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Journal articles on the topic 'Antibiotic synthesis/chemistry'

Author: Grafiati

Published: 4 June 2021

Last updated: 7 February 2022

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1

Ley, Steven V., J. Andrew Clase, Darren J. Mansfield, and Helen M. I. Osborn. "Synthesis and chemistry of the ionophore antibiotic tetronasin." Journal of Heterocyclic Chemistry 33, no. 5 (September 1996): 1533–44. http://dx.doi.org/10.1002/jhet.5570330509.

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2

Hanessian, Stephen, and René Roy. "Chemistry of spectinomycin: its total synthesis, stereocontrolled rearrangement, and analogs." Canadian Journal of Chemistry 63, no. 1 (January 1, 1985): 163–72. http://dx.doi.org/10.1139/v85-026.

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The total stereocontrolled synthesis of the antibiotic spectinomycin is described, based on the regiospecific functionalization and manipulation of appropriate starting materials. The tertiary ketol rearrangement of the antibiotic and its derivatives was studied and the stereochemical identity of spectinoic acid was established by chemical correlation. Dihydrospectinomycin derivatives undergo unusual solvolysis reactions.

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3

Nawfa, Refdinal, Adi Setyo Purnomo, and Herdayanto Sulistyo Putro. "Synthesis of Antibiotic Penicillin-G Enzymatically by Penicillium chrysogenum." Asian Journal of Chemistry 31, no. 10 (August 30, 2019): 2367–69. http://dx.doi.org/10.14233/ajchem.2019.21766.

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Penicillin-G antibiotic was used as the basic ingredient of making antibiotic type β-lactam such as tetracycline, amoxicillin, ampicillin and other antibiotics. Penicillin-G was splited into 6-amino penicillanic acid as the source of β-lactam. The biosynthetic pathway for the formation of penicillin-G in Penicillium chrysogenum cell through the formation of intermediates was carried out in the form of amino acids such as α-aminoadipate, L-cysteine, L-valine which are formed from glucose (food ingredients).The formation of 6-amino penicillanic acid is an amino acid combination of L-cysteine and L-valine, a step part of the formation of antibiotic penicillin-G in P. chrysogenum cells, thus, it is obvious that there are enzymes involved in its formation. The objective of this study was to examine the use of enzymes present in P. chrysogenum cells to produce penicillin-G and 6-amino penicillanic acid using the intermediate compounds α-aminoadipate, L-cysteine, L-valine and phenylacetic acid assisted by NAFA® coenzymes in P. chrysogenum cells which is more permeable. The research method started from producing biomass of P. chrysogenum cells that demonstrated penicillin-producing antibiotic capability, as the source of the enzyme, followed by addition of permeability treatment of P. chrysogenum cell membrane to get immobile of enzyme by its own cell therefore it can be used more than once. After that the enzyme activity was proven by adding α-aminoadipate, L-cysteine, L-valine, phenylacetic acid and NAFA® coenzyme for the formation of penicillin-G, whereas the addition of L-cystein, L-valine and NAFA® coenzyme were aimed to form 6-amino penicillanic acid. The results showed that P. chrysogenum is able to produce antibiotics with stationary early phase on day 6. The best increased permeability of P. chrysogenum cell membranes was obtained using a 1:4 of toluene:ethanol ratio mixture with the highest antibiotic concentration (130.06 mg/L) after testing for the enzymatic formation of antibacterial penicillin-G.

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4

Inami, Kaoru, and Tetsuo Shiba. "Total Synthesis of Antibiotic Althiomycin." Bulletin of the Chemical Society of Japan 58, no. 1 (January 1985): 352–60. http://dx.doi.org/10.1246/bcsj.58.352.

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5

Ozkal, Can B., and Süreyya Meric. "Photocatalytic Bacteria Inactivation by TiO2-Ag based Photocatalysts and the Effect on Antibiotic Resistance Profile." Current Analytical Chemistry 17, no. 1 (December 30, 2020): 98–106. http://dx.doi.org/10.2174/1573411016999200711145845.

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Background: In the last decade, research in the field of contaminants of emerging concern proliferated while special interest was focused on antibiotic-resistant bacteria, antibiotic resistance genes as widespread pollutants. Advanced oxidation processes have gained an essential attraction in the field of antibiotics degradation and bacteria inactivation Methods: Photocatalysts in the form of sol-gel based TiO2-Ag-xerogel and green synthesized nanocomposites TiO2-Ag compared with regard to their bacteria inactivation performances and effect on antibiotic resistance behaviour of target strain. Experiments were carried out at parallel plate reactor configuration under UV-A irradiation with an energy equivalent of solar conditions. PEG 600 and Cydonia oblanga seed extract were used as chemical and bio-chemical reducing-stabilizing agents respectively for the synthesis of TiO2-Ag nano-composite. Results: Photocatalyst type/size based alterations in antibiotic resistance profile of intact and post treatment bacteria cells were examined. Besides the improvement in bacteria inactivation kinetics, photocatalytic disinfection with Ag doped xerogels and TiO2-Ag nanocomposites have triggered alterations on E.coli DSM-498 resistance to tetracycline and aminoglycoside antibiotics. Conclusıon: Cydonia oblanga seed extract is proved to be a promising green substitute for the TiO2- Ag chemical synthesis procedure. Considering the aspects of the economic and environmental impact of nano-composite photocatalyst synthesis, cost reduction is achievable both in the sense of production and disposal. The complexity of water matrix must be considered in a way to determine the wide range applicability of the green synthesis of a nano-composite at the pilot scale.

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6

Ichim, Daniela Luminita, Letitia Doina Duceac, Constantin Marcu, Alin Constantin Iordache, Irina Mihaela Ciomaga, Alina Costina Luca, Elena Roxana Bogdan Goroftei, Geta Mitrea, Daniela Damir, and Liviu Stafie. "Synthesis and Characterization of Colistin Loaded Nanoparticles Used to Combat Multi-drug Resistant Microorganisms." Revista de Chimie 70, no. 10 (November 15, 2019): 3734–37. http://dx.doi.org/10.37358/rc.19.10.7635.

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Some infectious agents frequently act on human body. Multi-drug resistant microorganisms (MDR) develop the capacity to stabilize biofilms. The use of antimicrobials loaded nanoparticles can defeat antibiotic resistance mechanism. The major aim of this study was the synthesis and physico-chemical characterization of Colistin molecules intercalated nanoparticles in order to enhance antibiotic efficacy against multi-drug resistant microorganisms. Advanced characterization techniques were used to analyze new nanostructures containing antibiotics in order to improve antimicrobial efficacy of the free drug. Nano-encapsulated Colistin is presumed to be more efficient in the eradication of severe infections caused by MDR.

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7

LEY, S. V., J. A. CLASE, and D. J. MANSFIELD. "ChemInform Abstract: Synthesis and Chemistry of the Ionophore Antibiotic Tetronasin." ChemInform 27, no. 36 (August 5, 2010): no. http://dx.doi.org/10.1002/chin.199636315.

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8

LEY, S. V., J. A. CLASE, D. J. MANSFIELD, and H. M. I. OSBORN. "ChemInform Abstract: Synthesis and Chemistry of the Ionophore Antibiotic Tetronasin." ChemInform 28, no. 12 (August 4, 2010): no. http://dx.doi.org/10.1002/chin.199712271.

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9

Katoh, Tadashi, and Shiro Terashima. "Total Synthesis of Antitumor Antibiotic FR900482." Journal of Synthetic Organic Chemistry, Japan 55, no. 11 (1997): 946–57. http://dx.doi.org/10.5059/yukigoseikyokaishi.55.946.

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10

Chida, Noritaka, Masami Ohtsuka, Keiichi Nakazawa, and Seiichiro Ogawa. "Total synthesis of antibiotic hygromycin A." Journal of Organic Chemistry 56, no. 9 (April 1991): 2976–83. http://dx.doi.org/10.1021/jo00009a009.

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11

Marchart, Stefan, Alexey Gromov, and Johann Mulzer. "Total Synthesis of the Antibiotic Branimycin." Angewandte Chemie International Edition 49, no. 11 (February 9, 2010): 2050–53. http://dx.doi.org/10.1002/anie.200906453.

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12

Nie, Shenyou, Wei Li, and Biao Yu. "Total Synthesis of Nucleoside Antibiotic A201A." Journal of the American Chemical Society 136, no. 11 (March 11, 2014): 4157–60. http://dx.doi.org/10.1021/ja501460j.

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13

Xavier, Nuno M., and Amélia P. Rauter. "Environmentally friendly approaches to the synthesis of new antibiotics from sugars." Pure and Applied Chemistry 84, no. 3 (February 15, 2012): 803–16. http://dx.doi.org/10.1351/pac-con-11-11-11.

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In light of the biological importance of carbohydrates and their role when present in antibiotic agents, the design and synthesis of carbohydrate-based antibiotics has occupied a prominent place in drug discovery. This review focuses on synthetic carbohydrate antimicrobial agents, giving special emphasis to novel structures easily accessible from readily available carbohydrate precursors.

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14

Duceac, Letitia Doina, Geta Mitrea, Elena Ariela Banu, Madalina Irina Ciuhodaru, Irina Mihaela Ciomaga, Daniela Luminita Ichim, Marcu Constantin, and Alina Costina Luca. "Synthesis and Characterization of Carbapenem Based Nanohybrids as Antimicrobial Agents for Multidrug Resistant Bacteria." Materiale Plastice 56, no. 2 (June 30, 2019): 388–91. http://dx.doi.org/10.37358/mp.19.2.5191.

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Carbapenem antibiotics resistance is a medical threat in antibacterial therapy as the pathogen resistant strains easily evolve a multi-drug resistance action to other incurable agents. The protective transport of current antibiotic molecules using nano-carriers initiates a huge approach in the antibacterial therapy, allowing the nanohybrids to defeat all these health threat pathogen agents. Chitosan is a linear cationic polysaccharide being often used in medical area as a biocompatible encapsulating agent in antibiotic delivery nanosystems. This work refers to encapsulation of imipenem into biodegradable chitosan nanoparticles in order to destroy antibiotic-resistant bacteria and limit the microbial adhesion and multiplication. Nanoparticles were prepared by ion gelation method using tripolyphosphate as cross linking agent. The obtained hybrid nanocapsules were then characterized and evaluated as a potential nano-device to beat antimicrobial resistance.

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15

Shin, Chung-gi, Kazuo Okumura, Akinori Ito, and Dai Yoshioka. "Total Synthesis of Macrocyclic Antibiotic, Micrococcin P1." HETEROCYCLES 48, no. 7 (1998): 1319. http://dx.doi.org/10.3987/com-98-8152.

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16

Koreeda, Masato, and Wu Yang. "Chemistry of 1,2-Dithiins. Synthesis of the Potent Antibiotic Thiarubrine A." Journal of the American Chemical Society 116, no. 23 (November 1994): 10793–94. http://dx.doi.org/10.1021/ja00102a058.

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17

Annalakshmi, Muthaiah, Subbarayan Sumithra, Shen-Ming Chen, Tse-Wei Chen, and Xuei-Hong Zheng. "Facile synthesis of ultrathin NiSnO3 nanoparticles for enhanced electrochemical detection of an antibiotic drug in water bodies and biological samples." New Journal of Chemistry 44, no. 25 (2020): 10604–12. http://dx.doi.org/10.1039/d0nj01375g.

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The highly sensitive real-time detection of antibiotic drugs (nitrofurantoin; NFT) has drawn significant research attention due to the extensive use of antibiotics, which may cause serious threats to environment as well as living things.

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18

Fukase, Koichi, Manabu Kitazawa, Akihiko Sano, Kuniaki Shimbo, Hiroshi Fujita, Shingo Horimoto, Tateaki Wakamiya, and Tetsuo Shiba. "Total synthesis of peptide antibiotic nisin." Tetrahedron Letters 29, no. 7 (January 1988): 795–98. http://dx.doi.org/10.1016/s0040-4039(00)80212-9.

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19

Shaban, Mohamed A., Ossama M. Al Badry, Aliaa M. Kamala, and Mohamd Abd el Wahap Abd El-Gawad. "Synthesis and screening of quinolone antibiotic isosteres." Journal of Chemical Research 2008, no. 12 (December 1, 2008): 715–18. http://dx.doi.org/10.3184/030823408x389372.

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20

OHNO, Masaji, Susumu KOBAYASHI, and Masa-aki KURIHARA. "Antibiotic synthesis based on symmetrization-asymmetrization concept." Journal of Synthetic Organic Chemistry, Japan 44, no. 1 (1986): 38–48. http://dx.doi.org/10.5059/yukigoseikyokaishi.44.38.

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21

Zhang, Shiju, Xiaotong Li, Yan Wang, Yucong Zheng, Shiqing Han, Huilei Yu, and Shahua Huang. "Formal Synthesis of Gram-Negative Antibiotic Negamycin." Chinese Journal of Organic Chemistry 40, no. 2 (2020): 521. http://dx.doi.org/10.6023/cjoc201908025.

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22

Acosta, Jaime A. M., Ramesh Muddala, Luiz C. A. Barbosa, and John Boukouvalas. "Total Synthesis of the Antitumor Antibiotic Basidalin." Journal of Organic Chemistry 81, no. 15 (July 7, 2016): 6883–86. http://dx.doi.org/10.1021/acs.joc.6b01255.

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23

Fei, Zhongbo, Quanbing Wu, Lei Li, Qun Jiang, Bin Li, Like Chen, Hao Wang, et al. "New Synthesis for the Monobactam Antibiotic—LYS228." Journal of Organic Chemistry 85, no. 11 (May 15, 2020): 6854–61. http://dx.doi.org/10.1021/acs.joc.9b01916.

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24

Elkihel, L., J. Bourass, M. Dherbomez, and Y. Letourneux. "Synthesis of Aminocholesterol Derivatives with Antibiotic Properties." Synthetic Communications 27, no. 11 (June 1997): 1951–62. http://dx.doi.org/10.1080/00397919708006797.

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25

Nicolaou, K. C., D. P. Papahatjis, D. A. Claremon, R. L. Magolda, and R. E. Dolle. "Total synthesis of ionophore antibiotic X-14547A." Journal of Organic Chemistry 50, no. 9 (May 1985): 1440–56. http://dx.doi.org/10.1021/jo00209a017.

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26

Schow, Steven R., Susan Quinn DeJoy, Michael M. Wick, and S. S. Kerwar. "Diastereoselective Synthesis of the Antibiotic L-Azatyrosine." Journal of Organic Chemistry 59, no. 22 (November 1994): 6850–52. http://dx.doi.org/10.1021/jo00101a056.

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27

Khatri, Hem Raj, Hai Nguyen, James K. Dunaway, and Jianglong Zhu. "Total Synthesis of Antitumor Antibiotic Derhodinosylurdamycin A." Chemistry - A European Journal 21, no. 39 (August 6, 2015): 13553–57. http://dx.doi.org/10.1002/chem.201502113.

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28

Waalboer, Dennis C. J., Stefan H. A. M. Leenders, Tanja Schülin-Casonato, Floris L. van Delft, and Floris P. J. T. Rutjes. "Total Synthesis and Antibiotic Activity of Dehydrohomoplatencin." Chemistry - A European Journal 16, no. 37 (August 16, 2010): 11233–36. http://dx.doi.org/10.1002/chem.201001744.

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29

Lowe, Christopher, Yunlong Pu, and John C. Vederas. "Synthesis of (+)-obafluorin, a .beta.-lactone antibiotic." Journal of Organic Chemistry 57, no. 1 (January 1992): 10–11. http://dx.doi.org/10.1021/jo00027a006.

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30

Jiménez-Andreu, M. Mercedes, Francisco J. Sayago, and Carlos Cativiela. "An Improved Synthesis of the Antibiotic Dehydrophos." European Journal of Organic Chemistry 2018, no. 29 (July 10, 2018): 3965–73. http://dx.doi.org/10.1002/ejoc.201800689.

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31

Xiao, Guozhi, and Haiqing He. "Chemical Synthesis of the Nucleoside Antibiotic Capuramycin." European Journal of Organic Chemistry 2021, no. 26 (July 8, 2021): 3681–89. http://dx.doi.org/10.1002/ejoc.202100613.

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32

Chow, Hoi Yee, Delin Chen, and Xuechen Li. "Improved total synthesis of the antibiotic A54145B." Organic & Biomolecular Chemistry 18, no. 23 (2020): 4401–5. http://dx.doi.org/10.1039/d0ob00558d.

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33

Yamashita, Yu, Yoichi Hirano, Akiomi Takada, Hiroshi Takikawa, and Keisuke Suzuki. "Total Synthesis of the Antibiotic BE-43472B." Angewandte Chemie International Edition 52, no. 26 (May 15, 2013): 6658–61. http://dx.doi.org/10.1002/anie.201301591.

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34

Evans, David A., Robert L. Dow, Thomas L. Shih, James M. Takacs, and Robert Zahler. "Total synthesis of the polyether antibiotic ionomycin." Journal of the American Chemical Society 112, no. 13 (June 1990): 5290–313. http://dx.doi.org/10.1021/ja00169a042.

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35

Evans, David A., Stephen W. Kaldor, Todd K. Jones, Jon Clardy, and Thomas J. Stout. "Total synthesis of the macrolide antibiotic cytovaricin." Journal of the American Chemical Society 112, no. 19 (September 1990): 7001–31. http://dx.doi.org/10.1021/ja00175a038.

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36

Mangiaterra, Gianmarco, Elisa Carotti, Salvatore Vaiasicca, Nicholas Cedraro, Barbara Citterio, Anna La Teana, and Francesca Biavasco. "Contribution of Drugs Interfering with Protein and Cell Wall Synthesis to the Persistence of Pseudomonas aeruginosa Biofilms: An In Vitro Model." International Journal of Molecular Sciences 22, no. 4 (February 5, 2021): 1628. http://dx.doi.org/10.3390/ijms22041628.

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The occurrence of Pseudomonas aeruginosa (PA) persisters, including viable but non-culturable (VBNC) forms, subpopulations of tolerant cells that can survive high antibiotic doses, is the main reason for PA lung infections failed eradication and recurrence in Cystic Fibrosis (CF) patients, subjected to life-long, cyclic antibiotic treatments. In this paper, we investigated the role of subinhibitory concentrations of different anti-pseudomonas antibiotics in the maintenance of persistent (including VBNC) PA cells in in vitro biofilms. Persisters were firstly selected by exposure to high doses of antibiotics and their abundance over time evaluated, using a combination of cultural, qPCR and flow cytometry assays. Two engineered GFP-producing PA strains were used. The obtained results demonstrated a major involvement of tobramycin and bacterial cell wall-targeting antibiotics in the resilience to starvation of VBNC forms, while the presence of ciprofloxacin and ceftazidime/avibactam lead to their complete loss. Moreover, a positive correlation between tobramycin exposure, biofilm production and c-di-GMP levels was observed. The presented data could allow a deeper understanding of bacterial population dynamics during the treatment of recurrent PA infections and provide a reliable evaluation of the real efficacy of the antibiotic treatments against the bacterial population within the CF lung.

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37

Brimble, Margaret A. "Synthetic studies toward pyranonaphthoquinone antibiotics." Pure and Applied Chemistry 72, no. 9 (January 1, 2000): 1635–39. http://dx.doi.org/10.1351/pac200072091635.

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A furofuran annulation/oxidative rearrangement strategy was used to construct the basic skeleton of the pyranonaphthoquinone family of antibiotics. This synthetic methodology has been applied to the synthesis of the spiroacetal-containing pyranonaphthoquinone antibiotic griseusin A, to an analog of the C-glycoside medermycin, and to a dimeric pyranonaphthoquinone.

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38

Ho, Pak-Tsun, and Simmie Wong. "Branched-chain sugars in asymmetric synthesis. Total synthesis of marine antibiotic (−)-malyngolide." Canadian Journal of Chemistry 63, no. 8 (August 1, 1985): 2221–24. http://dx.doi.org/10.1139/v85-365.

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39

K. Mohapatra, Debendra, Rita Pal, Hasibur Rahaman, and Mukund K. Gurjar. "Stereoselective Formal Total Synthesis of Novel Antibiotic (-)-Centrolobine." HETEROCYCLES 80, no. 1 (2010): 219. http://dx.doi.org/10.3987/com-08-s(s)1.

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40

Shin, Chung-gi, Yasuhiro Yamada, Keiichiro Hayashi, Yasuchika Yonezawa, Kazuyuki Umemura, Tsuyoshi Tanji, and Juji Yoshimura. "Convenient Synthesis of Fragment E of Antibiotic, Nosiheptide." HETEROCYCLES 43, no. 4 (1996): 891. http://dx.doi.org/10.3987/com-96-7396.

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41

Ghosh, Samir, A. Sanjeev Kumar, G. N. Mehta, R. Soundararajan, and Subhabrata Sen. "Formal synthesis of piperazinomycin, a novel antifungal antibiotic." Arkivoc 2009, no. 7 (March 27, 2009): 72–78. http://dx.doi.org/10.3998/ark.5550190.0010.707.

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42

Groth, Ulrich, and Aris Kalogerakis. "Total Synthesis of the Angucylinone Antibiotic (+)-Rubiginone B2." Synlett, no. 12 (2003): 1886–88. http://dx.doi.org/10.1055/s-2003-41473.

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43

Garigipati, Ravi S., and Steven M. Weinreb. "Stereoselective total synthesis of the antitumor antibiotic (-)-bactobolin." Journal of Organic Chemistry 53, no. 17 (August 1988): 4143–45. http://dx.doi.org/10.1021/jo00252a060.

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44

Manchand, Percy S., Kin Chun Luk, Peter S. Belica, Satish C. Choudhry, Chung Chen Wei, and Milan Soukup. "A novel synthesis of the monobactam antibiotic carumonam." Journal of Organic Chemistry 53, no. 23 (November 1988): 5507–12. http://dx.doi.org/10.1021/jo00258a020.

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45

Okumura, Kazuo, Taishi Suzuki, Yutaka Nakamura, and Chung-gi Shin. "Total Synthesis of a Macrocyclic Antibiotic, Micrococcin P1." Bulletin of the Chemical Society of Japan 72, no. 11 (November 1999): 2483–90. http://dx.doi.org/10.1246/bcsj.72.2483.

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46

Wipf, Peter, and Yuntae Kim. "Synthesis of the Antitumor Antibiotic LL-C10037.alpha." Journal of Organic Chemistry 59, no. 13 (July 1994): 3518–19. http://dx.doi.org/10.1021/jo00092a004.

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47

Han, Sheng, Yuan-Zhen Xiong, Rui Huang, and Pei-Yu Chen. "A Convenient Synthesis of Carbapenem Antibiotic Ertapenem Sodium." Asian Journal of Chemistry 26, no. 12 (2014): 3464–66. http://dx.doi.org/10.14233/ajchem.2014.15964.

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48

Okumura, Kazuo, Yutaka Nakamura, and Chung-gi Shin. "Total Synthesis of a Macrocyclic Antibiotic, Micrococcin P." Bulletin of the Chemical Society of Japan 72, no. 7 (July 1999): 1561–69. http://dx.doi.org/10.1246/bcsj.72.1561.

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49

Covarrubias-Zúñiga, Adrián, José G. Avila-Zárraga, and David Arias Salas. "A Total Synthesis of the Antibiotic DB-2073." Synthetic Communications 33, no. 18 (September 2003): 3173–81. http://dx.doi.org/10.1081/scc-120023438.

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50

Shibasaki, Masakatsu, Yasuko Ishida, Genji Iwasaki, and Takamasa Iimori. "Asymmetric synthesis of the carbapenem antibiotic (+)-PS-5." Journal of Organic Chemistry 52, no. 15 (July 1987): 3488–89. http://dx.doi.org/10.1021/jo00391a073.

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