Academic literature on the topic 'Cis-3-(2 -chloro-3,3,3-trifluoroprop-1-en-1-yl)-2'
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Journal articles on the topic "Cis-3-(2 -chloro-3,3,3-trifluoroprop-1-en-1-yl)-2"
Rao, Guo-Wu, Xiao-Min Li, and Na-Bo Sun. "3-(2-Chloro-3,3,3-trifluoroprop-1-en-1-yl)-2,2-dimethyl-N-[3-(trifluoromethyl)phenyl]cyclopropanecarboxamide." Acta Crystallographica Section E Structure Reports Online 68, no. 6 (May 16, 2012): o1743. http://dx.doi.org/10.1107/s1600536812020922.
Full textSun, Na-Bo, Guo-Wu Rao, and Jian-Bo Chu. "1-{[3-(2-Chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropan-1-yl]carbonyl}-3-(methylsulfonyl)imidazolidin-2-one." Acta Crystallographica Section E Structure Reports Online 68, no. 6 (May 16, 2012): o1744. http://dx.doi.org/10.1107/s1600536812021216.
Full textYan, Fan-Yong, Dong-Qing Liu, Jing-Yun Wen, Yun-Ying Gao, and Ai-Mei Li. "3-[(E)-2-Chloro-3,3,3-trifluoroprop-1-en-1-yl]-N-(2-fluorophenyl)-2,2-dimethylcyclopropane-1-carboxamide." Acta Crystallographica Section E Structure Reports Online 67, no. 1 (December 11, 2010): o60. http://dx.doi.org/10.1107/s1600536810050464.
Full textLiu, Dong-Qing, Fan-Yong Yan, Yun-Ying Gao, Lei Guo, and Zi Kong. "3-[(E)-2-Chloro-3,3,3-trifluoroprop-1-en-1-yl]-N-(2-chlorophenyl)-2,2-dimethylcyclopropane-1-carboxamide." Acta Crystallographica Section E Structure Reports Online 67, no. 1 (December 11, 2010): o61. http://dx.doi.org/10.1107/s1600536810050634.
Full textPrasath, R., S. Sarveswari, Seik Weng Ng, and Edward R. T. Tiekink. "(2E)-3-(6-Chloro-2-methoxyquinolin-3-yl)-1-(2,4-dimethylquinolin-3-yl)prop-2-en-1-one." Acta Crystallographica Section E Structure Reports Online 69, no. 8 (July 20, 2013): o1274. http://dx.doi.org/10.1107/s1600536813019399.
Full textPrasath, R., S. Sarveswari, Seik Weng Ng, and Edward R. T. Tiekink. "(2E)-3-(2-Chloro-8-methylquinolin-3-yl)-1-(2,4-dimethylquinolin-3-yl)prop-2-en-1-one." Acta Crystallographica Section E Structure Reports Online 69, no. 8 (July 20, 2013): o1275. http://dx.doi.org/10.1107/s1600536813019405.
Full textPrasath, R., S. Sarveswari, Seik Weng Ng, and Edward R. T. Tiekink. "(2E)-3-(2-Chloro-8-methylquinolin-3-yl)-1-(2-methyl-4-phenylquinolin-3-yl)prop-2-en-1-one." Acta Crystallographica Section E Structure Reports Online 69, no. 8 (July 27, 2013): o1318. http://dx.doi.org/10.1107/s1600536813020229.
Full textLoh, Wan-Sin, Hoong-Kun Fun, S. Sarveswari, V. Vijayakumar, and B. Palakshi Reddy. "1-(6-Chloro-2-methyl-4-phenylquinolin-3-yl)-3-(3-methoxyphenyl)prop-2-en-1-one." Acta Crystallographica Section E Structure Reports Online 66, no. 1 (December 9, 2009): o91—o92. http://dx.doi.org/10.1107/s1600536809052179.
Full textPrasath, R., S. Sarveswari, Seik Weng Ng, and Edward R. T. Tiekink. "(2E)-3-(2-Chloro-7-methylquinolin-3-yl)-1-(6-chloro-2-methyl-4-phenylquinolin-3-yl)prop-2-en-1-one ethanol monosolvate." Acta Crystallographica Section E Structure Reports Online 69, no. 9 (August 14, 2013): o1414—o1415. http://dx.doi.org/10.1107/s1600536813022022.
Full textPrasath, R., S. Sarveswari, Seik Weng Ng, and Edward R. T. Tiekink. "(2E)-3-(6-Chloro-2-methoxyquinolin-3-yl)-1-(2-methyl-4-phenylquinolin-3-yl)prop-2-en-1-one acetone monosolvate." Acta Crystallographica Section E Structure Reports Online 69, no. 8 (July 27, 2013): o1319. http://dx.doi.org/10.1107/s1600536813020217.
Full textDissertations / Theses on the topic "Cis-3-(2 -chloro-3,3,3-trifluoroprop-1-en-1-yl)-2"
Grison, Claude. "Généralisation de la réaction d'alpha halogénation-carbonyloléfination et nouvelles applications en synthèse des acides dialkylphosphono-2-alcanoiques et des acides voisins apparentés alpha brome, alpha chlore et alpha fluore." Nancy 1, 1987. http://www.theses.fr/1987NAN10340.
Full textKhemiri, Rania. "La lambda-cyhalothrine comme pesticide privilégié en milieu agricole : étude la toxicocinétique des biomarqueurs pour le suivi de l’exposition chez des volontaires." Thèse, 2017. http://hdl.handle.net/1866/20567.
Full textLu, Yi-Chih, and 呂益誌. "Synthetic studies of the (7''R)-8-[1-(4'-hydroxy-3'-methoxyphenyl)prop-2-en-1-yl]galangin." Thesis, 2013. http://ndltd.ncl.edu.tw/handle/92332011961472886474.
Full text國立彰化師範大學
化學系
101
(7''R)-8-[1-(4'-Hydroxy-3'-methoxyphenyl)prop-2-en-1-yl]galangin, a new flavonoid isolated from Mexican propolis in 2010, displays preferential cytotoxicity against PANC-1 cells of human pancreatic cell line. First, the preparation of 8-bromo galangin was begun from the commercially available phloroglucinol. The phloroglucinol was converted by methylation and acetylation reactions to give dimethoxyphenyl acetate in two steps overall 49% yield. The dimethoxyphenyl acetate was transformed by Fries rearrangement in presence of AlCl3 to give acetophenone in 58% yield. Continually, to couple acetophenone and benzaldehyde with aldol condensation was performed to afford chalcone. The chalcone was converted to galangin by Algar-Flynn-Oyamada reactiont in existence of 20% NaOH and H2O2 in MeOH. However, it’s failed to get the desired galangin. Alternatively, the chrysin was employed by hydroxylation and bromination reactions to obtain the 8-bromo galangin in four steps overall 32% yield. On the other hand, the propiophenone was provided by Friedel-Crafts reaction of 2-methoxyphenol and propionic acid under BF3．OEt2 in 69% yield. In addition, propiophenone was converted to bromopropene under the presence of PBr3/ DMF in 70% yield, and then followed by SeO2 oxidation to give alcohol compound. The corresponding α-vinylstannane was successfully prepared in existence of t-BuLi/SnBu3Cl in moderate 59% yield. Finally, 8-bromo galangin and α-vinylstannane were transformed by Stille coupling reaction to afford the precursor (7''R)-8-[1-(4'-Hydroxy-3'-methoxyphenyl)prop-2-en-1-yl]galangin in 36% yield.
黃鈺雅. "(一) Lewis Acid-Promoted Intramolecular Cyclization of Silyl- Protected 2-(3-Arylpropargyltosylamino)methylcyclohex- 2-en-1-ols : Synthesis of Isoquinoline Derivatives (二) Brønsted Acid-Assisted Alkyne-Aldehyde Metathesis of 1-(3-Arylprop-2-yn-1-yl)-2-formylpyrrolidine : Synthesis of Pyrrolizine Derivatives." Thesis, 2014. http://ndltd.ncl.edu.tw/handle/09935030685465322120.
Full text國立臺灣師範大學
化學系
102
This thesis focuses on acid-promoted intramolecular cyclization of N-containing O-silyl-protected enynols and N-containing ynals. Three major reactions are discussed. First, FeCl3-promoted cyclization of O-silyl-protected 2-(3-arylpropargyltosylamino)methylcyclohex-2-en-1-ols in the air at room temperature produced isoquinoline derivatives containing an aryl(chloro)methylene moiety. In this process, FeCl3 acts as both the activating group and the chloride source. Second, BF3-promoted intramolecular cyclization of O-silyl-protected 2-(3-arylpropargyltosylamino)methylcyclohex- 2-en-1-ols in CH3CN at room temperature in the air provided octahydroisoquinolines having an amide moiety. Third, NHTf2-assisted alkyne-aldehyde metathesis of 1-(3-phenylprop-2-yn-1-yl)-2-formyl- pyrrolidine afforded tetrahydropyrrolizines at 80 ℃ under an atmosphere of nitrogen. The 2,3,5,7a-tetrahydro-1H-pyrrolizines gradually aromatized to 2,3-dihydro-1H-pyrrolizines in the air at ambient temperature.
Hsu, Hsiao-Ju, and 徐筱茹. "1. Intramolecular Diels-Alder Reactions of Azadienynes: Synthesis of Hexahydrobenzo[cd]indoles 2. BF3-Assisted Synthesis of Fluorinated Carbospirocycles from TBS-Protected 3-(5-Arylpent-4-yn-1-yl)cyclohex-2-en-1-ols." Thesis, 2013. http://ndltd.ncl.edu.tw/handle/73344075993909987522.
Full text國立臺灣師範大學
化學系
101
This study covers three separated topics. The first work is the synthesis of hexahydrobenzo[cd]indoles via intramolecular Diels-Alder reaction from 1-tosylpropargylamino-3-vinylcyclohex-2-enes. The reaction proceeded via [4+2] cycloaddition followed by oxidation to generate hexahydrobenzo[cd]- indoles. The second part of the thesis is the synthesis of fluorinated spiro[4.5]- decenes from tert-butyldimethyl-silyl-protected 3-(5-arylpent-4-yn-1-yl)cyclo- hex-2-en-1-ols using BF3•OEt2. In this reaction, BF3 reacted as both the Lewis acid and the fluoride source for cyclization/fluorination. The method provided an easy access to spirocyclic skeletons with concomitant formation of a C(sp2)−F bond. Finally, the gold(I)-catalyzed intramolecular cycloisomeri- zation of the 3-(N,3-diphenylpropiolamido)cyclohex-2-en-1-one proceeded through a cationic gold intermediate to afford a dihydroquinolinone. The reaction underwent an endo-dig cyclization to generate an iminium intermedi- ate followed by deprotonation/protodeauration to give a dihydroquinolinone and regenerate the Au(I) catalyst into the catalytic cycle.
Tsau, Yu-Shuo, and 曹育碩. "一、Lewis Acid-Promoted Intramolecular Cyclization of Silyl-Protected 3-(3-Arylpropargyltosylamino)methylcyclohex-2-en-1-ols: Synthesis of Azaspiro[4.5]dec-6-ene Derivatives 二、Brønsted Acid-Catalyzed and Lewis Acid-Assisted Intramolecular Cyclization of 2-Methyl-2,3-epoxy-4-(3-arylpropargyl)cyclohexan-1- ones: Synthesis of 7-Benzoylbicyclo[3.2.1]octan-2-one and Ar-yl(halo)methylenebicyclo[3.2.1]octan-2-one Derivatives." Thesis, 2014. http://ndltd.ncl.edu.tw/handle/59021650894423613213.
Full text國立臺灣師範大學
化學系
102
This thesis focuses on acid-promoted intramolecular cyclization of O-silyl-protected 3-(3-arylpropargyltosylamino)methylcyclohex-2-en-1-ols and 2-methyl-2,3-epoxy-4-(3-arylpropargyl)cyclohexan-1-ones. Two major reactions are discussed. First, BF3•OEt2-promoted intramolecular cyclization/ fluorination of O-silyl-protected 3-(3-arylpropargyltosylamino)methylcyclo- hex-2-en-1-ols at room temperature under an atmosphere of nitrogen afforded N-containig spiro[4.5]dec-6-ene derivatives containing a C(sp2)-F bond. In this process, boron trifluoride diethyl etherate acts as both the Lewis Acid and the fluoride source. Second, TfOH-catalyzed cyclization of 2-methyl-2,3-epoxy- 4-(3-aryl-propargyl)cyclohexan-1-ones at room temperature under an atmosphere of nitrogen provided 7-benzoylbicyclo[3.2.1]octan-2-one. The Lewis Acid (FeCl3 or BF3•OEt2)-assisted cyclization of the same substrate in air at room temperature afforded aryl(halo)methylenebicyclo[3.2.1]octan-2-one de-rivatives containing a C(sp2)-halo bond (halo = Cl or F).
Conference papers on the topic "Cis-3-(2 -chloro-3,3,3-trifluoroprop-1-en-1-yl)-2"
Zou, Wen-Sheng, Li-Wen Jiang, Shuang Jia, and Wu-Fu Zhu. "(E)-3-(dimethylamino)-1-(1H-indol-3-yl)prop-2-en-1-one." In 2017 2nd International Conference on Biological Sciences and Technology (BST 2017). Paris, France: Atlantis Press, 2018. http://dx.doi.org/10.2991/bst-17.2018.38.
Full textThippeswamy, G. B., D. Vijaykumar, B. S. Jayashree, M. A. Sridhar, J. Shashidhara Prasad, Alka B. Garg, R. Mittal, and R. Mukhopadhyay. "Synthesis and Crystal structure of 1-(3,5-dichloro-2-hydroxyphenyl)-3-(3-methylfuran-2-yl)prop-2-en-1-one." In SOLID STATE PHYSICS, PROCEEDINGS OF THE 55TH DAE SOLID STATE PHYSICS SYMPOSIUM 2010. AIP, 2011. http://dx.doi.org/10.1063/1.3605793.
Full textÖner, Nazmiye, Ömer Tamer, Adil Başoğlu, Davut Avcı, and Yusuf Atalay. "Density functional theory calculations on (2e)-3-(3-Bromo-4-methoxyphenyl)-1-(pyridin-2-yl) prop-2-en-1-one." In TURKISH PHYSICAL SOCIETY 32ND INTERNATIONAL PHYSICS CONGRESS (TPS32). Author(s), 2017. http://dx.doi.org/10.1063/1.4976468.
Full textMaes, Bert, Eddy Sotelo, Ernesto Cano, Reyes Laguna, Nuria Fraiz, Matilde Yáñez, Guy Lemière, et al. "2-Substituted 4-, 5- and 6-[(1E)-3-oxo-3-phenylprop-1-en-1-yl]pyridazin-3(2H)-ones and 2-Substituted 4,5-bis[(1E)-3-oxo-3-phenylprop-1-en-1-yl]pyridazin-3(2H)-ones as Potent Platelet Aggregation Inhibitors: Design, Synthesis and SAR Studies." In The 11th International Electronic Conference on Synthetic Organic Chemistry. Basel, Switzerland: MDPI, 2007. http://dx.doi.org/10.3390/ecsoc-11-01334.
Full textAnitha, K., A. Nataraj, and B. Narayana. "Spectroscopic studies and structural activity investigations of 2E-1-(3-bromothiophene-2-yl)-3-(4-chlorophenyl) prop-2-en-1-one." In 7TH NATIONAL CONFERENCE ON HIERARCHICALLY STRUCTURED MATERIALS (NCHSM-2019). AIP Publishing, 2019. http://dx.doi.org/10.1063/1.5114596.
Full textÖner, Nazmiye, Ömer Tamer, Davut Avci, and Yusuf Atalay. "A theoretical study on 3-(4-methoxyphenyl)-1-(pyridin-2-Yl) prop-2-en-1-one." In 9TH INTERNATIONAL PHYSICS CONFERENCE OF THE BALKAN PHYSICAL UNION (BPU-9). AIP Publishing LLC, 2016. http://dx.doi.org/10.1063/1.4944226.
Full textH., Ramakantha Puranik, Hadya Jayaramu Ravindra, Praveen B. Managutti, Shubha, Tayur N. Guru Row, and Harish Usha. "Synthesis, characterization, single crystal growth and hirshfield surface analysis of (2E)-3-(5-bromothiophen-2-yl)-1-(naphthalen-1-yl) prop-2-en-1-one." In PROCEEDINGS OF THE INTERNATIONAL CONFERENCE ON PHYSICS OF MATERIALS AND NANOTECHNOLOGY ICPN 2019. AIP Publishing, 2020. http://dx.doi.org/10.1063/5.0009166.
Full textAguiar, Antônio S. N., Jaqueline E. Queiroz, Pollyana P. Firmino, Wesley F. Vaz, Ademir J. Camargo, Gilberto L. B. de Aquino, Hamilton B. Napolitano, and Solemar S. Oliveira. "Experimental and theoretical study of the chalcone molecule (E)-3-(2,6-difluorophenyl)-1-(furan-2-yl)-prop-2-en-1-one." In VIII Simpósio de Estrutura Eletrônica e Dinâmica Molecular. Universidade de Brasília, 2020. http://dx.doi.org/10.21826/viiiseedmol202033.
Full textPrabhu, A. N., V. Upadhyaya, A. Jayarama, M. Srinivasulu, K. B. Manjunatha, G. Umesh, P. Predeep, Mrinal Thakur, and M. K. Ravi Varma. "Synthesis, Growth And Characterization of 1-(5-chlorothiophen-2-yl)-3-(2,4,5-Trimethoxyphenyl) Prop-2-en-1-one Single Crystal: A Potential NLO Material." In OPTICS: PHENOMENA, MATERIALS, DEVICES, AND CHARACTERIZATION: OPTICS 2011: International Conference on Light. AIP, 2011. http://dx.doi.org/10.1063/1.3643603.
Full textPodturkina, Alexandra, Oleg Ardashov, Alla Pavlova, and Tatyana Tolstikova. "(1<em>R</em>, 2<em>R</em>, 6<em>S</em>)-3-methyl-6-(prop-1-en-2-yl)cyclohex-3-ene-1,2-diol derivatives as promising compounds for anti-Parkinsonian activity." In 6th International Electronic Conference on Medicinal Chemistry. Basel, Switzerland: MDPI, 2020. http://dx.doi.org/10.3390/ecmc2020-07462.
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