Relevant bibliographies by topics / Fourier transform ion cyclotron resonance mass spectrometry

Academic literature on the topic 'Fourier transform ion cyclotron resonance mass spectrometry'

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Published: 4 June 2021
Last updated: 3 February 2022

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Journal articles on the topic "Fourier transform ion cyclotron resonance mass spectrometry"

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Marshall, Alan G. "Fourier transform ion cyclotron resonance mass spectrometry." Accounts of Chemical Research 18, no. 10 (October 1985): 316–22. http://dx.doi.org/10.1021/ar00118a006.

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Baykut, G., and J. R. Eyler. "Fourier transform ion cyclotron resonance mass spectrometry." TrAC Trends in Analytical Chemistry 5, no. 2 (February 1986): 44–49. http://dx.doi.org/10.1016/0165-9936(86)85009-9.

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Smith, Donald F., Errol W. Robinson, Aleksey V. Tolmachev, Ron M. A. Heeren, and Ljiljana Paša-Tolić. "C60Secondary Ion Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." Analytical Chemistry 83, no. 24 (December 15, 2011): 9552–56. http://dx.doi.org/10.1021/ac2023348.

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Marshall, Alan G., and Shenheng Guan. "Ion optics for Fourier transform ion cyclotron resonance mass spectrometry." Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment 363, no. 1-2 (September 1995): 397–405. http://dx.doi.org/10.1016/0168-9002(95)00058-5.

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Hendrickson, Christopher L., and Mark R. Emmett. "ELECTROSPRAY IONIZATION FOURIER TRANSFORM ION CYCLOTRON RESONANCE MASS SPECTROMETRY." Annual Review of Physical Chemistry 50, no. 1 (October 1999): 517–36. http://dx.doi.org/10.1146/annurev.physchem.50.1.517.

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Marshall, Alan G., Christopher L. Hendrickson, and George S. Jackson. "Fourier transform ion cyclotron resonance mass spectrometry: A primer." Mass Spectrometry Reviews 17, no. 1 (1998): 1–35. http://dx.doi.org/10.1002/(sici)1098-2787(1998)17:1<1::aid-mas1>3.0.co;2-k.

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Lobodin, Vladislav V., Joshua J. Savory, Nathan K. Kaiser, Paul W. Dunk, and Alan G. Marshall. "Charge Reversal Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." Journal of The American Society for Mass Spectrometry 24, no. 2 (January 8, 2013): 213–21. http://dx.doi.org/10.1007/s13361-012-0512-x.

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Schweikhard, L. "High-frequency fourier transform ion cyclotron resonance mass spectrometry." Journal of the American Society for Mass Spectrometry 4, no. 2 (February 1993): 177–81. http://dx.doi.org/10.1016/1044-0305(93)85074-8.

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Marshall, Alan G., and Lutz Schweikhard. "Fourier transform ion cyclotron resonance mass spectrometry: technique developments." International Journal of Mass Spectrometry and Ion Processes 118-119 (September 1992): 37–70. http://dx.doi.org/10.1016/0168-1176(92)85058-8.

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Pfändler, Peter, Geoffrey Bodenhausen, Jacques Rapin, Raymond Houriet, and Tino Gäumann. "Two-dimensional fourier transform ion cyclotron resonance mass spectrometry." Chemical Physics Letters 138, no. 2-3 (July 1987): 195–200. http://dx.doi.org/10.1016/0009-2614(87)80367-6.

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Dissertations / Theses on the topic "Fourier transform ion cyclotron resonance mass spectrometry"

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Hauschild, Jennifer M. "Fourier transform ion cyclotron resonance mass spectrometry for petroleomics." Thesis, University of Oxford, 2012. http://ora.ox.ac.uk/objects/uuid:8604a373-fb6b-4bc0-8dc1-464a191b1fac.

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The past two decades have witnessed tremendous advances in the field of high accuracy, high mass resolution data acquisition of complex samples such as crude oils and the human proteome. With the development of Fourier transform ion cyclotron resonance mass spectrometry, the rapidly growing field of petroleomics has emerged, whose goal is to process and analyse the large volumes of complex and often poorly understood data on crude oils generated by mass spectrometry. As global oil resources deplete, oil companies are increasingly moving towards the extraction and refining of the still plentiful reserves of heavy, carbon rich and highly contaminated crude oil. It is essential that the oil industry gather the maximum possible amount of information about the crude oil prior to setting up the drilling infrastructure, in order to reduce processing costs. This project describes how machine learning can be used as a novel way to extract critical information from complex mass spectra which will aid in the processing of crude oils. The thesis discusses the experimental methods involved in acquiring high accuracy mass spectral data for a large and key industry-standard set of crude oil samples. These data are subsequently analysed to identify possible links between the raw mass spectra and certain physical properties of the oils, such as pour point and sulphur content. Methods including artificial neural networks and self organising maps are described and the use of spectral clustering and pattern recognition to classify crude oils is investigated. The main focus of the research, the creation of an original simulated annealing genetic algorithm hybrid technique (SAGA), is discussed in detail and the successes of modelling a number of different datasets using all described methods are outlined. Despite the complexity of the underlying mass spectrometry data, which reflects the considerable chemical diversity of the samples themselves, the results show that physical properties can be modelled with varying degrees of success. When modelling pour point temperatures, the artificial neural network achieved an average prediction error of less than 10% while SAGA predicted the same values with an average accuracy of more than 85%. It did not prove possible to model any of the other properties with such statistical significance; however improvements to feature extraction and pre-processing of the spectral data as well as enhancement of the modelling techniques should yield more consistent and statistically reliable results. These should in due course lead to a comprehensive model which the oil industry can use to process crude oil data using rapid and cost effective analytical methods.
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Lin, Tzu-Yung. "Advanced electronics for Fourier-transform ion cyclotron resonance mass spectrometry." Thesis, University of Warwick, 2012. http://wrap.warwick.ac.uk/55048/.

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With the development of mass spectrometry (MS) instruments starting in the late 19th century, more and more research emphasis has been put on MS related subjects, especially the instrumentation and its applications. Instrumentation research has led modern mass spectrometers into a new era where the MS performance, such as resolving power and mass accuracy, is close to its theoretical limit. Such advanced performance releases more opportunities for scientists to conduct analytical research that could not be performed before. This thesis reviews general MS history and some of the important milestones, followed by introductions to ion cyclotron resonance (ICR) technique and quadrupole operation. Existing electronic designs, such as Fourier-transform ion cyclotron resonance (FT-ICR) preamplifiers (for ion signal detection) and radio-frequency (RF) oscillators (for ion transportation/filtering) are reviewed. Then the potential scope for improvement is discussed. Two new FT-ICR preamplifiers are reported; both preamplifiers operate at room temperature. The first preamplifier uses an operational amplifier (op amp) in a transimpedance configuration. When a 18-k feedback resistor is used, this preamplifier delivers a transimpedance of about 85 dB , and an input current noise spectral density of around 1 pA/ p Hz. The total power consumption of this circuit is around 310 mW when tested on the bench. This preamplifier has a bandwidth of fi3 kHz to 10 MHz, which corresponds to the mass-to-charge ratio, m/z, of approximately 18 to 61k at 12 T for FT-ICR MS. The transimpedance and the bandwidth can be adjusted by replacing passive components such as the feedback resistor and capacitor. The feedback and bandwidth limitation of the circuit is also discussed. When using an 0402 type surface mount resistor, the maximum possible transimpedance, without sacrificing its bandwidth, is approximated to 5.3 M . Under this condition, the preamplifier is estimated to be able to detect ~110 charges. The second preamplifier employs a single-transistor design using a different feedback arrangement, a T-shaped feedback network. Such a feedback system allows ~100-fold less feedback resistance at a given transimpedance, hence preserving bandwidth, which is beneficial to applications demanding high gain. The single-transistor preamplifier yields a low power consumption of ~5.7 mW, and a transimpedance of 80 dB in the frequency range between 1 kHz and 1 MHz (m/z of around 180 to 180k for a 12-T FT-ICR system). In trading noise performance for higher transimpedance, an alternative preamplifier design has also been presented with a transimpedance of 120 dB in the same frequency range. The previously reported room-temperature FT-ICR preamplifier had a voltage gain of about 25, a bandwidth of around 1 MHz when bench tested, and a voltage noise spectral density of ~7.4 nV/ p Hz. The bandwidth performance when connecting this preamplifier to an ICR cell has not been reported. However, from the transimpedance theory, the transimpedance preamplifiers reported in this work will have a bandwidth wider by a factor of the open-loop gain of the amplifier. In a separate development, an oscillator is proposed as a power supply for a quadrupole mass filter in a mass spectrometer system. It targets a stabilized output frequency, and a feedback control for output amplitude stabilization. The newly designed circuit has a very stable output frequency at 1 MHz, with a frequency tolerance of 15 ppm specified by the crystal oscillator datasheet. Within this circuit, an automatic gain control (AGC) unit is built for output amplitude stabilisation. A new transformer design is also proposed. The dimension of the quadrupole being used as a mass filter will be determined in the future. This circuit (in particular the transformer and the quadrupole connection/mounting device) will be finalised after the design of the quadrupole. Finally, this thesis concludes with a discussion between the gain and the noise performance of an FT-ICR preamplifier. A brief analysis about the correlation between the gain, cyclotron frequency, and input capacitance is performed. Future work is also suggested for extending this research.
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Qi, Yulin. "Advanced methods in Fourier transform ion cyclotron resonance mass spectrometry." Thesis, University of Warwick, 2013. http://wrap.warwick.ac.uk/57931/.

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Mass spectrometry (MS) is a powerful analytical technique used to characterize various compounds by measuring the mass-to-charge ratio (m/z). Among different types of mass analyzers, Fourier transform ion cyclotron resonance mass spectrometer (FT-ICR MS) is the instrument of choice for those working at the forefront of research, as it offers incomparable mass accuracy, resolving power, and the highest flexibility for hybrid instrumentation and fragmentation techniques. The FT-ICR MS requires professional and careful tuning to achieve its superior performance. Our work aims to review, develop and apply advanced methods to improve the data quality of FT-ICR and push the limits of the instrument. FT-ICR spectrometry has been limited to the magnitude-mode for 40 years due to the complexity of the phase-wrapping problem. However, it is well known that by correcting phase of the data, the spectrum can be plotted in the absorption-mode with a mass resolving power that is as much as two times higher than conventional magnitude-mode. Based on the assumption that the frequency sweep excitation produces a quadratic accumulation in an ion’s phase value, a robust manual method to correct all ions’ phase shifts has been developed, which allows a broadband FT-ICR spectrum to be plotted in the absorption-mode. The developed phasing method has then been applied to a large variety of samples (peptides, proteins, crude oil), different spectral acquisition-mode (broadband, narrowband), and different design of ICR cells (Infinity cell, ParaCell) to compare the performance with the conventional magnitude-mode spectra. The outcome shows that, by plotting the absorption-mode spectrum, not only is the spectral quality improved at no extra cost, but the number of detectable peaks is also increased. Additionally, it has been found that artifactual peaks, such as noise or harmonics in the spectrum can be diagnosed immediately in the absorption-mode. Given the improved characteristics of the absorption-mode spectrum, the following research was then focused on a data processing procedure for phase correction and the features of the phase function. The results demonstrate that in the vast majority of cases, the phase function needs to be calculated just once, whenever the instrument is calibrated. In addition, an internal calibration method for calculating the phase function of spectra with insufficient peak density across the whole mass range has been developed. The above research is the basis of the Autophaser program which allows spectra recorded on any FT-ICR MS to be phase corrected in an automated manner.
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Mullen, Steven Lawrence. "Fourier transform ion cyclotron resonance mass spectrometry of organometallic compounds /." The Ohio State University, 1987. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487325740718905.

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Weisbrod, Chad Randal. "Improvement of Fourier transform ion cyclotron resonance mass spectrometry detection technology." Pullman, Wash. : Washington State University, 2010. http://www.dissertations.wsu.edu/Thesis/Spring2010/c_weisbrod_060210.pdf.

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Gates, Paul Jonathan. "Fourier-transform ion cyclotron resonance mass spectrometry : analysis of natural products." Thesis, University of Cambridge, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.621612.

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Wills, Rebecca Helen. "High mass accuracy analytical applications of Fourier transform ion cyclotron resonance mass spectrometry." Thesis, University of Warwick, 2014. http://wrap.warwick.ac.uk/60050/.

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The performance capabilities of Fourier transform ion cyclotron resonance (FTICR) mass spectrometry are higher than any other type of mass spectrometer, making this technique suitable for a range of analytical applications. Here, FTICR mass spectrometry has been used for the structural analysis of polyketides and nonribosomal peptides, and in the identification of peptide binding sites of ruthenium(II) arene anticancer complexes. In both these applications, methods have been developed involving complementary tandem mass spectrometry techniques, specifically collision activated dissociation (CAD), electron induced dissociation (EID), and electron capture dissociation. In particular, CAD and EID have been shown to be effective in the structural characterisation of polyketides, with a method developed for distinguishing between two isomers of the polyketide lasalocid A. This method has been optimised and extended for application to non-ribosomal peptides enabling detailed structural information to be obtained with very high accuracy. Using CAD and ECD has enabled the identification of amino acids involved in binding ruthenium(II) complexes. Binding to phenylalanine and glutamic acid was observed in this work for the first time; coordination by histidine and methionine was also observed and is in agreement with previous work. Overall, new methods for highly accurate structural characterisation and binding site identification have been successfully designed and implemented.
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Schmidt, Eric Grayson. "Observation and control of ion motion in fourier transform ion cyclotron resonance mass spectrometry /." Digital version accessible at:, 1999. http://wwwlib.umi.com/cr/utexas/main.

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Tsybin, Youri. "High Rate Electron Capture Dissociation Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." Doctoral thesis, Uppsala universitet, Jonfysik, 2004. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-4136.

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Advances in science and technology during the past decade have greatly enhanced the level of the structural investigation of macromolecules – peptides and proteins. Biological mass spectrometry has become one of the most precise and sensitive techniques in peptide and protein analysis. However, increasing demands of biotechnological applications require further progress to be made. In the present thesis the development and improvement of peptide and protein characterization methods and techniques based on ion-electron and ion-photon reactions in electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry are described. The focus is on the development of the electron capture dissociation method, recently discovered by the group of professor McLafferty, into a high rate, efficient tandem mass spectrometrical technique. The rate and reliability of the electron capture dissociation technique were greatly increased by implementation of low-energy pencil electron beam injection systems based on indirectly heated dispenser cathodes. Further implementation of a hollow electron beam injection system combined, in a single experimental configuration, two rapid fragmentation techniques, high rate electron capture dissociation and infrared multiphoton dissociation. Simultaneous and consecutive irradiations of trapped ions with electrons and photons extended the possibilities for ion activation/dissociation reaction schemes and lead to improved peptide and protein characterization. Using these improvements, high rate electron capture dissociation was employed in time-limited experiments, such as liquid chromatography–tandem mass spectrometry and capillary electrophoresis-tandem mass spectrometry. The analytical applications of the developed techniques have been demonstrated in top-down sequencing of peptides and proteins up to 29 kDa, improved sequencing of peptides with multiple disulfide bridges and secondary fragmentation (w-ion formation), as well as extended characterization of peptide mixtures separated by liquid chromatography and capillary electrophoresis. For instance, the dissociation of peptides resulting from enzymatic digestion of proteins provided complementary structural information on peptides and proteins, as well as their post-translational modifications.
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Anupriya, Anupriya. "Gas Phase Structure Characterization Using Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." BYU ScholarsArchive, 2016. https://scholarsarchive.byu.edu/etd/6447.

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This dissertation investigates Fourier transform ion cyclotron resonance mass spectrometry (FTICR-MS) based techniques to study the impact of molecular structure on conformation and binding energetics. A novel method to determine collison cross sectional areas using FTICR (CRAFTI), initially developed by the Dearden lab, was applied to study the conformations of molecular systems with unique structural attributes in an attempt to explore the molecular range of CRAFTI. The systems chosen for CRAFTI studies include crown-ether alkylammonium complexes and biogenic amino acids. The results were found to be consistent with expected behavior, and strongly correlated with experimental measurements made using ion mobility spectrometry (IMS) and predictions from computations. The analytical sensitivity of CRAFTI was highlighted by its ability to distinguish the normal and branched structural isomers of butylamine. Besides conformation characterization, quantitative evaluation of binding was undertaken on metal ion-cryptand complexes on the FTICR instrument using sustained off-resonance irradiation-collision-induced dissociation (SORI CID) method. Complex formation and dissociation was found to be a strong function of both guest and host sizes which impacted steric selectivity, and polarizability. The results demonstrate the ability of FTICR to simultaneously determine structure, conformation and binding thereby providing comprehensive molecular characterization.
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Books on the topic "Fourier transform ion cyclotron resonance mass spectrometry"

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Saunders, William Hundley, and James M. Farrar. Techniques for the study of ion-molecule reactions. New York: Wiley, 1988.

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Wallace, James Ian. The analysis of biological molecules by electrospray ionisation Fourier transform ion cyclotron resonance (ESIFTICR) mass spectrometry. [s.l.]: typescript, 1999.

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Asamoto, B. Analytical Applications of Fourier Transform Ion Cyclotron Resonance Mass Spectrometry. Wiley-VCH, 1991.

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1951-, Buchanan Michelle V., American Chemical Society. Division of Analytical Chemistry., and American Chemical Society Meeting, eds. Fourier transform mass spectrometry: Evolution, innovation, and applications. Washington, DC: American Chemical Society, 1987.

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Zientek, Keith David. External ionization source improvements for fourier transform ion cyclotron resonance mass spectrometry. 2004.

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Bruce, Asamoto, ed. FT-ICR/MS: Analytical applications of Fourier transform ion cyclotron resonance mass spectrometry. New York, NY: VCH Publishers, 1991.

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Asamoto, Bruce. Ft-Icr/MS: Analytical Applications of Fourier Transform Ion Cyclotron Resonance Mass Spectrometry. Vch Pub, 1991.

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Asamoto, Bruce. FT-Icr/MS: Analytical Applications of Fourier Transform Ion Cyclotron Resonance Mass Spectrometry. VCH Publishers, 1991.

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Lang, Gui-hua Lisa. Studies of organometallic and biological systems with Fourier transform ion cyclotron resonance mass spectrometry. 1998.

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Watson, Clifford Hunter. Infrared multiphoton dissociation of gaseous ions studied by fourier transform ion cyclotron resonance mass spectrometry. 1986.

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Book chapters on the topic "Fourier transform ion cyclotron resonance mass spectrometry"

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Laude, David A., and Steven C. Beu. "Experimental Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." In Experimental Mass Spectrometry, 153–97. Boston, MA: Springer US, 1994. http://dx.doi.org/10.1007/978-1-4899-2569-5_5.

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Olimpieri, Laura, and Pietro Traldi. "Quadrupole Mass Filters, Quadrupole Ion Traps and Fourier Transform Ion Cyclotron Resonance Spectrometers." In Mass Spectrometry in Biomolecular Sciences, 177–200. Dordrecht: Springer Netherlands, 1996. http://dx.doi.org/10.1007/978-94-009-0217-6_9.

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Goodenowe, Dayan. "Metabolomic Analysis with Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." In Metabolic Profiling: Its Role in Biomarker Discovery and Gene Function Analysis, 125–39. Boston, MA: Springer US, 2003. http://dx.doi.org/10.1007/978-1-4615-0333-0_8.

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Wolff, Jeremy J., and I. Jonathan Amster. "Fourier Transform Ion Cyclotron Resonance and Magnetic Sector Analyzers for ESI and MALDI." In Electrospray and MALDI Mass Spectrometry, 365–409. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2012. http://dx.doi.org/10.1002/9780470588901.ch11.

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Rahbee, A. "Burg Algorithm Applied to Fourier Transform ION Cyclotron Resonance Mass Spectrometry." In Maximum Entropy and Bayesian Methods, 391–401. Dordrecht: Springer Netherlands, 1990. http://dx.doi.org/10.1007/978-94-009-0683-9_26.

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Ouvry-Patat, Séverine A., Matthew P. Torres, Craig A. Gelfand, Hung Hiang Quek, Michael Easterling, J. Paul Speir, and Christoph H. Borchers. "Top-Down Proteomics on a High-field Fourier Transform Ion Cyclotron Resonance Mass Spectrometer." In Mass Spectrometry of Proteins and Peptides, 215–31. Totowa, NJ: Humana Press, 2009. http://dx.doi.org/10.1007/978-1-59745-493-3_12.

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Plesko, S., P. Grossmann, M. Allemann, and H. P. Kellerhals. "Application of Secondary Ion Mass Spectrometry Combined with Fourier Transform Ion Cyclotron Resonance." In Springer Proceedings in Physics, 213–17. Berlin, Heidelberg: Springer Berlin Heidelberg, 1986. http://dx.doi.org/10.1007/978-3-642-82718-1_40.

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Emmett, Mark R., and Cheryl F. Lichti. "Ultrahigh-Resolution Lipid Analysis with Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." In Neuromethods, 21–43. New York, NY: Springer New York, 2017. http://dx.doi.org/10.1007/978-1-4939-6946-3_3.

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Marshall, Alan G., Tao-Chin Lin Wang, Ling Chen, and Tom L. Ricca. "New Excitation and Detection Techniques in Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." In ACS Symposium Series, 21–33. Washington, DC: American Chemical Society, 1987. http://dx.doi.org/10.1021/bk-1987-0359.ch002.

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Smith, R. D., J. E. Bruce, Q. Wu, X. Cheng, S. A. Hofstadler, G. A. Anderson, R. Chen, et al. "The Role of Fourier Transform Ion Cyclotron Resonance Mass Spectrometry in Biological Research — New Developments and Applications." In Mass Spectrometry in the Biological Sciences, 25–68. Totowa, NJ: Humana Press, 1996. http://dx.doi.org/10.1007/978-1-4612-0229-5_3.

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Conference papers on the topic "Fourier transform ion cyclotron resonance mass spectrometry"

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Marshall, Alan G. "Fourier transform ion cyclotron resonance mass spectrometry." In The eleventh international conference on fourier transform spectroscopy. AIP, 1998. http://dx.doi.org/10.1063/1.55826.

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Hannis, James C., David C. Muddiman, and Allison P. Null. "Genotyping complex short tandem repeats using electrospray ionization Fourier transform ion cyclotron resonance multistage mass spectrometry." In BiOS 2000 The International Symposium on Biomedical Optics, edited by Patrick A. Limbach, John C. Owicki, Ramesh Raghavachari, and Weihong Tan. SPIE, 2000. http://dx.doi.org/10.1117/12.380492.

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Schweikhard, Lutz. "Quadrature detection for the separation of the signals of positive and negative ions in fourier transform ion cyclotron resonance mass spectrometry." In NON-NEUTRAL PLASMA PHYSICS IV: Workshop on Non-Neutral Plasmas. AIP, 2002. http://dx.doi.org/10.1063/1.1454343.

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Schrader, Wolfgang, Saroj K. Panda, Jan T. Andersson, Mark Grutters, Malcolm Salisbury, and A. G. Shepherd. "Development of Fourier Transform-Ion Cyclotron Resonance Mass Spectrometry Protocol for the Analysis of Asphaltene Field Samples and Solubility Fractions." In SPE International Symposium on Oilfield Chemistry. Society of Petroleum Engineers, 2009. http://dx.doi.org/10.2118/121670-ms.

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Chai, Rukuan, Yuetian Liu, Yuting He, Qianjun Liu, and Wenhuan Gu. "Experimental Study on Direct Current Voltage Assisted Carbonated Water-Flooding Mechanism in Tight Oil Reservoir." In International Petroleum Technology Conference. IPTC, 2021. http://dx.doi.org/10.2523/iptc-21498-ms.

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Abstract Tight oil reservoir plays an increasingly important role in the world energy system, but its recovery is always so low. Hence, a more effective enhanced oil recovery (EOR) technology is urgently needed. Meanwhile, greenhouse effect is more and more serious, a more effective carbon capture and sequestration (CCS) method is also badly needed. Direct current voltage assisted carbonated water-flooding is a new technology that combines direct current voltage with carbonated water-flooding to enhance oil recovery and CO2 sequestration efficiency, simultaneously. Experimental studies were conducted from macroscopic-scale to microscopic-scale to study the performance and mechanism of direct current voltage assisted carbonated water-flooding. Firstly, core flood experiments were implemented to study the effect of direct current voltage assisted carbonated water on oil recovery and CO2 sequestration efficiency. Secondly, contact angle and interfacial tension/dilatational rheology were measured to analyze the effect of direct current voltage assisted carbonated water on crude oil-water-rock interaction. Thirdly, total organic carbon (TOC), gas chromatography (GC), and electrospray ionization-fourier transform ion cyclotron resonance-mass spectrometry (ESI FT ICR-MS) were used to investigate the organic composition change of produced effluents and crude oil in direct current voltage assisted carbonated water treatment. Through direct current voltage assisted carbonated water-flooding experiments, the following results can be obtained. Firstly, direct current voltage assisted carbonated waterflooding showed greater EOR capacity and CO2 sequestration efficiency than individual carbonated water and direct current voltage treatment. With the increase of direct current voltage, oil recovery increases to 38.67% at 1.6V/cm which much higher than 29.07% of carbonated water-flooding and then decreases, meanwhile, CO2 output decreases to only 35.5% at 1.6V/cm which much lower than 45.6% of carbonated water-flooding and then increases. Secondly, in direct current voltage assisted carbonated water-flooding, the wettability alteration is mainly caused by carbonated water and the effect of direct current can be neglected. While both carbonated water and direct current have evident influence on interfacial properties. Herein, with direct current voltage increasing, the interfacial tension firstly decreases and then increases, the interfacial viscoelasticity initially strengthens and then weakens. Thirdly, GC results indicated that crude oil cracking into lighter components occurs during direct current voltage assisted carbonated water-flooding, with the short-chain organic components increasing and the long-chain components decreasing. Meanwhile, TOC and ESI FT ICR-MS results illustrated that CO2 electroreduction do occur in direct current voltage assisted carbonated water-flooding with the dissolved organic molecules increases and the emergence of formic acid. Conclusively, the synergy of CO2 electrochemical reduction into formic acid in aqueous solution and the long-chain molecules electrostimulation pyrolysis into short ones in crude oil mutually resulted in the enhancement of crude oil-carbonated water interaction. This paper proposed a new EOR & CCS technology-direct current voltage assisted carbonated water-flooding. It showed great research and application potential on tight oil development and greenhouse gas control. More work needs to be done to further explore its mechanism. This paper constructs a multiscale & interdisciplinary research system to study the multidisciplinary (EOR&CCS) problem. Specifically, a series connected physical (Core displacement, Contact angle, and Interfacial tension/rheology measurements) and chemistry (TOC, GS, and ESI FT ICR-MS) experiments are combined to explore its regularity and several physics (Atomic physics) and chemistry (Electrochemistry/Inorganic Chemistry) theories are applied to explain its mechanisms.
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