Dissertations / Theses on the topic 'Chemical tests and reagents. Cyclopropane'
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Karunaratne, Veranja. "Donor-Acceptor reagents derived from 4-chloro-2-trimethylstannyl-1-butene, application to the total syntheses of (±)-\delta]9(12)-capnellene and (±)-pentalenene." Thesis, University of British Columbia, 1985. http://hdl.handle.net/2429/25810.
Full textScience, Faculty of
Chemistry, Department of
Graduate
Holt, Jay. "1,8-Diarylanthracenes as reagents for asymmetric synthesis." Diss., Georgia Institute of Technology, 1992. http://hdl.handle.net/1853/29902.
Full textWang, Lanquing. "Characterization of selenide drugs and their metabolites by hydride generation ICP-MS and HPLC/ICP-MS." Diss., Georgia Institute of Technology, 1995. http://hdl.handle.net/1853/28041.
Full textAdeosun, Adetenu Adebisi. "Novel alkylidenation, epimetallation and hydrometallation reactions of group 4 metal alkyls." Diss., Online access via UMI:, 2004. http://wwwlib.umi.com/dissertations/fullcit/3150494.
Full textBodzay, Steve J. "Organotin reagents toward the preparation of cyclic disulfides and related compounds." Thesis, McGill University, 1986. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=72827.
Full textNielsen, Randall Gunnar. "Preparation and characterization of immunological reagents for analytical applications." Diss., The University of Arizona, 1988. http://hdl.handle.net/10150/184395.
Full textFu, Yunyi Michael. "Development of a polymer-supported reagent for Trost-Lu isomerization reactions and reagents for Mitsunobu reactions." Click to view the E-thesis via HKUTO, 2008. http://sunzi.lib.hku.hk/hkuto/record/B39793989.
Full textFu, Yunyi Michael, and 付運毅. "Development of a polymer-supported reagent for Trost-Lu isomerization reactions and reagents for Mitsunobu reactions." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2008. http://hub.hku.hk/bib/B39793989.
Full textTerhune, Tammy Lee 1962. "Preparation of immunochemical reagents for a non-competitive assay for the detection of haptens." Thesis, The University of Arizona, 1988. http://hdl.handle.net/10150/276829.
Full textLau, Kwok-kin. "The chemistry of lanthanide complexes with amide and carboxylate ligands /." View the Table of Contents & Abstract, 2006. http://sunzi.lib.hku.hk/hkuto/record/B36584654.
Full textLau, Kwok-kin, and 劉國健. "The chemistry of lanthanide complexes with amide and carboxylate ligands." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2006. http://hub.hku.hk/bib/B45015491.
Full textHarden, John Michael. "Elucidation of key interactions between in situ chemical oxidation reagents and soil systems." Diss., Mississippi State : Mississippi State University, 2006. http://sun.library.msstate.edu/ETD-db/ETD-browse/browse.
Full textSpratt, Michael Phillip. "Solution and solid state NMR studies of fluorine tagging reagents." Diss., Virginia Polytechnic Institute and State University, 1985. http://hdl.handle.net/10919/49865.
Full textPh. D.
incomplete_metadata
Kan, Tze-wai Jovi. "Development of new polymer-supported reagents for organic synthesis, solvent effects in samarium promoted allylic alcohol cyclopropanation reactions and time resolved resonance studies of the photodeprotection of p-hydroxyphenacyl caged phototrigger compounds." Click to view the E-thesis via HKUTO, 2006. http://sunzi.lib.hku.hk/hkuto/record/B37925660.
Full textShelton, Kathy Rhea. "Kinetics of 3,5-diacetyl-1,4-dihydrolutidine in formaldehyde detection." Diss., Virginia Polytechnic Institute and State University, 1989. http://hdl.handle.net/10919/54420.
Full textPh. D.
Lau, Chi-yin. "Reductive aldol cyclizations using Stryker's reagent and polystyrene-supported triphenylarsine in carbon-carbon bond forming reactions." Click to view the E-thesis via HKUTO, 2007. http://sunzi.lib.hku.hk/hkuto/record/B39634450.
Full textLau, Chi-yin, and 劉志賢. "Reductive aldol cyclizations using Stryker's reagent and polystyrene-supported triphenylarsine in carbon-carbon bond forming reactions." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2007. http://hub.hku.hk/bib/B39634450.
Full textKan, Tze-wai Jovi, and 簡紫慧. "Development of new polymer-supported reagents for organic synthesis, solvent effects in samarium promoted allylic alcohol cyclopropanationreactions and time resolved resonance studies of the photodeprotectionof p-hydroxyphenacyl caged phototrigger compounds." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2006. http://hub.hku.hk/bib/B37925660.
Full textKirchhoefer, Patrick L. "A bridgehead organolithium reagent, the Retro-Nazarov reaction, and 4+3 cycloadditions with a nicotinic acid derivative /." free to MU campus, to others for purchase, 2004. http://wwwlib.umi.com/cr/mo/fullcit?p3164519.
Full textShi, Yunqing Nancy. "¹H NMR and HPLC studies of tetraarylporphyrin atropisomers." Scholarly Commons, 1993. https://scholarlycommons.pacific.edu/uop_etds/2250.
Full textBrumbaugh, William G. "Development of an integrative sampler for bioavailable metals in water /." free to MU campus, to others for purchase, 1997. http://wwwlib.umi.com/cr/mo/fullcit?p9842510.
Full textLearmonth, Robin Alec. "Studies in asymmetric synthesis." Thesis, Rhodes University, 1991. http://hdl.handle.net/10962/d1005018.
Full textAluoch, Austin Ochieng. "Metal enhanced detection of salivary proteins, Bacillus globigii and novel reagents for bioimaging & sensing." Diss., Online access via UMI:, 2007.
Find full textSilva, Aline Santana da [UNESP]. "Desenvolvimento de métodos quantitativos e de sistemas de screening para a determinação de glifosato." Universidade Estadual Paulista (UNESP), 2012. http://hdl.handle.net/11449/105723.
Full textCoordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)
O produto comercial Roundup®, contendo o glifosato como principal ingrediente ativo, é vendido mundialmente por ser um herbicida sistêmico, pós-emergente e não seletivo. Além disso, a alta eficiência no processo de remoção de plantas indesejadas e o aumento de culturas transgênicas favorecem seu uso extensivo. Embora não seja considerado um sério contaminante para o homem, o controle e monitoramento destes herbicidas são muito importantes. Desta forma, o presente projeto propõe o desenvolvimento de sistemas de screening e métodos analíticos limpos que possam ser aplicados à determinação de glifosato, uma vez que a literatura dispõe de poucos métodos de análise que visam à aplicação dos princípios da Química Verde. Os métodos propostos neste estudo foram espectroscopia de reflectância difusa, espectrofotometria e sistemas em fluxo, empregando análise por injeção em fluxo (FIA) e multi-bombas (MPFS), com detecção na região do UV-Vis. Os métodos de análise propostos são baseados na reação entre glifosato e p-dimetilaminocinamaldeído (p- DAC), em meio acidificado, com um máximo de reflecção ou absorção em 495 nm. Após a otimização das condições experimentais e validação dos métodos propostos, através de parâmetros como linearidade da curva analítica, exatidão, precisão, limite de detecção, limite de quantificação, recuperação e estudos de possíveis íons interferentes, estes foram aplicados em amostras de herbicidas comerciais e águas (naturais e de consumo humano). Os resultados obtidos na determinação de glifosato nas amostras de herbicidas comerciais empregando reflectância difusa concordaram com os resultados obtidos empregando análise por injeção em fluxo, os quais apresentaram teores de 378,8 g L-1 para a amostra A, 392,4 g L-1 para a amostra...
The commercial product Roundup®, containing the glyphosate as its main active ingredient, is marketed worldwide because it is a nonsystemic, post-emergent and nonselective herbicide. Moreover, the high efficiency in the process of the removal of unwanted plants and the increase in the introduction transgenic plants favor their extensive use. Although it has not been considered a serious contaminant to humans the control and monitoring of this herbicide are very importants. The present project proposes the development of screening systems and clear analytical methods that can be applied to determine the presence of glyphosate, since in the literature there are few methods of analysis that apply Green Chemistry’s principles. The proposed methods in this study were diffuse reflectance spectroscopy, spectrophotometry and flow systems, employing flow injection analysis (FIA) and multi-pumping (MPFS), with detection in the Uv-vis region. The proposed analysis methods are based in the reaction between glyphosate and p-dimethylaminocinnamaldehyde (p-DAC), in acid medium, it presents a reflection or absorption maximum in 495 nm. After the optimization of the experimental conditions and validation of the proposed methods, through parameters such as: linearity of the analytical curve, accuracy, precision, limit of detection, limit of quantification, recovery and study of possible interference ions, these were applied to commercial herbicides and water samples (naturals and for human consumption). The results obtained in the determination of glyphosate in the commercial herbicides employing diffuse reflectance were agree with the results obtained by employing flow injection analysis, which presented levels of 378.8 g L-1 to the A sample, 392.4 g L-1 to the B sample and 330.6 g L-1 to the C sample... (Complete abstract click electronic access below)
Silva, Aline Santana da. "Desenvolvimento de métodos quantitativos e de sistemas de screening para a determinação de glifosato /." Araraquara : [s.n.], 2012. http://hdl.handle.net/11449/105723.
Full textAbstract: The commercial product Roundup®, containing the glyphosate as its main active ingredient, is marketed worldwide because it is a nonsystemic, post-emergent and nonselective herbicide. Moreover, the high efficiency in the process of the removal of unwanted plants and the increase in the introduction transgenic plants favor their extensive use. Although it has not been considered a serious contaminant to humans the control and monitoring of this herbicide are very importants. The present project proposes the development of screening systems and clear analytical methods that can be applied to determine the presence of glyphosate, since in the literature there are few methods of analysis that apply Green Chemistry's principles. The proposed methods in this study were diffuse reflectance spectroscopy, spectrophotometry and flow systems, employing flow injection analysis (FIA) and multi-pumping (MPFS), with detection in the Uv-vis region. The proposed analysis methods are based in the reaction between glyphosate and p-dimethylaminocinnamaldehyde (p-DAC), in acid medium, it presents a reflection or absorption maximum in 495 nm. After the optimization of the experimental conditions and validation of the proposed methods, through parameters such as: linearity of the analytical curve, accuracy, precision, limit of detection, limit of quantification, recovery and study of possible interference ions, these were applied to commercial herbicides and water samples (naturals and for human consumption). The results obtained in the determination of glyphosate in the commercial herbicides employing diffuse reflectance were agree with the results obtained by employing flow injection analysis, which presented levels of 378.8 g L-1 to the A sample, 392.4 g L-1 to the B sample and 330.6 g L-1 to the C sample... (Complete abstract click electronic access below)
Orientador: Helena Redigolo Pezza
Coorientador: Leonardo Pezza
Banca: Ademir dos Santos
Banca: Matthieu Tubino
Banca: Carlos Roberto Bellato
Banca: Graziella Ciaramella Moita
Doutor
Goddard-Borger, Ethan D. "Some synthetic carbohydrate chemistry : natural product synthesis, rational inhibitor design and the development of a new reagent." University of Western Australia. School of Biomedical, Biomolecular and Chemical Sciences, 2008. http://theses.library.uwa.edu.au/adt-WU2009.0043.
Full textZhang, Yang. "Mechanistic studies and synthetic applications of Ce (IV) reagents /." Diss., 2005. http://gateway.proquest.com/openurl?url_ver=Z39.88-2004&rft_val_fmt=info:ofi/fmt:kev:mtx:dissertation&res_dat=xri:pqdiss&rft_dat=xri:pqdiss:3203831.
Full textVan, der Linde Gert Johannes. "Studie van die wisselwerking tussen reagense en minerale by die flottasie van apatiet." Thesis, 2015. http://hdl.handle.net/10210/14804.
Full textThe Phosphate Development Corporation (FOSKOR) recovers apatite from foscorite ore by a process of froth flotation. Four reagents are used viz. sodium hydroxide, water-glass, nonylphenol tetraglycol ether (EMU) and a fatty acid. The fatty acid is mainly composed of a mixture of oleic and linoleic acid in a ratio of 1,2:1. The aim of this study was to investigate the influence of the first three above-mentioned reagents on the adsorption of oleic, linoleic and linolenic acids on apatite and The Phosphate Development Corporation (FOSKOR) recovers apatite from foscorite ore by a process of froth flotation ...
Shen, Yang. "Chemical Fate Studies of Mining Reagents: Understanding the Decomposition Behavior under Various Conditions." Thesis, 2016. https://doi.org/10.7916/D8WS8T57.
Full text"Spectrofluorimetric determination of aluminium in food and antacid drugs with 8-hydroxyquinoline as reagent." Chinese University of Hong Kong, 1993. http://library.cuhk.edu.hk/record=b5887797.
Full textThesis (M.Phil.)--Chinese University of Hong Kong, 1993.
Includes bibliographical references (leaves 90-96).
Chapter I. --- Abstract --- p.i
Chapter II. --- Acknowledgment --- p.ii
Chapter III. --- Table of contents --- p.iii
Chapter IV. --- List of Tables and Figures 、 --- p.iv
Chapter Chapter 1. --- Introduction --- p.1
Chapter 1.1. --- General introduction
Chapter 1.2. --- Review of analytical methods for aluminium analysis
Chapter 1.3. --- Spectrofluorimetric determination of aluminium
Chapter 1.4. --- Project aim
Chapter Chapter 2. --- Experimental --- p.14
Chapter 2.1. --- Apparatus
Chapter 2.2. --- Reagents & Material
Chapter 2.3. --- Procedure
Chapter 2.4. --- Treatment of data
Chapter Chapter 3. --- Results and discussion --- p.24
Chapter 3.1. --- Optimization of experimental conditions
Chapter 3.2. --- Analytical Parameters
Chapter 3.3. --- Analytical results
Chapter Chapter 4. --- Conclusion --- p.89
Chapter Chapter 5. --- References --- p.90
Appendix --- p.97
Willemse, Johannes Alexander. "Carbon monoxide as reagent in the formylation of aromatic compounds." Thesis, 2008. http://hdl.handle.net/10210/433.
Full textProf. C.W. Holzapfel
Elephant, Dimpho Elvis. "A comparative study of the BCR sequential and batch extractions for wastes and waste-amended soil." Thesis, 2010. http://hdl.handle.net/10413/7357.
Full textThesis (M.Sc.)-University of KwaZulu-Natal, Pietermaritzburg, 2010.
"The enhancement of the activity of commercial antifungal agents using Aspalathus linearis synthesized gold nanoparticles." Thesis, 2015. http://hdl.handle.net/10210/13844.
Full textThe synthesis and application of gold nanoparticles (AuNPs) has been intensively studied worldwide. However, the toxicity of these nanoparticles is still a concern. We considered that various physiochemical methods used to synthesize AuNPs are energy driven, costly and require the use of harmful chemicals. Thus, this makes them not environmentally-friendly. The aim of this study was therefore to synthesize AuNPs via a greener route using Aspalathus linearis tea leaves. The AuNPs were used to coat eight commercial antifungal discs (i.e. amphotericin B, fluconazole, clotrimazole, econazole, flucytosine, ketoconazole, miconazole and nystatin) against four Aspergillus spp. for enhanced antifungal activity. The aqueous extract of A. linearis was characterized by high performance liquid chromatography and liquid chromatography–mass spectroscopy. The AuNPs were characterized using ultravioletvisible (UV-vis) spectroscopy, dynamic light scattering, nanoparticle tracking analysis, Fourier transforms infrared spectroscopy (FTIR), high-resolution transmission electron microscopy and X-ray diffraction. The toxicity of the synthesized AuNPs was studied by 3-(4, 5-dimethylthiazol-2-yl)-5-(3-carboxymethoxyphenyl)-2-(4-sulfophenyl)-2H-tetrazolium) assay and xCELLigence test on HepG-2 cell lines and results revealed very little to no toxicity of the AuNPs. The pristine antifungal and AuNPs coated antifungal discs were characterized by FTIR, scanning electron microscopy (SEM) and antifungal activity performed using the disc diffusion method. A strong resonance peak was observed at 529 nm of the AuNPs measured using UV-vis spectroscopy. Average size of AuNPs was ~44±1 nm and demonstrated excellent in-vitro stability under various solutions (5% NaCl, phosphate buffered saline) at varying pH levels. The SEM images revealed that the AuNPs were attached onto the coated antifungal discs when compared with the pristine antifungal discs. Antifungal results indicated that AuNPs significantly (p<0.001) enhanced the antifungal activity of the coated antifungal discs against the tested fungi when compared to the pristine antifungal discs. The AuNPs coated econazole disc exhibited the greatest (broad spectrum) activity than other antifungal agents tested. In conclusion, A. linearis can be used as a reducing agent in the synthesis of stable AuNPs. Furthermore, the AuNPs coated antifungal discs demonstrated considerable antifungal activity over the pristine antifungal discs...