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Relevant bibliographies by topics / Asymmetric synthesis

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Academic literature on the topic 'Asymmetric synthesis'

Author: Grafiati

Published: 4 June 2021

Last updated: 25 July 2025

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Journal articles on the topic "Asymmetric synthesis"

1

Chen, Fen-Er, and Lei Chen. "Total Synthesis of Camptothecins: An Update." Synlett 28, no. 10 (2017): 1134–50. http://dx.doi.org/10.1055/s-0036-1588738.

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Over the last few decades, considerable research efforts have been directed toward the development of effective chemical syntheses of camptothecin and its analogs. The last comprehensive review of this area was published in 2003 and many effective new methods have since been reported for the stereoselective synthesis of the camptothecin alkaloids. In this account, we have summarized most of the novel synthetic approaches developed for the synthesis of camptothecins during the last decade. We have focused on strategies for the construction of the pentacyclic ring system and the different method

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2

Arseniyadis, S., P. Q. Huang, D. Piveteau, and H. P. Husson. "Asymmetric synthesis." Tetrahedron 44, no. 9 (1988): 2457–70. http://dx.doi.org/10.1016/s0040-4020(01)81697-5.

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3

Jurczak, Janusz, and Tomasz Bauer. "Glyoxylic acid derivatives in asymmetric synthesis." Pure and Applied Chemistry 72, no. 9 (2000): 1589–96. http://dx.doi.org/10.1351/pac200072091589.

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Synthesis of chiral derivatives of glyoxylic acid with special emphasis on N-glyoxyloyl-(2R)-bornane-10,2-sultam is presented. Investigation of glyoxylic acid chiral derivatives in various stereocontrolled organic syntheses showed their excellent ability to provide products of high optical purity. Application of our methodology to the synthesis of natural products and their analogs is presented.

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Devi, Runjun, and Sajal Kumar Das. "Studies directed toward the exploitation of vicinal diols in the synthesis of (+)-nebivolol intermediates." Beilstein Journal of Organic Chemistry 13 (March 21, 2017): 571–78. http://dx.doi.org/10.3762/bjoc.13.56.

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While the exploitation of the Sharpless asymmetric dihydroxylation as the source of chirality in the synthesis of acyclic molecules and saturated heterocycles has been tremendous, its synthetic utility toward chiral benzo-annulated heterocycles is relatively limited. Thus, in the search for wider applications of Sharpless asymmetric dihydroxylation-derived diols for the synthesis of benzo-annulated heterocycles, we report herein our studies in the asymmetric synthesis of (R)-1-((R)-6-fluorochroman-2-yl)ethane-1,2-diol, (R)-1-((S)-6-fluorochroman-2-yl)ethane-1,2-diol and (S)-6-fluoro-2-((R)-oxi

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Khangarot, Rama Kanwar, Manisha Khandelwal, and Sumit Kumar Ray. "Syntheses and Applications of Singh’s Catalyst." Synthesis 52, no. 23 (2020): 3577–82. http://dx.doi.org/10.1055/s-0040-1707235.

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Singh’s catalyst has emerged as one of the most promising and valuable catalysts in the field of asymmetric synthesis. Since its discovery, it has proven to be one of the best organocatalysts for asymmetric direct aldol reactions, and is equally efficient in aqueous and organic media. In this Short Review, we summarize reactions utilizing Singh’s catalyst under various conditions.1 Introduction2 Synthesis of Singh’s Catalyst3 Applications in Asymmetric Synthesis4 Conclusion

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6

Deng, Yongming, Qing-Qing Cheng, and Michael Doyle. "Asymmetric [3+3] Cycloaddition for Heterocycle Synthesis." Synlett 28, no. 14 (2017): 1695–706. http://dx.doi.org/10.1055/s-0036-1588453.

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Asymmetric syntheses of six-membered ring heterocycles are important research targets not only in synthetic organic chemistry but also in pharmaceuticals. The [3+3]-cycloaddition methodology is a complementary strategy to [4+2] cycloaddition for the synthesis of heterocyclic compounds. Recent progress in [3+3]-cycloaddition processes provide powerful asymmetric methodologies for the construction of six-membered ring heterocycles with one to three heteroatoms in the ring. In this account, synthetic efforts during the past five years toward the synthesis of enantioenriched six-membered ring hete

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7

Dhayalan, Vasudevan, Rambabu Dandela, K. Bavya Devi, and Ragupathy Dhanusuraman. "Synthesis and Applications of Asymmetric Catalysis Using Chiral Ligands Containing Quinoline Motifs." SynOpen 06, no. 01 (2022): 31–57. http://dx.doi.org/10.1055/a-1743-4534.

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AbstractIn the past decade, asymmetric synthesis of chiral ligands containing quinoline motifs, a family of natural products displaying a broad range of structural diversity and their metal complexes, have become the most significant methodology for the generation of enantiomerically pure compounds of biological and pharmaceutical interest. This review provides comprehensive insight on the plethora of nitrogen-based chiral ligands containing quinoline motifs and organocatalysts used in asymmetric synthesis. However, it is confined to the synthesis of quinoline-based chiral ligands and metal co

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PFANDER, H. "ChemInform Abstract: Carotenoid Synthesis. Asymmetric Syntheses." ChemInform 28, no. 6 (2010): no. http://dx.doi.org/10.1002/chin.199706303.

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Huang, Deng-Ming, Hui-Jing Li, Jun-Hu Wang, and Yan-Chao Wu. "Asymmetric total synthesis of talienbisflavan A." Organic & Biomolecular Chemistry 16, no. 4 (2018): 585–92. http://dx.doi.org/10.1039/c7ob02837g.

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The first asymmetric total syntheses of talienbisflavan A and bis-8,8′-epicatechinylmethane as well as a facile synthesis of bis-8,8′-catechinylmethane has been accomplished from readily available starting materials by using a newly developed direct regioselective methylenation of catechin derivatives as one of the key steps.

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Pereira, Ana Margarida, Honorina Cidade, and Maria Elizabeth Tiritan. "Stereoselective Synthesis of Flavonoids: A Brief Overview." Molecules 28, no. 1 (2023): 426. http://dx.doi.org/10.3390/molecules28010426.

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Stereoselective synthesis has been emerging as a resourceful tool because it enables the obtaining of compounds with biological interest and high enantiomeric purity. Flavonoids are natural products with several biological activities. Owing to their biological potential and aiming to achieve enantiomerically pure forms, several methodologies of stereoselective synthesis have been implemented. Those approaches encompass stereoselective chalcone epoxidation, Sharpless asymmetric dihydroxylation, Mitsunobu reaction, and the cycloaddition of 1,4-benzoquinone. Chiral auxiliaries, organo-, organomet

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Dissertations / Theses on the topic "Asymmetric synthesis"

1

Case-Green, S. C. "Double asymmetric synthesis." Thesis, University of Oxford, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.293361.

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Ridge, Katerina. "Absolute asymmetric synthesis." Thesis, University of Surrey, 2007. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.493053.

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One possible way of achieving absolute asymmetric synthesis is by "freezing" the chirality of a molecule by crystaUisation. This work is a study of the synthesis of :ertain imides which have potential for axial chirality and are likely to undergo spontaneous resolution on crystallisation. The synthesis starts from achiral compounds and therefore, if it does yield chiral crystals by spontaneous resolution, it can be classified as absolute asymmetric synthesis.

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3

Lewis, Neil. "Asymmetric piperidine synthesis." Thesis, University of Nottingham, 1995. http://eprints.nottingham.ac.uk/13293/.

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It has been demonstrated that bakers' yeast reduction of 1-tert-butyl-2-methyl 3-oxo-piperidine-1,2-dicarboxylate gives (2R, 3S), 1-tert-butyl-2-methyl 3-hydroxy-piperidine-1,2-dicarboxylate in 80% chemical yield with >99% d.e. and >97% e.e. Also bakers' yeast reduction of 1-tert-butyl-3-ethyl 4-oxo-piperidine-1,3-dicarboxylate gives (3R, 4S), 1-tert-butyl-3-ethyl4-hydroxy-piperidine-1,3-dicarboxylate in 74% chemical yield with >99% d.e. and >93% e.e. The optical purity and absolute configurations of the hydroxy-ester derivatives were determined by conversion into the corresponding chiral bis-

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Pedersen, Daniel Sejer. "Asymmetric cyclopropane synthesis." Thesis, University of Cambridge, 2006. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.613762.

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Harris, Matthew Eben. "Asymmetric lactam synthesis." Thesis, University of Warwick, 2013. http://wrap.warwick.ac.uk/58635/.

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Broad-Spectrum Chemokine Inhibitors (BSCIs) are a novel type of antiinflammatory drug, discovered by Fox and colleagues. We have shown that the syntheses of C-substituted γ-thialactams are possible via a modular approach starting from the simple amino acid cystine. These compounds are a new class of GPCR ligand, showing BSCI activity comparable to their non-sulfur counterparts. Initial migratory data suggests that these lactams are inhibitors of leukocyte migration and comparable to the analogous BSCI lactams at μM concentrations, with decreased activity at the nM scale. Efforts have been made

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Ravindran, Swarnam Shanthi. "Studies in asymmetric synthesis." Thesis, Rhodes University, 1994. http://hdl.handle.net/10962/d1005017.

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The stereoselectivity of TiCI₄-catalysed Mukaiyama reactions of a camphor acetal-derived chiral silyl enol ether with a range of substituted aromatic aldehydes has been examined. The enantiomeric excess in each of the resulting ß-hydroxy ketones, determined by ¹H NMR spectroscopy using the lanthanide chiral shift reagent Pr(Etcf₃), ranged between 9 and 13%. The stereo-directing potential of the camphor acetal as a chiral auxiliary in the α-benzylation of carboxylate esters has been studied; the acids were chosen to illustrate substituent effects on asymmetric induction. The observed diastereos

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7

Wang, Ziyu, та 汪子玉. "Organocatalytic asymmetric synthesis of dihydrodibenzofurans and asymmetric aziridination of α-nitroalkenes". Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2012. http://hdl.handle.net/10722/193388.

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The synthesis of useful chiral skeletons from simple achiral starting materials is always the dream of organic chemists. In the past decades, organocatalysis has been rapidly developed and has become one of the most important methods in asymmetric catalysis. The aim of this thesis is to develop asymmetric methods for the construction of useful chiral skeletons based on organocatalytic chemistry. Many natural products and biologically important compounds contain the hydrogenated dibenzofuran (Figure 1) as a common sub-structure. In the first part of this thesis, the first amine-catalysed asymm

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8

White, Rachael A. "Asymmetric Synthesis of Prostaglandins." Digital WPI, 2005. https://digitalcommons.wpi.edu/etd-theses/735.

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Prostaglandins (PGs) are medicinally interesting because of the wide variety of roles they play in the body. PGs are ubiquitous and can be found in the reproductive system, the nervous system, the cardiovascular system, and the immune system. Accordingly, PGs are an important therapeutic target for pharmaceutical companies, and an efficient synthesis is highly desirable. Past research indicates that an approach to prostaglandins via a chiral acetylenic ester or amide provides a promising method for control of C-15 geometry. This project seeks to validate a key stereospecific reduction of an en

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9

Ambler, P. W. "Asymmetric synthesis of cyclopropanes." Thesis, University of Oxford, 1988. https://ora.ox.ac.uk/objects/uuid:958e77c2-d15e-4d8f-af84-36dca36e4215.

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This thesis is concerned with the asymmetric synthesis of cyclopropyl derivatives via the use of chiral iron acyl complexes of the type (η<sup>5</sup>-C<sub>5</sub>H<sub>5</sub>)Fe(CO)(PPh<sub>3</sub>)(COCH=CR'R), Chapter 1 reviews previous routes to optically active cyclopropyl derivatives and reviews the use of the chiral auxiliary (η<sup>5</sup>-C<sub>5</sub>H<sub>5</sub>)Fe(CO)(PPh<sub>3</sub>) for asymmetric synthesis. Chapter 2 describes the synthesis of the complexes (η<sup>5</sup>-C<sub>5</sub>H<sub>5</sub>)Fe(CO)(PPh<sub>3</sub>)(COCH=CRR') and presents a conformational an

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10

Dixon, Darren J. "Asymmetric synthesis of andrimid." Thesis, University of Oxford, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.337813.

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Books on the topic "Asymmetric synthesis"

1

1958-, Aitken R. Alan, and Kilényi S. N, eds. Asymmetric synthesis. Blackie Adacemie & Professional, 1992.

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2

Richard, Stephenson G., ed. Advanced asymmetric synthesis. Chapman & Hall, 1996.

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Aitken, R. Alan, and S. Nicholas Kilényi, eds. Asymmetric Synthesis. Springer Netherlands, 1992. http://dx.doi.org/10.1007/978-94-011-1346-5.

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1958-, Aitken R. Alan, and Kilényi S. N, eds. Asymmetric synthesis. Blackie Academic & Professional, 1994.

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1958-, Aitken R. Alan, and Kilényi S. N, eds. Asymmetric synthesis. Blackie Academic & Professional, 1992.

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A, Aitken R., and Kilenyi S. N, eds. Asymmetric synthesis. Blackie Academic, 1992.

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D, Morrison James, ed. Asymmetric synthesis. Academic Press, 1985.

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8

Ojima, Iwao. Catalytic asymmetric synthesis. 3rd ed. John Wiley, 2010.

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Ojima, Iwao, ed. Catalytic Asymmetric Synthesis. John Wiley & Sons, Inc., 2010. http://dx.doi.org/10.1002/9780470584248.

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Ojima, Iwao, ed. Catalytic Asymmetric Synthesis. John Wiley & Sons, Inc., 2000. http://dx.doi.org/10.1002/0471721506.

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Book chapters on the topic "Asymmetric synthesis"

1

Aitken, R. A. "Chirality." In Asymmetric Synthesis. Springer Netherlands, 1992. http://dx.doi.org/10.1007/978-94-011-1346-5_1.

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Aitken, R. A. "The description of stereochemistry." In Asymmetric Synthesis. Springer Netherlands, 1992. http://dx.doi.org/10.1007/978-94-011-1346-5_2.

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3

Parker, D., and R. J. Taylor. "Analytical methods: determination of enantiomeric purity." In Asymmetric Synthesis. Springer Netherlands, 1992. http://dx.doi.org/10.1007/978-94-011-1346-5_3.

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Aitken, R. A., and J. Gopal. "Sources and strategies for the formation of chiral compounds." In Asymmetric Synthesis. Springer Netherlands, 1992. http://dx.doi.org/10.1007/978-94-011-1346-5_4.

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Kilenyi, S. N. "First- and second-generation methods: chiral starting materials and auxiliaries." In Asymmetric Synthesis. Springer Netherlands, 1992. http://dx.doi.org/10.1007/978-94-011-1346-5_5.

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Kilenyi, S. N., and R. A. Aitken. "Third- and fourth-generation methods: asymmetric reagents and catalysts." In Asymmetric Synthesis. Springer Netherlands, 1992. http://dx.doi.org/10.1007/978-94-011-1346-5_6.

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Kilenyi, S. N. "Asymmetric total synthesis." In Asymmetric Synthesis. Springer Netherlands, 1992. http://dx.doi.org/10.1007/978-94-011-1346-5_7.

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8

Shintani, Ryo, and Tamio Hayashi. "Asymmetric Synthesis." In Modern Organonickel Chemistry. Wiley-VCH Verlag GmbH & Co. KGaA, 2005. http://dx.doi.org/10.1002/3527604847.ch9.

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9

Chen, Chuan-Feng, and Yun Shen. "Asymmetric Synthesis." In Helicene Chemistry. Springer Berlin Heidelberg, 2016. http://dx.doi.org/10.1007/978-3-662-53168-6_7.

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Talapatra, Sunil Kumar, and Bani Talapatra. "Asymmetric Synthesis." In Basic Concepts in Organic Stereochemistry. Springer International Publishing, 2022. http://dx.doi.org/10.1007/978-3-030-95990-6_5.

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Conference papers on the topic "Asymmetric synthesis"

1

Zhang, Yang. "Spatially Aware Interpolation Synthesis Method for MR Images Based on Asymmetric Mask Coding." In 2024 3rd International Conference on Cloud Computing, Big Data Application and Software Engineering (CBASE). IEEE, 2024. https://doi.org/10.1109/cbase64041.2024.10824639.

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Monteiro, J. L., A. F. Torre, M. P. Paixão, and A. G. Corrêa. "Asymmetric synthesis of pyranocumarins under greener conditions." In 15th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-bmos2013_2013101414540.

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Carmona, Rafaela C., and Carlos Roque D. Correia. "Asymmetric Arylation of Indenes via Heck-Matsuda Reaction." In 15th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-bmos2013_201381992939.

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Ishikawa, Eloisa E., and Luiz F. Silva Jr. "Studies Towards Asymmetric Total Synthesis of Populene D." In 15th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-bmos2013_2013913144428.

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Deobald, Anna Maria, Arlene G. Corrêa, and Márcio W. Paixão. "Application of New Organocatalysts on Asymmetric Epoxidation of Chalcones." In 14th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-14bmos-r0188-2.

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Ribeiro, Joyce Benzaquem, Raquel de Oliveira Lopes, Luciana Dalla Vechia, Aline de Souza Ramos, Selma Gomes Ferreira Leite, and Rodrigo Octavio Mendonça Alves de Souza. "Asymmetric reduction of 4-Bromo-Acetophenone using whole cells." In 14th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-14bmos-r0206-1.

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Ahmad, Anees, and Luiz F. Silva Jr. "Asymmetric Ring Contraction Reactions Mediated by Chiral I(III)." In 15th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-bmos2013_201398181055.

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Balike, Krishna Prasad, Subhash Rakheja, and Ion Stiharu. "Optimization of Asymmetric Damper Parameters of an Automotive Suspension for Minimal Camber Angle Variations." In ASME 2010 International Design Engineering Technical Conferences and Computers and Information in Engineering Conference. ASMEDC, 2010. http://dx.doi.org/10.1115/detc2010-28375.

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Asymmetric dampers invariably employed in automotive suspensions are known to cause ‘damper jacking’. The influence of the damper jacking on the suspension kinematic responses, particularly variations in the camber angle, are generally ignored while synthesizing a damper. This study presents influences of damper asymmetry on the camber angle variations of a double wishbone type of suspension together with the dynamic responses under measured urban road inputs. Simulation studies employing a kineto-dynamic quarter-car model comprising a bilinear damper revealed increase in the camber angle vari

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Feu, Karla S., Sandrina I. R. M. Silva, Marco A. F. M. Junior, Alexander F. de la Torre, Arlene G. Corrêa, and Márcio W. Paixão. "PEG: An Efficient Green Solvent for Organocatalytic Asymmetric Michael Addition." In 15th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-bmos2013_2013820194343.

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Gajaweera, Ruwan N., and Larry F. Lind. "Coupling Matrix Synthesis for Asymmetric Filter Topologies." In 2008 IEEE MTT-S International Microwave Workshop Series on Art of Miniaturizing RF and Microwave Passive Components (IMWS). IEEE, 2008. http://dx.doi.org/10.1109/imws.2008.4782266.

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Reports on the topic "Asymmetric synthesis"

1

Reilly, S. D., D. R. Click, S. K. Grumbine, B. L. Scott, and J. G. Watkins. Asymmetric catalysis in organic synthesis. Office of Scientific and Technical Information (OSTI), 1998. http://dx.doi.org/10.2172/677032.

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Watkins, B. E., and J. H. Satcher. The synthesis and characterization of new iron coordination complexes utilizing an asymmetric coordinating chelate ligand. Office of Scientific and Technical Information (OSTI), 1995. http://dx.doi.org/10.2172/108153.

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Veeck, A. C. 1: Mass asymmetric fission barriers for {sup 98}Mo; 2: Synthesis and characterization of actinide-specific chelating agents. Office of Scientific and Technical Information (OSTI), 1996. http://dx.doi.org/10.2172/414344.

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