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Journal articles on the topic 'Fluorofori'

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Author: Grafiati

Published: 10 March 2023

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1

Chai, Jin Young, Hyojin Cha, Sung-Sik Lee, Young-Ho Oh, Sungyul Lee, and Dae Yoon Chi. "Mechanistic study of nucleophilic fluorination for the synthesis of fluorine-18 labeled fluoroform with high molar activity from N-difluoromethyltriazolium triflate." RSC Advances 11, no. 11 (2021): 6099–106. http://dx.doi.org/10.1039/d0ra09827b.

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Route a: desired S_N2 reaction of fluoride to form fluoroform with high molar activity; route b: side reaction to form methyl fluoride; route c: side reaction to form difluorocarbene to give fluoroform with lower molar activity.

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2

Champion, J. P., and G. Graner. "Fluoroform." Molecular Physics 58, no. 3 (June 20, 1986): 475–84. http://dx.doi.org/10.1080/00268978600101301.

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3

Kyasa, ShivaKumar. "Fluoroform (CHF3)." Synlett 26, no. 13 (June 11, 2015): 1911–12. http://dx.doi.org/10.1055/s-0034-1380924.

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4

Punna, Nagender, Takuya Saito, Mikhail Kosobokov, Etsuko Tokunaga, Yuji Sumii, and Norio Shibata. "Stereodivergent trifluoromethylation of N-sulfinylimines by fluoroform with either organic-superbase or organometallic-base." Chemical Communications 54, no. 34 (2018): 4294–97. http://dx.doi.org/10.1039/c8cc01526k.

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5

Fujihira, Yamato, Yumeng Liang, Makoto Ono, Kazuki Hirano, Takumi Kagawa, and Norio Shibata. "Synthesis of trifluoromethyl ketones by nucleophilic trifluoromethylation of esters under a fluoroform/KHMDS/triglyme system." Beilstein Journal of Organic Chemistry 17 (February 12, 2021): 431–38. http://dx.doi.org/10.3762/bjoc.17.39.

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A straightforward method that enables the formation of biologically attractive trifluoromethyl ketones from readily available methyl esters using the potent greenhouse gas fluoroform (HCF3, HFC-23) was developed. The combination of fluoroform and KHMDS in triglyme at −40 °C was effective for this transformation, with good yields as high as 92%. Substrate scope of the trifluoromethylation procedure was explored for aromatic, aliphatic, and conjugated methyl esters. This study presents a straightforward trifluoromethylation process of various methyl esters that convert well to the corresponding trifluoromethyl ketones. The tolerance of various pharmacophores under the reaction conditions was also explored.

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6

Miloserdov, Fedor M., and Vladimir V. Grushin. "Alcoholysis of fluoroform." Journal of Fluorine Chemistry 167 (November 2014): 105–9. http://dx.doi.org/10.1016/j.jfluchem.2014.06.006.

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7

Carbonnel, Elodie, Tatiana Besset, Thomas Poisson, Daniel Labar, Xavier Pannecoucke, and Philippe Jubault. "18F-Fluoroform: a 18F-trifluoromethylating agent for the synthesis of SCF218F-aromatic derivatives." Chemical Communications 53, no. 42 (2017): 5706–9. http://dx.doi.org/10.1039/c7cc02652h.

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8

Bao, Junwei Lucas, Xin Zhang, and Donald G. Truhlar. "Predicting pressure-dependent unimolecular rate constants using variational transition state theory with multidimensional tunneling combined with system-specific quantum RRK theory: a definitive test for fluoroform dissociation." Physical Chemistry Chemical Physics 18, no. 25 (2016): 16659–70. http://dx.doi.org/10.1039/c6cp02765b.

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9

Ma, Qiao, and Gavin Chit Tsui. "Trifluoromethylation of α-diazoesters and α-diazoketones with fluoroform-derived CuCF3: synergistic effects of co-solvent and pyridine as a promoter." Organic Chemistry Frontiers 6, no. 1 (2019): 27–31. http://dx.doi.org/10.1039/c8qo00834e.

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10

Ramos-Torres, Karla M., Yu-Peng Zhou, Bo Yeun Yang, Nicolas J. Guehl, Moon Sung-Hyun, Sanjay Telu, Marc D. Normandin, Victor W. Pike, and Pedro Brugarolas. "Syntheses of [11C]2- and [11C]3-trifluoromethyl-4-aminopyridine: potential PET radioligands for demyelinating diseases." RSC Medicinal Chemistry 11, no. 10 (2020): 1161–67. http://dx.doi.org/10.1039/d0md00190b.

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11

Köckinger, Manuel, Tanja Ciaglia, Michael Bersier, Paul Hanselmann, Bernhard Gutmann, and C. Oliver Kappe. "Utilization of fluoroform for difluoromethylation in continuous flow: a concise synthesis of α-difluoromethyl-amino acids." Green Chemistry 20, no. 1 (2018): 108–12. http://dx.doi.org/10.1039/c7gc02913f.

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Difluoromethylated esters, malonates and amino acids (including the drug eflornithine) are obtained by a gas–liquid continuous flow protocol employing the abundant waste product fluoroform as an atom-efficient reagent.

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12

Torrie, B. H., O. S. Binbrek, and B. M. Powell. "Structure of solid fluoroform." Molecular Physics 87, no. 5 (April 10, 1996): 1007–13. http://dx.doi.org/10.1080/00268979600100691.

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13

Zanardi, Alessandro, Maxim A. Novikov, Eddy Martin, Jordi Benet-Buchholz, and Vladimir V. Grushin. "Direct Cupration of Fluoroform." Journal of the American Chemical Society 133, no. 51 (December 28, 2011): 20901–13. http://dx.doi.org/10.1021/ja2081026.

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14

Yoo, Wesley J., and Larry T. Taylor. "Supercritical Fluid Extraction of Polychlorinated Biphenyls and Organochlorine Pesticides from Freeze-Dried Tissue of Marine Mussel, Mytilus eduli." Journal of AOAC INTERNATIONAL 80, no. 6 (November 1, 1997): 1336–46. http://dx.doi.org/10.1093/jaoac/80.6.1336.

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Abstract Supercritical fluid extractions (SFEs) of 21 polychlorinated biphenyls (PCBs) and 8 organochlorine pesticides (OCPs) from freeze-dried mussel tissue are compared with traditional Soxhlet extractions. The aim was to determine the efficacy of supercritical CO2 to extract these 2 classes of lipophilic compounds. A spike study to determine the feasibility of on-line cleanup by inclusion of an inert matrix (activated alumina) in the extraction vessel showed that the chemical integrity of the PCBs was not compromised, whereas some DDTs were decomposed to their respective metabolites. Relatively long static extraction time, higher density, and lower temperature yielded quantitative recoveries of PCBs from freeze-dried mussel tissue with good reproducibilities. Recoveries of OCPs were nonquantitative and highly variable. Finally, the efficacy of fluoroform (CHF3) as an alternative supercritical fluid to selectively extract PCBs and OCPs was studied. Fluoroform yielded nonquantitative and variable recoveries of PCBs and OCPs, but its use eliminated the need for in situ alumina to retain coextracted lipids from the matrix.

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15

Geri, Jacob B., and Nathaniel K. Szymczak. "Recyclable Trifluoromethylation Reagents from Fluoroform." Journal of the American Chemical Society 139, no. 29 (July 13, 2017): 9811–14. http://dx.doi.org/10.1021/jacs.7b05408.

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16

Bocquet, R., D. Boucher, W. D. Chen, J. Cosleou, and J. Demaison. "The Submillimeterwave Spectrum of Fluoroform." Journal of Molecular Spectroscopy 158, no. 2 (April 1993): 494–96. http://dx.doi.org/10.1006/jmsp.1993.1096.

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17

Kohls, Emilija, Anastas Mishev, and Ljupčo Pejov. "Solvation of fluoroform and fluoroform–dimethylether dimer in liquid krypton: A theoretical cryospectroscopic study." Journal of Chemical Physics 139, no. 5 (August 7, 2013): 054504. http://dx.doi.org/10.1063/1.4816282.

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18

Lang, E. W., F. X. Prielmeier, H. Radkowitsch, and H. D. Lüdemann. "High Pressure NMR Study of the Molecular Dynamics of Liquid Fluoroform and Deutero-Fluoroform." Berichte der Bunsengesellschaft für physikalische Chemie 91, no. 10 (October 1987): 1025–33. http://dx.doi.org/10.1002/bbpc.19870911010.

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19

Okusu, Satoshi, Etsuko Tokunaga, and Norio Shibata. "Difluoromethylation of Terminal Alkynes by Fluoroform." Organic Letters 17, no. 15 (July 16, 2015): 3802–5. http://dx.doi.org/10.1021/acs.orglett.5b01778.

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20

Zhang, Yuan, Motohiro Fujiu, Hiroki Serizawa, and Koichi Mikami. "Organocatalysis approach to trifluoromethylation with fluoroform." Journal of Fluorine Chemistry 156 (December 2013): 367–71. http://dx.doi.org/10.1016/j.jfluchem.2013.07.018.

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21

Mori, Toshiaki, Yuri Tsuchiya, and Yoshio Okahata. "Polymerizations of Tetrafluoroethylene in Homogeneous Supercritical Fluoroform and in Detergent-Free Heterogeneous Emulsion of Supercritical Fluoroform/Water." Macromolecules 39, no. 2 (January 2006): 604–8. http://dx.doi.org/10.1021/ma051930b.

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22

Havlas, Zdenek, Tomas Kovar, and Rudolf Zahradnik. "Does fluoroformic acid exist?" Journal of the American Chemical Society 107, no. 25 (December 1985): 7243–46. http://dx.doi.org/10.1021/ja00311a002.

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23

Maruyama, Kenichi, Daichi Saito, and Koichi Mikami. "(Sila)Difluoromethylation of Fluorenyllithium with CF3H and CF3TMS." SynOpen 02, no. 03 (July 2018): 0234–39. http://dx.doi.org/10.1055/s-0037-1610361.

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Difluoromethylation of the C9-H site of the fluorene ring using lithium base and fluoroform (CF3H), which is one of the most cost-effective difluoromethylating reagents, is attained to give difluoromethylated fluorenes with an all-carbon quaternary center. The Ruppert–Prakash reagent (CF3TMS) can also be applied to the present reaction system, providing siladifluoromethylated fluorenes that can be utilized for sequential carbon–carbon bond-forming reactions through activation of the silyl group.

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24

Ingrosso, Francesca, Branka M. Ladanyi, Benedetta Mennucci, and Giovanni Scalmani. "Solvation of Coumarin 153 in Supercritical Fluoroform." Journal of Physical Chemistry B 110, no. 10 (March 2006): 4953–62. http://dx.doi.org/10.1021/jp056226b.

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25

Yang, Xinkan, Lisi He, and Gavin Chit Tsui. "Hydroxytrifluoromethylation of Alkenes Using Fluoroform-Derived CuCF3." Organic Letters 19, no. 9 (April 25, 2017): 2446–49. http://dx.doi.org/10.1021/acs.orglett.7b01085.

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26

Carlotti, M., G. Di Lonardo, L. Fusina, A. Trombetti, and B. Carli. "The far-infrared spectrum of fluoroform (CHF3)." Journal of Molecular Spectroscopy 123, no. 1 (May 1987): 135–44. http://dx.doi.org/10.1016/0022-2852(87)90266-9.

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27

Sedlionoka, Elīna, and Jeļena Kirilova. "AMINOACIDS LIKE FLUORESCENT MARKERS FOR BIOMATERIALS." HUMAN. ENVIRONMENT. TECHNOLOGIES. Proceedings of the Students International Scientific and Practical Conference, no. 24 (April 22, 2020): 168–71. http://dx.doi.org/10.17770/het2020.24.6770.

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Mūsdienās fluorescentas metodes ir plaši izmantotas vairākās zinātnes un medicīnas nozarēs: luminiscējošie materiāli ir nozīmīgi imunoķīmijā, in situ hibridizācijas fluorescencē, šūnu pētījumos, citoķīmijā, medicīniskos izmeklējumos un citur. Fluorescentā iekrāsošana ir process, kura gaitā notiek fluorofora kovalentā pievienošana pētāmai molekulai. Tagad ir izpētītas vairākās luminiscentas iezīmes olbaltumvielu, lipīdu un nukleīnskābju vizualizēšanai. Proteīnu vizualizācijai bioķīmiķi un biologi plaši izmanto luminiscentu iezīmi FITC, kura līdzīgi projektā pielietotam marķierim satur izotiocianāta grupējumu, kas spēj reaģēt ar aminogrupām un tādā veidā iezīmēt biomateriālu, kurā ir aminogrupas (amiboskābes, olbaltumvielas u.c.).

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28

Zhang, Cai. "Application of fluoroform in trifluoromethylation and diﬂuoromethylation reactions." Arkivoc 2017, no. 1 (March 12, 2017): 67–83. http://dx.doi.org/10.24820/ark.5550190.p009.884.

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29

Sharma, Gitanjali, David Turton, Graham Smith, Philip Miller, and Gabriela Kramer-Marek. "[18F]Fluoroform radiolabelling of the CHK1 inhibitor CCT245737." Nuclear Medicine and Biology 96-97 (May 2021): S48—S49. http://dx.doi.org/10.1016/s0969-8051(21)00343-7.

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30

Närger, U., J. R. de Bruyn, M. Stein, and D. A. Balzarini. "Coexistence curve of fluoroform near its critical point." Physical Review B 39, no. 16 (June 1, 1989): 11914–19. http://dx.doi.org/10.1103/physrevb.39.11914.

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31

Song, W., N. Patel, and M. Maroncelli. "A 2-Site Model for Simulating Supercritical Fluoroform." Journal of Physical Chemistry B 106, no. 34 (August 2002): 8783–89. http://dx.doi.org/10.1021/jp021079s.

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32

Russell, Jamie, and Nicolas Roques. "Effective nucleophilic trifluoromethylation with fluoroform and common base." Tetrahedron 54, no. 45 (November 1998): 13771–82. http://dx.doi.org/10.1016/s0040-4020(98)00846-1.

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33

Kometani, Noritsugu, Yuji Hoshihara, Yoshiro Yonezawa, Okitsugu Kajimoto, Kimihiko Hara, and Naoki Ito. "Rotational Dynamics of Coumarin 153 in Supercritical Fluoroform." Journal of Physical Chemistry A 108, no. 44 (November 2004): 9479–83. http://dx.doi.org/10.1021/jp047854g.

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34

Okusu, Satoshi, Etsuko Tokunaga, and Norio Shibata. "ChemInform Abstract: Difluoromethylation of Terminal Alkynes by Fluoroform." ChemInform 46, no. 52 (December 2015): no. http://dx.doi.org/10.1002/chin.201552065.

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35

Corbett, P., A. Tarr, and E. Whittle. "The Vapour Phase Brominations of Fluoroform and Methane." Bulletin des Sociétés Chimiques Belges 71, no. 11-12 (September 2, 2010): 778–79. http://dx.doi.org/10.1002/bscb.19620711127.

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36

Wynne, Dolores C., and Philip G. Jessop. "Cyclopropanation Enantioselectivity Is Pressure Dependent in Supercritical Fluoroform." Angewandte Chemie International Edition 38, no. 8 (April 19, 1999): 1143–44. http://dx.doi.org/10.1002/(sici)1521-3773(19990419)38:8<1143::aid-anie1143>3.0.co;2-y.

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37

Fourrier, M., and M. Redon. "A new CW FIR lasing medium: Methyl fluoroform." Optics Communications 64, no. 6 (December 1987): 534–36. http://dx.doi.org/10.1016/0030-4018(87)90284-7.

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38

Zhang, Yuan, Motohiro Fujiu, Hiroki Serizawa, and Koichi Mikami. "ChemInform Abstract: Organocatalysis Approach to Trifluoromethylation with Fluoroform." ChemInform 45, no. 18 (April 17, 2014): no. http://dx.doi.org/10.1002/chin.201418042.

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39

Меликова, С. М., К. С. Рутковский, Д. Н. Щепкин, С. Махолл, and В. Херребут. "Криоспектроскопическое исследование резонансных мультиплетов ν-=SUB=-s-=/SUB=- ~2ν-=SUB=-b-=/SUB=- в молекуле CHF-=SUB=-3-=/SUB=-." Оптика и спектроскопия 129, no. 8 (2021): 1019. http://dx.doi.org/10.21883/os.2021.08.51197.2002-21.

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The sequences of Fermi resonances vs~2vb in the IR spectrum of a solution of fluoroform (CHF3) in liquefied krypton are investigated. Here vs is the CH stretching vibration, vb is the bending vibration. It is shown that for a correct description of resonance multiplets (polyads) at a high degree of vibrational excitation, it is necessary to use an extended set of spectroscopic parameters. In particular, it is necessary to take into account the dependence of the anharmonic interaction constant asbb on the vibrational quantum numbers. The conclusions are generalized for the arbitrary case of the CH-chromophore CHX3.

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40

Rasu, Loorthuraja, Ben Rennie, Mark Miskolzie, and Steven H. Bergens. "A Fortuitous, Mild Catalytic Carbon–Carbon Bond Hydrogenolysis by a Phosphine-Free Catalyst." Australian Journal of Chemistry 69, no. 5 (2016): 561. http://dx.doi.org/10.1071/ch15792.

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The putative catalyst trans-[Ru((S,S)-skewphos)(H)2((R,R)-dpen)] (skewphos = 2,4-bis(diphenylphosphino)pentane; dpen = 1,2-diphenylethylenediamine) transforms the trifluoroacetyl amide 2,2,2-trifluoro-1-(piperidin-1-yl)ethanone under mild conditions (4 atm H2, room temperature, 4–24 h, 1 mol-% Ru, 15 mol-% KOtBu in tetrahydrofuran) to generate the formylated amine 1-formylpiperidine and fluoroform via C–C bond hydrogenolysis. Catalysts are also prepared by reacting cis-[Ru(η3-C3H5)(MeCN)2(COD)]BF4 (COD = 1,5-cyclooctadiene) with diamine ligands in situ. Low-temperature NMR studies provided insight into this reaction.

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41

Aharon, Cheryl, and Shlomo Rozen. "Using fluoroform for constructing aromatic and heterocyclic trifluoromethylselenyl compounds." Journal of Fluorine Chemistry 250 (October 2021): 109866. http://dx.doi.org/10.1016/j.jfluchem.2021.109866.

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42

Reimann, Bernd, Konstantin Buchhold, Sascha Vaupel, Bernhard Brutschy, Zdeněk Havlas, Vladimír Špirko, and Pavel Hobza. "Improper, Blue-Shifting Hydrogen Bond between Fluorobenzene and Fluoroform†." Journal of Physical Chemistry A 105, no. 23 (June 2001): 5560–66. http://dx.doi.org/10.1021/jp003726q.

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43

Potash, Shay, and Shlomo Rozen. "General Synthesis of Trifluoromethyl Selenides Utilizing Selenocyanates and Fluoroform." Journal of Organic Chemistry 79, no. 22 (November 12, 2014): 11205–8. http://dx.doi.org/10.1021/jo5022844.

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44

Folléas, Benoît, Ilan Marek, Jean-F. Normant, and Laurent Saint Jalmes. "Fluoroform: an efficient precursor for the trifluoromethylation of aldehydes." Tetrahedron Letters 39, no. 19 (May 1998): 2973–76. http://dx.doi.org/10.1016/s0040-4039(98)00391-8.

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45

Parsons, Drew F., Bradley I. Boone, Philip G. Jessop, and Susan C. Tucker. "Electrostriction effects on competing transition states in supercritical fluoroform." Journal of Supercritical Fluids 24, no. 2 (November 2002): 173–81. http://dx.doi.org/10.1016/s0896-8446(02)00032-3.

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46

He, Lisi, Xinkan Yang, and Gavin Chit Tsui. "Domino Hydroboration/Trifluoromethylation of Alkynes Using Fluoroform-Derived [CuCF3]." Journal of Organic Chemistry 82, no. 12 (May 31, 2017): 6192–201. http://dx.doi.org/10.1021/acs.joc.7b00755.

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47

Chabinyc, Michael L., and John I. Brauman. "Unusual Ionic Hydrogen Bonds: Complexes of Acetylides and Fluoroform." Journal of the American Chemical Society 122, no. 36 (September 2000): 8739–45. http://dx.doi.org/10.1021/ja000806z.

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48

Pashaev Mamed Alirza Ogly, Baskakov Oleg Igorevitch, Polevoy Boris Ivanovitch, and Dyubko Stanislav Filippovitch. "Centrifugal distortion in the submillimete rotational spectrum of fluoroform." Journal of Molecular Spectroscopy 131, no. 1 (September 1988): 1–8. http://dx.doi.org/10.1016/0022-2852(88)90100-2.

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49

Folléas, Benoı̂t, Ilan Marek, Jean-F. Normant, and Laurent Saint-Jalmes. "Fluoroform: an Efficient Precursor for the Trifluoromethylation of Aldehydes." Tetrahedron 56, no. 2 (January 2000): 275–83. http://dx.doi.org/10.1016/s0040-4020(99)00951-5.

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50

Nishimura, Hiroyuki, and Yoshiharu Nakamura. "Total Electron Scattering Cross Sections for Fluoroform and Trifluoroiodomethane." Journal of the Physical Society of Japan 74, no. 4 (April 2005): 1160–69. http://dx.doi.org/10.1143/jpsj.74.1160.

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