Relevant bibliographies by topics / Differential scanning calorimetry

Academic literature on the topic 'Differential scanning calorimetry'

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Published: 4 June 2021
Last updated: 17 November 2023

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Journal articles on the topic "Differential scanning calorimetry"

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Samuni, A. M., D. J. A. Crommelin, N. J. Zuidam, and Y. Barenholz. "Differential scanning calorimetry." Journal of Thermal Analysis and Calorimetry 51, no. 1 (January 1998): 37–48. http://dx.doi.org/10.1007/bf02719009.

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Quitzsch, K. "Differential Scanning Calorimetry." Zeitschrift für Physikalische Chemie 203, Part_1_2 (January 1998): 259–60. http://dx.doi.org/10.1524/zpch.1998.203.part_1_2.259a.

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Tachoire, H., and V. Torra. "New trends in differential scanning calorimetry." Canadian Journal of Chemistry 67, no. 6 (June 1, 1989): 983–90. http://dx.doi.org/10.1139/v89-150.

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Recent applications of differential scanning calorimetry in the study of solid–solid transformations are presented. The importance of the deconvolution of the thermograms and of the modelling of the calorimetric equipment is stressed.Investigations of the phase transformations of the martensitic type in shape-memory alloys have made clear the influence of thermomechanical treatment of the material and have evaluated the influence of defects on the dynamics of transformation. A combination of calorimetric and acoustical observations has demonstrated irreversibilities, even in the so-called thermoelastic transitions. Keywords: martensitic transformation, differential scanning calorimetry, entropy production, thermomechanical treatments, acoustic emission.
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Hourston, D. J., M. Song, H. M. Pollock, and A. Hammiche. "Modulated differential scanning calorimetry." Journal of thermal analysis 49, no. 1 (July 1997): 209–18. http://dx.doi.org/10.1007/bf01987441.

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Gill, P. S., S. R. Sauerbrunn, and M. Reading. "Modulated differential scanning calorimetry." Journal of Thermal Analysis 40, no. 3 (September 1993): 931–39. http://dx.doi.org/10.1007/bf02546852.

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Sandu, Constantine, and Rakesh K. Singh. "Modeling differential scanning calorimetry." Thermochimica Acta 159 (January 1990): 267–98. http://dx.doi.org/10.1016/0040-6031(90)80115-f.

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Reading, M., A. Luget, and R. Wilson. "Modulated differential scanning calorimetry." Thermochimica Acta 238 (June 1994): 295–307. http://dx.doi.org/10.1016/s0040-6031(94)85215-4.

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Marti, E., E. Kaisersberger, and E. Füglein. "Multicycle differential scanning calorimetry." Journal of Thermal Analysis and Calorimetry 101, no. 3 (May 19, 2010): 1189–97. http://dx.doi.org/10.1007/s10973-010-0851-4.

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Cser, F., F. Rasoul, and E. Kosior. "Modulated Differential Scanning Calorimetry." Journal of thermal analysis 50, no. 5-6 (December 1997): 727–44. http://dx.doi.org/10.1007/bf01979203.

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Roussel, F., and J. M. Buisine. "Modulated differential scanning calorimetry." Journal of Thermal Analysis 47, no. 3 (September 1996): 715–25. http://dx.doi.org/10.1007/bf01981806.

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Dissertations / Theses on the topic "Differential scanning calorimetry"

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Thompson, M. "Matrix effects in differential scanning calorimetry." Thesis, Open University, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.281223.

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Nikolopoulos, Christos. "Mathematical modelling of modulated-temperature differential scanning calorimetry." Thesis, Heriot-Watt University, 1997. http://hdl.handle.net/10399/659.

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Dumitrescu, Oana Roxana. "Simultaneous differential scanning calorimetry : Fourier Transform infrared spectroscopy." Thesis, Cranfield University, 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.421231.

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Jiang, Zhong. "Temperature modulated differential scanning calorimetry : modelling and applications." Thesis, University of Aberdeen, 2000. http://digitool.abdn.ac.uk/R?func=search-advanced-go&find_code1=WSN&request1=AAIU603190.

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The research described in this thesis focused on the TMDSC technique with respect to both theoretical problems and applications. Theoretically, modelling work has been performed to address the effects of heat transfer in the measuring cell on both dynamic and quasi-isothermal TMDSC experiments. The problems of heat transfer generally influence the measured complex heat capacity and phase angle values, but eventually affect the precise measurements of other frequency dependent quantities such as the in-phase and out-of-phase heat capacities. A procedure has been suggested to correct the measured phase angle obtained by dynamic TMDSC using the scaled complex heat capacity trace (Chapter 3). The modulation frequency dependence of the instrumental phase angle has been fully investigated using more realistic models in terms of various heat transfer interface qualities, sample properties and sensor properties. In these models, it is emphasised that the measured temperatures are the sensor temperatures rather than the sample temperatures, thus, the contributions of the sensor's properties to the heat transfer are, for the first time, separated from the overall effects (Chapter 4 and Chapter 5). The consequent effects of heat transfer on the sample's heat capacity measurements are investigated based on the models suggested (Chapter 6). All the modelling results are compared with the corresponding experimental data obtained by ADSC (Mettler-Toledo Ltd) and they are in good agreement. Ripples and fluctuations which appear on the experimental signals during the glass transition and cold crystallisation transition have been simulated using* a simple model in which the period of the modulation signals changes with the time during the transitions, and then, been shown to be artefacts of the Fourier transformation process used by TMDSC evaluations (Chapter 7). The applications of TMDSC to both research and commercial samples are reported in terms of differing either the experimental conditions or the thermal history of the sample. Separating of time dependent kinetic processes from the time independent dynamic processes has been applied on the studies of the glass transition (for polycarbonate and poly(ethylene terephthalate)), the cold crystallisation (for poly(ethylene terephthalate)), the melting transition (for poly(ethylene terephthalate) and lead/tin alloys), the clearing transition of a liquid crystal polymer, and the vitrification of an epoxy resin under quasi-isothermal conditions. The main conclusion drawn from these studies is that the in-phase heat capacity is greatly influenced by the frequency of the temperature modulations even when the underlying heating (or cooling) rate remains the same. This strongly implies that the sample undergoes different structural change under different modulation conditions for the melting transition and clearing transition, but not for the glass transition and cold crystallisation. However, the interpretations of the in-phase heat capacity and out-of- phase heat capacity still need to be clarified. The detection of the glass transition and clearing point for the liquid crystal polymers, and the determination of wax appearance temperature for crude oils, show the ability of TMDSC for combining the sensitivity of a measurement at high instantaneous heating or cooling rates with the resolution obtained by measuring at a low underlying heating or cooling rates. The work on the isothermal curing of the epoxy resins displays the ability of TMDSC on measuring the heat capacity of the sample and its variation under the quasi-isothermal conditions. The frequency dependent complex heat capacity during the glass transition provides a window to measure the apparent activation energy of the transition, which is different, in some extent, from the window used by conventional DSC. The results are correlated by a shift factor. Some shortcomings of TMDSC, however, have been noticed in both modelling and application work. Firstly, any experiments for the purpose of either understanding or the quantitative measurements of TMDSC output quantities should be performed under carefully selected conditions which can satisfy the linear response assumption. Secondly, some signals in particular those associated with kinetic processes may not be fully sampled by TMDSC due to the limit of the observing window of a modulation. Thirdly, when the sensitivity is improved on TMDSC by separating the kinetics processes and noises from the dynamic processes, the TMDSC evaluation procedure introduces mathematical artefacts into the output signals. As a consequence, it is preferable to include as many temperature modulations as possible within any transition being studied in order to obtain good quality experimental signals by eliminating or minimising these artefacts, which, however, is not an easy task for some very abrupt transitions such as melting of metals.
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Murray, John. "A differential scanning calorimetry study of some metal 2,4 pentanedionates." Thesis, Federation University Australia, 1987. http://researchonline.federation.edu.au/vital/access/HandleResolver/1959.17/97253.

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The sublimation enthalpy of beryllium (II), aluminium (III), chromium (III), iron (III), cobalt (III), nickel (II), copper (II), oxovanadium (IV) and zirconium (IV) 2,4 -pentanedionate complexes has been determined by vacuum Differential Scanning Calorimetry (DSC), subsequent to benzoic acid being proposed as calibrant for this technique. In conjunction with existing thermochemical data for these complexes, metal-ligand homolytic bond dissociation energies are calculated and are rationalized in terms of the ionic size of the coordinated meta and the crystal field stabilization energies for the complex. Old and new methods for the determination of sublimation enthalpy are reviewed and the present data collectively reveal the versatility and precision of DSC fort the direct determination of sublimation enthalpies of metal complexes. The new sublimation enthalpy data presented for metal 2-4- pentanedionate complexes effectively ends the controversy associated with the previously reported corresponding data/
Master of Applied Science
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Pinto, Rafaela Rocha 1985. "Determinação da capacidade calorífica a pressão constante de ácidos graxos através da calorimetria exploratória diferencial." [s.n.], 2011. http://repositorio.unicamp.br/jspui/handle/REPOSIP/266859.

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Orientador: Maria Alvina Krähenbühl
Dissertação (mestrado) - Universidade Estadual de Campinas, Faculdade de Engenharia Química
Made available in DSpace on 2018-08-18T13:18:26Z (GMT). No. of bitstreams: 1 Pinto_RafaelaRocha_M.pdf: 1796419 bytes, checksum: 6a9da7357c387302b7688841d36db606 (MD5) Previous issue date: 2011
Resumo: Nos últimos anos tem aumentado o interesse em combustíveis oriundos de fontes renováveis como é o caso do biodiesel. Tendo em vista que os ácidos graxos são componentes de óleos e gorduras, usados para a produção do biodiesel em reações de transesterificação, e cujas propriedades ainda são bastante escassas na literatura, o objetivo do presente trabalho foi o de contribuir com dados experimentais de capacidade calorífica (cp) de ácidos graxos, constituintes de óleos e gorduras. Tais dados são necessários para os balanços de energia e para o projeto de equipamentos visando a purificação de óleos, bem como para o cálculo de reações químicas. A análise térmica diferencial é uma técnica dinâmica que vem sendo muito utilizada na determinação de dados térmicos, como capacidade calorífica, temperaturas de mudanças de estado, determinação da pureza de substâncias, entre outras. O cp é a medida da quantidade de energia necessária por unidade de massa (ou mol) de uma substância para elevar sua temperatura em um grau. Neste trabalho foram determinados os dados de cp dos seguintes ácidos graxos em fase líquida e pressão ambiente: ácido caprílico (C8:0), ácido cáprico (C10:0), ácido láurico (C12:0), ácido mirístico (C14:0), ácido palmítico (C16:0), ácido esteárico (C18:0), ácido oléico (C18:1) e ácido linoléico (C18:2). Para determinar a capacidade calorífica dos ácidos graxos, foi utilizado o Calorímetro Exploratório Diferencial - DSC da TA Instruments. Os dados experimentais foram processados pelo método do software Thermal Specialty Library versão 2.2 e pelo método da Amplitude. Os resultados mostraram que a capacidade calorífica aumenta com a temperatura e com o tamanho da cadeia carbônica. Entre os métodos avaliados não houve diferença entre os resultados obtidos. Os dados experimentais foram comparados com dados obtidos pelo método de contribuição de grupos e os desvios relativos chegaram a 15 %. O intervalo de temperatura de exploração foi de 308 K (35 ºC) a 573 K (300 ºC)
Abstract: In recent years the interest in renewable sources of fuels such as biodiesel has been increasing. Considering that fatty acids are components of fats and oils, used in the production of biodiesel in the transesterification reactions, and whose properties are still quite scarce in the literature, the purpose of this study was to contribute with experimental data of heat capacity (cp) of fatty acid constituents of oils and fats. Such data are needed for energy balances, for the design of equipment aimed at purification of oils and also for the calculation of chemical reactions. Differential thermal analysis is a dynamic technique that has been widely used in the determination of thermal data such as heat capacity, purity determination, phase change temperatures and others. The cp is the amount of energy required per unit mass (or mole) of a substance to raise its temperature by one degree. The cp were determined, in liquid phase and at atmospheric pressure, of the following fatty acids: caprylic acid (C8:0), capric acid (C10:0), lauric acid (C12:0), myristic acid (C14:0), palmitic acid (C16:0), stearic acid (C18:0), oleic acid (C18:1) and linoleic acid (C18:2). To determine the heat capacities of the fatty acids, a Differential Scanning Calorimeter - DSC, of TA Instruments, was used. The experimental data were processed using the Thermal Specialty Library (version 2.2) software and the method of vertical displacement. The results showed that the heat capacity increased with temperature and with the length of the alkyl chains. A comparison of the two methods showed no difference between the resulting information, and when the data from the experiments were compared with the data obtained from the group contribution method, there was a relative deviation of 15%. The working temperature range was from 308 K (35 ºC) to 573 K (300 ºC)
Mestrado
Desenvolvimento de Processos Químicos
Mestre em Engenharia Química
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Gouni, Sreeja Reddy. "Cure Kinetics of Benzoxazine/Cycloaliphatic Epoxy Resin by Differential Scanning Calorimetry." Thesis, California State University, Long Beach, 2018. http://pqdtopen.proquest.com/#viewpdf?dispub=10689461.

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Understanding the curing kinetics of a thermoset resin has a significant importance in developing and optimizing curing cycles in various industrial manufacturing processes. This can assist in improving the quality of final product and minimizing the manufacturing-associated costs. One approach towards developing such an understanding is to formulate kinetic models that can be used to optimize curing time and temperature to reach a full cure state or to determine time to apply pressure in an autoclave process. Various phenomenological reaction models have been used in the literature to successfully predict the kinetic behavior of a thermoset system. The current research work was designed to investigate the cure kinetics of Bisphenol-A based Benzoxazine (BZ-a) and Cycloaliphatic epoxy resin (CER) system under isothermal and nonisothermal conditions by Differential Scanning Calorimetry (DSC). The cure characteristics of BZ-a/CER copolymer systems with 75/25 wt% and 50/50 wt% have been studied and compared to that of pure benzoxazine under nonisothermal conditions. The DSC thermograms exhibited by these BZ-a/CER copolymer systems showed a single exothermic peak, indicating that the reactions between benzoxazine-benzoxazine monomers and benzoxazine-cycloaliphatic epoxy resin were interactive and occurred simultaneously. The Kissinger method and isoconversional methods including Ozawa-Flynn-Wall and Freidman were employed to obtain the activation energy values and determine the nature of the reaction. The cure behavior and the kinetic parameters were determined by adopting a single step autocatalytic model based on Kamal and Sourour phenomenological reaction model. The model was found to suitably describe the cure kinetics of copolymer system prior to the diffusion-control reaction. Analyzing and understanding the thermoset resin system under isothermal conditions is also important since it is the most common practice in the industry. The BZ-a/CER copolymer system with 75/25 wt% ratio which exhibited high glass transition temperature compared to polybenzoxazine was investigated under isothermal conditions. The copolymer system exhibited the maximum reaction rate at an intermediate degree of cure (20 to 40%), indicating that the reaction was autocatalytic. Similar to the nonisothermal cure kinetics, Kamal and Sourour phenomenological reaction model was adopted to determine the kinetic behavior of the system. The theoretical values based on the developed model showed a deviation from the obtained experimental values, which indicated the change in kinetics from a reaction-controlled mechanism to a diffusion-controlled mechanism with increasing reaction conversion. To substantiate the hypothesis, Fournier et al?s diffusion factor was introduced into the model, resulting in an agreement between the theoretical and experimental values. The changes in cross-linking density and the glass transition temperature (Tg) with increasing epoxy concentration were investigated under Dynamic Mechanical Analyzer (DMA). The BZ-a/CER copolymer system with the epoxy content of less than 40 wt% exhibited the greatest Tg and cross-linking density compared to benzoxazine homopolymer and other ratios.

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Snell, Andrew John Roger. "Application of Differential Scanning Calorimetry to Characterize Thin Film Deposition Processes." Cleveland State University / OhioLINK, 2010. http://rave.ohiolink.edu/etdc/view?acc_num=csu1280943337.

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Song, Mo. "Applications of modulated-temperature differential scanning calorimetry to multi-component polymer materials." Thesis, Lancaster University, 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.337256.

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Belkharchouche, Mohamed. "Pressure differential scanning calorimetry studies and its relevance to in-situ combustion." Thesis, University of Salford, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.280747.

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Books on the topic "Differential scanning calorimetry"

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Höhne, G. W. H., W. F. Hemminger, and H. J. Flammersheim. Differential Scanning Calorimetry. Berlin, Heidelberg: Springer Berlin Heidelberg, 2003. http://dx.doi.org/10.1007/978-3-662-06710-9.

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Höhne, G. W. H., W. Hemminger, and H. J. Flammersheim. Differential Scanning Calorimetry. Berlin, Heidelberg: Springer Berlin Heidelberg, 1996. http://dx.doi.org/10.1007/978-3-662-03302-9.

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1941-, Hemminger W., and Flammersheim H. -J, eds. Differential scanning calorimetry. 2nd ed. Berlin: Springer, 2003.

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Reading, Mike, and Douglas J. Hourston, eds. Modulated Temperature Differential Scanning Calorimetry. Dordrecht: Springer Netherlands, 2006. http://dx.doi.org/10.1007/1-4020-3750-3.

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Höhne, G. Differential scanning calorimetry: An introduction for practitioners. Berlin: Springer-Verlag, 1996.

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Höhne, G. Differential scanning calorimetry: An introduction for practitioners. 2nd ed. Berlin: Springer, 2003.

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Elkordy, Amal Ali. Applications of calorimetry in a wide context: Differential scanning calorimetry, isothermal titration calorimetry and microcalorimetry. Rijeka, Croatia: Intech, 2013.

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Bershteĭn, V. A. Differential scanning calorimetry of polymers: Physics, chemistry, analysis, technology. Edited by Egorov V. M. New York: Ellis Horwood, 1994.

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Bershtĕin, V. A. Differential scanning calorimetry of polymers: Physics, chemistry, analysis, technology. Edited by Egorov V. M. New York: Ellis Horwood, 1994.

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Callanan, Jane E. Feasibility study for the development of standards using differential scanning calorimetry. Gaithersburg, MD: U.S. Dept. of Commerce, National Bureau of Standards, 1985.

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Book chapters on the topic "Differential scanning calorimetry"

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Vergnaud, J. W., and J. Bouzon. "Differential Scanning Calorimetry." In Cure of Thermosetting Resins, 213–68. London: Springer London, 1992. http://dx.doi.org/10.1007/978-1-4471-1915-9_13.

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Godin, Biana, Elka Touitou, Rajaram Krishnan, Michael J. Heller, Nicolas G. Green, Hossein Nili, David J. Bakewell, et al. "Differential Scanning Calorimetry." In Encyclopedia of Nanotechnology, 565. Dordrecht: Springer Netherlands, 2012. http://dx.doi.org/10.1007/978-90-481-9751-4_100176.

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Akash, Muhammad Sajid Hamid, and Kanwal Rehman. "Differential Scanning Calorimetry." In Essentials of Pharmaceutical Analysis, 199–206. Singapore: Springer Singapore, 2019. http://dx.doi.org/10.1007/978-981-15-1547-7_17.

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Wagner, Matthias. "Differential Scanning Calorimetry." In Thermal Analysis in Practice, 66–143. München: Carl Hanser Verlag GmbH & Co. KG, 2017. http://dx.doi.org/10.3139/9781569906446.007.

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Wagner, Matthias. "Differential Scanning Calorimetry." In Thermal Analysis in Practice, 66–143. München, Germany: Carl Hanser Verlag GmbH & Co. KG, 2018. http://dx.doi.org/10.1007/978-1-56990-644-6_7.

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Höhne, G. W. H., W. F. Hemminger, and H. J. Flammersheim. "Introduction." In Differential Scanning Calorimetry, 1–7. Berlin, Heidelberg: Springer Berlin Heidelberg, 2003. http://dx.doi.org/10.1007/978-3-662-06710-9_1.

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Höhne, G. W. H., W. F. Hemminger, and H. J. Flammersheim. "Types of Differential Scanning Calorimeters and Modes of Operation." In Differential Scanning Calorimetry, 9–30. Berlin, Heidelberg: Springer Berlin Heidelberg, 2003. http://dx.doi.org/10.1007/978-3-662-06710-9_2.

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Höhne, G. W. H., W. F. Hemminger, and H. J. Flammersheim. "Theoretical Fundamentals of Differential Scanning Calorimeters." In Differential Scanning Calorimetry, 31–63. Berlin, Heidelberg: Springer Berlin Heidelberg, 2003. http://dx.doi.org/10.1007/978-3-662-06710-9_3.

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Höhne, G. W. H., W. F. Hemminger, and H. J. Flammersheim. "Calibration of Differential Scanning Calorimeters." In Differential Scanning Calorimetry, 65–114. Berlin, Heidelberg: Springer Berlin Heidelberg, 2003. http://dx.doi.org/10.1007/978-3-662-06710-9_4.

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Höhne, G. W. H., W. F. Hemminger, and H. J. Flammersheim. "DSC Curves and Further Evaluations." In Differential Scanning Calorimetry, 115–46. Berlin, Heidelberg: Springer Berlin Heidelberg, 2003. http://dx.doi.org/10.1007/978-3-662-06710-9_5.

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Conference papers on the topic "Differential scanning calorimetry"

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Szczech, Sebastian. "Differential Scanning Calorimetry Calibration and Heat Capacity." In Differential Scanning Calorimetry Calibration and Heat Capacity. US DOE, 2023. http://dx.doi.org/10.2172/1995262.

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Sebastian, Szczech. "Differential Scanning Calorimetry(DSC) Calibration and Measurement." In Differential Scanning Calorimetry(DSC) Calibration and Measurement. US DOE, 2023. http://dx.doi.org/10.2172/1989874.

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Wang, B., and Q. Lin. "MEMS-based AC differential scanning calorimetry." In TRANSDUCERS 2011 - 2011 16th International Solid-State Sensors, Actuators and Microsystems Conference. IEEE, 2011. http://dx.doi.org/10.1109/transducers.2011.5969293.

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Vyku Ganesan and Kurt A Rosentrater. "Characterization of DDGS Using Differential Scanning Calorimetry." In ASABE/CSBE North Central Intersectional Meeting. St. Joseph, MI: American Society of Agricultural and Biological Engineers, 2007. http://dx.doi.org/10.13031/2013.24188.

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Giddings, D. M., and D. I. Weinstein. "Diesel Fuel Deicer Evaluation Using Differential Scanning Calorimetry." In International Congress & Exposition. 400 Commonwealth Drive, Warrendale, PA, United States: SAE International, 1990. http://dx.doi.org/10.4271/900346.

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Trník, Anton, Tomáš Húlan, Ján Ondruška, and Martin Keppert. "Differential scanning calorimetry of illite/smectite – CaCO3 mixtures." In CENTRAL EUROPEAN SYMPOSIUM ON THERMOPHYSICS 2021 (CEST 2021). AIP Publishing, 2021. http://dx.doi.org/10.1063/5.0069599.

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Ondro, Tomáš, Omar Al-Shantir, and Anton Trník. "Kinetic analysis of illite dehydroxylation from differential scanning calorimetry." In CENTRAL EUROPEAN SYMPOSIUM ON THERMOPHYSICS 2019 (CEST). AIP Publishing, 2019. http://dx.doi.org/10.1063/1.5114059.

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Faruque, Sk Abdul Kader Md, and Supratic Chakraborty. "Differential scanning calorimetry in determining kinetics parameter of Si oxidation." In DAE SOLID STATE PHYSICS SYMPOSIUM 2015. Author(s), 2016. http://dx.doi.org/10.1063/1.4947860.

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Devireddy, Ramachandra V., Debopam Raha, and John C. Bischof. "Measurement of Water Transport During Freezing Using Differential Scanning Calorimetry." In ASME 1996 International Mechanical Engineering Congress and Exposition. American Society of Mechanical Engineers, 1996. http://dx.doi.org/10.1115/imece1996-0748.

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Abstract A new technique using Differential Scanning Calorimeter (DSC) was developed to investigate water transport in whole tissue slices (1–5 mm3) and suspended cells during freezing. The tissue and cellular DSC data were correlated to water transport data by freeze substitution tissue microscopy and standard cellular cryomicroscopy techniques respectively. Sprague Dawley liver tissue and a (non-attached) lymphocyte (Epstein Bar Virus Transformed, EBVT) human cell system, were chosen as our tissue and cell model systems. The DSC was used to quantitatively monitor the heat released by water transported from the cell to the frozen vascular/ extracellular space in both systems at 5°C/min. Cryomicroscopy experiments verified that at a slow cooling rate of 5°C/min no intracellular ice formation (IIF) occurred in either system. The sub-zero volumes of the tissue and cells were obtained as a function of temperature by both DSC and cryomicroscopy. By fitting a model of water transport for cells and tissues, dV/dt = f (Vb, B, T (t), Lp (Lpg, ELp)), to the DSC data for both systems, the following biophysical parameters were obtained, for rat liver tissue: Lpg = 2.25 μm/min-atm, ELp = 75.76 kcal/mole, and for EBVT lymphocytes: Lpg = 0.15 μm/min-atm, ELp = 28.78 kcal/mole. These results compare favorably to a recent study which found water transport parameters in whole liver tissue (Pazhayannur and Bischof, 1996) and to the single cell cryomicroscopy data we obtained in this study. The DSC technique is shown to be a fast and powerful method to obtain dynamic water transport information during cell and tissue freezing.
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Shuya, Matthew, Holley Baron, and Cristino Tiberio. "Understanding Field Performance of Paraffin Inhibitors Using Differential Scanning Calorimetry." In SPE Canadian Energy Technology Conference. SPE, 2022. http://dx.doi.org/10.2118/208978-ms.

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Abstract The standard test procedure for paraffin inhibitor evaluations in oil and gas production over the past 20 years has been cold finger analysis. With the emergence of unconventional Canadian oil and gas production from tight reservoirs such as the Montney and Duvernay formations, mounting paraffin treatment issues have been observed. The limitations of cold finger analysis have become increasingly evident when relating product evaluation data to field performance data. Baker Hughes has developed a method to evaluate paraffin inhibitors using differential scanning calorimetry (DSC) that exhibits key improvements over cold finger analysis. The results of an investigation between product evaluation testing through DSC and field performance data is presented. DSC analysis is commonly used in the oil and gas industry for cloud point or wax appearance temperature (WAT) determination of crude oil by detecting the point at which paraffin crystals form. It has commonly been presumed that detection of cloud point shifting can be accomplished with paraffin inhibitor chemistries; however, contradictory evidence obtained through thorough investigation within the industry refutes this claim. This is due to the fact that standard paraffin inhibitors work to disrupt paraffin crystal growth and agglomeration, instead of paraffin crystal suppression. Many programs identified through DSC testing methodology have been successfully implemented in a variety of field applications including both conventional and unconventional production. Moreover, field application monitoring data correlates to product selection and treatment rate data obtained through DSC analysis far better than results acquired through cold finger analysis. Additionally, analysis through DSC is far less susceptible to commonly experienced interferences observed in cold finger analysis such as high asphaltene content of specific crude oils, or paraffin content of condensate. Paraffin inhibitor evaluation through DSC allows for improved understanding of intended paraffin inhibitor programs for oil and gas producers, especially those experiencing difficult to treat paraffin issues in higher temperature tight reservoirs.
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Reports on the topic "Differential scanning calorimetry"

1

Marangoni, Alejandro G., and M. Fernanda Peyronel. Differential Scanning Calorimetry. AOCS, April 2014. http://dx.doi.org/10.21748/lipidlibrary.40884.

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Szczech, Sebastian. Differential Scanning Calorimetry Calibration and Heat Capacity. Office of Scientific and Technical Information (OSTI), October 2023. http://dx.doi.org/10.2172/2203731.

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Fleszar, Mark F. Lead-Tin Solder Characterization by Differential Scanning Calorimetry. Fort Belvoir, VA: Defense Technical Information Center, January 2000. http://dx.doi.org/10.21236/ada373333.

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Black, Patrick B., and Dean Pidgeon. Purity Determination of Standard Analytical Reference Materials by Differential Scanning Calorimetry. Fort Belvoir, VA: Defense Technical Information Center, May 1990. http://dx.doi.org/10.21236/ada224669.

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Fleszar, Mark F. Differential Scanning Calorimetry as a Quality Control Method for Epoxy Resin Prepreg. Fort Belvoir, VA: Defense Technical Information Center, December 1988. http://dx.doi.org/10.21236/ada204291.

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Edgar, Alexander Steven. A Modulated Differential Scanning Calorimetry Method for Characterization of Poly(ester urethane) Elastomer. Office of Scientific and Technical Information (OSTI), March 2018. http://dx.doi.org/10.2172/1427360.

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Beyer, Frederick L., Eugene Napadensky, and Christopher R. Ziegler. Characterization of Polyamide 66 Obturator Materials by Differential Scanning Calorimetry and Size-Exclusion Chromatography. Fort Belvoir, VA: Defense Technical Information Center, December 2005. http://dx.doi.org/10.21236/ada444191.

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Story, Natasha Claire. Investigating the Thermal Behavior of Polymers by Modulated Differential Scanning Calorimetry (MDSC) – A Review. Office of Scientific and Technical Information (OSTI), June 2020. http://dx.doi.org/10.2172/1633549.

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Coker, Eric. The oxidation of aluminum at high temperature studied by Thermogravimetric Analysis and Differential Scanning Calorimetry. Office of Scientific and Technical Information (OSTI), October 2013. http://dx.doi.org/10.2172/1096501.

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Author, Unknown. PR-138-162-R02 Degree of Reaction of Fusion-Bonded Epoxy Coatings. Chantilly, Virginia: Pipeline Research Council International, Inc. (PRCI), December 1986. http://dx.doi.org/10.55274/r0012138.

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This document describes a test method for the degree of reaction of fusion-bonded epoxy coatings by direct-current resistivity. This method covers the determination of a transition temperature of cured fusion-bonded epoxy coatings by measurement of the changes in direct-current resistivity of the coating with temperature. Comparison of this temperature with the degree of reaction for that coating material as determined by differential scanning calorimetry will allow the estimation of the degree of reaction of the coating sample being tested.
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