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Journal articles on the topic 'Cp2TiCl'

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Author: Grafiati

Published: 6 September 2023

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1

Cozak, Daniel, Abdelhakim Mardhy, and André Morneau. "Titanocene derivatives of purine and adenine. Synthesis and characterization of reaction products with (η5-C5H5)2Ti(CO)2, (η5-C5H5)2TiCl, and (η5-C5H5)2TiCl2." Canadian Journal of Chemistry 64, no. 4 (April 1, 1986): 751–59. http://dx.doi.org/10.1139/v86-121.

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The reaction of CpTi(CO)2 (1), Cp2TiCl (2), and Cp2TiCl2 (3) (Cp = η5-C5H5) with purine (PuH) and adenine (AdH) in organic solvents is described. The compound 1 reacts with both molecules in an oxidative fashion giving Cp2Ti(C5H3N4)(C5H4N4) (4) and (Cp2Ti)2(C5H3N5) (5) with concomitant liberation of molecular carbon monoxide and hydrogen (4:1) following a first order rate law in metal complex. The compound 2 forms an adduct compound Cp2TiCl(C5H4N4) (6) with PuH. Monosubstituted derivatives Cp2TiCl(C5H3N4) (7) and Cp2TiCl(C5H4N5) (8) are formed from the reaction of the deprotonated bases with 3. In addition to the usual elemental analysis, the characteristic ir, 1H nmr, epr, and ms results are given for the new compounds.

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2

Maué, Paul G., and Dieter Fenske. "Zur Reaktion von [Cp2TiCl2] und [CpTiCl3] mit E(SiMe3)2 (E = S, Se) Die Kristallstrukturen von [Cp3Ti2S2Cl], [Cp4Ti2S2Cl2], [Cp3Ti2Se2Cl] und [Cp4Ti4Se7O] / Reaction of [Cp2TiCl2] and [CpTiCl3 ] with E(SiMe 3)2 (E = S. Se) The Crystal Structures of [Cp3Ti2S2Cl], [Cp3Ti2S2Cl2], [Cp3Ti2Se2Cl] and [Cp4Ti4Se7O]." Zeitschrift für Naturforschung B 43, no. 10 (October 1, 1988): 1213–18. http://dx.doi.org/10.1515/znb-1988-1001.

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Abstract The reaction of [Cp2TiCl2 ] with E(SiMe3)2 leads to dinuclear Ti complexes. In [Cp3Ti2S2Cl] (1) and [Cp3Ti2Se2Cl] (3) two μ2 -S(Se) ligands bridge the Cp2Ti and CpTiCl units, respectively in contrast to these, [Cp4Ti2S2Cl2] (2) contains a μ2η1-S2 bridge connecting two Cp2TiCl fragments. A similar reaction of [CpTiCl3] with Se(SiMe3)2 leads to the tetranuclear cluster [Cp4Ti4Se7O] (4). 4 consists of a Ti4 -tetrahedron which encloses an oxygen atom.

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3

Thewalt, Ulf, and Reinhard Friedrich. "Cp2TiIV-Komplexe mit Oximatoliganden / Cp2TiIV Complexes with Oximato Ligands." Zeitschrift für Naturforschung B 46, no. 4 (April 1, 1991): 475–82. http://dx.doi.org/10.1515/znb-1991-0409.

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The reaction of Cp2TiCl2 with oximes in the two phase system (CHCl3, Cp2TiCl2)/(H2O, NaOH, oxime) leads to ionic complexes of the type [Cp2TiIV(H2O)(oximato)]+X-. Several complexes of this type were prepared. They are surprisingly stable against air and water. The following compounds are described in detail: [Cp2Ti(H2O)(ONC6H10)]NO3 (8) containing a cyclohexanoneoximato ligand, and two complexes with 1,4-cyclohexanedionedioximato ligands, namely the mononuclear complex [Cp2Ti(H2O)(ONC6H8NOH)]Cl · H2O (9) and the dinuclear complex [Cp2Ti(H2O)(ONC6H8NO)(H2O)TiCp2](NO3)2 · 4H2O (10). X-ray structure determinations show, that the ON fragment of the oximato ligand acts as side-on bonded three-electron donating ligand. The Ti atom thus has an 18-electron configuration.

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4

Breunig, H. J., O. Moldovan, M. Nema, U. Rosenthal, C. I. Rat, and R. A. Varga. "Formation of [Cp2TiSbMe2]2, [Cp2TiSb(SiMe3)2]2 and [Cp2TiCl]2·2Mes4Sb2." Journal of Organometallic Chemistry 696, no. 2 (January 2011): 523–26. http://dx.doi.org/10.1016/j.jorganchem.2010.09.007.

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5

Srivastava, A. K., O. P. Pandey, and S. K. Sengupta. "Synthesis, Spectral and Antimicrobial Studies of Bis(cyclopentadienyl)titanium(IV) Derivatives with Schiff Bases Derived from 2-Amino-5-phenyl-1,3,4-thiadiazole." Bioinorganic Chemistry and Applications 3, no. 3-4 (2005): 289–97. http://dx.doi.org/10.1155/bca.2005.289.

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The reactions of bis(cyclopentadienyl)titanium(IV) dichloride with Schiff bases derived by condensing 2- amino-5-phenyl-1,3,4-thiadiazole with benzaldehyde (SPT), 4-nitrobenzaldehyde (SNT), 4-methoxybenzaldehyde (SMT), 2-hydroxybenzaldehyde (SSTH) or 2-hydroxyacetophenone (SATH) have been studied in refluxing tetrahydrofuran and complexes of types [Cp2TiCl(SB)]Cl (SB= SPT, SNT or SMT) and [Cp2Ti(SB')]Cl (SB'H= SSTH or SATH) have been isolated. Tentative structural conclusions are drawn for these reaction products based upon elemental analyses, electrical conductance, magnetic moment and spectral (UV-vis, IR and1H NMR) data. Studies were conducted to assess the growth-inhibiting potential of the complexes synthesized, and the ligands, against various fungal and bacterial strains.

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6

Rosales, Jennifer, Gustavo Cabrera, and José Justicia. "Exploring Short and Efficient Synthetic Routes Using Titanocene(III)-Catalyzed Reactions: Total Synthesis of Natural Meroterpenes with Trisubstituted Unsaturations." Molecules 27, no. 8 (April 8, 2022): 2400. http://dx.doi.org/10.3390/molecules27082400.

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The stereo- and regioselective total syntheses of OMe derivatives of the scarce bioactive meroterpenoids makassaric acid (1) and fascioquinol B (2) have been accomplished. The synthetic sequences are based on the following three efficient and selective catalytic reactions: Cu-catalyzed addition of Grignard compounds to an epoxide; a regioselective Barbier-type reaction, catalyzed by Cp2TiCl; and regio- and stereoselective bioinspired cyclization, also catalyzed by Cp2TiCl. These three key processes allow us to obtain the main skeletons of 1 and 2 in a few steps. The valuable synthetic proposal shown in this work provides fast access to scarce, structurally complex meroterpenes with promising biological activities, which are a sustainable source for later studies and applications in medicine.

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7

Song, Li-Cheng, Cong Han, Qing-Mei Hu, and Zhi-Pan Zhang. "Synthesis of new organotitanium (IV) complexes Cp2Ti(SeR)2 and Cp2TiCl(SeR) via tandem reactions involving `Cp2Ti' intermediate. Crystal structures of Cp2TiCl(SeR) (R=p-ClC6H4, p-BrC6H4)." Inorganica Chimica Acta 357, no. 8 (June 2004): 2199–204. http://dx.doi.org/10.1016/j.ica.2003.06.011.

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8

Rosales Martínez, Antonio, Juan F. García-Martín, and Ignacio Rodríguez-García. "Cp2TiCl/H2O as a Sustainable System for the Reduction of Organic Functional Groups: Potential Application of Cp2TiCl/D2O to the Analysis of Bioactive Phenols in Olive Oil." Processes 11, no. 4 (March 23, 2023): 979. http://dx.doi.org/10.3390/pr11040979.

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Significant efforts have been made toward developing sustainable reduction reactions of organic and bioorganic compounds. In these studies, the selection of reagents and solvents has played a very important role in the development of environment-friendly methodologies. In this context, the reducing agent Cp2TiCl/H2O has been introduced as a safe, efficient, selective, and low-cost reagent, and thus as a sustainable alternative for the reduction of organic compounds. To facilitate understanding of the reductions mediated by this system, in this study we focus on describing the intermediates, mechanisms, and representative examples. Finally, a reflection is made on the future perspectives of this reducing agent, including its analog Cp2TiCl/D2O as a powerful tool for the preparation of deuterated phenols, which can be successfully used as an internal standard for analyzing bioactive phenols in olive oil.

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9

Rosales, Antonio, and Ignacio Rodríguez-García. "Cp2TiCl/D2O/Mn, a formidable reagent for the deuteration of organic compounds." Beilstein Journal of Organic Chemistry 12 (July 25, 2016): 1585–89. http://dx.doi.org/10.3762/bjoc.12.154.

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Cp2TiCl/D2O/Mn is an efficient combination, sustainable and cheap reagent that mediates the D-atom transfer from D2O to different functional groups and can contribute to the synthesis of new deuterated organic compounds under friendly experimental conditions and with great economic advantages.

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10

Castro Rodríguez, María, Ignacio Rodríguez García, Roman Nicolay Rodríguez Maecker, Laura Pozo Morales, J. Enrique Oltra, and Antonio Rosales Martínez. "Cp2TiCl: An Ideal Reagent for Green Chemistry?" Organic Process Research & Development 21, no. 7 (June 22, 2017): 911–23. http://dx.doi.org/10.1021/acs.oprd.7b00098.

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11

Gordon, Jonathan, Sven Hildebrandt, Kendra R. Dewese, Sven Klare, Andreas Gansäuer, T. V. RajanBabu, and William A. Nugent. "Demystifying Cp2Ti(H)Cl and Its Enigmatic Role in the Reactions of Epoxides with Cp2TiCl." Organometallics 37, no. 24 (November 30, 2018): 4801–9. http://dx.doi.org/10.1021/acs.organomet.8b00793.

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12

Morcillo, Sara P., Delia Miguel, Araceli G. Campaña, Luis Álvarez de Cienfuegos, José Justicia, and Juan M. Cuerva. "Recent applications of Cp2TiCl in natural product synthesis." Org. Chem. Front. 1, no. 1 (2014): 15–33. http://dx.doi.org/10.1039/c3qo00024a.

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13

Kool, Lawrence B., Marvin D. Rausch, Helmut G. Alt, Max Herberhold, Brigitte Wolf, and Ulf Thewalt. "Structural and spectroscopic comparison of the complexes Cp2M(PMe3)(CO) (M = Ti, Zr, Hf), (C9H7)2Ti(PMe3)(CO) and Cp2TiCl(PMe3); X-ray structures of Cp2Ti(PMe3)(CO) and Cp2TiCl(PMe3)." Journal of Organometallic Chemistry 297, no. 2 (December 1985): 159–69. http://dx.doi.org/10.1016/0022-328x(85)80414-9.

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14

Rosales Martínez, Antonio. "Cp2TiCl is a useful reagent to teach multidisciplinary chemistry." Educación Química 32, no. 5 (October 4, 2021): 191. http://dx.doi.org/10.22201/fq.18708404e.2021.5.77418.

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15

Hardouin, Christophe, Floris Chevallier, Bernard Rousseau, and Eric Doris. "Cp2TiCl-Mediated Selective Reduction of α,β-Epoxy Ketones." Journal of Organic Chemistry 66, no. 3 (February 2001): 1046–48. http://dx.doi.org/10.1021/jo001358g.

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16

Monleón, Laura M., Manuel Grande, and Josefa Anaya. "Radical cyclisation of epoxynitrile-2-azetidinones mediated by Cp2TiCl." Tetrahedron 63, no. 14 (April 2007): 3017–25. http://dx.doi.org/10.1016/j.tet.2007.01.049.

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17

Moisan, Lionel, Christophe Hardouin, Bernard Rousseau, and Eric Doris. "Cp2TiCl-mediated selective reduction of α,β-unsaturated ketones." Tetrahedron Letters 43, no. 11 (March 2002): 2013–15. http://dx.doi.org/10.1016/s0040-4039(02)00170-3.

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18

Hansen, Thomas, Sussie L. Krintel, Kim Daasbjerg, and Troels Skrydstrup. "A convenient synthesis of glycals employing in-situ generated Cp2TiCl." Tetrahedron Letters 40, no. 33 (August 1999): 6087–90. http://dx.doi.org/10.1016/s0040-4039(99)01266-6.

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19

Márquez, Irene R., Alba Millán, Araceli G. Campaña, and Juan M. Cuerva. "Cp2TiCl-catalyzed highly stereoselective intramolecular epoxide allylation using allyl carbonates." Org. Chem. Front. 1, no. 4 (2014): 373–81. http://dx.doi.org/10.1039/c4qo00012a.

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20

Rosales Martínez, Antonio, Laura Pozo Morales, and Emilio Díaz Ojeda. "Cp2TiCl-catalyzed, concise synthetic approach to marine natural product (±)-cyclozonarone." Synthetic Communications 49, no. 19 (July 9, 2019): 2554–60. http://dx.doi.org/10.1080/00397911.2019.1633671.

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21

Morcillo, Sara P., Delia Miguel, Araceli G. Campana, Luis Alvarez de Cienfuegos, Jose Justicia, and Juan M. Cuerva. "ChemInform Abstract: Recent Applications of Cp2TiCl in Natural Product Synthesis." ChemInform 45, no. 25 (June 5, 2014): no. http://dx.doi.org/10.1002/chin.201425250.

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22

Asandei, Alexandru D., and Gobinda Saha. "Cp2TiCl-catalyzed living radical polymerization of styrene initiated from peroxides." Journal of Polymer Science Part A: Polymer Chemistry 44, no. 3 (2005): 1106–16. http://dx.doi.org/10.1002/pola.21206.

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23

Grande, Manuel, Laura Monleón, and Josefa Anaya. "Acyl Radicals from Nitriles Promoted by Cp2TiCl in β-Lactam Chemistry." Synlett 2010, no. 08 (April 15, 2010): 1227–30. http://dx.doi.org/10.1055/s-0029-1219830.

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24

Grande, Manuel, Laura Monleón, and Josefa Anaya. "Approach to Substituted Methylcarbapenems and Benzocarbacephems by Radical Cyclization Using Cp2TiCl." Synlett 2007, no. 08 (May 8, 2007): 1243–46. http://dx.doi.org/10.1055/s-2007-980336.

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25

Moisan, Lionel, Christophe Hardouin, Bernard Rousseau, and Eric Doris. "ChemInform Abstract: Cp2TiCl-Mediated Selective Reduction of α,β-Unsaturated Ketones." ChemInform 33, no. 26 (May 21, 2010): no. http://dx.doi.org/10.1002/chin.200226051.

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26

Hardouin, Christophe, Floris Chevallier, Bernard Rousseau, and Eric Doris. "ChemInform Abstract: Cp2TiCl-Mediated Selective Reduction of α,β-Epoxy Ketones." ChemInform 32, no. 27 (May 25, 2010): no. http://dx.doi.org/10.1002/chin.200127105.

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27

Paradas, Miguel, Araceli G. Campaña, Maria Luisa Marcos, Jose Justicia, Ali Haidour, Rafael Robles, Diego J. Cárdenas, J. Enrique Oltra, and Juan M. Cuerva. "Unprecedented H-atom transfer from water to ketyl radicals mediated by Cp2TiCl." Dalton Transactions 39, no. 37 (2010): 8796. http://dx.doi.org/10.1039/c001689f.

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28

Hansen, Thomas, Sussie L. Krintel, Kim Daasbjerg, and Troels Skrydstrup. "ChemInform Abstract: A Convenient Synthesis of Glycals Employing in situ Generated Cp2TiCl." ChemInform 30, no. 44 (June 13, 2010): no. http://dx.doi.org/10.1002/chin.199944233.

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29

Spencer, Roxanne P., and Jeffrey Schwartz. "Variously substituted glycals are readily prepared from glycosyl bromides using (Cp2TiCl)2." Tetrahedron Letters 37, no. 25 (June 1996): 4357–60. http://dx.doi.org/10.1016/0040-4039(96)00865-9.

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30

Bermejo, Francisco, and Celso Sandoval. "Cp2TiCl-Promoted Isomerization of Trisubstituted Epoxides toexo-Methylene Allylic Alcohols on Carvone Derivatives." Journal of Organic Chemistry 69, no. 16 (August 2004): 5275–80. http://dx.doi.org/10.1021/jo049358u.

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31

Asandei, Alexandru D., Yanhui Chen, Gobinda Saha, and Isaac W. Moran. "Cp2TiCl-catalyzed radical chemistry: living styrene polymerizations from epoxides, aldehydes, halides, and peroxides." Tetrahedron 64, no. 52 (December 2008): 11831–38. http://dx.doi.org/10.1016/j.tet.2008.08.106.

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32

Begum, Sabnam, and Tushar Kanti Chakraborty. "Cp2TiCl-Mediated Reductive Cyclization: Total Synthesis of Pestalotiolactone A, Myrotheciumone A, and Scabrol A." Journal of Organic Chemistry 86, no. 17 (August 2, 2021): 11812–21. http://dx.doi.org/10.1021/acs.joc.1c01243.

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33

Khan, Hina P. A., and Tushar Kanti Chakraborty. "Application of Cp2TiCl-Promoted Radical-Induced Cyclization: An Expeditious Access to [a]-Annelated Indoles." Journal of Organic Chemistry 85, no. 12 (May 29, 2020): 8000–8012. http://dx.doi.org/10.1021/acs.joc.0c00817.

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34

Asandei, Alexandru D., and Yanhui Chen. "Cp2TiCl-Catalyzed SET Reduction of Aldehydes: A New Initiating Protocol for Living Radical Polymerization." Macromolecules 39, no. 22 (October 2006): 7549–54. http://dx.doi.org/10.1021/ma0604791.

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35

Asandei, Alexandru D., and Gobinda Saha. "Cp2TiCl-Catalyzed Epoxide Radical Ring Opening: A New Initiating Methodology for Graft Copolymer Synthesis." Macromolecules 39, no. 26 (December 2006): 8999–9009. http://dx.doi.org/10.1021/ma0618833.

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36

SPENCER, R. P., and J. SCHWARTZ. "ChemInform Abstract: Variously Substituted Glycals Are Readily Prepared from Glycosyl Bromides Using (Cp2TiCl)2." ChemInform 27, no. 41 (August 4, 2010): no. http://dx.doi.org/10.1002/chin.199641205.

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37

von Gudenberg, Dorothea Wolff, Hak-Chul Kang, Werner Massa, Kurt Dehnicke, C�cilia Maichle-M�ssmer, and Joachim Str�hle. "Silanolato-Komplexe von Titan und Zirconium. Die Kristallstrukturen von Cp2TiCl(OSiPh3) und Cp2ZrCl(OSiPh3)." Zeitschrift f�r anorganische und allgemeine Chemie 620, no. 10 (October 1994): 1719–24. http://dx.doi.org/10.1002/zaac.19946201010.

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38

Fenske, D., A. Grissinger, E. M. Hey-Hawkins, and J. Magull. "Zur Reaktion von [Cp2TiCl]2 und TiCl4 mit LiE(SiMe3)2 (E = P, As) und P(SiMe3)3 Die Kristallstrukturen von [Cp2TiP(SiMe3)2], [(Cp2Ti)2ClAs(SiMe3)2] und [TiCl3 {P(SiMe3)3}2]." Zeitschrift f�r anorganische und allgemeine Chemie 595, no. 1 (April 1991): 57–66. http://dx.doi.org/10.1002/zaac.19915950109.

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39

Kunkely, Horst, and Arnd Vogler. "Photoreactivity of Titanocene Pentasulfide." Zeitschrift für Naturforschung B 53, no. 2 (February 1, 1998): 224–26. http://dx.doi.org/10.1515/znb-1998-0214.

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Abstract The electronic spectrum of Cp2TiS5 shows a long-wavelength absorption at λ max = 492 nm which is assigned to the lowest-energy S52- → TiIV ligand-to-metal charge transfer (LMCT) transition. The photolysis of the complex in CH2CI2 leads to the formation of Cp2TiCl2 and elemental sulfur. It is suggested that LMCT excitation initiates a reductive elimination with the extrusion of S5 while the reduced titanocene is reoxidized by the solvent.

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40

Khan, Hina P. A., Dipendu Das, and Tushar Kanti Chakraborty. "Application of Cp2TiCl-Promoted Radical Cyclization: A Unified Strategy for the Syntheses of Iridoid Monoterpenes." Journal of Organic Chemistry 83, no. 11 (May 16, 2018): 6086–92. http://dx.doi.org/10.1021/acs.joc.8b00752.

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41

Chakraborty, Tushar Kanti, Rajarshi Samanta, and Sanjib Das. "Radical-Mediated Opening of 2,3-Epoxy Alcohols Using Cp2TiCl: Stereoselective Construction of Quaternary Chiral Centers†." Journal of Organic Chemistry 71, no. 8 (April 2006): 3321–24. http://dx.doi.org/10.1021/jo0600961.

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42

Avdeev, A. V., L. I. Gvinter, and V. Z. Sharf. "Hydrogenation and isomerization of allylbenzene in the presence of the (Cp2TiCl)2-LiAlH4 catalytic system." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 38, no. 3 (March 1989): 655–57. http://dx.doi.org/10.1007/bf00958075.

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43

Monlen, Laura M., Manuel Grande, and Josefa Anaya. "Synthesis of polycyclic ?-lactams. Evolution of tertiary radicals generated by Cp2TiCl from 1,5- and 1,6-epoxynitriles." Tetrahedron 68, no. 52 (December 2012): 10794–805. http://dx.doi.org/10.1016/j.tet.2011.11.015.

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44

Asandei, Alexandru D., Yanhui Chen, Isaac W. Moran, and Gobinda Saha. "Similarities and differences of epoxide, aldehyde and peroxide initiators for Cp2TiCl-catalyzed styrene living radical polymerizations." Journal of Organometallic Chemistry 692, no. 15 (July 2007): 3174–82. http://dx.doi.org/10.1016/j.jorganchem.2007.01.042.

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45

Chakraborty, Tushar Kanti, Rajarshi Samanta, and Krishnan Ravikumar. "Studies on radical cyclization of 2,3-epoxy alcohols containing a β-(alkoxy)acrylate moiety using Cp2TiCl." Tetrahedron Letters 48, no. 36 (September 2007): 6389–92. http://dx.doi.org/10.1016/j.tetlet.2007.06.139.

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46

Chakraborty, Tushar K., and Sanjib Das. "Synthesis of chiral 1,3-diols by radical-mediated regioselective opening of 2,3-epoxy alcohols using cp2TiCl." Tetrahedron Letters 43, no. 12 (March 2002): 2313–15. http://dx.doi.org/10.1016/s0040-4039(02)00241-1.

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47

Barrero, Alejandro F., M. Mar Herrador, José F. Quílez del Moral, Pilar Arteaga, Jesús F. Arteaga, María Piedra, and Elena M. Sánchez. "Reductive Coupling of Terpenic Allylic Halides Catalyzed by Cp2TiCl: A Short and Efficient Asymmetric Synthesis of Onocerane Triterpenes." Organic Letters 7, no. 12 (June 2005): 2301–4. http://dx.doi.org/10.1021/ol050335r.

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48

Liu, Xiao-hui, Zhong-min Dong, Xiu-lan Tang, and Yue-sheng Li. "Synthesis and characterization of hyperbranched polymers via Cp2TiCl-catalyzed self-condensing vinyl polymerization using glycidyl methacrylate as inimer." Polymer 51, no. 4 (February 2010): 854–59. http://dx.doi.org/10.1016/j.polymer.2009.12.042.

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49

Chakraborty, Tushar K., and Sanjib Das. "ChemInform Abstract: Synthesis of Chiral 1,3-Diols by Radical-Mediated Regioselective Opening of 2,3-Epoxy Alcohols Using Cp2TiCl." ChemInform 33, no. 26 (May 21, 2010): no. http://dx.doi.org/10.1002/chin.200226088.

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50

Anaya, Josefa, Manuel Grande, Laura M. Monleón, and Ramón M. Sánchez. "Synthesis and reactivity against Cp2TiCl of 4-isoprenyl-β-lactams. Trapping of N-titanoimidoyl radicals from cyanoformyl-2-azetidinones." Tetrahedron 74, no. 38 (September 2018): 5415–26. http://dx.doi.org/10.1016/j.tet.2018.01.003.

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