Academic literature on the topic 'Flow Synthesis'
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Journal articles on the topic "Flow Synthesis"
Yoshida, Jun-ichi, Aiichiro Nagaki, and Daisuke Yamada. "Continuous flow synthesis." Drug Discovery Today: Technologies 10, no. 1 (March 2013): e53-e59. http://dx.doi.org/10.1016/j.ddtec.2012.10.013.
Full textXuefan Gu, Xuefan Gu, Peng Wang Peng Wang, Zhen Guo Zhen Guo, Weichao Du Weichao Du, and Sanbao Dong Sanbao Dong. "Synthesis and Evaluation of Hydroxymethyl Tetramides as Flow Improvers for Crude Oil." Journal of the chemical society of pakistan 42, no. 4 (2020): 488. http://dx.doi.org/10.52568/000658.
Full textXuefan Gu, Xuefan Gu, Peng Wang Peng Wang, Zhen Guo Zhen Guo, Weichao Du Weichao Du, and Sanbao Dong Sanbao Dong. "Synthesis and Evaluation of Hydroxymethyl Tetramides as Flow Improvers for Crude Oil." Journal of the chemical society of pakistan 42, no. 4 (2020): 488. http://dx.doi.org/10.52568/000658/jcsp/42.04.2020.
Full textKamptmann, Sonja B., and Steven V. Ley. "Facilitating Biomimetic Syntheses of Borrerine Derived Alkaloids by Means of Flow-Chemical Methods." Australian Journal of Chemistry 68, no. 4 (2015): 693. http://dx.doi.org/10.1071/ch14530.
Full textJunkers, Thomas, and Richard Hoogenboom. "Advanced polymer flow synthesis." European Polymer Journal 80 (July 2016): 175–76. http://dx.doi.org/10.1016/j.eurpolymj.2016.05.006.
Full textKobayashi, Shū. "Flow “Fine” Synthesis: High Yielding and Selective Organic Synthesis by Flow Methods." Chemistry - An Asian Journal 11, no. 4 (October 20, 2015): 425–36. http://dx.doi.org/10.1002/asia.201500916.
Full textMougeot, Romain, Philippe Jubault, Julien Legros, and Thomas Poisson. "Continuous Flow Synthesis of Propofol." Molecules 26, no. 23 (November 26, 2021): 7183. http://dx.doi.org/10.3390/molecules26237183.
Full textWatts, Paul, and Charlotte Wiles. "Micro reactors, flow reactors and continuous flow synthesis." Journal of Chemical Research 36, no. 4 (April 1, 2012): 181–93. http://dx.doi.org/10.3184/174751912x13311365798808.
Full textBritton, Joshua, and Colin L. Raston. "Multi-step continuous-flow synthesis." Chemical Society Reviews 46, no. 5 (2017): 1250–71. http://dx.doi.org/10.1039/c6cs00830e.
Full textKyprianou, Dimitris, Michael Berglund, Giovanni Emma, Grzegorz Rarata, David Anderson, Gabriela Diaconu, and Vassiliki Exarchou. "Synthesis of 2,4,6-Trinitrotoluene (TNT) Using Flow Chemistry." Molecules 25, no. 16 (August 6, 2020): 3586. http://dx.doi.org/10.3390/molecules25163586.
Full textDissertations / Theses on the topic "Flow Synthesis"
Simon, Mark David. "Fast flow biopolymer synthesis." Thesis, Massachusetts Institute of Technology, 2017. http://hdl.handle.net/1721.1/117929.
Full textCataloged from PDF version of thesis.
Includes bibliographical references (pages 125-129).
This thesis describes the development and application of fast flow solid phase synthesis for the preparation of peptides and phosphorodiamidate morpholino oligomers (PMOs), as well as the application of fast, reliable peptide synthesis to study non-natural protein folding and function. In the first chapter, solid supported peptide synthesis was accelerated using flow by continuously delivering preheated solvents and reagents to the solid support at high flow rate, thereby maintaining maximal concentrations, quickly exchanging reagents, and eliminating the need to heat reagents after they were added to the vessel. In the second chapter, these chemical principles were expanded upon and mechanical challenges particular to accelerated solid phase synthesis were overcome to build a fully automated fast flow peptide synthesizer than incorporates amino acids in as little as 40 seconds each. First, mechanical systems were developed to rapidly switch between the many reagents needed for peptide synthesis while maintaining the proper stoichiometry of all reaction components at all times. Second, conditions under which reagents did not appreciably degrade during storage or synthesis were found. Finally, synthetic outcomes were substantially improved by increasing temperature without degrading the protected, resin bound peptide. The third chapter describes the expansion of fast flow synthesis to PMOs. A 10-fold acceleration of PMO synthesis was realized using mechanical systems adapted from chapter 1, increasing the reaction temperature to 90°C, and introducing a Lewis acid catalyst. The acidity of the deprotection reagent was reduced to prevent cleavage of the backbone during 3' detritylation. In the final chapter, a "D-scan" of two small proteins, the disulfide-rich Ecballium elaterium trypsin inhibitor II (EETI-II) and a minimized Z domain of protein A (Z33), is reported. For each protein, the chirality of one amino acid at a time was inverted to generate a series of diastereomers, and study the critical stereocenters of EETI-I and Z33. Twelve out of 30 EETI-II analogs folded and were high-affinity trypsin inhibitors, but most active analogs were less stable to reduction than EETI-II. Similarly, twelve Z33 analogs retained high binding affinity to IgG, but most were substantially less stable than WT-Z33.
by Mark David Simon.
Ph. D.
Mijalis, Alexander James. "Automated flow peptide synthesis." Thesis, Massachusetts Institute of Technology, 2018. http://hdl.handle.net/1721.1/118272.
Full textCataloged from PDF version of thesis.
Includes bibliographical references.
Though reported by Merrifield nearly sixty years ago, batch solid phase peptide synthesis remains slow at minutes to hours per residue. Here we report a fully automated, flow based approach to solid phase polypeptide synthesis with amide bond formation in seven seconds and total synthesis times of forty seconds per amino acid residue. Crude peptide purities and isolated yields were comparable to standard batch solid phase peptide synthesis. Process monitoring with absorbance spectroscopy allows for the immediate detection and rapid optimization of difficult-to-synthesize peptides. This instrument is flexible and allows for synthesis of peptide nucleic acids, glycopeptides, removal of orthogonal amine protecting groups, and click chemistry on the solid phase. At full capacity, this approach to peptide synthesis can yield tens of thousands of individual 30-mer peptides per year.
by Alexander James Mijalis.
Ph. D.
Hayes, Simon Jonathan. "Flow system for heterocyclic synthesis." Thesis, Cardiff University, 2007. http://orca.cf.ac.uk/54663/.
Full textPhillips, Thomas William. "Flow synthesis of silver nanowires." Thesis, Imperial College London, 2016. http://hdl.handle.net/10044/1/64907.
Full textRoper, Kimberley Ann. "New flow chemistry methods for organic synthesis." Thesis, University of Cambridge, 2013. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.607846.
Full textKelly, Liam P. (Liam Porter). "Development of a continuous-flow synthesis of neostigmine methylsulfate and studies toward a continuous-flow synthesis of lisinopril." Thesis, Massachusetts Institute of Technology, 2019. https://hdl.handle.net/1721.1/122853.
Full textCataloged from PDF version of thesis.
Includes bibliographical references.
[color illustration] Herein, we describe the development of a continuous flow synthesis of neostigmine methyl sulfate, an acetylcholinesterase inhibitor on the WHO list of essential medicines, and the transfer of the synthesis into a next-generation reconfigurable frame developed by our collaborators. Starting from 3-dimethylaminophenol, the synthesis provides a throughput of approximately 46.8 g/day (or 93,600 doses/day) of crude neostigmine methyl sulfate. The synthesis also showcases a prototype in-line evaporation unit that operates without any added carrier gas. Dr. Christina Dai performed early screening of lithium bases. Dr. Yuqing Cui and Dr. Naomi Briggs developed the downstream purification sequence. Dr. Nopphon Weeranoppanant developed the in-line evaporator and, along with Dr. Dale Thomas, assisted with performing the synthesis within their developed frame. Liam P. Kelly developed the continuous synthesis of neostigmine methyl sulfate. [color illustration] Lisinopril is a member of a large family of ACE inhibitors generally known as N-carboxyethyl dipeptides. Of this family, lisinopril is the most commonly prescribed. All known routes to lisinopril require isolation of several synthetic intermediates and protecting group manipulations, thus, development of an efficient continuous synthesis would provide great benefit. Herein we describe our investigation of several routes to generate intermediates of lisinopril with the end goal of a fully continuous synthesis, high material throughput, and minimal protecting group manipulations. Liam P. Kelly performed all work described within this chapter.
by Liam P. Kelly.
Ph. D.
Ph.D. Massachusetts Institute of Technology, Department of Chemistry
Lau, Shing Hing. "Organic synthesis : taming chemistry using enabling technologies." Thesis, University of Cambridge, 2018. https://www.repository.cam.ac.uk/handle/1810/273347.
Full textPrinzi, Roberta. "Synthesis of functional polymers by flow processes." Master's thesis, Alma Mater Studiorum - Università di Bologna, 2018. http://amslaurea.unibo.it/15804/.
Full textOnder, Aylin. "Synthesis Of Zeolite Membranes In Flow System." Master's thesis, METU, 2012. http://etd.lib.metu.edu.tr/upload/12614815/index.pdf.
Full textC and 220°
C, and the corresponding system pressures were approximately 20 and 30 bars for MFI and SAPO-34, respectively. The CH4 and n-C4H10 single gas permeances were measured through MFI membranes and the performance of membranes was investigated in the separation of equimolar CH4/n-C4H10 mixtures. The best MFI membrane had a CH4 single gas permeance of 1.45x10-6 mol/m2-s-Pa and CH4/n-C4H10 ideal selectivity of 35 at 25oC. The membranes preferentially permeated n-C4H10 in the separation of mixtures. The n-C4H10/CH4 separation selectivity was 43.6 with a total permeance of approximately 0.8x10-6 mol/m2-s-Pa at 25oC. The ideal selectivities of CO2/CH4 of SAPO-34 membrane synthesized in stagnant medium were 227, and >
1000 at 220 and 200oC, respectively. Formation of amorphous structure and the additional secondary phases (impurities) were observed on SAPO-34 membranes synthesized in recirculating flow system. The results showed that it is possible to produce SAPO-34 and high quality MFI membranes by a recirculating flow system operating at elevated temperature.
Nagy, Kevin David. "Catalyst immobilization techniques for continuous flow synthesis." Thesis, Massachusetts Institute of Technology, 2011. http://hdl.handle.net/1721.1/70405.
Full textCataloged from PDF version of thesis.
Includes bibliographical references (p. 181-199).
Catalytic processes are ubiquitous in both research and industrial settings. As continuous flow processes continue to gain traction in research labs and fine and pharmaceutical chemical processes, new opportunities exist for implementing previously difficult catalytic transformations. The major goal of this thesis is to expand and evaluate techniques for immobilized catalyst systems relevant to continuous flow. Fundamental studies in characterizing mixing, dispersion, and residence time distributions in small scale continuous flow systems are also presented. Given the numerous benefits associated with studying chemical processes at small length scales, microfluidic devices are the tool of choice for most studies in this thesis. Thermomorphic solvents offer the potential for homogeneous catalytic processes with biphasic catalyst recovery and recycle. A major limitation of these processes is the number of synthetically useful thermomorphic solvent combinations demonstrated in literature. A screening program using the modified UNIFAC (Dortmund) activity coefficient model to evaluate phase splitting behavior has been developed to predict thermomorphic behavior. Calculation of 861 binary solvent combinations results in 43 potential thermomorphic and 44 biphasic solvent combinations. Extension of the program to ternary solvents resulted in a new class of ternary solvents that display thermomorphic behavior with tunable critical solution temperatures. Evaluation of thermomorphic processes as a general method is presented. Traditional catalyst immobilization techniques rely on covalent grafting and are well suited to continuous flow processing due to the strong interactions of the catalyst to the support. Fluorous physisorption, which relies on interactions between a fluorous support and a fluorous-tagged catalyst, is characterized and presented as an immobilization technique for flow chemistry. The use of a fluorous-tagged Co(III)-salen catalyst to effect the ring opening of epoxyhexane with water is presented. Application of the platform to the ring closing metathesis of N,Ndiallyltosylamide using a fluorous-tagged Hoveyda-Grubbs metathesis catalyst results in significantly accelerated loss of activity over time compared to the salen catalyst. Use of continuous flow selective adsorption reactors to enhance catalytic processes is presented. Continuous feeds of a homogeneous catalyst into a sorbent where the catalyst displays an affinity for the sorbent results in accumulation of the catalyst in the packed bed. The net effect is an enhancement in turnover frequency and turnover number relative to homogeneous flow. Application of this platform to a Lewis acid catalyzed Diels-Alder reaction results in an order of magnitude improvement in turnover frequency compared to batch and homogeneous flow.
by Kevin David Nagy.
Ph.D.
Books on the topic "Flow Synthesis"
Yoshida, Jun-Ichi. Basics of flow microreactor synthesis. Tokyo: Springer, 2015.
Find full textYoshida, Jun-ichi. Basics of Flow Microreactor Synthesis. Tokyo: Springer Japan, 2015. http://dx.doi.org/10.1007/978-4-431-55513-1.
Full textTundo, Pietro. Continuous flow methods in organic synthesis. New York: Ellis Horwood, 1991.
Find full textSharma, Upendra K., and Erik V. Van der Eycken, eds. Flow Chemistry for the Synthesis of Heterocycles. Cham: Springer International Publishing, 2018. http://dx.doi.org/10.1007/978-3-319-94328-2.
Full textLuis, S. V. Chemical reactions and processes under flow conditions. Cambridge, UK: RSC Publishing, 2010.
Find full textHuntington, Del, and Jerilyn C. Wen. Access rights: A synthesis of highway practice. Washington, D.C: Transportation Research Board, National Research Council, 2005.
Find full textHabana, Nathan C. Vadose flow synthesis for the Northern Guam Lens Aquifer. Agana, Guam]: Water and Environmental Research Institute of the Western Pacific (WERI), University of Guam, 2009.
Find full textJ, Skoch G., Prahst P. S, and United States. National Aeronautics and Space Administration., eds. Aerodynamic synthesis of a centrifugal impeller using CFD and measurements. [Washington, DC: National Aeronautics and Space Administration, 1997.
Find full textSaito, Yuki. Multistep Continuous Flow Synthesis of Fine Chemicals with Heterogeneous Catalysts. Singapore: Springer Nature Singapore, 2023. http://dx.doi.org/10.1007/978-981-19-7258-4.
Full textA, Ladd J., Yuhas A. J, and United States. National Aeronautics and Space Administration., eds. Dynamic inlet distortion prediction with a combined computational fluid dynamics and distortion synthesis approach. [Washington, DC: National Aeronautics and Space Administration, 1996.
Find full textBook chapters on the topic "Flow Synthesis"
Grass, Werner, Wolf-Dieter Tiedemann, Carlos Delgado Kloos, and André Marin López. "Synthesis Flow." In Practical Formal Methods for Hardware Design, 81–96. Berlin, Heidelberg: Springer Berlin Heidelberg, 1997. http://dx.doi.org/10.1007/978-3-642-60641-0_5.
Full textTaraate, Vaibbhav. "ASIC Design Flow." In ASIC Design and Synthesis, 13–26. Singapore: Springer Singapore, 2021. http://dx.doi.org/10.1007/978-981-33-4642-0_2.
Full textCrissman, Harry A. "Bromodeoxuridine Procedures for Analysis of DNA Synthesis." In Flow Cytometry, 245–58. Berlin, Heidelberg: Springer Berlin Heidelberg, 1993. http://dx.doi.org/10.1007/978-3-642-84616-8_16.
Full textFinkbeiner, Bernd, Niklas Metzger, and Yoram Moses. "Information Flow Guided Synthesis." In Computer Aided Verification, 505–25. Cham: Springer International Publishing, 2022. http://dx.doi.org/10.1007/978-3-031-13188-2_25.
Full textFrank, R., H. Leban, M. Kraft, and H. Gausepohl. "Continuous flow peptide synthesis." In Peptides, 215–16. Dordrecht: Springer Netherlands, 1988. http://dx.doi.org/10.1007/978-94-010-9595-2_63.
Full textVanden Bussche, K. M., G. F. Froment, W. Glasz, H. Bosch, and L. L. Vandierendonck. "Reversed Flow Methanol Synthesis." In Energy Efficiency in Process Technology, 1154–68. Dordrecht: Springer Netherlands, 1993. http://dx.doi.org/10.1007/978-94-011-1454-7_102.
Full textCortadella, J., M. Kishinevsky, A. Kondratyev, L. Lavagno, and A. Yakovlev. "Design Flow." In Logic Synthesis for Asynchronous Controllers and Interfaces, 13–27. Berlin, Heidelberg: Springer Berlin Heidelberg, 2002. http://dx.doi.org/10.1007/978-3-642-55989-1_2.
Full textFukuyama, Takahide, Akihiro Furuta, and Ilhyong Ryu. "Continuous Flow Synthesis Using Recyclable Reaction Media." In Sustainable Flow Chemistry, 25–42. Weinheim, Germany: Wiley-VCH Verlag GmbH & Co. KGaA, 2017. http://dx.doi.org/10.1002/9783527689118.ch2.
Full textShang, Minjing, and Volker Hessel. "Synthesis and Application of H2O2in Flow Reactors." In Sustainable Flow Chemistry, 43–72. Weinheim, Germany: Wiley-VCH Verlag GmbH & Co. KGaA, 2017. http://dx.doi.org/10.1002/9783527689118.ch3.
Full textChatjigeorgiou, Ioannis K. "Inner Flow Models." In Synthesis Lectures on Ocean Systems Engineering, 71–102. Cham: Springer International Publishing, 2023. http://dx.doi.org/10.1007/978-3-031-24827-6_4.
Full textConference papers on the topic "Flow Synthesis"
Mohanty, Priti Sundar. "Synthesis and Characterization of Polyelectrolyte Grafted Charged Colloidal Particles." In FLOW DYNAMICS: The Second International Conference on Flow Dynamics. AIP, 2006. http://dx.doi.org/10.1063/1.2204506.
Full textBaxendale, Ian R. "Continuous Chemical Synthesis in Flow." In 15th Brazilian Meeting on Organic Synthesis. São Paulo: Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-speech12.
Full textLy, Vincent, and Chandra Kambhamettu. "Mobile Scene Flow Synthesis." In 2013 IEEE International Symposium on Multimedia (ISM). IEEE, 2013. http://dx.doi.org/10.1109/ism.2013.85.
Full textChu, Qing, Sarah Knepper, James Nagy, and Stuart Jefferies. "Fast PSF reconstruction using the frozen flow hypothesis." In Signal Recovery and Synthesis. Washington, D.C.: OSA, 2011. http://dx.doi.org/10.1364/srs.2011.smc4.
Full textYamamoto, G. "Route to the Synthesis of Binder-Free SWCNT Solids with Enhanced Mechanical Properties." In FLOW DYNAMICS: The Second International Conference on Flow Dynamics. AIP, 2006. http://dx.doi.org/10.1063/1.2204535.
Full textFlores, Marcella C., Ivaldo I. Junior, Felipe K. Sutili, Ivana C. R. Leal, Leandro S. M. e. Miranda, and Rodrigo O. M. A. de Souza. "Towards Biocatalytic Reactions Under Continuous Flow Conditions." In 14th Brazilian Meeting on Organic Synthesis. São Paulo: Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-14bmos-r0098-1.
Full textScott-Fleming, Ian, Keith Hege, David Clyde, Donald Fraser, and Andrew Lambert. "Gradient-based optical flow techniques for tracking image motion due to atmospheric turbulence." In Signal Recovery and Synthesis. Washington, D.C.: OSA, 2001. http://dx.doi.org/10.1364/srs.2001.stub3.
Full textMurray, Philip R. D., Duncan L. Browne, Julio C. Pastre, and Steven V. Ley. "Continuous Flow-Processing of Organometallic Reagents Using an Advanced Peristaltic Pumping System and the Telescoped Flow Synthesis of (E/Z)-Tamoxifen." In 15th Brazilian Meeting on Organic Synthesis. São Paulo: Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-bmos2013_2013914162643.
Full textBombana, Massimo, Patrizia Cavalloro, Salvatore Conigliaro, Roger B. Hughes, Gerry Musgrave, and Giuseppe Zaza. "Design-flow and synthesis for ASICs." In the 32nd ACM/IEEE conference. New York, New York, USA: ACM Press, 1995. http://dx.doi.org/10.1145/217474.217544.
Full textBhat, Kiran S., Steven M. Seitz, Jessica K. Hodgins, and Pradeep K. Khosla. "Flow-based video synthesis and editing." In ACM SIGGRAPH 2004 Papers. New York, New York, USA: ACM Press, 2004. http://dx.doi.org/10.1145/1186562.1015729.
Full textReports on the topic "Flow Synthesis"
Parsons, Jean Louise, and Kristen Deanne Morris. Synthesis Flow. Ames (Iowa): Iowa State University. Library, January 2019. http://dx.doi.org/10.31274/itaa.9546.
Full textEvans, Amanda. Favipiravir Flow Synthesis. Office of Scientific and Technical Information (OSTI), October 2020. http://dx.doi.org/10.2172/1673355.
Full textTremblay, T., and M. Lamothe. New contributions to the ice-flow chronology in the Boothia-Lancaster Ice Stream catchment area. Natural Resources Canada/CMSS/Information Management, 2022. http://dx.doi.org/10.4095/331062.
Full textTremblay, T., and M. Lamothe. New contributions to the ice-flow chronology in the Boothia-Lancaster ice-stream catchment area, Nunavut. Natural Resources Canada/CMSS/Information Management, 2023. http://dx.doi.org/10.4095/331424.
Full textVarga, Gabriella A., Amichai Arieli, Lawrence D. Muller, Haim Tagari, Israel Bruckental, and Yair Aharoni. Effect of Rumen Available Protein, Amimo Acids and Carbohydrates on Microbial Protein Synthesis, Amino Acid Flow and Performance of High Yielding Cows. United States Department of Agriculture, August 1993. http://dx.doi.org/10.32747/1993.7568103.bard.
Full textSmall, Leo J., Harry Pratt, Chad Staiger, Rachel Irene Martin, Travis Mark Anderson, Babu Chalamala, Thiagarajan Soundappan, Monika Tiwari, and Venkat R. Subarmanian. Vanadium Flow Battery Electrolyte Synthesis via Chemical Reduction of V2O5 in Aqueous HCl and H2SO4. Office of Scientific and Technical Information (OSTI), January 2017. http://dx.doi.org/10.2172/1342368.
Full textMcGuire, Mark A., Amichai Arieli, Israel Bruckental, and Dale E. Bauman. Increasing Mammary Protein Synthesis through Endocrine and Nutritional Signals. United States Department of Agriculture, January 2001. http://dx.doi.org/10.32747/2001.7574338.bard.
Full textBurton Davis, Gary Jacobs, Wenping Ma, Khalid Azzam, Janet ChakkamadathilMohandas, and Wilson Shafer. Sensitivity of Fischer-Tropsch Synthesis and Water-Gas Shift Catalystes to Poisons form High-Temperature High-Pressure Entrained-Flow (EF) Oxygen-Blown Gasifier Gasification of Coal/Biomass Mixtures. Office of Scientific and Technical Information (OSTI), September 2009. http://dx.doi.org/10.2172/1002145.
Full textBurtron Davis, Gary Jacobs, Wenping Ma, Khalid Azzam, Dennis Sparks, and Wilson Shafer. Sensitivity of Fischer-Tropsch Synthesis and Water-Gas Shift Catalysts to Poisons from High-Temperature High-Pressure Entrained-Flow (EF) Oxygen-Blown Gasifier Gasification of Coal/Biomass Mixtures. Office of Scientific and Technical Information (OSTI), September 2010. http://dx.doi.org/10.2172/1002146.
Full textDavis, Burton, Gary Jacobs, Wenping Ma, Dennis Sparks, Khalid Azzam, Janet Chakkamadathil Mohandas, Wilson Shafer, and Venkat Ramana Rao Pendyala. Sensitivity of Fischer-Tropsch Synthesis and Water-Gas Shift Catalysts to Poisons from High-Temperature High-Pressure Entrained-Flow (EF) Oxygen-Blown Gasifier Gasification of Coal/Biomass Mixtures. Office of Scientific and Technical Information (OSTI), September 2011. http://dx.doi.org/10.2172/1052997.
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