrass re-establishment. The UTC turf maintained a high percentage of living green ryegrass into the summer and 20% live ryegrass on August 8, 2006 which is roughly six weeks before the next overseeding.

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Umeda, Kai. "Evaluation of Herbicides for Khakiweed Control." College of Agriculture and Life Sciences, University of Arizona (Tucson, AZ), 2008. http://hdl.handle.net/10150/216657.

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Speedzone at 4.0 pt/A provided rapid control of khakiweed and gave 82% control at 17 days after treatment in one of three experiments. Spotlight at 1.0 pt/A alone was only effective at about 50%. BAS-514 and BAS-790 were not effective against khakiweed when applied alone. In a second experiment, sequential applications of Speedzone and Spotlight plus Turflon Ester provided exceptional control of greater than 95%. Initial applications of the POST applications that were combined with Gallery offered control of new emerging seedlings of khakiweed. Monument combined with Gallery gave decreased khakiweed control compared to Monument applied alone. An antagonistic effect could be occurring with the tank-mix combination of the two herbicides. Carfentrazone containing products, QuickSilver at 2 oz/A alone was not effective on khakiweed compared to the package mix product Speedzone. For the ALS-inhibiting herbicides, flazasulfuron and Certainty were the least effective while penoxsulam and Image were comparable to Monument in providing about 50% control.

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Agostineto, Mauricio Crestani. "Efeito de características da calda e estádio da corda-de-viola na eficácia de carfentrazone-ethyl e saflufenacil." Universidade do Estado de Santa Catarina, 2015. http://tede.udesc.br/handle/handle/1214.

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Weeds can cause significant yield losses in the agriculture, among them we can point out morning-glory species in many crops. To control that weed, we can use herbicides inhibiting protoporphyrinogen IX oxidase, in a selective way for a variety of crops. The objectives were: (i) to relate the response of Ipomoea hederifolia and Ipomoea quamoclit with the variation of doses of carfentrazone-ethyl and saflufenacil, of spray temperature at the moment of spraying, and of spray volume used; and (ii) to compare the efficacy of those herbicides sprayed isolately or mixed to glyphosate. Experiments were carried out from dose-response with carfentrazone-ethyl (0, 0.25, 0.5, 1, 2, 4, 5, 7.5, 10, 20, 35, 50, and 75 g ha-1 of the labeled herbicide Aurora®, 400 g a.i. L-1, FMC) and with saflufenacil (0, 0.125, 0.25, 0.5, 1, 2, 2.5, 5, 7.5, 10, 20, 35, and 50 g ha-1 of the labeled herbicide Heat®, 700 g a.i. kg-1, Basf), of variation of spray temperature (10 to 30 oC) and of variation of spraying volume (150 to 250 L ha-1). Evaluations were performed 14 days after spraying. In spite of showing differential response in relation to the dry mass accumulation, doses from 4 mL ha-1 of Aurora® and 5 g ha-1 of Heat® killed plants for both I. hederifolia and I. quamoclit. For carfentrazone-ethyl, increasing 10 L ha-1 in the spray volume reduced dry mass by 1.43% and 1.26% for I. hederifolia and I. quamoclit, respectively, while for saflufenacil, the reduction was by 12.73% and 11.30%, respectively for both species. For carfentrazone-ethyl, increasing 1 oC of spray temperature of reduced the dry mass by 0.22% and 0.35% for I. hederifolia and I. quamoclit, respectively, while for saflufenacil the reduction was by 0.56% and 0.30%, respectively for both species. The mix of carfentrazone-ethyl or saflufenacil with glyphosate provided a reduction by, at least, 10% greater of dry mass of I. hederifolia. We concluded that: carfentrazone-ethyl and saflufenacil are highly efficient to control I. hederifolia and I. quamoclit; increasing the spray volume and spray temperature provide greater efficacy to control both species, for both herbicides; and the mix with glyphosate improve the efficacy of controlling I. hederifolia for both herbicides
As plantas daninhas podem causar perdas significativas de produtividade na agricultura, dentre as quais se destacam as cordas-de-viola em diversos cultivos. Para seu controle podem ser utilizados herbicidas inibidores da enzima protoporfirinogênio IX oxidase, de maneira seletiva para diversos cultivos. Os objetivos foram: (i) relacionar a resposta de Ipomoea hederifolia e Ipomoea quamoclit com a variação da dose de carfentrazone-ethyl e saflufenacil, da temperatura da calda no momento da aplicação e do volume de calda aplicado; e (ii) comparar a eficácia destes herbicidas aplicados isoladamente e em mistura com glyphosate. Foram realizados experimentos de dose-resposta com carfentrazone-ethyl (0; 0,25; 0,5; 1; 2; 4; 5; 7,5; 10; 20; 35; 50 e 75 g ha-1 do produto comercial Aurora®, 400 g i.a. L-1, FMC) e com saflufenacil (0; 0,125; 0,25; 0,5; 1; 2; 2,5; 5; 7,5; 10; 20; 35 e 50 g ha-1 do produto comercial Heat®, 700 g i.a. kg-1, Basf), de variação de temperatura de calda (10 a 30 oC) e de variação de volume de calda (150 a 250 L ha-1). Avaliações de massa seca foram efetuadas 14 dias após a aplicação. Apesar de apresentarem resposta diferenciada quanto ao acúmulo de massa seca, doses a partir de 4 mL ha-1 de Aurora® e 5 g ha-1 de Heat® causaram a morte de plantas de I. hederifolia e I. quamoclit. Para carfentrazone-ethyl, o aumento de cada 10 L ha-1 no volume de calda aplicado reduziu a massa seca em 1,43% e 1,26% para I. hederifolia e I. quamoclit, respectivamente; enquanto para saflufenacil, a redução foi de 12,73% e 11,30%, respectivamente para essas espécies. Para carfentrazone-ethyl, o aumento de cada 1 oC na temperatura da calda reduziu a massa seca em 0,22% e 0,35% para I. hederifolia e I. quamoclit, respectivamente, enquanto para saflufenacil a redução foi de 0,56% e 0,30%, respectivamente para essas espécies. A mistura de carfentrazone-ethyl ou saflufenacil com glyphosate proporcionou redução de no mínimo 10% maior na massa seca de I. hederifolia. Conclui-se que: carfentrazone-ethyl e saflufenacil são altamente eficazes no controle de I. hederifolia e I. quamoclit; o aumento no volume de calda e na temperatura da calda proporcionam maior eficácia de controle dessas espécies, para ambos os herbicidas; e a mistura com glyphosate aumenta a eficácia de controle de I. hederifolia para ambos os herbicidas

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Xavier, Elouize. "Mecanismos de resistência e resposta aos herbicidas inibidores da ALS e da PROTOX em Euphorbia heterophylla L." Universidade Tecnológica Federal do Paraná, 2014. http://repositorio.utfpr.edu.br/jspui/handle/1/858.

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Euphorbia heterophylla (EPHHL) é uma importante planta daninha na agricultura mundial, e a resistência aos herbicidas dificulta ainda mais o seu controle. Assim, conhecer o nível de resistência, os seus mecanismos e a persistência destas populações resistentes nas lavouras é fundamental para o estabelecimento de estratégias de prevenção e manejo. Foram realizados experimentos, objetivando estudar a resistência de EPHHL aos herbicidas inibidores da ALS e PROTOX nos níveis bioquímico, de planta e populacional. O capítulo I objetivou confirmar a ocorrência de resistência aos inibidores da ALS e determinar se existe resistência cruzada aos herbicidas dos grupos químicos das imidazolinona, sulfoniluréia, pirimidil-benzoato e sulfonanilida em biótipos de EPHHL com resistência múltipla (ALS e PROTOX). O capítulo II objetivou confirmar a existência de novos biótipos de EPHHL com resistência a PROTOX nos estados do Paraná e Rondônia e determinar se existe resistência cruzada aos herbicidas dos grupos químicos difeniléteres, ftalamida, triazolinona, oxadiazol e pirimidinedione. O capítulo III objetivou comparar a atividade da enzima ALS de biótipos com resistência múltipla com biótipo suscetível, na ausência e na presença dos herbicidas inibidores enzimáticos imazapyr, imazethapyr e nicosulfuron. O capítulo IV objetivou caracterizar as atividades das enzimas peroxidase, catalase e superóxido dismutase, em biótipos de EPHHL suscetível e com resistência múltipla, pela aplicação de herbicidas inibidores da PROTOX. E o capítulo V objetivou identificar a persistência de populações resistentes aos inibidores da ALS de EPHHL em lavouras da região Sudoeste e Oeste do Paraná que apresentavam resistência em levantamento prévio e verificar a existência de resistência de EPHHL ao glifosato nestas lavouras. Os resultados destes capítulos confirmaram que os biótipos de EPHHL Bom Sucesso do Sul, Vitorino, Vilhena e Medianeira, com suspeita de resistência múltipla aos inibidores da ALS e PROTOX, apresentam a resistência aos herbicidas inibidores da ALS e da PROTOX e esta sendo cruzada aos 4 grupos químicos dos inibidores da ALS e aos 5 grupos químicos dos inibidores da PROTOX, testados. A resistência dos biótipos de EPHHL aos inibidores da ALS é atribuída à menor sensibilidade da enzima a estes herbicidas. A atividade das enzimas antioxidantes superóxido dismutase, peroxidase e catalase, para os biótipos resistentes e suscetível é dependente do herbicida e da dose utilizada e pode ser um dos mecanismos envolvidos na resistência aos inibidores da PROTOX. Os biótipos de EPHHL resistentes aos herbicidas inibidores da ALS permanecem nas áreas mesmo após longo período de constatação da resistência. Plantas de EPHHL com resistência aos inibidores da PROTOX também permanecem nas áreas, no entanto em menor frequência.
Euphorbia heterophylla (EPHHL) is an important weed species in world agriculture and its control becomes difficult due to herbicide resistance. To develop proper EPHHL management strategies it is important to know the level and the mechanisms of resistance and persistence of resistant populations in the fields. Experiments were carried out to study the resistance of EPHHL to ALS and PROTOX inhibitors at biochemical, plant and population levels. The objectives on chapter I are to confirm the occurrence of resistance to ALS inhibitors and to determine whether there is cross resistance to other chemical groups, such as imidazolinone, sulfonylurea, pyrimidinyl (thio) benzoates and triazolopyrimidines in biotypes of EPHHL with multiple resistance (ALS and PROTOX). The objectives on chapter II are to confirm the existence of new EPHHL biotypes with resistance PROTOX in the states of Paraná and Rondônia and to determine whether there is cross resistance to other chemical group, such as diphenyl ethers, N-phenyl-phthalimide, triazolinone, oxadiazole and pyrimidinedione. The objectives on chapter III are to evaluate the activity of the ALS enzyme from biotypes with multiple resistance and to compare it to the enzyme activity of susceptible population in the absence and in the presence of the herbicides imazapyr, imazethapyr and nicosulfuron. The objectives on chapter IV is to characterize the activity of several antioxidant enzymes, such as peroxidase, catalase and superoxide dismutase in EPHHL biotypes treated with PROTOXinhibiting herbicides. The objective on chapter V are to identify the persistence of EPHHL populations resistant to ALS inhibitors on fields from Southwest and Western Paraná that were resistant in a previous survey and check for resistance to glyphosate in EPHHL these crops. The results support the hypothesis that EPHHL biotypes from Bom Sucesso do Sul, Vitorino, Vilhena and Medianeira have multiple resistance to ALS and PROTOX inhibitors. Four EPHHL biotypes are cross-resistant to all ALS chemical groups and five populations are cross-resistant to the PROTOX inhibitors tested. The resistance to ALS inhibitors on the EPHHL biotypes evaluated is attributed to the lower sensitivity of the herbicide target enzyme. The activity of all antioxidant enzymes, both on the resistant and susceptible biotypes, is dependent of the herbicide and on the dose used and can be one of the mechanisms of resistance to PROTOX inhibitors. The biotypes of EPHHL resistant to ALS-inhibiting herbicides remain in the area even after long-term observation of resistance. The resistance to PROTOX inhibitors also remains in areas, but less frequently.

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Carvalho, Fernando Tadeu de [UNESP]. "Influência das características do sulco de plantio de cana-de-açúcar (Saccharum spp. L.) na uniformidade de deposição da pulverização de herbicidas em pré-emergência." Universidade Estadual Paulista (UNESP), 1999. http://hdl.handle.net/11449/100039.

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O presente trabalho foi desenvolvido com o objetivo de estimar a deposição da pulverização na superfície do sulco de plantio da cana-de-açúcar composto por patamar, parede e fundo do sulco, através de dois métodos de aplicação: tratorizada, com volume de calda de 200 L/ha e aérea, com volume de calda de 40 L/ha, com o avião voando no sentido da linha e perpendicularmente à linha de plantio. Analisou-se também a região da parede do sulco onde a deposição é mais irregular e identificou-se os tipos de sulcos mais adequados à aplicação de herbicidas. As análises do perfil do terreno de áreas das plantio de cana-de-açúcar, foram realizadas em nove usinas do Estado de São Paulo, sendo três em áreas de solo de textura arenosa, três em solo de textura média e três em solo de textura argilosa. Os dados foram coletados em dez sulcos seguidos e a média permitiu estabelecer o perfil médio do sulco de plantio de cada usina. A análise da deposição da calda foi realizada na Usina Unialco. A calda foi preparada diluindo-se sulfato de cobre em água, na dose de 1 kg / ha. As gotas da calda pulverizada, foram coletadas em lâminas de vidro, que foram distribuídas nos patamares, paredes e fundos dos sulcos dos vários sulcos avaliados. A análise da concentração de cobre nas lâminas, realizada no aparelho espectrofotômetro de absorção atômica, proporcionou a quantificação do volume de calda pulverizada nas diferentes regiões do sulco. Os dados foram analisados estatisticamente através do teste t. Observou-se que a irregularidade do terreno em áreas de plantio de cana-de-açúcar, desuniformiza a deposição da calda de pulverização. A quantidade de produto depositada na parede do sulco, depende do seu ângulo de inclinação e pode ser estimada multiplicando-se a dose aplicada pelo cosseno do...
The present work was developed with the objective of estimating the deposition of the spray solution in the surface of the furrow of plantation of the sugar-cane composition for landing, wall and fund of the furrow, through two application methods: for tractor, with 200 L/ha and aerial, with 40 L/ha, with the airplane flying in the sense of the line and perpendicular to the plantation line. It was also analyzed the area of the wall of the furrow where the deposition is more irregular and was identified the types of profiles more adapted to the herbicidas application. The analyses of the profile of the land of areas of sugar-cane plantation, they were accomplished in nine mills of the State of São Paulo, being three in areas of soil of sandy texture, three in soil of medium texture and three in soil of loamy texture. The data were collected in ten followed furrows, in each mill and the average of the ten furrows provided the medium profile of the furrow of plantation of each mill. The analysis of the deposition of the spray solution was accomplished in Mill Unialco. The solution was prepared being diluted copper sulfate, in water, in the dose of 1 kg / ha. The drops of the sprayed were collected in glass sheets, that were distributed in the landings, walls and funds of the furrows of the several appraised furrows. The analysis of the copper concentration in the sheets, accomplished in the apparel spectrum-fotometro of atomic absorption, provided the identification of the values of the volume of sprayed in the different areas of the furrow. The data were analyzed through the test t. Was observed that the irregularity of the land, in areas of plantation of sugar-cane doesn't make the deposition of the spray solution. The amount of product deposited in the wall of the furrow, depends on its inclination angle and it can...(Complete abstract click electronic access below)

34

Tanaka, Robson Hitoshi [UNESP]. "Eficácia de fluridone para o controle de Egeria spp. em caixas d'água e em represa de pequeno porte sem fluxo de água." Universidade Estadual Paulista (UNESP), 2001. http://hdl.handle.net/11449/86466.

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O presente projeto teve por objetivo avaliar a eficácia do herbicida fluridone para o controle das plantas aquáticas do gênero Egeria e seu efeito na qualidade da água em caixas d'água e em represa de pequeno porte, sem fluxo de água. No experimento em caixas d'água, foram avaliados os efeitos de doses crescentes de fluridone, nas formulações líquida e granulada, sobre as espécies Egeria densa Planchon e Egeria najas Planchon. Foram testadas as concentrações de 10, 20, 40, 80 e 150 ppb de fluridone na formulação líquida e 20, 40, 80 e 150 ppb na granulada. Utilizou-se 40 caixas d'água de fibra de vidro, com volume de 320 litros e cada uma constituiu uma parcela, com vinte plantas de cada espécie, cultivadas a partir de fragmentos apicais de 0,2 m de comprimento. O delineamento experimental utilizado foi o de blocos ao acaso, com dez tratamentos e quatro repetições. Realizou-se uma única aplicação, avaliando-se os sintomas de intoxicação das plantas aos 8, 15, 29, 35, 51 e 63 dias após a aplicação, realizada em junho de 1.998. Os resultados indicaram que o fluridone, nas concentrações de 80 e 150 ppb, em ambas as formulações, foi eficaz no controle das duas espécies. Nos tratamentos com concentrações de 10, 20 e 40 ppb na formulação líquida e de 20 e 40 ppb na formulação granulada, constatou-se a recuperação das plantas na última avaliação, realizada aos 63 dias após a aplicação do herbicida. Nestes tratamentos e nesta época, os resíduos de fluridone na água eram inferiores a 10 ppb. Nas condições do experimento, Egeria najas mostrou-se mais sensível que Egeria densa na primeira avaliação, porém o resultado final foi similar. No experimento em represa de pequeno porte sem fluxo de água, avaliou-se o efeito da manutenção das concentrações de fluridone no controle de Egeria najas... .
This project aimed to evaluate the efficacy of the herbicide fluridone to control aquatic plants from the genus Egeria and its effect on water quality in outdoor tanks and a small size pond. The experiment in tanks had the purpose to evaluate the effect of increasing rates of fluridone in two formulations, liquid and pellet, in the control of the species Egeria densa Planchon and Egeria najas Planchon. Concentrations of 10, 20, 40, 80 and 150 ppb of the liquid formulation and 20, 40, 80 and 150 ppb of the pellet were used. Forty fiberglass tanks with 320 liters of volume were used. In each tank, 20 plants of each species were planted using apical cuttings of 0,2 m. The experimental design used was randomized blocks, with 10 treatments and 4 replications. A single application of the herbicide was made in July 1998 and evaluations of symptoms were done at 8, 15, 29, 35, 51 and 63 days after the application. Results showed that fluridone, at 80 and 150 ppb of both liquid and pellet formulations, was efficient to control both species. Concentrations of 10, 20 and 40 ppb of the liquid formulation and 20 and 40 ppb of the pellet allowed the plants to regrowth at the last evaluation. In those treatments, fluridone residues in water, analyzed at 63 days after the herbicide application, were lower than 10 ppb. In the experimental condition of outdoor tanks, Egeria najas showed to be more sensitive to the herbicide in the former evaluation, but the final result was similar to that obtained for Egeria densa. In the experiment at the small size pond, the effect of keeping the fluridone concentration for an extended period of time on the control of Egeria najas was evaluated. One 1,980 square meter pond was treated seven times with fluridone, aiming to keep herbicide concentrations in water between 10 and 20 ppb... (Complete abstract, click electronic address below).

35

Chiquetti, Samanta Cristina. "Eficiencia da triplice lavagem em unidades de recebimento de embalagens de agrotoxicos." [s.n.], 2005. http://repositorio.unicamp.br/jspui/handle/REPOSIP/258152.

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Orientador: Egle Novaes Teixeira
Dissertação (mestrado) - Universidade Estadual de Campinas, Faculdade de Engenharia Civil, Arquitetura e Urbanismo
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Resumo: Os agrotóxicos têm sido usados na agricultura, mundialmente, para proteger as plantações e solos do ataque de pragas. As formulações de agrotóxicos devem ser acondicionadas em embalagens seguras e adequadas a cada tipo de produto. Após o uso da formulação, as embalagens vazias, contaminadas com resíduo de agrotóxicos, devem ser descartadas de maneira correta e segura, sendo a forma recomendada, no Brasil, a tríplice lavagem. Neste trabalho foi avaliada a eficiência da tríplice lavagem realizada em embalagens de agrotóxicos enviadas à Central de Recebimento de Embalagens Vazias, em Piracicaba, São Paulo, através da análise dos quatro ingredientes ativos mais comercializados nesta região: glifosato, MSMA, ametrina e tebutiurom. Foram analisadas, 75 embalagens de glifosato, 72 de MSMA, 70 de ametrina e 104 de tebutiurom. Os resultados demonstraram que 34,67 % das embalagens com glifosato, 58,33 % das com MSMA, 75,71 % das com ametrina e 73,07 % das com tebutiurom estavam em não conformidade com a norma vigente, ou seja, com um resíduo remanescente acima de 0,01 %. Concluiu-se que as embalagens analisadas apresentaram elevada percentagem dos princípios ativos, indicando que as tríplices lavagens foram executadas em desacordo à forma recomendada
Abstract: Pesticide formulations have been used in agriculture worldwide to protect the crops and soils from the attack of any pest. These formulations must be stored in safe containers proper to each kind of product. After use, the empty containers contaminated with pesticide residues must be disposed correctly and safely by triple rinse, the technical legislation recommended in Brazil. The aim of this study is to evaluate the efficiency of the triple rinse in empty pesticide containers that had been sent to the Collection site in Piracicaba region, São Paulo, through the analysis of the four main active ingredients traded in this region: gliphosate, MSMA, amethrin and tebuthiuron. In total, 75 gliphosate containers, 72 MSMA containers, 70 amethrin containers and 104 tebuthiuron containers were examined. The results were 34,67 % of the tebuthiuron containers, 58,33% of the MSMA containers, 75,71 % of the amethrin containers and 73,07 % of the tebuthiuron containers examined presented non-conformity with the actual technical legislation, that is, with residues above 0,01 %. This study concluded that the containers examined presented a high per cent of residue and that the triple rinse has not been executed according to the recommended technical legislation
Mestrado
Saneamento e Ambiente
Mestre em Engenharia Civil

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Fernandes, Glaura Scantamburlo Alves. "Toxidade reprodutiva do diuron em ratos machos adultos." [s.n.], 2005. http://repositorio.unicamp.br/jspui/handle/REPOSIP/318044.

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Abstract:

Orientador: Wilma De Grava Kempinas
Dissertação (mestrado) - Universidade Estadual de Campinas, Instituto de Campinas
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Resumo: O diuron (3-(3,4-diclorofenil)-1,1-dimetilurea) é um herbicida uréico cuja DL50 oral aguda em raios é igual a 3400 mg/Kg. É muito utilizado na agricultura e seus efeitos no organismo animal ainda são pouco conhecidos, principalmente no sistema reprodutor. O objetivo deste trabalho foi avaliar o possível efeito tóxico do diuron no sistema reprodutor masculino. Para tanto, ratos machos adultos (9 ou 10 animais por grupo) receberam durante trinta dias consecutivos, por gavage (via oral). 125 ou 250 mg/Kg/dia de diuron (grau técnico) dissolvido em óleo de milho. O grupo controle recebeu apenas o veículo, segundo o mesmo protocolo experimental. Ao final do tratamento, os órgãos reprodutores, fígado e rins foram coletados e pesados. Alguns dos testículos e epídídimos foram utilizados para a contagem de espermatozóides e amostras de fígado e rins para quantificar resíduos de diuron por cromatografia gasosa. Um outro grupo de animais foi avaliado quanto ao comportamento sexual e fertilidade, sendo acasalados com fêmeas em estro natural. Ao final do tratamento, resíduos de diuron foram encontrados no fígado de todos os ratos tratados e houve aumento do peso desse órgão nas duas doses. A exposição ao diuron não provocou diferenças estatisticamente significativas nas concentrações de testosterona. produção espermática diária, reservas espermáticas no epidídimo e morfologia dos espermatozóides. O comportamento sexual não se alterou devido ao tratamento, porém houve diminuição estatisticamente significativa do número de fetos produzidos por ratas que acasalaram com machos tratados com a menor dose. Concluiu-se que a dose de 125 mg/Kg de diuron administrada nessas condições experimentais, foi tóxica do ponto de vista reprodutivo.
Abstract: Diuron (3,4-dichlorophenyl)-1,1-dimethylurea) is a ureic herbicide whose acute oral LD50 in rats is 3400 mg/Kg. It is widely utilized in agriculture and its effects in the animal organism are still poorlv known, especially in the reproductive system. The aim of this work was to evaluate a possible toxic effect of diuron on the male reproductive system. For this, adult male rats (9 or 10 animals per group) received, for 30 consecutive days, by oral gavage. 125 or 250 mg/Kg/day of diuron (technical grade) dissolved in corn oil. The control group received only the vehicle, following the same experimental protocol. At the end of the treatment, male reproductive organs, liver and kidneys were collected and weighed. Some of the testis and epididymis were utilized for sperm counts, and samples of liver and kidneys to quantify diuron residues, by gas chromatography, Another group of animals was evaluated with respect to sexual behavior and fertility, being mated with females in natural estrous. At the end of the treatment, residues of diuron were found in the liver of all treated rats and there was an increase of the weight of this organ in both doses. The exposure to diuron did not provoke statistically significant differences in testosterone concentration, daily sperm production, sperm reserves in the epididymis or sperm morphology. Sexual behavior was not altered due to the treatment, however there was statistically significant diminution in the number of fetuses produced by rats that mated with males treated with the lower dose. It was concluded that the dose of 125 mg/Kg of diuron. administered in these experimental conditions, was toxic from the reproductive point of view.
Mestrado
Biologia Celular
Mestre em Biologia Celular e Estrutural

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Peixoto, André Luís de Castro. "Degradação do herbicida amicarbazona por fotólise direta e H2O2/UV em reator fotoquímico anular coaxial." Universidade de São Paulo, 2013. http://www.teses.usp.br/teses/disponiveis/3/3137/tde-10072014-235955/.

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A amicarbazona constitui-se em um herbicida do grupo das triazolinonas, desenvolvida para substituir a atrazina no mercado mundial. Diversas tecnologias têm sido estudadas objetivando a remoção de pesticidas de efluentes aquosos, procurando estudar os mecanismos de degradação envolvidos e o grau de toxicidade dos fotoprodutos gerados. Neste sentido, este trabalho tem como objetivo principal o estudo de degradação do princípio ativo amicarbazona, em solução aquosa, por fotólise direta, propondo estruturas químicas de produtos de transformação em um estudo teórico-fundamental. Foram avaliados parâmetros como concentração de herbicida, pH do meio reacional, concentração de oxigênio dissolvido, concentração de nitrato e de isopropanol como supressor de radicais livres. Dentre os parâmetros avaliados no processo de fotólise, o valor do pH do meio reacional influencia consideravelmente o mecanismo de fotodegradação do herbicida amicarbazona, favorecendo ou desfavorecendo a formação de determinado intermediário. Verificou-se que a molécula de amicarbazona gera como produto de degradação primário a molécula de amicarbazole, principalmente em meio ácido, como resultado de mecanismo de deaminação. Por sua vez, a utilização de processo UV/H2O2 foi capaz de proporcionar degradação completa da amicarbazona em tempo reacional máximo de 60 minutos. Contudo, mesmo com a utilização de agente oxidante auxiliar, não houve mineralização completa da amicarbazona, havendo 58% de redução de carbono orgânico dissolvido na melhor condição experimental estudada.
Amicarbazone is a triazolinone herbicide developed to substitute atrazine in the world market. Several technologies have been studied aiming at the removal of pesticides from wastewater, seeking to study the degradation mechanisms involved and the degree of toxicity of the photoproducts formed. In this context, the main goal of this work is to study the degradation of amicarbazone in aqueous solution by direct photolysis, suggesting possible chemical structures for the transformation products according to a theoretical and fundamental approach. Parameters such as herbicide concentration, pH, dissolved oxygen concentration, nitrate concentration, and propan-2-ol as a free radical scavenger were considered. Among the parameters studied in the photolysis process, the pH showed influence on the photochemical mechanism of amicarbazone degradation, favoring or not the formation of particular intermediates. It was found that the photolysis generates amicarbazole as the primary degradation product in acidic medium as a result of the deamination mechanism. The use of UV/H2O2 process enabled the complete degradation of amicarbazone in a reaction time of 60 minutes at most. However, even with the use of the auxiliary oxidant reactant, the complete mineralization of amicarbazone was not achieved, with 58% reduction of dissolved organic carbon in the best experimental condition studied.

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Maciel, Cleber Daniel de Goes. "Simulação do caminhamento de herbicidas em diferentes tipos e quantidades de palhadas utilizadas no sistema de plantio direto /." Botucatu : [s.n.], 2001. http://hdl.handle.net/11449/86471.

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Orientador: Edivaldo Domingues Velini
Banca: Silvio José Bicudo
Banca: Julio Cezar Durigan
Resumo: O presente trabalho teve como objetivos a quantificação da produção de biomassa seca das principais palhadas utilizadas como cobertura morta em sistemas de plantio direto, nos Estados do Paraná e Mato Grosso do Sul, bem como a avaliação das dinâmicas de molhamento e o comportamento de um traçante (simulando herbicidas), em diferentes coberturas mortas. No levantamento de biomassa foram amostrados os resíduos culturais de cevada (Hordeum vulgare L.), azevém (Lolium multiflorum), trigo (Triticum aestivum), aveias colhida e rolada (A. strigosa Schieb), milho (Zea mays), milheto (Penisetum americanum) e capim-braquiária (Brachiaria decumbens Stapf). As frequências acumuladas dos dados originais forma adequadamente ajustados segundo modelo de Gompertz, apresentando elevada precisão (Rø > 0,9873). Os restos culturais de milho e trigo apresentaram a maior e menor uniformidades de distribuição do peso de matéria seca, respectivamente. Os estudos de dinâmica de molhamento e recuperação do corante FDC-1 foram desenvolvidos através de simulação de chuva artificial sobre 3000, 6000 e 9000 Kg de matéria seca ha elevado a -1, utilizando sete tipos de palhas. Destacam-se em, ambos os casos, o ajuste adequado dos dados originais ao modelo de Mitscherlich (Rø > 0,9064 e > 0,9758). Os resultados indicam uma tendência de uniformização na retenção da água das chuva entre os diferentes tipos de palhadas, com o aumento da quantidade de cobertura utilizada. A formação de "pontos secos" associados a "canais preferenciais de escorrimento", induzem a menor capacidade de embebição e retenção da água das chuvas pelas palhadas. As quantidades totais do corante FDC-1 que atingiram o solo foram relativamente uniformes, após precipitações entre 10 e 20 mm, independente do tipo e quantidade de palha, indicando que ambas características pouco interferem na capacidade do traçante em transpor a cobertura morta.
Abstract: The presente work had as objectives to quantify the production of dry cultural residues of the man straws used as mulches in no-till systems, in the State of Paraná and Mato Grosso do Sul, as well as, to evaluate the wetting dynamic and the behavior of a dye (simulating herbicides), in different cultural residues. In the biomass survey it were evaluated the cultural residues (Kg of dry matter ha raised -1) of barley (Hordeum vulgare L.), perennial ryegrass (Lolium multiflorum), wheat (Triticum aestivum), harvested oat (Avena strigosa Schieb), rolled oat (Avena strigosa Schieb), corn (Zea mays), millet (Penisetum americanum) and braquiária grass (Brachiaria decumbens Stapf). The acumullated frequencies of the original data fitted well to the Gompertz model (Rø > 0,9064 e > 0,9758). The most and least uniform distribution of the cultural residues in the field were observed for corn and wheat respectivelly. The studies of the wetting dynamic and recovery of the dye FDC-1 were developed through simulation of artificial rain on 3000, 6000 and 9000 Kg of dry matter ha raised -1 of seven types of straws. The data fitted well to the Mitscherlich (Rø > 0,9064 and > 0,9758). The results indicated an uniformity tendency in the retention of the rain water among the different types of straws, with the increase of th amont of mulch. The formation fo "dry points" associated to "preferential channels of running off", reduces the capacity of absorption and retention of the rain water by the straws. The total amounts of the dye FDC-1 that reached the soil were relatively uniform, after precipitations between 10 and 20 mm, independt of the type and amount of straw, indicating that both characteristics have minimum efects in the capacity of the dye in transporting the straw.
Mestre

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Alves, Elza. "Seletividade de herbicidas para gramíneas forrageiras tropicais aplicados em pré e pós-emergência /." Botucatu : [s.n.], 2001. http://hdl.handle.net/11449/86467.

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Resumo: O presente trabalho constou de oito estudos, que foram realizados em casa-de-vegetação, nos quais avaliou-se a seletividade de diferentes herbicidas, aplicados em pré e pós-emergência, em algumas gramíneas forrageiras tropicais: Brachiaria decumbens Stapf cv. Basilisk, Brachiaria brizantha (Hochst) Stapf cv. Marandu, Panicum maximum Jacq cv. Tanzânia e Panicum maximum Jacq cv. Mombaça. Os herbicidas e doses utilizadas, em g i.a /ha, foram: (i) aplicados em pós-emergência, imazethapyr a 50 e 100, metsulfuron-methyl a 1,0 e 2,0, chlorimuron-ethyl a 7,5 e 15, nicosulfuron a 25 e 50, bentazon a 360 e 720, diclofop-metil 140 e 280, fenoxaprop-ethyl a 30 e 60, atrazine 1.500 e 3.000 e ametryne a 625 e 1.250 e (ii) aplicados em pré-emergência, alachlor a 1.680 e 3.360, metolachlor 1.200 e 2.400, diuron a 800 e 1.600, imazaquin a 75 e 150, imazapyr a 250 e 500, imazethapyr a 50 e 100, clomazone a 450 e 900, flumetsulam a 70 e 140, ametryne a 625 e 1.250, metribuzin a 525 e 1.050 e trifluralin a 900 e 1.800, além de testemunha sem aplicação de herbicidas. Utilizou-se delineamento inteiramente casualizado com os tratamentos em seis repetições. O consumo de calda de aplicação foi de 180 L/ha e a barra de aplicação continha quatro bicos de jato plano, tipo Teejet 110.02 espaçados de 0,50 m e posicionados a 0,50 m de altura dos vasos. Avaliou-se a intoxicação das plantas com uma escala visual de notas e, no final dos estudos, a altura e massa da matéria seca de plantas. Para o P. maximum cv. Mombaça, apenas os herbicidas imazaquin, na menor dose, imazethapyr e flumetsulam aplicados em pré-emergência, foram seletivos; os herbicidas metsulfuron-methyl, chlorimuron-ethyl, nicosulfuron, diclofop-methil, atrazine e ametryne aplicados em pós-emergência, foram visualmente seletivos para a cultivar Mombaça. Para o P. maximum cv. Tanzânia, os herbicidas... (Resumo completo, clicar acesso eletrônico abaixo).
Abstract: This research was accomplished in eight experiments, carried out in green house with the aim of to avaluating the selectivity of different herbicides, applied at pre and post-emergence, in the following tropical grass forages: Brachiaria decumbens Stapf cv. Basilisk, Brachiaria brizantha (Hochst) Stapf cv. Marandu, Panicum maximum Jacq cv. Tanzânia and Panicum maximum Jacq cv. Mombaça. The herbicides and doses (g a.e. /ha) acessed were (i) pulverized in post-emergence imazethapyr at 50 and 100, metsulfuron-methyl at 1,0 and 2,0, chlorimuron-ethyl at 7,5 and 15, nicosulfuron at 25 and 50, bentazon at 360 and 720, diclofop-metil at 140 and 280, fenoxaprop-ethyl at 30 and 60, atrazine at 1.500 and 3.000 and ametryne at 625 and 1.250, (ii) in pre-emegency, alachlor at 1.680 and 3.360, metolachlor at 1.200 and 2.400, diuron at 800 and 1.600, imazaquin at 75 and 150, imazapyr at 250 and 500, imazethapyr at 50 and 100, clomazone at 450 and 900, flumetsulam at 70 and 140, ametryne at 625 and 1.250, metribuzin at 525 and 1.050, trifluralin at 900 and 1.800, and a control plot. The experimental design was totally randomized, with the trataments with six replications. The application solution consumed was 180 L/ha and the application bar had four TEEJET 110.02 plain jet nozzle, at 0,5 m height from each other and at 0,5 m from the pulverized pots. The plants intoxication was evaluated by a visual grade scale. At the end of the study plant height and dry matter weight were evaluated. To P. maximum cv. Mombaça, only imazaquin at the lower dose, imazethapyr and flumetsulam applied in preemergency acted selectively. The post-emergence herbicides, metsulfuron-methyl, chlorimuron-ethyl, nicosulfuron, diclofop-methil, atrazine and ametryne were visually selectives to Mombaça cultivar. To P. maximum cv. Tanzânia, the post-emergence herbicides... (Complete abstract, click electronic address below).
Orientador: Dagoberto Martins
Coorientador: Francisco H. Dubbern de Souza
Banca: Pedro Luis da Costa A. Alves
Banca: Ciniro Costa
Mestre

40

Sanchez, Jessica Andrea Albañil. "Efeitos comparativos de herbicidas à base de glifosato sobre parâmetros oxidativos e qualidade espermática no peixe estuarino Jenynsia multidentata." reponame:Repositório Institucional da FURG, 2015. http://repositorio.furg.br/handle/1/6097.

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O uso de agrotóxicos vem aumentando nos últimos anos em decorrência da ampliação das áreas de plantio e presença de pragas mais resistentes. No Rio Grande do Sul / Brasil, as culturas de arroz são consideradas como as principais responsáveis pelo lançamento destes produtos nos corpos d’água, uma vez que o Estado concentra 61% da rizicultura irrigada do país. Dentre os herbicidas mais utilizados nestas plantações estão variações de Roundup® , cujo princípio ativo é o glifosato. O modo de ação do glifosato como herbicida consiste na inibição da EPSPS, uma enzima-chave envolvida na biossíntese de amionoácidos essenciais de vegetais. Apesar disso, alguns estudos têm demonstrado que o glifosato pode atingir diferentes espécies animais, consideradas como espécies não-alvo. Tendo em vista o exposto, o objetivo do trabalho foi determinar, comparativamente possíveis efeitos que as formulações à base de glifosato, Roundup Original® (RO), Roundup Transorb® (RT) e Roundup WG® (RWG), possam estar causando à peixes que habitam regiões onde estes herbicidas são lançados. Para tanto, foi feito um teste agudo de mortalidade utilizando-se as concentrações de 0,5, 1 e 5 mg.L-1 de glifosato, calculado a partir da sua concentração em cada formula, e escolheu-se aquela onde não houveram animais mortos para avaliação de parâmetros oxidativos e qualidade espermática de exemplares de Jenynsia multidentitata. Apenas na concentração de 0,5 mg.L-1 de glifosato não houve mortalidade em nenhuma formulação, entretanto, os resultados mostraram que acima desta, a RT provocou maior mortalidade. Quanto aos parâmetros oxidativos, houve um desequilíbrio entre as defesas antioxidantes e a geração de espécies reativas de oxigênio (EROs) com consequente dano no fígado dos peixes. Esta situação foi mais evidenciada nos animais expostos ao RO que apresentaram aumento de EROs e redução na capacidade antioxidante total às 24 h de teste o que se refletiu num aumento expressivo de lipoperoxidação (LPO) às 96 h. Com relação aos parâmetros de qualidade espermática, apenas as análises de motilidade, funcionalidade mitocondrial e integridade de DNA dos espermatozoides apresentaram-se sob efeito dos herbicidas, sendo a motilidade o parâmetro mais sensível, pois foi inibida pelo glifosato nas 3 formulações experimentais (RO, RT e RWG) em 24 e 96 h de exposição. Assim, podemos concluir que os herbicidas à base de glifosato causam danos à espécie de peixe J. multidentata, induzindo o estresse oxidativo e influenciando negativamente na reprodução por afetar a qualidade espermática dos machos. No que compete à análise comparativa das formulações, a RT parece ser a mais tóxica por provocar maior mortalidade, no entanto, quando em concentração não letal e ambientalmente relevante como é o caso de 0,5 mg.L-1 de glifosato, a RO, que contém maior quantidade dos chamados componentes “inertes”, provoca maior dano oxidativo, nos entanto as 3 formulações influenciam igualmente a qualidade espermática.
The use of pesticides has increased in recent years due to the expansion of planting areas and the presence of more resistant pests. In Rio Grande do Sul / Brazil, the rice crops are considered to be primarily responsible for the launch of these products in water bodies, since the state concentrates 61% of irrigated rice culture in the country. Among the most widely used herbicides in these plantations, are variations of Roundup®, whose active ingredient is glyphosate. The mode of action of glyphosate as an herbicide is the inhibition of EPSPS, a key enzyme involved in the biosynthesis of essential amionoacids in plants. Nevertheless, some studies have shown that glyphosate can achieve different animal species, considered as non-target species. In the view of the above, the purpose of this study was to determine comparatively the effects of the glyphosate-based formulations, Roundup Original® (RO), Roundup Transorb® (RT) and Roundup WG® (RWG), may be causing in fish that inhabit these regions where herbicides are released. For that, an acute mortality test was performed with 0.5, 1 e 5 mg.L-1 of glyphosate, calculated following its concentration in each formulation, and we chosen the one that did not cause mortalities in fish to evaluate oxidative parameters and sperm quality of Jenynsia multidentitata. Only at a concentration of 0.5 mg.L-1 of glyphosate, there was no mortality in any formulation, however, the results showed that above this, RT caused higher mortality. As for the oxidative parameters, there was an imbalance between antioxidant defenses and the generation of reactive oxygen species (ROS) with consequent damage in fish liver. This situation was more evident in animals exposed to RO, where was observed an increase in ROS and a decrease in total antioxidant capacity at 24 h of test, that reflected in a significant increase in LPO at 96 h. With respect to sperm quality, only the motility analysis, mitochondrial functionality and DNA integrity of sperm are presented under the effect of herbicides, being motility the most sensitive parameter because it was inhibited by glyphosate in the 3 experimental formulations (RO RT and RWG) at 24 and 96 h of exposure. In summary, we conclude that the glyphosate-based herbicides cause damage to the fish species J. multidentata, inducing oxidative stress and negatively influencing reproduction. As it is for the comparative analysis, the RT appears to be the most toxic since it causes increased mortality, however, when at non-lethal and environmentally relevant concentration such as 0.5 mg.L-1 of glyphosate, RO which contains higher amounts of components called "inert", causes increased oxidative damage, but the 3 formulations affects sperm quality in the same intensity.

41

Li, Hwei-Yiing. "Mechanisms of action and selectivity of the cyclohexen-one herbicide cycloxydim (BAS 517)." Diss., Virginia Tech, 1990. http://hdl.handle.net/10919/39985.

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The activity and the selectivity of cycloxydim {2-[1-(ethoxyimino)butylJ-3-hydroxy- 5-(2H-tetrahydrothiopyran-3-yl)-2-cyclohexen-l-one}, code designation BAS 517, were examined flIst with etiolated seedlings of com (Zea mays L.) and soybean [Glycine max (L.) Merr.]. Etiolated soybean seedlings were not affected by cycloxydim. The degree of growth inhibition of com varied with concentration of cycloxydim and incubation time. Compared to mesocotyls and coleoptiles, radicles of corn were the most sensitive to cycloxydim. Meristematic tissues appeared to be the site of action of cycloxydim as root meristems were the first to show symptoms. A band of reddening tissue developed at meristematic tips followed by the complete cessation of root growth. In a study comparing activities of technical grade and formulated cycloxydim and sethoxydim, {2-[ l-(ethoxyimino )butyl}- 5-[2-(ethylthio )propy11-3-hydroxy-2-cyclohexen-l-one}, formulated compounds were more potent than the technical grade chemicals without formulation additives. Technical sethoxydim was more potent than technical cycloxydim. Root tips excised from com and soybean seedlings were used subsequently for cycloxydim treatments. The activity and selectivity of cycloxydim expressed at the isolated root tip level were similar to those of cycloxydim bioassayed with whole seedlings. However, root tips appeared to be more sensitive than the whole seedlings. Injury at the tissue and cell levels of the 2-mm root tips that were treated with various concentrations of cycloxydim was examined after 24 hours incubation. Concentrations of 0.1, 1, and 10 μM cycloxydim caused severe cell vacuolization. A gradient of decreasing injury from epidermal cells toward the center of roots was observed. This pattern of injury appeared to reflect the penetration of cycloxydim into roots along a concentration gradient.
Ph. D.

42

Scruggs, Eric Brandon. "Control and Fecundity of Palmer Amaranth (Amaranthus palmeri) and Common Ragweed (Ambrosia artemisiifolia) from Soybean Herbicides Applied at Various Growth and Development Stages." Thesis, Virginia Tech, 2020. http://hdl.handle.net/10919/98467.

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Palmer amaranth (Amaranthus palmeri) and common ragweed (Ambrosia artemisiifolia) are two of the most troublesome weeds in soybean. Both weeds possess widespread resistance to glyphosate and acetolactate synthase (ALS) inhibiting herbicides resulting in the use of protoporphyrinogen oxidase- (PPO) inhibitors to control these biotypes, although PPO-resistant biotypes are increasing. New soybean herbicide-resistant trait technologies enable novel herbicide combinations. Combinations of two herbicide sites-of-action (SOA) improved control 19 to 25% and 14 to 19% of Palmer amaranth and common ragweed, respectively, versus using one SOA (mesotrione, dicamba, 2,4-D, or glufosinate alone). Seed production of 5 to 10 cm Palmer amaranth and common ragweed was reduced greater than 76% by fomesafen, auxin (dicamba and 2,4-D), or glufosinate containing treatments. Some weeds survived and set seed even when treated at the proper size. As weed size increased from 10 to 30 cm, control diminished and fecundity increased, underscoring the importance of proper herbicide application timing. Effective preemergence herbicides reduced the number of weeds present at the postemergence application compared to no treatment, reducing the likelihood of herbicide resistance development. Dicamba, 2,4-D, or glufosinate applied alone or auxin + glufosinate combinations reduced Palmer amaranth seed production greater than 95% when applied at first visible female inflorescence; this first report, in addition to previous reports on individual herbicides, indicates this application timing may be useful for soil seed bank management. This research informs mitigation of herbicide resistance spread and development.
Master of Science in Life Sciences
Over 30 million hectares of soybeans were harvested in 2019 in the United States, totaling over $31 billion in value. Two of the most troublesome weeds in soybean, Palmer amaranth (Amaranthus palmeri) and common ragweed (Ambrosia artemisiifolia) can cause even greater yield reductions in soybean, up to 79 to 95%, respectively. Frequent, exclusive, and repeated use of a single herbicide has led to multiple herbicide-resistance in both of these weeds. Co-applying two effective herbicides reduces the likelihood of resistance development. New soybean varieties have been genetically modified for resistance to herbicides that were previously unusable, allowing new herbicide combinations. Research was established to investigate these herbicide options to control and reduce seed production of Palmer amaranth and common ragweed with the overarching goal of mitigating herbicide resistance, particularly resistance to protoporphyrinogen oxidase (PPO) inhibiting herbicides, which are a critical part of herbicide options in soybean production. Preemergence herbicides are vital tools in herbicide programs, reducing the number of weeds present at a postemergence application and thereby reducing the risk of herbicide resistance development to the postemergence herbicide. PPO herbicides (flumioxazin, sulfentrazone, or fomesafen) applied preemergence reduced Palmer amaranth and common ragweed density at the postemergence application 82 to 89% and 53 to 94%, respectively. The preemergence herbicide used did not affect control four weeks after the postemergence herbicides were applied. Postemergence herbicides were applied targeting three weed heights: 5 to 10 cm (ideal), 10 to 20 cm, and 20 to 30 cm. Control decreased as weed height increased and larger weeds had greater biomass and seed production, underscoring the importance of proper herbicide application timing. The single site-of-action treatments dicamba, 2,4-D, glufosinate, or fomesafen resulted in greater than 85 and 92% morality of 5 to 10 cm Palmer amaranth and common ragweed, respectively. Palmer amaranth and common ragweed control improved by 19 to 25% and 14 to 19%, respectively, when using two herbicide sites-of-action increased versus using one SOA (mesotrione, dicamba, 2,4-D, or glufosinate alone). The use of two herbicide sites of action resulted in maximum biomass reductions, depending on weed height, of 57 to 96% and 73 to 85% for Palmer amaranth and common ragweed, respectively. Dicamba, 2,4-D, glufosinate alone and in combination with fomesafen reduced seed production (relative to the nontreated) of 5 to 10 cm Palmer amaranth and common ragweed greater than 98 and 76%, respectively. Dicamba, 2,4-D, and glufosinate applied alone or auxin (dicamba and 2,4-D) and glufosinate combinations reduced Palmer amaranth seed production greater than 95% when applied at first visible female inflorescence. This indicates that these herbicides may be useful in soil weed seed bank management. This research reinforces the utility of PPO herbicides for preemergence control and their efficacy postemergence when combined with another effective herbicide, a practice known to reduce herbicide resistance development. This research also reinforces the potential for dicamba, 2,4-D, or glufosinate to reduce weed seed production when applied at a delayed timing. Future research should investigate the progeny of these weeds treated with herbicides at a delayed timing to evaluate the potential for this practice to reduce herbicide resistance development.

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Bevilaqua, Natalia da Cunha. "Dinâmica e ação do nicosulfuron em híbridos de milho /." Botucatu, 2019. http://hdl.handle.net/11449/181829.

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Orientador: Caio Antonio Carbonari
Banca: Edivaldo Domingues Velini
Banca: Natália Corniani
Resumo: O herbicida nicosulfuron se destaca entre os principais utilizados em pós-emergência na cultura do milho. Dentre as tecnologias disponíveis no mercado, alguns híbridos podem ser considerados tolerantes ao nicosulfuron, e essa sensibilidade diferencial está relacionada com o ambiente, o estádio de desenvolvimento da planta e a dose de herbicida utilizada. A seletividade de herbicidas é geralmente determinada em função da fitointoxicação e do efeito do produto nas características morfológicas e fisiológicas das plantas. De modo que o objetivo do trabalho foi determinar a sensibilidade de híbridos de milho ao herbicida nicosulfuron por meio de marcadores bioquímicos. O primeiro experimento foi conduzido em casa-de-vegetação com delineamento experimental inteiramente casualizado com 4 repetições em esquema fatorial 4 x 2 (híbridos x doses), o herbicida foi aplicado nas doses 0 e 120 g i.a. ha-1 quando as plantas se encontravam no estádio fenológico V3. Foram realizadas avaliações da taxa de transporte de elétrons (ETR), fitointoxicação e altura aos 1, 3, 7 e 14 dias após a aplicação (DAA). Aos 14 DAA as plantas foram coletadas para determinação da massa seca. Dentre os híbridos utilizados selecionou-se o mais sensível e o mais tolerante para a realização de análises de determinação dos teores do ácido aminobutírico, e dos aminoácidos valina, leucina e isoleucina, nesses mesmos períodos de avaliação. O segundo experimento foi disposto em delineamento inteiramente casualizado com 5... (Resumo completo, clicar acesso eletrônico abaixo)
Abstract: Nicosulfuron stands out among the principal post-emergent herbicides used in the maize crop. Among the commercial technologies available, there are some hybrids considered tolerant to this molecule and can present a differential sensitivity, process which is related to the environment, growth stage and herbicide dose. The objective of the study was to determine the sensitivity of corn hybrids to the herbicide nicosulfuron by means of biochemical markers. The first experiment was carried out under greenhouse conditions in a completely randomized design with four replications in a factorial scheme 4 x 2 (hybrids x doses). The herbicide was applied at 0 and 120 g a.i. ha-1, when the plants were in the V3 stage. Electron transport rate (ETR), phytointoxication and plant height were evaluated at 1, 3, 7 and 14 days after treatment (DAT). Plants were collected at 14 DAT to determine its dry weight. The most sensitive and tolerant hybrids were selected to determinate the content of 2-aminobutyric acid and valine, leucine and isoleucine amino acids, in the same evaluation period. The second experiment was arranged in a completely randomized design with five replications in a factorial scheme 8 x 2 (hybrids x doses), the nicosulfuron was applied at 0 and 120 g a.i. ha-1. The experiment was conducted in different periods, for V2 and V6 maize growing stage. One day after the herbicide application, the plants were collected to determine the content of nicosulfuron, 2-aminobutyric and quinic acid, as well as valine, leucine and isoleucine amino acids. During the experiment, the ETR was evaluated at 1, 7, 10, 14, 21 and 28 DAT, and the variables plant height and phytointoxication at 7, 14, 21 and 28 DAT. At 7 DAT the chlorophyll content was determined. Plants were collected at 28 DAT to determine the shoot dry weight. In the first experiment, the collection of the plants one day after application was considered the ...
Mestre

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Ranasinghe, Sanjaya. "Role of herbicides in longleaf pine flatwoods restoration pine growth, understory vegetation response and fate of applied herbicides /." [Gainesville, Fla.] : University of Florida, 2003. http://purl.fcla.edu/fcla/etd/UFE0001443.

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45

Diesel, Francielli. "Persistência no solo, seletividade para espécies cultivadas e interação de saflufenacil com herbicidas causadores de estresse oxidativo." Universidade Tecnológica Federal do Paraná, 2013. http://repositorio.utfpr.edu.br/jspui/handle/1/526.

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CAPES
Saflufenacil é um novo herbicida que está sendo introduzido comercialmente no Brasil. Muitos fatores são necessários para que um herbicida tenha sucesso comercial, dentre eles destaca-se a seletividade para culturas de interesse, eficácia sobre espécies daninhas e segurança no ambiente. Dois experimentos foram conduzidos a campo e quatro em casa-de-vegetação. No primeiro estudo foram testados sete períodos de semeadura de feijão após a aplicação do herbicida (0, 5, 10, 15, 25, 35 e 50 DAA), na ausência e presença de herbicida saflufenacil (0 e 29,4 g i.a. ha-1). No segundo estudo, duas concentrações de saflufenacil (0; 14,7 e 29,4 g i.a. ha-1) foram testadas em dez cultivares de feijão. Para ambos os testes, foram avaliados o estande, estatura de plantas e componentes de rendimento. O primeiro bioensaio foi realizado em esquema triifatorial 8 x 5 x 4 , sendo o primeiro fator as concentrações de saflufenacil (0; 2,45; 4,9; 9,8; 14,7; 19,6; 24,5 e 29,4 g i.a. ha-1), o segundo as espécies bioindicadoras pepino, melancia, cabotiá, abobrinha e beterraba. Realizaram-se avaliações de estande e estatura de planta, massas das partes aéreas verde (MPAV) e seca (MPAS) e o terceiro fator períodos de avaliação (5, 10, 15 e 20 DAS). O segundo e terceiro bioensaios foram realizados simultaneamente, sendo os tratamentos constituídos pelas épocas de coleta do solo após a aplicação de saflufenacil (29,4 g i.a. ha-1) (0, 5, 10, 15, 25, 35, 50 e 100 dias após aplicação). Em um deles foi utilizado o pepino e no outro a beterraba como bioindicadores da presença de saflufenacil no solo. Foram determinadas as mesmas variáveis do primeiro bioensaio. Os tratamentos foram saflufenacil (0; 0,35; 0,7; 1,4; 2,1 e 2,8 g i.a. ha-1) aplicado de forma isolada ou associada ao paraquat (0, 1 e 3 g ha-1), metribuzin (0; 38,4 e 105,6 g i.a. ha-1) e clomazone (0, 288 e 504 g i.a. ha-1). Foram realizadas determinações de controle visual, MPAV e MPAS. A aplicação de saflufenacil em pré-emergência requer intervalo entre 10 e 25 dias após sua aplicação para ser realizada a semeadura da cultivar de feijão IPR-Tiziu. A cultivar Talismã apresentou maior tolerância a saflufenacil, enquanto a cultivar Jalo Precoce apresentou maior sensibilidade ao herbicida. As espécies que apresentaram maior sensibilidade ao saflufenacil foram o pepino e a beterraba. A persistência do saflufenacil em Latossolo Vermelho distroférrico, determinada por bioensaio com pepino e beterraba, situou-se entre 25 e 35 dias após a aplicação do herbicida. Para a variável controle de A. tenella, houve sinergismo para as associações das maiores doses de saflufenacil com paraquat e metribuzin, mas não com clomazone. Para a MPAS, todas as associações foram sinérgicas, indepententemente do herbicida ou da dose empregada.
Saflufenacil is a new herbicide which is being deployed commercially in Brazil. Many factors are necessary toward successful of commercially herbicide, among them stands out the selectivity for interests crops, the effectiveness under weed species and the environment safety. In the first one were experienced seven periods of sowing bean after saflufenacil application (0, 5, 10, 15, 25, 35 e 50 AHA) in the absence and presence of saflufenacil herbicide (0 e 29,4 g a.i. ha-1). In the second one two saflufenacil concentrations (0; 14,7 e 29,4 g a.i. ha-1) were tested into ten bean cultivars. For both tests were determined the stand, plant high, yield and yield components. The first bioassay was carried out in a completely randomized design (CRD) with three replications in a factorial design 8 x 5 x 4, where the first factor is saflufenacil concentrations (0, 2.45, 4.9, 9.8, 14.7, 19.6, 24, 5 and 29.4 g ai ha-1), the second the bioindicators cucumber, watermelon, cabotiá, summer squash and beets the third factor periods (5, 10, 15 and 20 DAS). Evaluations were performed booth and plant height, mass of fresh (MPAV) and dry (MPAS) shoots. The second and third bioassays were conducted simultaneously, and the treatments consisted of soil sampling times after saflufenacil spraying (29.4 g ai ha-1) (0, 5, 10, 15, 25, 35 , 50 and 100 days). In one bioassay we used cucumber and in the second we used beet as biomarkers for the presence of saflufenacil the soil. The same variables were determined from the first bioassay. Treatments were saflufenacil (0, 0.35, 0.7, 1.4, 2.1 and 2.8 g ai ha-1) applied alone or combined with paraquat (0, 1 and 3 g ai ha-1 ), metribuzin (0, 38.4 and 105.6 g ai ha-1) and clomazone (0, 288 and 504 g ai ha-1). The evaluated variables were visual control, and MPAV MPAS. The application of pre-emergence saflufenacil requires between 10 and 25 days after application to be performed seeding bean cultivar IPR-Tiziu. The BRS Talismã cultivar showed higher tolerance to saflufenacil, while the cultivar Jalo Precoce showed greater sensitivity to the herbicide. The species with the highest sensitivity to saflufenacil were cucumber and beet. The persistence of saflufenacil in Latossolo Vermelho distroférrico determined by bioassay with cucumber and beets, was between 25 and 35 days after herbicide application. For the A. tenella control, there was synergism for combinations saflufenacil with higher doses of paraquat and metribuzin, but not with clomazone. For MPAV and MPAS, all associations were synergistic, independently of herbicide or dose that was used.

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Oveson, Dawn. "Efficacy of Soybean Herbicides on Annual Morninglory." TopSCHOLAR®, 2001. http://digitalcommons.wku.edu/theses/691.

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Field experiments were established in 2000 and 2001 at the Agricultural Research and Education Complex in Bowling Green, Kentucky to evaluate herbicide efficacy on annual morningglory (Ipomoea spp.) species and other weeds. A randomized complete block design was utilized in each study with each treatment being replicated three times. Plots consisted of four 76 cm rows, 9.1 m in length. The two center rows of each plot were treated, with the outside rows of each plot serving as a weedy check. Crop response, weed control, and grain yield data were collected. Four different experiments were conducted. Two experiments utilized treatments of glyphosate and sulfosate alone and with tankmixes on glyphosate-tolerant soybeans. Two experiments examined various herbicide tankmixes applied to non-glyphosatetolerant soybeans. Soybean injury influenced by postemergence treatments of glyphosate and sulfosate alone and with chlorimuron-ethyl ranged from 0 to 5% four days after treatment (DAT) with the addition of chlorimuron-ethyl resulting in greater injury. Morningglory control 14 DAT ranged from 48 to 63% with sulfosate at 700 g ai/ha providing less control than glyphosate at 1120 g ai/ha. No treatment differences occurred 29 and 42 DAT. No statistical differences among treatments occurred among other weed species evaluated. Soybean injury influenced by postemergence treatments of glyphosate and sulfosate alone and with fomesafen and chloransulam-methyl 4 DAT ranged from 0 to 17% with the addition of fomesafen resulting in greater injury than the addition of chloransulam-methyl. Momingglory control 14 DAT ranged from 60 to 88% with glyphosate + imazethapyr at 840 + 71 g ai/ha providing the least control and sulfosate + fomesafen at 700 + 201 g ai/ha providing greater control. Soybean injury influenced by pre and postemergence treatments 7 DAT ranged from 0 to 30% in conventional soybeans. Applications of carfentrazone resulted in the greatest injury. Momingglory control 20 days after planting (DAP) ranged from 0 to 99% with chloransulam + sulfentrazone providing the highest control. Momingglory control 28 DAT ranged from 30 to 99% with s-metolachlor + metribuzin + acifluorfen + fenoxaprop-ethyl + fluazifop-P providing the least control. Common cocklebur control ranged from 13% to 97% 20 DAP with pendimethalin + imazethapyr providing the least control. Treatments containing aciflourfen + bentazon controlled common cocklebur > 80% 28 DAT. Soybean injury influenced by preemergence and postemergence treatments 7 DAT in conventional soybeans ranged from 0 to 33% with sulfentrazone + clomazone + chlorimuron-ethyl + carfentrazone resulting in the greatest injury. Momingglory control 7 DAT ranged from 0 to 99% with sulfentrazone + clomazone plus chlorimuron-ethyl + carfentrazone having the greatest control. Momingglory control 28 DAT ranged from 82 to 94% with no differences among treatment.

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Ramaswamy, Kiran. "Precision application of herbicides in corn fields." Thesis, McGill University, 2013. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=114199.

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The primary objective of this thesis was to develop a system through which precision spraying of herbicides could be applied to a corn field at an early post-emergence stage of development. The initial hypotheses underlying this thesis were that it was possible to: 1) capture a series of digital images using a tractor-mounted camera; 2) tag these images using a Global Positioning System (GPS); 3) develop an algorithm to detect weeds in an image; 4) develop a weed map using a series of images tagged with the presence or absence of weeds; and 5) significantly reduce the amount of spraying needed by spraying only areas known to contain weeds, thus reducing both costs and environmental impact.The experimental conditions consisted of a field of corn crop 12-17 days into their development stage and at the 3-5 leaf stage of development. A tractor-mounted camera interfaced to a GPS system and linked to a laptop computer was used for gathering images of the corn field.Due to the complexities involved in separating weeds the crop, the bulk of the thesis work was dedicated to the analysis of different algorithms through which weeds could be identified and weed maps could be created. The algorithm selected for the identification of weeds was the greenness method, using a pixel-by-pixel analysis of the red-green-blue (RGB) intensity values. The weed-tagged images were used to develop a series of algorithms to create weed maps. These algorithms utilized a set of image aggregation methods in order to establish a spray- or no-spray value for each location on the field, which were then plotted to demonstrate the locations of the field to be sprayed. The algorithms were validated through the use of the bootstrap statistical method. Once done, the potential herbicide savings for each weed mapping algorithm were evaluated. The results indicated that the algorithms had the potential to yield a maximum herbicide savings of 76% when compared with blanket spraying of the entire field. Factors that influenced the potential herbicide savings included the weed density necessary before spraying is employed, the number of images chosen to aggregate, and the size of the field as a whole. Seven algorithms were 100% successful in detecting weeds. Validation testing revealed that, when compared with a control situation in which 100% of the field would be sprayed, the algorithm that sprayed the smallest percentage of the field while still eliminating all weeds yielded a potential 10% herbicide savings; under the same parameters, the best performing real-time algorithm yielded a potential 9% herbicide savings. Therefore, it was determined that a solution involving the real-time acquisition and processing of video data and using the greenness method for weed detection could be employed in order to obtain savings in herbicide application.
L'objectif principal de cette thèse était de développer un système par lequel l'application précise des herbicides pourrait être appliquée à un champ de maïs qui est dans un stade précoce post levée de développement. Les hypothèses de cette thèse étaient qu'il était possible de: 1) capturer une série d'images à l'aide d'une caméra montée sur un tracteur; 2) marquer ces images en utilisant un système de positionnement global (GPS); 3) développer un algorithme pour détecter les mauvaises herbes dans une image; 4) de développer une carte des mauvaises herbes à l'aide d'une série d'images étiqueté avec la présence ou l'absence de mauvaises herbes, et 5) réduire considérablement la quantité d'herbicides nécessaire par appliquer des herbicides seulement dans les zones connues pour contenir les mauvaises herbes, ce qui va permettre la réduction des coûts et des impacts environnementaux. Les conditions expérimentales se composait d'un champ de maïs 12-17 jours après le début de leur phase de développement et au stade 3-5 feuilles du développement. Une caméra montée sur tracteur et relié à un système GPS et un ordinateur portable a été utilisé pour recueillir des images du champ de maïs.En raison de la complexité de distinguer les mauvaises herbes, la majorité du travail a été consacré à l'analyse des algorithmes d'identification et cartographie des mauvaises herbes. L'algorithme choisi pour l'identification des mauvaises herbes a été la méthode de verdure, en utilisant une analyse pixel par pixel des valeurs d'intensité rouge-vert-bleu (RGB).Les images de mauvaises herbes marquées ont été utilisées pour développer une série d'algorithmes pour créer des cartes des mauvaises herbes. Ces algorithmes ont utilisé un ensemble de méthodes d'agrégation d'image afin d'établir une valeur indiquant si les herbicides doit être appliqués pour chaque endroit sur le terrain. En utilisant ces valeurs, des cartes des mauvaises herbes ont été créés pour montrer les endroits identifiées. Les algorithmes ont été validés par utiliser l'algorithme bootstrap. Une fois cela fait, les économies d'herbicides potentiels pour chaque algorithme de cartographie des mauvaises herbes ont été évaluées. Les résultats ont indiqué que les algorithmes avait le potentiel de produire des économies d'herbicides maximales de 76% par rapport à l'application des herbicides à la totalité du champ. Facteurs qui ont influé les économies d'herbicides potentiels inclus la densité des mauvaises herbes nécessaires avant l'application des herbicides, le nombre d'images choisies à l'agrégation, et la taille du champ. Sept algorithmes ont réussi à détecter 100% des mauvaises herbes.Tests de validation ont révélé que, en comparaison avec une situation de contrôle dans lequel les herbicides seront appliquer à 100% du champ, l'algorithme qui appliquait le plus petit pourcentage des herbicides en éliminant toutes les mauvaises herbes à des économies potentielles d'herbicides de 10%; selon les mêmes paramètres, l'algorithme en temps réel le plus performante avait une économie potentielle d'herbicides 9%. Donc, il a été déterminé qu'une solution impliquant l'acquisition et le traitement en temps réel des données vidéo et en utilisant la méthode verdure pour la détection des mauvaises herbes pourrait être employée afin d'obtenir des économies substantielles en application de l'herbicide.

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De, Jimenez Juana Ramos. "Determination of some acid herbicides in soils." Thesis, University of Bristol, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.279758.

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49

Haugrud, Nathan Hans. "Cultivation to Supplement Residual Herbicides in Sugarbeet." Thesis, North Dakota State University, 2018. https://hdl.handle.net/10365/29217.

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The migration of waterhemp (Amaranthus tuberculatus) into northern sugarbeet (Beta vulgaris) growing regions has prompted sugarbeet producers to utilize inter-row cultivation in their weed management program as no currently registered herbicides can control glyphosate-resistant waterhemp postemergence. Field experiments were conducted to evaluate cultivation efficacy on waterhemp and common lambsquarters (Chenopodium album) and to evaluate cultivation safety on sugarbeet. Cultivation efficacy experiments demonstrated cultivation removes 65% of waterhemp and has no effect on further waterhemp emergence, but can be deleterious to common lambsquarters control if cultivation is timed before sugarbeet canopy closure. The ideal time to implement inter-row cultivation in sugarbeet is after sugarbeet canopy is closed and can suppress further weed emergence. Cultivation safety experiments demonstrated three cultivations as late as August 16 had no effect on sugarbeet yield and quality. Cultivation is a valuable tool to control glyphosate-resistant weeds with no deleterious effects if used correctly.
Sugarbeet Research and Education Board of Minnesota and North Dakota

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Klupinski, Theodore P. "Degradation of nitroaromatic herbicides in wetland sediments /." The Ohio State University, 2002. http://rave.ohiolink.edu/etdc/view?acc_num=osu1486457871785094.

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Dissertations / Theses on the topic 'Herbicides'

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