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Journal articles on the topic 'Bromopropane'

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Author: Grafiati

Published: 10 December 2022

Last updated: 28 January 2023

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1

Varma, B. H. Rajesh, and B. Sreenivasa Rao. "Gas Chromatography-Head Space-Mass Spectrometry Sensor based Quality Control of Dobutamine Hydrochloride Bulk Material for a mutagenic impurity, 2-bromopropane." Research Journal of Chemistry and Environment 27, no. 2 (January 15, 2023): 54–61. http://dx.doi.org/10.25303/2702rjce054061.

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In the process of making dobutamine hydrochloride, there is a possibility in the development of 2-bromopropane. The 2-bromopropane falls within the genotoxic group and is typically toxic and cancer suspicious agent. In order to monitor and then evaluate 2-bromopropane trace levels in dobutamine hydrochloride pharmaceutical samples, the gas chromatography technique with mass spectrometer analyser is described in this work. The separation of 2-bromopropane deployed DB-624 analysis column (30 m x 0.32 mm, 1.8 μm). The carrier gas utilized was helium flowing at a steady rate of 1.0 mL/min. At thermal setting of 220 °C, an injector operated in split mode (1:10). Selected ion monitoring pattern was choosen for the mass spectrometer analyzer to operate in. The applied technique provided adequate accuracy in addition to precision and superior linearity in the concentration span of 1.03 ppm to 15.00 ppm for 2- bromopropane. The approach was noted to be sensitive with LOD values for 2-bromopropane of 0.34 ppm. The recovery statistics of the standard addition approach provided affirmation that the stated method had efficaciously applied in terms of selectivity for enumeration of 2-bromopropane in dobutamine hydrochloride solutions with no interference.

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2

Ichihara, Gaku. "Neuro-reproductive toxicities of 1-bromopropane and 2-bromopropane." International Archives of Occupational and Environmental Health 78, no. 2 (December 10, 2004): 79–96. http://dx.doi.org/10.1007/s00420-004-0547-9.

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3

Yu, Xiaozhong, Gaku Ichihara, Junzoh Kitoh, Zhenlin Xie, Eiji Shibata, Michihiro Kamijima, and Yasuhiro Takeuchi. "Neurotoxicity of 2-Bromopropane and 1-Bromopropane, Alternative Solvents for Chlorofluorocarbons." Environmental Research 85, no. 1 (January 2001): 48–52. http://dx.doi.org/10.1006/enrs.2000.4226.

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4

Ichihara, G. "Neurotoxicity of 1-bromopropane." SANGYO EISEIGAKU ZASSHI 40, Special (1998): 414. http://dx.doi.org/10.1539/sangyoeisei.kj00001990238.

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5

KIM, Hyeon Yeong, Yong Hyun CHUNG, Kwan Hyung YI, Jung Gil KIM, and Il Je YU. "LC50 of 2-Bromopropane." INDUSTRIAL HEALTH 34, no. 4 (1996): 403–7. http://dx.doi.org/10.2486/indhealth.34.403.

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6

MAENG, Seung Hee, and Il Je YU. "Mutagenicity of 2-Bromopropane." INDUSTRIAL HEALTH 35, no. 1 (1997): 87–95. http://dx.doi.org/10.2486/indhealth.35.87.

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7

Garnier, R. "Toxicité du 1-bromopropane." Archives des Maladies Professionnelles et de l'Environnement 79, no. 2 (April 2018): 177–78. http://dx.doi.org/10.1016/j.admp.2018.01.002.

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8

Zhao, Wenyuan, Kazuo Aoki, Tonxing Xie, and Junichi Misumi. "Electrophysiological Changes Induced by Different Doses of 1‐Bromopropane and 2‐Bromopropane." Journal of Occupational Health 41, no. 1 (January 1999): 1–7. http://dx.doi.org/10.1539/joh.41.1.

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9

Zong, Cai, Xiao Zhang, Chinyen Huang, Jie Chang, C. Edwin Garner, Toshihiro Sakurai, Masashi Kato, Sahoko Ichihara, and Gaku Ichihara. "Role of cytochrome P450s in the male reproductive toxicity of 1-bromopropane." Toxicology Research 5, no. 6 (2016): 1522–29. http://dx.doi.org/10.1039/c6tx00164e.

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10

Yang, Su, Xiaoxuan Guo, Xiaomei Pan, Liuyu Gu, Xueping Liu, Lijing Gao, and Guomin Xiao. "Synthesis of Brominated Alkanes via Heterogeneous Catalytic Distillation over Al2O3/SO42−/ZrO2." Catalysts 11, no. 12 (November 30, 2021): 1464. http://dx.doi.org/10.3390/catal11121464.

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Concentrated sulfuric acid is generally used as a catalyst for producing brominated alkanes in traditional methods, but is highly corrosive and difficult to separate. This work reports the preparation of bromopropane from n-propanol based on a reactive distillation strategy combined with alumina-modified sulfated zirconia (Al2O3/SO42−/ZrO2) as a heterogenous catalyst. As expected, under the optimum reaction conditions (110 °C), the yield of bromopropane was 96.18% without side reactions due to the reactive distillation strategy. Meanwhile, the microscopic morphology and performance of Al2O3/SO42−/ZrO2 were evaluated by X-ray diffraction (XRD), scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), Brunner–Emmet–Teller (BET), Fourier transform infrared spectroscopy (FT–IR), and other characterization methods. The results confirmed that the morphology of zirconia sulfate is effectively regulated by the modification method of alumina, and more edges and angles provide more catalytic acid sites for the reaction. Furthermore, Al2O3/SO42−/ZrO2 exhibited high stability and remarkable reusability due to the strong chemical bond Zr–Al–Zr. This work provides a practical method for the preparation of bromopropane and can be further extended to the preparation of other bromoalkanes.

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11

Ichihara, Gaku, Nobuyuki Asaeda, Toshihiko Kumazawa, Yoshiaki Tagawa, Michihiro Kamijima, Xiaozhong Yu, Hidetaka Kondo, et al. "Testicular Toxicity of 2‐Bromopropane." Journal of Occupational Health 38, no. 4 (October 1996): 205–6. http://dx.doi.org/10.1539/joh.38.205.

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12

Yu, X. "Neuro- and testicular toxicity of 2-bromopropane and 1-bromopropane, alternative solvents for chlorofluorocarbons." SANGYO EISEIGAKU ZASSHI 40, Special (1998): 710. http://dx.doi.org/10.1539/sangyoeisei.kj00001990531.

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13

SEKIGUCHI, Soichiro, and Takeshi HONMA. "Influence of 2-Bromopropane on Reproductive System. 2-Bromopropane Inhibits Forced Ovulation in Mice." INDUSTRIAL HEALTH 36, no. 3 (1998): 297–99. http://dx.doi.org/10.2486/indhealth.36.297.

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14

OHNISHI, Akio, Toru ISHIDAO, Takahiko KASAI, Keiichi ARASHIDANI, and Hajime HORI. "Neurotoxicity of 1-Bromopropane in Rats." Journal of UOEH 21, no. 1 (1999): 23–28. http://dx.doi.org/10.7888/juoeh.21.23.

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15

Chalupka, Stephanie. "Reducing Workplace Exposure to 1-Bromopropane." Workplace Health & Safety 62, no. 3 (March 1, 2014): 128. http://dx.doi.org/10.3928/21650799-20140219-08.

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16

Chalupka, Stephanie. "Reducing Workplace Exposure to 1-Bromopropane." Workplace Health & Safety 62, no. 3 (March 2014): 128. http://dx.doi.org/10.1177/216507991406200308.

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17

Cheryl Hogue. "US EPA to regulate 1-bromopropane." C&EN Global Enterprise 98, no. 31 (August 17, 2020): 15. http://dx.doi.org/10.1021/cen-09831-polcon2.

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18

Robinson, Richard. "BROMOPROPANE, OZONE-SPARING SOLVENT, IS NEUROTOXIC." Neurology Today 4, no. 12 (December 2004): 15. http://dx.doi.org/10.1097/00132985-200412000-00010.

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19

Mingyi, Wang, Yang Hongfang, Wu Anxin, and Pan Xinfu. "Facile Total Synthesis of Isopregomisin." Journal of Chemical Research 23, no. 2 (February 1999): 158–59. http://dx.doi.org/10.1177/174751989902300246.

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Isopregomisin, a diarylbutane-lignan, has been synthesized by a short and efficient route starting from pyrogallol; the synthesis involves a novel selective demethylation reaction and the coupling reaction of the Grignard reagent produced from an aryl bromopropane with ( E)-2- tert-butyl-3-phenyloxaziridine.

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20

Martínez-Avilés, Mónica, Claudette M. Rosado-Reyes, and Joseph S. Francisco. "Hydroxyl-Radical-Initiated Oxidation Mechanism of Bromopropane." Journal of Physical Chemistry A 112, no. 34 (August 2008): 7930–38. http://dx.doi.org/10.1021/jp8034506.

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21

Sekiguchi, Soichiro, Goro Asano, Megumi Suda, and Takeshi Honma. "Influence of 2-bromopropane on reproductive system—Short-term administration of 2-bromopropane inhibits ovulation in F344 rats." Toxicology and Industrial Health 16, no. 7-8 (August 2000): 277–83. http://dx.doi.org/10.1177/074823370001600704.

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22

Kawai, Toshio, Akito Takeuchi, Yuriko Miyama, Kunihiro Sakamto, Zuo-Wen Zhang, Kae Higashikawa, and Masayuki Ikeda. "Biological monitoring of occupational exposure to 1-bromopropane by means of urinalysis for 1-bromopropane and bromide ion." Biomarkers 6, no. 5 (January 2001): 303–12. http://dx.doi.org/10.1080/13547500110034817.

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23

Wisniak, Jaime. "Phase Equilibria in the Systems Ethyl Methanoate + 1-Bromopropane, Ethyl Methanoate + Cyclohexane, and Ethyl Methanoate + 1-Bromopropane + Cyclohexane." Journal of Chemical & Engineering Data 41, no. 3 (January 1996): 468–73. http://dx.doi.org/10.1021/je950292x.

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24

Sekiguchi, S., M. Suda, Y. L. Zhai, and T. Honma. "Effects of 1-bromopropane, 2-bromopropane, and 1,2-dichloropropane on the estrous cycle and ovulation in F344 rats." Toxicology Letters 126, no. 1 (January 2002): 41–49. http://dx.doi.org/10.1016/s0378-4274(01)00429-5.

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25

Meinike, T., L. Engelmann, M. Olzmann, and K. Scherzer. "Rate coefficients for the reactions of hydrogen atoms with 1-bromopropane, 2-bromopropane, 1-bromobutane, and 2-bromobutane." International Journal of Chemical Kinetics 30, no. 10 (1998): 721–27. http://dx.doi.org/10.1002/(sici)1097-4601(1998)30:10<721::aid-kin4>3.0.co;2-x.

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26

Shimamura, Yuko, Ryo Inagaki, Hiroshi Honda, and Shuichi Masuda. "Does External Exposure of Glycidol-Related Chemicals Influence the Forming of the Hemoglobin Adduct, N-(2,3-dihydroxypropyl)valine, as a Biomarker of Internal Exposure to Glycidol?" Toxics 8, no. 4 (December 13, 2020): 119. http://dx.doi.org/10.3390/toxics8040119.

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Glycidyl fatty acid esters (GE) are constituents of edible oils and fats, and are converted into glycidol, a genotoxic substance, in vivo. N-(2,3-dihydroxypropyl)valine (diHOPrVal), a hemoglobin adduct of glycidol, is used as a biomarker of glycidol and GE exposure. However, high background levels of diHOPrVal are not explained by daily dietary exposure to glycidol and GE. In the present study, several glycidol-related chemicals (glycidol, (±)-3-chloro-1,2-propanediol, glycidyl oleate, epichlorohydrin, propylene oxide, 1-bromopropane, allyl alcohol, fructose, and glyceraldehyde) that might be precursors of diHOPrVal, were administered to mice, and diHOPrVal formation from each substance was examined with LC-MS/MS. DiHOPrVal was detected in animals treated with glycidol and glycidyl oleate but not in mice treated with other chemicals (3-MCPD, epichlorohydrin, propylene oxide, 1-bromopropane, allyl alcohol, fructose, and glyceraldehyde). The amount of diHOPrVal per administered dose produced from other chemicals was negligible compared to the amounts associated with dietary glycidol and GE. The present study provides important knowledge for exploring other sources for internal exposure to glycidol.

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27

Omura, Minoru, Mangen Zhao, Yesid Romero, and Naohide Inoue. "Toxicity of 2‐Bromopropane on Spermatogonia and Spermatocyte." Journal of Occupational Health 39, no. 1 (January 1997): 1–2. http://dx.doi.org/10.1539/joh.39.1.

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28

Choi, Kyeong Sook, Byung Yeol Chun, Jung Sun Park, Yang Ho Kim, and Young Hahn Moon. "Neuropsychiatric Symptoms of Workers Exposed to 2-Bromopropane." Korean Journal of Occupational and Environmental Medicine 9, no. 2 (1997): 301. http://dx.doi.org/10.35371/kjoem.1997.9.2.301.

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29

Omura, M. "Histopathological evidence that 2-bromopropane selectively damages spermatogonia." SANGYO EISEIGAKU ZASSHI 40, Special (1998): 416. http://dx.doi.org/10.1539/sangyoeisei.kj00001990240.

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30

Frasch, H. Frederick, G. Scott Dotson, and Ana M. Barbero. "In vitro Human Epidermal Penetration of 1-Bromopropane." Journal of Toxicology and Environmental Health, Part A 74, no. 19 (October 2011): 1249–60. http://dx.doi.org/10.1080/15287394.2011.595666.

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31

Britt E. Erickson. "Suit seeks US air regulation for 1-bromopropane." C&EN Global Enterprise 98, no. 33 (August 31, 2020): 15. http://dx.doi.org/10.1021/cen-09833-polcon4.

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32

Kawai, T., Y. Okada, T. Odachi, S. Horiguchi, Z. W. Zhang, C. S. Moon, and M. Ikeda. "Diffusive Sampling and Biological Monitoring of 2-Bromopropane." Archives of Environmental Contamination and Toxicology 33, no. 1 (July 1, 1997): 23–28. http://dx.doi.org/10.1007/s002449900218.

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33

Rala, Sarbjit. "Electrochemical Synthesis of Organoantimony Compounds and their Coordination Compounds." Asian Journal of Chemistry 31, no. 3 (2019): 642–46. http://dx.doi.org/10.14233/ajchem.2019.21730.

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Electrochemical reactions of bromoethane, 1-bromopropane, 1-chlorobutane and chlorobenzene have been carried out in acetonitrile at sacrificial antimony anode using tetrabutylammonium chloride as supporting electrolyte. The products isolated from the anode compartment have been characterized by elemental analysis and infrared spectral studies and are identified as organoantimony compounds. Coordination compounds of same have been synthesized with ligand (1,10-phenanthroline and 2,2'-bipyridyl). All these reactions proceed with high current efficiencies.

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34

Miao, R., B. Ding, Y. Zhang, R. Zhao, Y. Li, and B. Zhu. "Large-scale label-free proteomics analysis of occupational poisoned patients of 1-bromopropane, workers exposed to 1-bromopropane and healthy individuals." Human & Experimental Toxicology 37, no. 1 (January 25, 2017): 3–12. http://dx.doi.org/10.1177/0960327117689911.

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35

Honma, T. "P155 Inhibitory action of 2-bromopropane on animal ovulation." SANGYO EISEIGAKU ZASSHI 41, Special (1999): 311. http://dx.doi.org/10.1539/sangyoeisei.kj00001991070.

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36

Cho, Young-Chang, Thanh Nguyen, So-Yeon Park, Kwonseop Kim, Hyung Kim, Hye Jeong, Kyung Kim, and Hangun Kim. "Bromopropane Compounds Increase the Stemness of Colorectal Cancer Cells." International Journal of Molecular Sciences 18, no. 9 (September 1, 2017): 1888. http://dx.doi.org/10.3390/ijms18091888.

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37

Ichihara, Gaku, Joseph Keith Miller, Aldona Ziolkokwska, Seiichiro Itohara, and Yasuhiro Takeuchi. "Neurological Disorders in Three Workers Exposed to 1‐Bromopropane." Journal of Occupational Health 44, no. 1 (January 2002): 1–7. http://dx.doi.org/10.1539/joh.44.1.

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38

Ishikawa, H. "H206 Teratogenic effects of 2-bromopropane on mouse embryos." SANGYO EISEIGAKU ZASSHI 41, Special (1999): 512. http://dx.doi.org/10.1539/sangyoeisei.kj00001991268.

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39

ICHIHARA, Gaku, Joseph Keith MILLER, Aldona ZIOLKOKWSKA, Seiichiro ITOHARA, and Yasuhiro TAKEUCHI. "Neurological Disorders in Three Workers Exposed to 1-Bromopropane." SANGYO EISEIGAKU ZASSHI 44, no. 1 (2002): A1. http://dx.doi.org/10.1539/sangyoeisei.kj00002552659.

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40

Yamada, T. "Exposure to 1-Bromopropane Causes Ovarian Dysfunction in Rats." Toxicological Sciences 71, no. 1 (January 1, 2003): 96–103. http://dx.doi.org/10.1093/toxsci/71.1.96.

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41

Ichihara, Gaku, Weihua Li, Eiji Shibata, Xuncheng Ding, Hailan Wang, Yideng Liang, Simeng Peng, et al. "Neurologic Abnormalities in Workers of a 1-Bromopropane Factory." Environmental Health Perspectives 112, no. 13 (September 2004): 1319–25. http://dx.doi.org/10.1289/ehp.6995.

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42

Jones, Mark E., and G. Barney Ellison. "A gas-phase E2 reaction: methoxide ion and bromopropane." Journal of the American Chemical Society 111, no. 5 (March 1989): 1645–54. http://dx.doi.org/10.1021/ja00187a017.

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43

Ishidao, Toru, Naoki Kunugita, Yukiko Fueta, Keiichi Arashidani, and Hajime Hori. "Effects of inhaled 1-bromopropane vapor on rat metabolism." Toxicology Letters 134, no. 1-3 (August 2002): 237–43. http://dx.doi.org/10.1016/s0378-4274(02)00171-6.

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44

Urbina, Andres S., Victoria M. Boulos, Matthias Zeller, Denilson Mendes de Oliveira, and Dor Ben-Amotz. "Binding-Induced Unfolding of 1-Bromopropane in α-Cyclodextrin." Journal of Physical Chemistry B 124, no. 48 (November 18, 2020): 11015–21. http://dx.doi.org/10.1021/acs.jpcb.0c08630.

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45

Huang, Zhenlie, Sahoko Ichihara, Shinji Oikawa, Jie Chang, Lingyi Zhang, Shijie Hu, Hanlin Huang, and Gaku Ichihara. "Hippocampal phosphoproteomics of F344 rats exposed to 1-bromopropane." Toxicology and Applied Pharmacology 282, no. 2 (January 2015): 151–60. http://dx.doi.org/10.1016/j.taap.2014.10.016.

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46

Zhang, Song, Yanmei Wang, Bifeng Tang, Qiusha Zheng, and Bing Zhang. "Ultraviolet photodissociation of 1-bromopropane at 234 and 267nm." Chemical Physics Letters 413, no. 1-3 (September 2005): 129–34. http://dx.doi.org/10.1016/j.cplett.2005.07.056.

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47

Nelson,, David D., Joda C. Wormhoudt, Mark S. Zahniser, Charles E. Kolb, Malcolm K. W. Ko, and Debra K. Weisenstein. "OH Reaction Kinetics and Atmospheric Impact of 1-Bromopropane." Journal of Physical Chemistry A 101, no. 27 (July 1997): 4987–90. http://dx.doi.org/10.1021/jp970874g.

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48

Yu, IJ, YH Chung, CH Lim, SH Maeng, JY Lee, HY Kim, SJ Lee, et al. "Reproductive toxicity of 2-bromopropane in Sprague Dawley rats." Scandinavian Journal of Work, Environment & Health 23, no. 4 (August 1997): 281–88. http://dx.doi.org/10.5271/sjweh.221.

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49

Cepeda, Emilio A., Raquel Bravo, and José M. Lomas. "Solubilities of Fatty Acids and Triglycerides in 1-Bromopropane." Journal of Chemical & Engineering Data 57, no. 4 (March 8, 2012): 1160–64. http://dx.doi.org/10.1021/je201181k.

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50

Kubát, Pavel, and Josef Pola. "CO2 laser photosensitized dehydrobromination of bromoethane and 1-bromopropane. A hot-tube radical-chain reaction with molecular mechanism." Collection of Czechoslovak Chemical Communications 50, no. 7 (1985): 1548–52. http://dx.doi.org/10.1135/cccc19851548.

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Contrary to the gas-phase hot-tube reaction taking place by a blend of a molecular and radical-chain mechanism, the cw CO2 laser induced dehydrobromination of bromoethane and 1-bromopropane occurs by only a molecular mechanism which is substantiated with reaction rates and products in the absence and the presence of radical-chain inhibitor (propene) and in the presence of chloroethane. The results point out the importance of hot walls for the initiation of radical-chain dehydrobromination.

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