Academic literature on the topic 'Energy Dispersive Analysis X-ray (EDAX)'

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Journal articles on the topic "Energy Dispersive Analysis X-ray (EDAX)"

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Bedboudi, H., A. Bourbia, M. Draissia, and M. Y. Debili. "X-Ray Diffraction Studies of Nanostructured Metallic Alloys." Journal of Nano Research 3 (October 2008): 45–58. http://dx.doi.org/10.4028/www.scientific.net/jnanor.3.45.

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X-ray tools are being powerful methods for qualitative and quantitative analyses of nanocrystalline materials This work is an overview of detailed X-ray investigations relative to microstructural studies applied for a refined binary Al-based alloys thin films system as samples deposited on glass substrates. Energy dispersive analysis of X-ray (EDAX), X-ray diffraction (XRD) and transmission electron microscopy (TEM) methods were used to determine the chemical composition, the microstructure parameters and the solubility of copper in aluminum.
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Chauhan, Harendra Pratap Singh, Sapana Joshi, Abhilasha Bakshi, and Jaswant Carpenter. "Structural investigation on toluene-3,4-dithiolatoantimony(iii) alkyldithiocarbonate complexes: thermal, powder XRD and biological studies." New Journal of Chemistry 39, no. 3 (2015): 2279–88. http://dx.doi.org/10.1039/c4nj02094d.

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On thermal decomposition of the mixed sulfur donor antimony(iii) complexes, we obtained antimony sulfide at 600 °C, which was confirmed by scanning electron microscopy (SEM) and energy dispersive X-ray analysis (EDAX).
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Bamzai, K. K., Nidhi Kachroo, Vishal Singh, and Seema Verma. "Synthesis, Characterization, and Thermal Decomposition of Pure and Dysprosium Doped Yttrium Phosphate System." Journal of Materials 2013 (April 18, 2013): 1–8. http://dx.doi.org/10.1155/2013/359514.

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Yttrium phosphate and dysprosium doped yttrium phosphate were synthesized from aqueous solutions using rare earth chloride, phosphoric acid, and traces of ammonium hydroxide. The synthesized material was then characterized for their structural investigations using powder X-ray diffraction (XRD) analysis and scanning electron microscopy (SEM) supplemented with energy dispersive X-ray analysis (EDAX). The spectroscopic investigations were carried out using Fourier transform infrared (FTIR) spectroscopy. The thermal stability was studied using differential thermogravimetric analysis (DTA), thermogravimetric analysis (TGA), and differential scanning calorimetry (DSC) techniques. X-ray diffraction analysis reveals that both yttrium phosphate and dysprosium doped yttrium phosphate belong to tetragonal system with lattice parameter Å, Å and Å, Å, respectively. The stoichiometry of the grown composition was established by energy dispersive X-ray analysis. The EDAX analysis suggests the presence of water molecules. The presence of water molecules along with orthophosphate group and metallic ion group was confirmed by FTIR analysis. Thermogravimetric analysis suggests that decomposition in case of yttrium phosphate takes place in three different stages and the final product stabilizes after 706°C, whereas in case of dysprosium doped yttrium phosphate the decomposition occurs in two different stages, and the final product stabilizes after 519°C.
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Rao, Rameshwar, V. Rajendar, and K. Venkateswara Rao. "Structural and Optical Properties of ZnO Nano Particles Synthesised by Mixture of Fuel Approach in Solution Chemical Combustion." Advanced Materials Research 629 (December 2012): 273–78. http://dx.doi.org/10.4028/www.scientific.net/amr.629.273.

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Zinc oxide has been used for many applications, for example optoelectronic devices, ceramics, catalysts, pigments, varistors and many other important applications. In this study, ZnO nanoparticles were synthesized by mixture of fuel approach in solution chemical combustion method. Mixtures of Urea and Zinc salts were mixed at room temperature resulting in spontaneous ignition because these are hypergolic materials resulting in production of ZnO nanopowder. The crystal structure and size of the synthesized powder were determined by X- ray diffractometer (XRD), which revealed that the synthesized ZnO nanopowder has the pure wurtzite structure having average crystallite size of 30nm. Morphological studies were carried out by scanning electron microscopy (SEM), Energy Dispersive X-ray analysis (EDAX) was carried out by Scanning electron microscopy (SEM) with energy dispersive X-ray spectroscopy (EDAX), Optical studies were examined by FT-IR and UV-Visible absorption spectrum and the particle size was estimated from Nanoparticle size analyzer.
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AMARSINGH BHABU, K., J. DHIVYA SARANYA, and T. R. RAJASEKARAN. "PREPARATION AND CHARACTERIZATION OF Ce0.8Y0.2O2 NANOPOWDERS USING SOL-GEL METHOD." International Journal of Modern Physics: Conference Series 22 (January 2013): 533–44. http://dx.doi.org/10.1142/s2010194513010635.

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Nanopowders of Ce0.8Y0.2O2 were prepared by sol-gel via hydrolysis method for different hours. The prepared powders are characterized by powder X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), Scanning electron microscope (SEM) and analyzed by UV-visible spectroscopy, Photoluminescence (PL) and Energy dispersive X-ray analysis (EDAX). Cubic fluorite structure of the prepared samples was confirmed by powder X-ray diffraction and the grain size of the prepared samples in the range of 12 to 33 nm. The functional groups of the prepared nanopowders are identified by FTIR spectra. The band gap energy obtained from the UV spectra. From the photoluminescence spectra, there is a mirror image relation between absorption and emission spectra. The purity of the prepared samples is confirmed by EDAX measurements.
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Sivanand, R., S. Chellammal, and S. Manivannan. "Synthesis, Structural Analysis of Cadmium Sulphide Nanocrystallites." Materials Science Forum 969 (August 2019): 169–74. http://dx.doi.org/10.4028/www.scientific.net/msf.969.169.

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In this paper, the effect of size variation of cadmium sulphide nanocrystallites which have been prepared by precipitation method is analyzed. These prepared samples were studied using X-ray diffraction (XRD), Scanning electron microscopy (SEM), and Energy dispersive analysis of spectroscopy (EDAX) techniques. SEM analysis represents the morphological nature of prepared samples and EDAX indicates the confirmation of elements present in the sample. XRD analysis determines the size of the samples and identifies the structure using miller indices (h k l values) of the nanocrystallies matches with JCPDS. From the XRD analysis, the size variation which depends on dopant, capping agent are discussed and corresponding results are reported in this paper.
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Sangu, V., Rajeswari C. Raja, K. Shenbagam, and N. Sowmiya. "Green synthesis of magnesium oxide nanoparticles: characterisation for sonocatalytic ability to remove Alizarin Red S dye in aqueous solution." Research Journal of Chemistry and Environment 27, no. 2 (January 15, 2023): 106–13. http://dx.doi.org/10.25303/2702rjce1060113.

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In this present work, MgO nanoparticles have been successfully synthesized by using Tribulus Terrestris leaf extract and were characterized by UV-Vis spectrophotometer. Dispersity and surface morphology were analyzed by dynamic light scattering and scanning electron microscope (SEM). Crystal nature and purity of the MgO nanoparticles were analyzed using X-ray diffraction analysis (XRD) and energy dispersive X-ray analysis (EDAX). FTIR analysis showed functional groups present in the phytochemicals of Tribulus Terrestris plant extract responsible for reduction and stabilization of MgO nanoparticles. The sonocatalytic efficiency of MgO nanoparticles was examined by degrading Alizarin Red S (ARS) under ultrasonic sound irradiation. Green synthesized MgO nanoparticles effectively degraded the dye nearly 95% within 5 hrs. of exposer time.
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Chellamal, S., A. P. Karthikeyan, P. Harsha, and S. Manivannan. "Structural Properties of Size Variation of Nanocrystallites." Applied Mechanics and Materials 813-814 (November 2015): 226–29. http://dx.doi.org/10.4028/www.scientific.net/amm.813-814.226.

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Silver doped cadmium sulphide nanocrystallites (CdS:Ag), undoped cadmium sulphide nanocrystallites (CdS), have been synthesized by the chemical precipitation method. Nanocrystalline materials are confirmed by the scanning electron microscopy method. The presented elements are identified by EDAX (Energy Dispersive X-ray Analysis). X-ray diffraction Method (XRD) is used to calculate the average size of the prepared sample. Morphological studies (SEM) are used to analyse the nature of the sample. The results are reported in this paper.
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Naskar, Amit Kumar, S. K. De, and Anil K. Bhowmick. "Surface Chlorination of Ground Rubber Tire and its Characterization." Rubber Chemistry and Technology 74, no. 4 (September 1, 2001): 645–61. http://dx.doi.org/10.5254/1.3544964.

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Abstract Ground rubber tire (GRT) powders were chlorinated by trichloroisocyanuric acid (TCLCA). GRT powders of different chlorination levels were characterized by X-ray photoelectron spectroscopy (XPS), energy dispersive X-ray spectroscopy (EDAX), attenuated total reflection infrared (ATR-IR) spectroscopy, thermal, dielectric, and stress—strain properties on molded GRT specimens. Surface energy of the powders was estimated. Dynamic mechanical thermal analysis of molded GRT specimen reveals a biphasic structure. Plasticized poly(vinyl chloride) (PVC) compound, when blended with chlorinated GRT, shows improved physical properties in comparison to non-chlorinated GRT.
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Mayall, Frederick, and David Wild. "A silver tattoo of the nasal mucosa after silver nitrate cautery." Journal of Laryngology & Otology 110, no. 6 (June 1996): 609–10. http://dx.doi.org/10.1017/s0022215100134395.

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AbstractWe report a silver tattoo of the nasal mucosa that occurred after silver nitrate cautery for nasal bleeding. Ths type of tattoo is a very rare potential mimic of melanoma and appears not to have been described before. It has similar features to an amalgam tattoo of the oral mucosa on histology and energy dispersive X-ray analysis (EDAX).
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Dissertations / Theses on the topic "Energy Dispersive Analysis X-ray (EDAX)"

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Canli, Sedat. "Thickness Analysis Of Thin Films By Energy Dispersive X-ray Spectroscopy." Master's thesis, METU, 2010. http://etd.lib.metu.edu.tr/upload/12612822/index.pdf.

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EDS is a tool for quantitative and qualitative analysis of the materials. In electron microscopy, the energy of the electrons determines the depth of the region where the X-rays come from. By varying the energy of the electrons, the depth of the region where the X-rays come from can be changed. If a thin film is used as a specimen, different quantitative ratios of the elements for different electron energies can be obtained. Unique thickness of a specific film on a specific substrate gives unique energy-ratio diagram so the thickness of a thin film can be calculated by analyzing the fingerprints of the energy-ratio diagram of the EDS data obtained from the film.
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Slater, Thomas Jack Alfred. "Three dimensional chemical analysis of nanoparticles using energy dispersive X-ray spectroscopy." Thesis, University of Manchester, 2015. https://www.research.manchester.ac.uk/portal/en/theses/three-dimensional-chemical-analysis-of-nanoparticles-using-energy-dispersive-xray-spectroscopy(3eb607a2-eb03-4d45-b9eb-71b0ca45c2db).html.

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The aim of this thesis is to investigate the methodology of three dimensional chemical imaging of nanoparticles through the use of scanning transmission electron microscope (STEM) – energy dispersive X-ray (EDX) spectroscopy. In this thesis, an absorption correction factor is derived for spherical nanoparticles that can correct X-ray absorption effects. Quantification of EDX spectra of nanoparticles usually neglects X-ray absorption within the nanoparticle but may lead to erroneous results, thus an absorption correction is important for accurate compositional quantification. The absorption correction presented is verified through comparison with experimental data of Au X-ray peaks in spherical Au nanoparticles and is found to agree excellently. This absorption correction allows accurate compositional quantification of large ( > 100 nm) particles with STEM-EDX.Three dimensional chemical mapping is achievable through the use of EDX spectroscopy with electron tomography. Here, the methodology of STEM-EDX tomography is fully explored, with a focus on how to avoid artefacts introduced through detector shadowing and low counts per pixel. A varied-time acquisition scheme is proposed to correct for detector shadowing that is shown to provide a more constant intensity over a series of projections, allowing a higher fidelity reconstruction. The STEM-EDX tomography methodology presented is applied to the study of AgAu nanoparticles synthesized by the galvanic replacement reaction. The elemental distribution as a function of the composition of the as-synthesized nanoparticles is characterised and a reversal in the element segregated to the surface of the nanoparticles is found. The composition at which the reversal takes place is shown to correlate with a peak in the catalytic yield of a three component coupling reaction. It is hypothesized that a continuous Au surface results in the optimum catalytic conditions for the reaction studied, which guides the use of galvanically prepared AgAu nanoparticles as catalysts.
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Kumari, Maini S. M. "Development of a breast tissue diffraction analysis system using energy dispersive X-ray diffraction." Thesis, University College London (University of London), 2012. http://discovery.ucl.ac.uk/1370578/.

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Research groups have shown that diffraction techniques could be applied for characterising materials. In particular, Energy Dispersive X-ray Diffraction (EDXRD) technique has been successfully used in characterising materials such as plastics, drugs and biological tissues. The size of breast tissues used for characterisation so far has been small, in the range of mm. In order to exploit the fullness of the EDXRD technique in characterising breast tissues and hence enable early and precise breast tumour detection, the presented research work takes the existing research work a step forward by developing a breast tissue diffraction analysis system wherein breast-sized tissue-equivalent materials have been studied for tumour detection and an optimised EDXRD system for breast tissue analysis has been presented. For the development of this breast tissue analysis diffraction system, a ray-tracing model of the EDXRD system has been developed. The model has been used to predict diffraction spectra. These model predictions have been further used to optimize system parameters for an EDXRD system so it could be used for breastsized samples. Materials like plastics, pharmaceutical drugs and tissues have been characterised on this optimized system. The diffraction spectra collected have been used to build a diffraction spectrum database which has been further used to generate diffraction images for detection of tumour of size as small as 0.5 cm. Following this abstract, in the thesis, Chapter 1 introduces how X-rays interact with matter and what research groups have achieved so far in breast tissue diffraction. Ray-tracing model of EDXRD system forms Chapter 2 wherein the system parameters along with the corrections used in the model and model predictions have been presented. The characterisation of materials using optimized EDXRD system has been detailed in Chapter 3. Chapter 4 elaborates the generation of diffraction images. Chapter 5 presents the conclusions and suggests future work. The thesis ends with a list of references.
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Menendez-Alonso, Elena. "Trace metal and speciation analysis using ion-exchange and energy dispersive X-ray fluorescence spectrometry." Thesis, University of Plymouth, 2000. http://hdl.handle.net/10026.1/896.

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Studies have been carried out on specific ion-exchange (Dowex 50W-X8 and Dowex 1-X8) and chelation (Chelex-100) resins, in order to determine their physical and chemical characteristics, to understand and explain their limits of function and to optimise their use as substrates in trace metal and speciation measurement by EDXRF. Structural information was obtained by scanning electron microscopy and x-ray microanalysis showing a homogeneous distribution of functional groups and retained ions on both sectioned and whole resins. Particle size experiments performed on Dowex 50W-X8 (38 - 840 µm) showed that this parameter has no effect on the relationship between intensity of fluorescence and concentration or mass of resin. Inter-element effects were not observed in the analysis of multielemental specimens prepared on ion-exchange / chelation media by EDXRF. This indicates that the proposed method has a significant advantage when compared with other methodologies. A theoretical ‘model’, based on the formation of thin films on the surface of the resin beads, has been proposed in order to link and explain the effects observed in these experiments. The use of a batch retention system has shown distinct advantages over using columns in terms of linearity, accuracy, precision, rapidity and simplicity. Parameters such as pH and ionic strength of the solution, concentration of competing ions and volume of the sample have been proven to be critical. The maximum retention capacity has been determined as 3.2, 1.1 and 0.67 mEq/g for Dowex 50W-X8, Dowex 1-X8 and Chelex-100 respectively. The optimum mass of resin for XRF analysis was found to be 0.5 g, for all resins tested. The linear range covered 4 to 5 orders of magnitude. These findings show the potential of the investigated media to overcome instrumental and sample limitations. Based on the physico-chemical information found, methodologies for three different applications of the resins to EDXRF determinations have been developed and their analytical possibilities explored. The multi-elemental determination of metals in sewage sludge digests was achieved by retaining the metals on Dowex 50W-X8 at pH 2 and Chelex-100 at pH 4. Chelex-100 allows quantitative recoveries for Cu and Zn. A wider range of elements was determined on Dowex 50W-X8, although with poorer recoveries (60 - 90%). The limits of detection were 10 - 21 µg when Dowex 50W-X8 was used and 8 - 49 µg for Chelex-100. The method was validated by the analysis of a certified material. The determination of Kβ/Kα intensity ratios for Cr and Mn species and its potential as a tool for direct elemental speciation has also been studied. A difference in Kβ/Kα between the oxidation states of the analytes was only observed during the analysis of solutions of the metal species by EDXRF at the 98% level of confidence. Finally, the speciation and preconcentration of Cr(III) and Cr(VI) in waters has been performed by retention on Dowex 50W-X8 and Dowex 1-X8 followed by EDXRF determination. Efficient recoveries and preconcentration factors of up to 500 were achieved, leading to limits of detection of 30 µg/L for Cr(VI) and 40 µg/L for Cr(III). This method is simple, fast and inexpensive, allowing quantitative recoveries in the speciation of chromium in waste waters.
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Cook, Emily Jane. "Analysis of energy dispersive x-ray diffraction profiles for material identification, imaging and system control." Thesis, University College London (University of London), 2008. http://discovery.ucl.ac.uk/1446057/.

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This thesis presents the analysis of low angle X-ray scatter measurements taken with an energy dispersive system for substance identification, imaging and system control. Diffraction measurements were made on illicit drugs, which have pseudo- crystalline structures and thus produce diffraction patterns comprising a se ries of sharp peaks. Though the diffraction profiles of each drug are visually characteristic, automated detection systems require a substance identification algorithm, and multivariate analysis was selected as suitable. The software was trained with measured diffraction data from 60 samples covering 7 illicit drugs and 5 common cutting agents, collected with a range of statistical qual ities and used to predict the content of 7 unknown samples. In all cases the constituents were identified correctly and the contents predicted to within 15%. Soft tissues exhibit broad peaks in their diffraction patterns. Diffraction data were collected from formalin fixed breast tissue samples and used to gen erate images. Maximum contrast between healthy and suspicious regions was achieved using momentum transfer windows 1.04-1.10 and 1.84-1.90 nm_1. The resulting images had an average contrast of 24.6% and 38.9% compared to the corresponding transmission X-ray images (18.3%). The data was used to simulate the feedback for an adaptive imaging system and the ratio of the aforementioned momentum transfer regions found to be an excellent pa rameter. Investigation into the effects of formalin fixation on human breast tissue and animal tissue equivalents indicated that fixation in standard 10% buffered formalin does not alter the diffraction profiles of tissue in the mo mentum transfer regions examined, though 100% unbuffered formalin affects the profile of porcine muscle tissue (a substitute for glandular and tumourous tissue), though fat is unaffected.
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Gullayanon, Rutchanee. "A calibration methodology for energy dispersive X-ray fluorescence measurements based upon synthetically generated reference spectra." Diss., Georgia Institute of Technology, 2011. http://hdl.handle.net/1853/42771.

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This research developed an on-line measurement systemfor determining the amount of fluorochemicals on carpet fibers using energy-dispersive X-ray fluorescence (EDXRF).This system is designed as a complementary tool to an existingchemical burn test certified by the American Association ofTextile Chemists and Colorists (AATCC), which is performed off-line on randomly selected carpet samples and time consuming.This research reviewed XRF principles and determined parameters that affect XRF spectra such as measurement time, measurement number, X-ray tube voltage, X-ray tube current, primary beam filter, and carpet characteristics. For this application, XRF calibrations must be performed for carpets of all styles and types. However, preparing actual carpet calibration samples is expensive. This research introduced a methodology to synthetically generate reference spectra using XRF spectra from standard fluorochemical stock solution samples and from base carpet samples for each carpet type to be tested. Thus, actual, physical standards are not required for each carpet type or style. This study showed that the synthetically generated XRF spectra alone were not always sufficient to guarantee the confidence interval required by the certified AATCC test. Thus, it is recommended that for on-line implementation, burn test results should be used to create a historical data base for each carpet type to reduce margin of error for calibrations generated from the synthetic spectra.
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Chisholm, Daniel J. "Use of Principle Component Analysis for the identification and mapping of phases from energy-dispersive x-ray spectra." Thesis, Monterey, Calif. : Springfield, Va. : Naval Postgraduate School ; Available from National Technical Information Service, 1999. http://handle.dtic.mil/100.2/ADA359572.

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Parajuli, Prabin. "EXPERIMENTAL INVESTIGATION OF CORROSION OF COATED CAST IRON ROTORS IN THE AUTOMOTIVE INDUSTRY." OpenSIUC, 2020. https://opensiuc.lib.siu.edu/theses/2711.

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Electric and hybrid vehicles uses regenerative braking, where application of the brake triggers the electric motor to work as a generator to produce electricity, which in turn charges the battery. This results in much less use of the friction brake, changing the corrosion and wear behavior of the rotor surface. There is a need for research on this topic, since fully electric or hybrid vehicles are replacing combustion engines due to concerns about global warming and climate change. Here the corrosion behavior of coated cast iron vehicle rotors in 3.5wt% NaCl is studied. The corrosion study has been performed using electrochemical methods such as cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS). All the coated samples were provided by Pure Forge Rotors. Based on the results from SEM and EDX, the coating is atomic forge proprietary coating, and the base material is gray cast iron. Our primary objective is to study the corrosion behavior of coated, non-coated and friction-tested samples. CV experiments indicate a shift in the corrosion potential and corrosion current density due to changes in the nature of the exposed surface. Cross-sectional SEM showed the thickness of the coating to be 16-23 µm. After friction testing, the friction layer created by rubbing the brake pad over the rotor plays a role in corrosion resistance, but this depends on the type of brake pad material (i.e. semi-metallic, non-asbestos organic and low metallic). Results showed that friction film that forms after testing against non-asbestos organic pads provides the highest corrosion resistance amongst the three brake pad materials.
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Green, Heather F. "Casting no shadow : overlapping soilscapes of European-Indigenous interaction in northern Sweden." Thesis, University of Stirling, 2012. http://hdl.handle.net/1893/13133.

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The Sámi’s past activities have been documented historically from a European perspective, and more recently from an anthropological viewpoint, giving a generalised observation of the Sámi, during the study period of AD200-AD1800, as semi-nomadic hunter gatherers, with several theories suggesting that interaction with Europeans, through trade, led to the adoption of European activities by certain groups of the Sámi (Eiermann, 1923; Paine, 1957; Manker and Vorren, 1962; Bratrein, 1981; Mathiesen et al, 1981; Meriot, 1984). However, there is almost no information on the impact the Sámi had on the landscape, either before or after any adoption of European activities, and none investigating what cultural footprint or indicators would remain from Sámi or European occupation and/or activity within the typically podzolic soils of Northern Sweden. Consequently the thesis aims to contribute to the gap in knowledge through the formation of a podzol model identifying the links between anthropogenic activity and the alteration of podzol soils, and through the creation of soils based models which identify the cultural indicators associated with both Sámi and European activity; formed from the identification of cultural indicators retained within known Sámi and European sites. The methods used to obtain the information needed to achieve this were the pH and magnetic susceptibility from bulk soil samples and micromorphological and chemical analysis of thin section slides through the use of standard microscopy and X-ray fluorescence from a scanning electron microscope. The analysis revealed that the Sámi had an extremely low impact on the landscape, leaving hard to detect cultural indicators related to reindeer herding in the form of reindeer faecal material with corresponding phosphorous peaks in the thin section slides. The European footprint however, was markedly different and very visible even within the acidic soil environment. The European indicators were cultivation based and included phosphorous and aluminium peaks as well as a deepened, highly homogenised plaggen style anthropogenic topsoil rich in ‘added’ materials. An abandoned European site which visibly and chemically shows the formation of a secondary albic horizon within the anthropogenic topsoil also provides an insight into the delicate balance of cultivated soil in northern Sweden, whilst reinforcing the outputs identified in the podzol model. Due to the almost invisible Sámi footprint on the landscape, areas of overlap were impossible to identify however, there was no evidence of the adoption of European cultivation activities at any of the Sámi sites investigated. The only known area of interaction between the two cultures was an official market place which had been a Sámi winter settlement prior to its use as a market site. This site showed none of the reindeer based Sámi indicators or the cultivation based European indicators, but did contain pottery fragments which could be linked to trade or occupation. Overall, the thesis reinforces the low impact expected of the semi-nomadic Sámi and sheds light on the underlying podzolic processes influencing the anthropogenically modified soils of Northern Sweden. The podzol model is reinforced by several findings throughout the thesis and the soils based cultural indicator models for both Sámi and European activity have been successfully tested against independent entomological and palynological data and therefore provide reliable reference material for future studies.
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Yamane, H., T. Kawano, K. Tatsumi, Y. Fujimichi, and S. Muto. "Site occupancy determination of Eu/Y doped in Ca2SnO4 phosphor by electron channeling microanalysis." Elsevier, 2011. http://hdl.handle.net/2237/20827.

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Books on the topic "Energy Dispersive Analysis X-ray (EDAX)"

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Energy dispersive x-ray fluorescence analysis. Warszawa: PWN, 1989.

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Garratt-Reed, A. J. Energy-dispersive X-ray analysis in the electron microscope. Oxford: BIOS, 2003.

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C, Jackson John. A method of quantitative analysis of trace elements in silicate rocks by energy-dispersive X-ray fluorescence spectroscopy. [Denver, Colo.?]: U.S. Dept. of the Interior, Geological Survey, 1988.

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Jackson, John C. A method of quantitative analysis of trace elements in silicate rocks by energy-dispersive X-ray fluorescence spectroscopy. [Denver, Colo.?]: U.S. Dept. of the Interior, Geological Survey, 1988.

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Budd, P. M. Light-element analysis in the transmission electron microscope, WEDX and EELS. Oxford: Oxford University Press, 1988.

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1943-, Goodhew Peter J., and Royal Microscopical Society, eds. Light-element analysis in the transmission electron microscope. Oxford: Oxford University Press (for) Royal Microscopical Society, 1988.

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Wang, Yinkun. Energy dispersive x-ray diffraction system: A response function for the CZT detector and an analysis of noise a low momentum transfer arguments. Sudbury, Ont: Laurentian University, School of Graduate, 2006.

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Bell, DC. Energy Dispersive X-ray Analysis in the Electron Microscope. Garland Science, 2003.

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Bell, Les, and Garrett-Reed. Energy Dispersive X-Ray Analysis in the Electron Microscope. Taylor & Francis Group, 2003.

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Frs, M. Ashby, John C. Russ, R. Kiessling, and J. Charles. Fundamentals of Energy Dispersive X-Ray Analysis: Butterworths Monographs in Materials. Elsevier Science & Technology Books, 2013.

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Book chapters on the topic "Energy Dispersive Analysis X-ray (EDAX)"

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Heslop-Harrison, J. S. "Energy Dispersive X-Ray Analysis." In Modern Methods of Plant Analysis, 244–77. Berlin, Heidelberg: Springer Berlin Heidelberg, 1990. http://dx.doi.org/10.1007/978-3-642-83611-4_9.

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Potts, P. J. "Energy dispersive x-ray spectrometry." In A Handbook of Silicate Rock Analysis, 286–325. Dordrecht: Springer Netherlands, 1987. http://dx.doi.org/10.1007/978-94-015-3988-3_9.

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Potts, P. J. "Energy dispersive x-ray spectrometry." In A Handbook of Silicate Rock Analysis, 286–325. Boston, MA: Springer US, 1987. http://dx.doi.org/10.1007/978-1-4615-3270-5_9.

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Schneider, Reinhard. "Energy-Dispersive X-Ray Spectroscopy (EDXS)." In Surface and Thin Film Analysis, 293–310. Weinheim, Germany: Wiley-VCH Verlag GmbH & Co. KGaA, 2011. http://dx.doi.org/10.1002/9783527636921.ch18.

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Bacsó, J., Á. Pázsit, and A. Somogyi. "Energy Dispersive X-Ray Fluorescence Analysis." In Nuclear Methods in Mineralogy and Geology, 165–215. Boston, MA: Springer US, 1998. http://dx.doi.org/10.1007/978-1-4615-5363-2_4.

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Gooch, Jan W. "Energy Dispersive X-Ray Analysis (EDXRA)." In Encyclopedic Dictionary of Polymers, 268. New York, NY: Springer New York, 2011. http://dx.doi.org/10.1007/978-1-4419-6247-8_4416.

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Aiginger, H., M. Benedikt, and R. Görgl. "Energy Dispersive Measurement of X-Ray Tube Spectra." In Advances in X-Ray Analysis, 137–47. Boston, MA: Springer US, 1997. http://dx.doi.org/10.1007/978-1-4615-5377-9_17.

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Derbyshire, G. E., W. I. Helsby, A. J. Dent, S. A. Wright, R. C. Farrow, G. N. Greaves, C. Morrell, and G. J. Baker. "Current and Future Energy Dispersive Exafs Detector Systems." In Advances in X-Ray Analysis, 177–85. Boston, MA: Springer US, 1991. http://dx.doi.org/10.1007/978-1-4615-3744-1_18.

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Gurvich, Yury M. "Energy Dispersive Analysis for Quality Assurance of Aluminum Alloys." In Advances in X-Ray Analysis, 265–72. Boston, MA: Springer US, 1987. http://dx.doi.org/10.1007/978-1-4613-1935-1_31.

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Iida, Atsuo, Yohichi Gohshi, and Tadashi Matsushita. "Energy Dispersive X-Ray Fluorescence Analysis Using Synchrotron Radiation." In Advances in X-Ray Analysis, 61–68. Boston, MA: Springer US, 1985. http://dx.doi.org/10.1007/978-1-4613-2471-3_10.

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Conference papers on the topic "Energy Dispersive Analysis X-ray (EDAX)"

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Yaguchi, T., M. Konno, T. Kamino, M. Ogasawara, K. Kaji, T. Ohnishi, and M. Watanabe. "3D Observation of Elemental Distribution of Si-Device using a Dedicated FIB/STEM System." In ISTFA 2005. ASM International, 2005. http://dx.doi.org/10.31399/asm.cp.istfa2005p0382.

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Abstract A technique for preparation of a pillar shaped sample and its multi-directional observation of the sample using a focused ion beam (FIB) / scanning transmission electron microscopy (STEM) system has been developed. The system employs an FIB/STEM compatible sample rotation holder with a specially designed rotation mechanism, which allows the sample to be rotated 360 degrees [1-3]. This technique was used for the three dimensional (3D) elemental mapping of a contact plug of a Si device in 90 nm technology. A specimen containing a contact plug was shaped to a pillar sample with a cross section of 200 nm x 200 nm and a 5 um length. Elemental analysis was performed with a 200 kV HD-2300 STEM equipped with the EDAX genesis Energy dispersive X-ray spectroscopy (EDX) system. Spectrum imaging combined with multivariate statistical analysis (MSA) [4, 5] was used to enhance the weak X-ray signals of the doped area, which contain a low concentration of As-K. The distributions of elements, especially the dopant As, were successfully enhanced by MSA. The elemental maps were .. reconstructed from the maps.
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Ma, Man Man Mani, Ze Zhu, and Yan Cheong Chan. "Environmental impact analysis of smartwatch using SimaPro8 tools and energy dispersive X-ray spectroscopy (EDX) technique." In 2017 IEEE 19th Electronics Packaging Technology Conference (EPTC). IEEE, 2017. http://dx.doi.org/10.1109/eptc.2017.8277438.

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Masudi, Houshang, and Richard B. Griffin. "Tribo-Chemistry of Particles Collected During In Situ Gasification of Texas Lignite." In ASME 1997 Turbo Asia Conference. American Society of Mechanical Engineers, 1997. http://dx.doi.org/10.1115/97-aa-085.

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Particles collected during in situ gasification of Texas lignite experiments were analyzed for chemical elements. Results obtained by energy dispersive x-ray analysis revealed that the dominating elements in both particles and lignite are Si, S, Al, Fe, and Ca. The concentration of these elements depends on the selected region and varies within the particle size range. Semi-quantitative analysis revealed the same results. This paper presents the scanning electron microscopy (SEM) micrograph and energy dispersive x-ray analysis (EDXA) for particles and Rockdale lignite.
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Yun, YeoHeung, Zhongyun Dong, Dianer Yang, Vesselin Shanov, Zhigang Xu, Charles Sfeir, Amos Doepke, and Mark Schulz. "Biodegradable Mg for Bone Implants: Corrosion and Osteoblast Culture Studies." In ASME 2008 International Mechanical Engineering Congress and Exposition. ASMEDC, 2008. http://dx.doi.org/10.1115/imece2008-69224.

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Corrosion and cell culture experiments were performed to evaluate magnesium (Mg) as a possible biodegradable implant material. The corrosion current and potential of a Mg disk were measured in different physiological solutions. The corrosion currents in cell culture media were found to be higher than in deionized water, which verifies that corrosion of Mg occurs faster in chloride solution. Weight loss, open-circuit potential, and electrochemical impedance spectroscopy measurements were also performed. The Mg specimens were also characterized using an environmental scanning electron microscope and energy-dispersive x-ray analysis (EDAX). The x-ray analysis showed that in the cell culture media a passive interfacial layer containing oxygen, chloride, phosphate, and potassium formed on the samples. U2OS cells were then co-cultured with a Mg specimen for up to one week. Based on visual observation, cell growth and function were not significantly altered by the presence of the corroding Mg sample. These initial results indicate that Mg may be suitable as a biodegradable implant material. Future work will develop small sensors to investigate interfacial biocompatibility of Mg implants.
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He, D. Y., N. Dong, and J. M. Jiang. "Corrosion Behavior of Arc Spraying Nickel Based Coating." In ITSC2007, edited by B. R. Marple, M. M. Hyland, Y. C. Lau, C. J. Li, R. S. Lima, and G. Montavon. ASM International, 2007. http://dx.doi.org/10.31399/asm.cp.itsc2007p0561.

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Abstract In this paper, Ni-based cored wires were prepared by using NiCr strip to wrap metal powders of Ni, Cr, Mo, CrB. Ni-based coatings were prepared by electric arc spraying process. The microstructures of Ni-Cr-Mo and Ni-Cr-B coatings were investigated by means of scanning electron microscopy (SEM) and energy-dispersive analysis (EDAX) and X-ray diffraction (XRD) analysis. The coatings have compact surface and presented the bonding strength higher than 40MPa. Corrosion-resistance performance of coatings was evaluated by salt-spray- test and electrochemical corrosion test. The results showed that Ni-based coatings containing Mo (5%) element or B element (2-4%) had better anti-chlorine ion corrosion performance than that of Ni-based coatings without Mo element, and PS45 (Ni-Cr-Ti) coating. The anti-chlorine ion corrosion coatings could be used for resolving the corrosion protection problem of the equipments and piping contacting sour, alkali, salt liquid in the petrochemical engineering.
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An, Ping, Yandong He, Shitao Wang, Yanping Bai, and Yilong Hao. "Failure Investigation and Analysis of Abnormal Capacitance of Accelerometer After ICP Release." In 2008 Second International Conference on Integration and Commercialization of Micro and Nanosystems. ASMEDC, 2008. http://dx.doi.org/10.1115/micronano2008-70201.

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An abnormal capacitance case of capacitive accelerometer after inductive coupled plasma (ICP) release was investigated to solve the failure problem. scanning electron microscopy (SEM)/transmission electron microscopy (TEM), energy dispersive x-ray spectroscopy (EDX), X-Ray transmission inspection, epoxy resin filling/polishing were used to identify the possible root cause. Failure analysis results confirmed that abnormal capacitance occurred by some connecting combs. Based on the results of three ways to analysis, it was concluded that the abnormal capacitance was not due to the contamination between combs of accelerometer and the substrate, but due to the connection between some combs caused by the ICP etching ununiformity. The static capacitance and resistance test results also testified this conclusion.
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Li, J., K. Brew, K. Cheng, V. Chan, N. Arnold, A. Gasasira, R. Pujari, et al. "Low Angle Annular Dark Field Scanning Transmission Electron Microscopy Analysis of Phase Change Material." In ISTFA 2021. ASM International, 2021. http://dx.doi.org/10.31399/asm.cp.istfa2021p0206.

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Abstract In this work, we investigate mushroom type phase-change material (PCM) memory cells based on Ge2Sb2Te5. We use low-angle annular dark field (LAADF) STEM imaging and energy dispersive X-ray spectroscopy (EDX) to study changes in microstructure and elemental distributions in the PCM cells before and after SET and RESET conditions. We describe the microscope settings required to reveal the amorphous dome in the RESET state and present an application example involving the failure analysis of a PCM test array made with devices fabricated at IBM’s Albany AI Hardware Research Center.
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Blalock, Travis, Xiao Bai, and Afsaneh Rabiei. "Effect of Substrate Temperature on Properties of Nano-Scale Functionally Graded Calcium Phosphate Coatings." In ASME 2006 International Manufacturing Science and Engineering Conference. ASMEDC, 2006. http://dx.doi.org/10.1115/msec2006-21047.

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The effect of substrate temperature and processing parameters on microstructure and crystallinity of calcium phosphate coatings deposited on heated substrates in an Ion Beam Assisted Deposition (IBAD) system are being studied. The experimental procedures include mechanical testing and film thickness measurements using bonding strength and profilometery. Cross-sectional scanning transmission electron microscopy (STEM) with energy dispersive X-ray spectroscopy (EDX) through the thickness of the film as well as scanning electron microscopy (SEM) with EDX at the top surface of the film was performed to evaluate the microstructure of the film. The coating crystallinity was studied through X-ray diffraction (XRD). The information gained from current analysis on the set temperature coatings will be used to refine the processing techniques of the Functionally Graded Hydroxyapatite (FGHA) coating.
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Porat, Ronnie, Andreas Porst, Joerg Lohse, Guido Matke, and Matthias Rebien. "The use of integrated Energy (EDX) and Wavelength (WDX) Dispersive X-ray system for defects root cause analysis in an advanced logic fab." In 2010 21st Annual IEEE/SEMI Advanced Semiconductor Manufacturing Conference (ASMC). IEEE, 2010. http://dx.doi.org/10.1109/asmc.2010.5551432.

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Ting, Chao-Cheng, Ya-Chi Liu, Hsuan-Hsien Chen, Chung-Ching Tsai, and Liwen Shih. "Root Cause Analysis and Correction of Single Metal Contact Open-Induced Scan Chain Failure in 90 nm Node VLSI." In ISTFA 2017. ASM International, 2017. http://dx.doi.org/10.31399/asm.cp.istfa2017p0317.

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Abstract In this paper, the localization of open metal contact for 90nm node SOC is reported based on Electron Beam Absorbed Current (EBAC) technique and scan diagnosis for the first time. According to the detected excess carbon, silicon and oxygen signals obtained from X-ray energy dispersive spectroscopy (EDX), the failure was deemed to be caused by the incomplete removal of silicate photoresist polymer formed during the O2 plasma dry clean before copper plating. Based on this, we proposed to replace the dry clean with diluted HF clean prior to the copper plating, which can significantly remove the silicate polymers and increase the yield.
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Reports on the topic "Energy Dispersive Analysis X-ray (EDAX)"

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Veloso, J. F. C. A., J. M. F. dos Santos, C. A. N. Conde, and R. E. Morgado. The application of a microstrip gas counter to energy-dispersive x-ray fluorescence analysis. Office of Scientific and Technical Information (OSTI), July 1996. http://dx.doi.org/10.2172/266749.

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Webb, P. C., P. J. Potts, and J. S. Watson. A versatile method for analysis of oxide ore samples by energy dispersive X-ray fluorescence (ED-XRF). Natural Resources Canada/ESS/Scientific and Technical Publishing Services, 1993. http://dx.doi.org/10.4095/193298.

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Goldstein, S. J. Development of energy-dispersive X-ray fluorescence as a mobile analysis method for hazardous metals in transuranic waste. Office of Scientific and Technical Information (OSTI), September 1998. http://dx.doi.org/10.2172/674571.

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Lacerda Silva, P., G. R. Chalmers, A. M. M. Bustin, and R. M. Bustin. Gas geochemistry and the origins of H2S in the Montney Formation. Natural Resources Canada/CMSS/Information Management, 2022. http://dx.doi.org/10.4095/329794.

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The geology of the Montney Formation and the geochemistry of its produced fluids, including nonhydrocarbon gases such as hydrogen sulfide were investigated for both Alberta and BC play areas. Key parameters for understanding a complex petroleum system like the Montney play include changes in thickness, depth of burial, mass balance calculations, timing and magnitudes of paleotemperature exposure, as well as kerogen concentration and types to determine the distribution of hydrocarbon composition, H2S concentrations and CO2 concentrations. Results show that there is first-, second- and third- order variations in the maturation patterns that impact the hydrocarbon composition. Isomer ratio calculations for butane and propane, in combination with excess methane estimation from produced fluids, are powerful tools to highlight effects of migration in the hydrocarbon distribution. The present-day distribution of hydrocarbons is a result of fluid mixing between hydrocarbons generated in-situ with shorter-chained hydrocarbons (i.e., methane) migrated from deeper, more mature areas proximal to the deformation front, along structural elements like the Fort St. John Graben, as well as through areas of lithology with higher permeability. The BC Montney play appears to have hydrocarbon composition that reflects a larger contribution from in-situ generation, while the Montney play in Alberta has a higher proportion of its hydrocarbon volumes from migrated hydrocarbons. Hydrogen sulphide is observed to be laterally discontinuous and found in discrete zones or pockets. The locations of higher concentrations of hydrogen sulphide do not align with the sulphate-rich facies of the Charlie Lake Formation but can be seen to underlie areas of higher sulphate ion concentrations in the formation water. There is some alignment between CO2 and H2S, particularly south of Dawson Creek; however, the cross-plot of CO2 and H2S illustrates some deviation away from any correlation and there must be other processes at play (i.e., decomposition of kerogen or carbonate dissolution). The sources of sulphur in the produced H2S were investigated through isotopic analyses coupled with scanning electron microscopy, energy dispersive spectroscopy, and mineralogy by X-ray diffraction. The Montney Formation in BC can contain small discrete amounts of sulphur in the form of anhydrite as shown by XRD and SEM-EDX results. Sulphur isotopic analyses indicate that the most likely source of sulphur is from Triassic rocks, in particular, the Charlie Lake Formation, due to its close proximity, its high concentration of anhydrite (18-42%), and the evidence that dissolved sulphate ions migrated within the groundwater in fractures and transported anhydrite into the Halfway Formation and into the Montney Formation. The isotopic signature shows the sulphur isotopic ratio of the anhydrite in the Montney Formation is in the same range as the sulphur within the H2S gas and is a lighter ratio than what is found in Devonian anhydrite and H2S gas. This integrated study contributes to a better understanding of the hydrocarbon system for enhancing the efficiency of and optimizing the planning of drilling and production operations. Operators in BC should include mapping of the Charlie Lake evaporites and structural elements, three-dimensional seismic and sulphate ion concentrations in the connate water, when planning wells, in order to reduce the risk of encountering unexpected souring.
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