Academic literature on the topic 'Aging of bitumen materials'

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Journal articles on the topic "Aging of bitumen materials"

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Zeng, Guodong, Jianjing Zhang, Hongming Huang, Xin Xiao, and Chuanqi Yan. "A Comparative Study for Creep and Recovery Behavior Characterization of Modified Bitumens Using the MSCR Test." Coatings 13, no. 8 (August 16, 2023): 1445. http://dx.doi.org/10.3390/coatings13081445.

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In recent decades, the application of modified bitumens has experienced tremendous growth. However, due to the varying modification mechanism of different modifiers, the creep and recovery properties of modified bitumen have not been comprehensively understood. This study aims to evaluate the creep and recovery properties of several representative modified bitumens using the multi-stress creep recovery (MSCR) test. The MSCR test can highlight the unique delayed elasticity of modified bitumen and it uses a high stress level, which is more comparable to the field. In particular, this test also aims to identify the effects of different aging conditions. To do so, a total of 15 bitumens, including 7 elastomeric-modified bitumens, 5 non-elastomeric-modified bitumens, and 3 plain bitumens, were prepared and examined. Furthermore, 10 different aging conditions were considered. The results suggest that the generation mechanism of elasticity varies for different modified bitumens. There are two types of elasticities, which are energy elasticity and entropy elasticity, and their differences need more attention in the road bitumen material community. Aging changes the percentages of contributions from energy elasticity and entropy elasticity to the bitumen’s overall recovery performance. The increase in “bad” energy elasticity may compensate for part of the “good” entropy elasticity loss, but overall, the bitumen’s recovery rate is decreasing and the ratio of energy elasticity is increasing, which might hinder the bitumen’s road performance.
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Li, Mingxia, Elham Fini, Xiaomin Jia, Baiyang Song, and Yanhong Wang. "Effect of Aging on Healing Capacity of Bituminous Composites Containing Polyphosphoric Acid." Materials 16, no. 9 (April 24, 2023): 3333. http://dx.doi.org/10.3390/ma16093333.

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This study examines how aging affects the healing capacity of bituminous composites containing polyphosphoric acid (PPA). PPA is commonly used in bituminous composites to enhance its elasticity, however, PPA effectiveness highly depends on other constituents on the matrix and the environmental (internal and external) factors. In terms of internal factors, the interplay between PPA and various bitumen modifiers have been extensively studied. Here, we study how external factors such as exposure to ultraviolet radiation affect PPA’s efficacy, measured in terms of change in bitumen’s healing index. The study results showed that the introduction of PPA to bituminous composites significantly increases the bitumen healing index, however, the change in the healing index becomes less pronounced as aging progresses. The presence of additives such as taconite were found to affect the effect of PPA on bitumen’s healing index. For instance, bitumens containing 30% taconite showed the highest increase in their healing index in the presence of PPA among studied scenarios. Overall, bitumen containing PPA had a higher healing index than those without PPA regardless of the extent of aging and dosage of modifiers. This, in turn, indicates that PPA is highly effective for enhancing bitumen healing. This can be attributed to the role of PPA in promoting intermolecular interactions within the bitumen matrix.
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Geçkil, Tacettin. "Physical, Chemical, Microstructural and Rheological Properties of Reactive Terpolymer-Modified Bitumen." Materials 12, no. 6 (March 20, 2019): 921. http://dx.doi.org/10.3390/ma12060921.

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In this study, the change in the physical, chemical, microstructural, and rheological properties of a road bitumen modified with reactive terpolymer (Elvaloy®RET) was investigated. For this purpose, four different Elvaloy®RET percentages (0%, 0.4%, 0.8%, and 1.2% by wt.) were mixed with B 160/220 bitumen. Firstly, the obtained samples were subjected to a short and long-term aging process using a rotating thin-film oven test and pressurized aging vessel, respectively. Then, the engineering characteristics of the samples were investigated using X-ray diffraction, scanning electron microscopy, and conventional and Superpave bitumen tests. The results showed that Elvaloy®RET reacted with the main macromolecular groups in the bitumen, and that the modified bitumens behaved as a homogenous single phase structure as a result of this reaction. Conventional tests showed that Elvaloy®RET-modified bitumens were much harder than pure bitumen and had better aging resistance. Furthermore, the penetration classes of these bitumens changed and their temperature sensitivities decreased significantly. Rheological tests showed that the Elvaloy®RET additive increased the resistance of the bitumen against fatigue cracking and particularly permanent deformation. Moreover, the high temperature performance class of the bitumen also increased. However, parallel to the hardening of the bitumen, a reduction in its resistance to cracking at low temperature was observed.
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Fatemi, Saeed, Jafar Bolouri Bazaz, and Seyed Ali Ziaee. "Laboratory Investigation of Using Calcium Lignosulfonate as an Oxidation Inhibitor in Bitumen." Advances in Civil Engineering 2022 (January 31, 2022): 1–17. http://dx.doi.org/10.1155/2022/1488958.

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Asphalt mixtures are the major constituent of road constructions. Those mixtures expose to high-temperature levels during the construction process and their life cycle. The bitumen aging occurred because of the harmful effects of elevated temperatures upon the asphalt mixtures, which leads to oxidation, evaporation, and physical hardening within the bitumen structure. The aging phenomenon can intensify the hardness and brittleness of bitumen, which negatively affects the performance of asphalt mixtures. Researchers have investigated different types of bitumen additives to diminish the negative effects of bitumen aging, among which biomass additives are more attractive for researchers because that additives are organic and mainly emanate from waste materials. The current study investigated the effect of calcium lignosulfonate (CLS) at four quantities (i.e., 5%, 10%, 15%, and 20% by the weight of base bitumen) as an antiaging bitumen additive on physical, workability, thermal susceptibility, rheological, and chemical properties of 60/70 penetration grade bitumen. The results revealed that although the addition of CLS into the bitumen enhanced the rigidity of bitumen against rutting failure at high-temperature conditions, the CLS-modified bitumen was more susceptible to fatigue failure than the virgin bitumen at low-temperature regions. The workability analysis showed that the CLS powder could improve the bitumen’s consistency against permanent deformation at high-temperature levels. Although the bitumen’s viscosity increased because of CLS modification, the CLS-modified bitumen provided acceptable workability based on the Superpave specifications. Outcomes from the rheological test revealed that the addition of CLS into the bitumen improved the rutting resistance of bituminous mixtures at high-temperature levels. The SARA analysis indicated that the hardening of CLS-modified samples emanated from the formation of asphaltenes within the bitumen because of CLS incorporation. Different types of aging indices, including PRP, SPI, VAI, and AIRF, which were calculated in this research, showed that the presence of CLS within the bitumen could retard the bitumen’s aging process.
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Evdokimova, N. G., A. R. Makhmutova, N. T. Aliyeva, and E. A. Guseinova. "PRODUCTION OF THERMOSTABLE ROAD BITUMENS BY THE METHOD OF "OXIDATION-COMPOUNDING"." Azerbaijan Chemical Journal, no. 4 (December 8, 2022): 102–8. http://dx.doi.org/10.32737/0005-2531-2022-4-102-108.

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The paper proposes a technology for producing petroleum road bitumen by compounding deeply oxidized bitumen with tar, pre-oxidized to various temperatures, in order to produce binders stable to the processes of thermo-oxidative aging. The rate of technological and chemical aging of tar and bitumen has been studied. It was found that tar is most susceptible to technological, and bitumen to chemical aging. It is shown that the use of tar pre-oxidation technology is a promising direction in bitumen production in the production of standard grades of bitumen binders. The obtained compounded bitumens have high extensibility values at 250C and maximum tensile force, which characterizes their high cohesive properties, as well as high values of the needle penetration depth at 00C and low brittleness temperatures, which indicate good low-temperature properties of bitumen. It has been revealed that the use of oxidized tar with a softening point of 360C during compounding with deeply oxidized bitumen can achieve the minimum values of softening temperature change after aging and obtain standard bitumen grades BND 70/100 and BND 100/130 according to GOST 33133-2014. The resulting compounded bitumen is less susceptible to destructive and thermo-oxidative aging processes and can be effectively used for paving
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Grynyshyn, О. B., М. І. Donchenko, V. V. Kochubei, and Y. Y. Khlibyshyn. "Main features of the technological process of aging of bitumen obtained from the residues from Ukrainian crude oil processing." Voprosy Khimii i Khimicheskoi Tekhnologii, no. 3 (June 2023): 54–62. http://dx.doi.org/10.32434/0321-4095-2023-148-3-54-62.

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The effects of the technological process of aging of bitumen obtained from the residues from processing of Ukrainian crude oil on the bitumen’s operational characteristics, structural-group composition, and thermal stability have been studied. The aging of bitumen with a thickness of 2 mm has been conducted under laboratory conditions at a temperature of 1630C for 5 and 10 h. Two types of bitumen, oxidized bitumen BND 60/90 and distillation bitumen BD 130/200, have been examined. It has been found that the bitumen quality worsens due to the technological process of aging, e.g. the bitumen hardness and refractoriness increase whereas the elasticity and frost resistance decrease. It has also been shown that, because of the technological process of aging, the content of resins in the bitumen decreases, the content of asphaltenes increases, and the content of oil components does not change significantly. The structural type of the oxidized bitumen changes thereat from a "sol–gel" type to a "gel" type. For the distillation bitumen, the structural type does not change. The derivatographic analysis has revealed that the bitumen thermal stability increases due to the technological process of aging. The reason for this is a decrease in the content of paraffinic ingredients in the bitumen along with the bitumen structure compaction due to the aging.
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Wang, Xiaofeng, Haoyan Guo, Bo Yang, Xingwen Chang, Chenguang Wan, and Zhenjun Wang. "Aging Characteristics of Bitumen from Different Bituminous Pavement Structures in Service." Materials 12, no. 3 (February 10, 2019): 530. http://dx.doi.org/10.3390/ma12030530.

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The aging of bitumen seriously affects the service life of bituminous pavements. At present, there are many related researches on bitumen aging, but most of them focus on aging endured in indoor surroundings and conditions. Therefore, the conclusions obtained cannot reflect the actual aging changes of bitumen in bituminous pavements in service. In order to study the comprehensive aging process and mechanism of bitumen under the influence of service, we studied bridge deck, traffic lane, and ramp with bituminous pavement structures in service. The bitumen samples obtained from the core samples in different bituminous pavement structures were characterized by gel permeation chromatography (GPC), Fourier transform infrared spectroscopy (FTIR), dynamic shear rheometer (DSR), and fluorescence microscope (FM). The aging degree of different bitumen was analyzed, and conclusions were drawn on changes to bitumen aging from different pavement structures. The results showed that the aging degree of bitumen from the upper layer was the most serious, the aging degree of bitumen at the middle layer was weaker than that of bitumen from the upper layer, and the aging degree of bitumen from the bottom layer was the weakest for the different bituminous pavement structures. The aging of bitumen mainly occurred due to oxygen absorption. After aging, viscoelastic components of bitumen changed, and bitumen became harder. The macromolecule of bitumen could be divided into small molecules, and the small molecular weight of bitumen became large. The styrene-butadiene-styrene (SBS) modifier in the modified bitumen became granular after aging, and it appeared as a single phase in bitumen. The aging changes characterized by different analytical methods showed that the aging degree of bitumen from different layers of bituminous pavement structures in service was different. Effective measures should therefore be taken in time to decrease further aging of bitumen from the upper layer of bituminous pavements due to its inevitable early aging in service.
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Filippi, Sara, Miriam Cappello, Manuel Merce, and Giovanni Polacco. "Effect of Nanoadditives on Bitumen Aging Resistance: A Critical Review." Journal of Nanomaterials 2018 (November 27, 2018): 1–17. http://dx.doi.org/10.1155/2018/2469307.

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Starting from the eighties, the use of nanoadditives registered an increasing attention in the scientific and patent literature, especially for the case of polymeric nanocomposites. In the last decade, this involved bituminous materials, modified either with nanosized fillers or with polymeric nanocomposites. One of the expected benefits is an increased resistance of the binder to aging. After a short introduction underlining the uncertainties and risks of artefacts in aging tests, a review is given, focusing on the antiaging properties of layered silicates, which are by far the most important nanoadditives for bitumens. Together with layered silicates, other materials such as nanohydrated lime, nanosilica, and layered double hydroxides are mentioned. Preparation and characterization of the binary bitumen/layered silicate and ternary bitumen/layered silicate/polymer systems are described in order to individuate the aspects that influence the antiaging effect. Even if the available literature is quite abundant and unanimously confirms that nanoadditives may improve bitumen durability, there is a lack of studies clarifying the involved mechanisms. As it is for conventional fillers, it seems to be a combination of physical and chemical interactions. Nanoadditives with different chemistries, porosities, and interlayer spacings differently absorb the polar components from the bitumen, thus affecting their predisposition to oxidative aging.
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Mohamed, Abdullahi Ali, Soon Yee Wong, Lau Teck Leong, Mohd Ahmadullah Farooqi, Ramadhansyah Putra Jaya, Zaid Hazim Al-Saffar, and Haryati Yaacob. "Durability Phenomena of Bitumen and Bituminous Pavement Materials." Open Civil Engineering Journal 15, no. 1 (September 30, 2021): 279–89. http://dx.doi.org/10.2174/1874149502115010279.

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The durability of asphaltic mixtures, in addition to traffic loading, is greatly influenced by the extremes environmental parameters. For instance, at higher temperatures, bitumen becomes soft, thereby reducing the stiffness of asphalt mixtures and making them vulnerable to rutting. On the other hand, at lower temperatures, the stiffness of bitumen is increased, reducing the flexibility of asphaltic concrete and rendering it prone to fatigue failure. Therefore, this evaluation is an extensive research study on the durability of binder and asphalt mixture with their phenomena. Besides that, this paper intends to delve into the various testing methods and measures adopted to evaluate aging and slowing it down. It also presents a critical review of these methods and proposes a future course of action to better address aging issues. According to the evaluation, the behavior of bitumen on the basis of its source varies; when it is mixed with bitumen modifiers, aggregates, and other filler materials, its behavior becomes even more complex. Hence the understanding of the phenomenon of aging is important and the significance cannot be overemphasized. Extensive research work has been done over the last seven decades to evolve the understanding of short- and long-term aging and to improve the durability of asphaltic mixtures. Generally, the aging of bitumen under the influence of both environment and traffic is irreversible as well as inevitable. Apart from entailing hefty maintenance budgets, it remains a challenge to the researchers to slow down aging.
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Celauro, Clara, Edwina Saroufim, Maria Chiara Mistretta, and Francesco Paolo La Mantia. "Influence of Short-Term Aging on Mechanical Properties and Morphology of Polymer-Modified Bitumen with Recycled Plastics from Waste Materials." Polymers 12, no. 9 (August 31, 2020): 1985. http://dx.doi.org/10.3390/polym12091985.

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Polymer-modified bitumen (PMB) is bitumen that has been specifically engineered with polymer for providing enhanced performance in service. The aging of bitumen is a main aspect that is able to affect its final performance: during the production phase in a hot mix plant, all the binders experience short-term aging due to the high processing temperature. The same is true during the production of the modified binder, when the polymer is dispersed at high temperature in the bitumen mass. This paper aims at studying the effect of short-term aging when using different types of modifiers such as recycled polymers obtained from waste materials. A 50/70 penetration-grade bitumen has been modified, and bitumen characterization has been carried out before and after short-term aging; conventional tests, viscosity measurements, and dynamical mechanical analysis have been used to investigate the properties. Different aging indices have been determined for predicting the effect of short-term aging based on the type of modifier. Furthermore, the morphology of the modified bitumen has been investigated via fluorescent microscopy, before and after aging, in order to highlight morphological changes due to aging. The results confirm that aging affects all the modified binders, due to the thermal stress imposed during PMBs production. Nevertheless, polymer modification is proved to reduce the aging effect in terms of an increase in the elastic modulus as experienced by the original binder.
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Dissertations / Theses on the topic "Aging of bitumen materials"

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Twagira, Elias Mathaniya. "Influence of durability properties on performance of bitumen stabilised materials." Thesis, Stellenbosch : University of Stellenbosch, 2010. http://hdl.handle.net/10019.1/3993.

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Thesis (PhD (Civil Engineering))--University of Stellenbosch, 2010.
ENGLISH ABSTRACT: In both developing and developed countries, to ensure sustained economic growth the quest for optimal roads performance is an extremely high priority. A global increase in the use of foamed bitumen and bitumen emulsion materials (BSMs) as a solution to roads maintenance, rehabilitation, and upgrading has become evident. This is driven by environmental policies aimed at conserving energy and limiting the exploitation of new borrows pits. It has therefore become imperative that BSMs are used optimally, and, in order to achieve this, practitioners need to understand the mechanisms that influence durability and long-term performance. The changes in the behaviour of materials and the failure mechanisms of BSM mixes are long-term phenomena. This implies that the study of the physicochemical and mechanical properties of the mixes is vital. Therefore, a fundamental understanding of the moisture damage and age-hardening characteristics, which are related to materials’ properties, is required. The main objective of this study is to advance BSM technology by assessing the influence of the selected materials on durability behaviour and long-term performance in all phases of application (i.e. mix design, construction, and in-service condition). This study begins with a comprehensive literature review of research dealing with the interactions of binder and mineral aggregates. The properties of bitumen (foamed bitumen or bitumen emulsion) and mineral aggregates were reviewed. This was followed by review into the colloidal behaviour of foam and emulsion and physicochemical and mechanical interaction with mineral aggregates. Factors influencing the interaction of BSMs were then identified. Finally, the fundamental theories on thermodynamics, hydrodynamics, and electrokinetics were used to describe the step-by-step process by which adhesive bonding and cohesion occur in BSMs. The mixture durability in terms of moisture damage was investigated. To achieve this aim, the physical and mechanical moisture-induced damage process was analysed. The test control parameters were established and a laboratory device to quantify these parameters designed. New moisture conditioning procedures were developed and demonstrated in this study. From the moisture induction simulation test (MIST) procedure, it became evident that pulsing water pressures into compacted and cured BSM mixes simulates the hydrodynamic effect that occurs in the field due to dynamic traffic loading. The different mix matrices typically applicable to the recycling processes – such as Hornfels-RAP and Quartzite crushed stone, stabilised with either foamed bitumen or bitumen emulsion and the addition of active filler (cement or lime) – were investigated. It was found that a new moisture-conditioning procedure using the MIST device and monotonic triaxial testing can distinguish those BSM mixes that are resistant to moisture damage from those that are less resistant. The validation of the MIST and monotonic test results was done using the APT device, which is the MMLS3 wet trafficking test. The results on both tests showed good correlations in evaluating and screening BSMs in terms of moisture susceptibility. Field temperature data was collected and a model to accurately simulate the curing of BSMs was identified and proposed for further investigation and validation. It was found from the field temperature data collected in this study that the temperature gradient on the study site varied according to the depth of the BSMs (that is, 10oC-17oC during winter and 17oC– 47oC during summer). Understanding the influence of the temperature conductivity and rate of evaporation is important for inferring moisture damage and age-hardening behaviour and proper selection of BSMs. The age-hardening behaviour of BSMs is linked to the durability properties and longterm performance of these materials. The fundamental characteristics associated with shortand long-term age hardening were investigated in this study. The short-term dimension involved assessing the age-hardening characteristics of the binder (foamed bitumen colloids and bitumen emulsion droplets) prior to the production of BSMs. The long-term study involved extracting and recovering the binder from the briquettes (made from different mixes) compacted in the laboratory and cores extracted from different field pavement sections which were in service for 8-10 years. The study found that the length of time bitumen is kept in circulation in the laboratory plant at elevated temperature (170oC–180oC) before making BSM-foam contributes to the ageing of the binder, especially after eight hours. The foaming process in itself was found not to alter the bitumen properties. It is recommended that a temperature range between 160oC- 165oC be used for the production of foamed bitumen with softer bitumen. This will not compromise its quality. In addition, the time of circulation of bitumen in laboratory plant should not be longer than three (3) hours. The rheological properties of the bitumen recovered from laboratory briquettes and cores from field pavement show that age hardening on foamed bitumen and bitumen emulsion during in-service life occurred. The ageing also seemed to be dependent on the effect of traffic, with trafficked areas (i.e. on-wheel path and inner-wheel path) experiencing more ageing than untrafficked areas (i.e. between-wheel path). However, the extraction and recovery process was found to be complex, and produce uncertain results. Although the results show that binders in BSMs undergo age hardening, its distinct behaviour in BSM performance was not obvious from the extensive tests carried out in this study. The last part of the study contains its conclusions and recommendations. The study provides an insight into fundamental material durability properties, and this will assist in improving the current procedure for selection, combining and formulation of the mix matrices for BSMs. In addition, the study provides guidelines that will enable practitioners to confidently apply a mix that is durable and long-lasting. The specific durability-related issues addressed in this study are substance for future research. This novel solution to the application of BSMs will benefit all parties involved in the development of pavement recycling technology.
AFRIKAANSE OPSOMMING: Om volgehoue ekonomiese groei te verseker in beide ontwikkelende en ontwikkelde lande, geniet die soeke na die optimale werkverrigting van paaie ’n baie hoë prioriteit. ‘n Wêreldwye toename in die gebruik van skuimbitumen en bitumen-emulsiemateriale (BSMs) as ’n oplossing vir padonderhoud, rehabilitasie en opgradering is merkbaar. Dit word meegebring deur die omgewingsbeleide wat die ontginning van nuwe leengroewe beperk en besparing van energie bevorder. Die korrekte gebruik van hierdie materiale vereis dat die meganismes wat die duursaamheid en langtermyn-werkverrigting daarvan beïnvloed, deeglik verstaan word. Die verandering in materiaalgedrag en falingsmeganismes van BSM materiale is langtermynverskynsels. Dit impliseer dat bestudering van die fisiochemiese en meganiese eienskappe van die mengsels uiters belangrik is. Dis dus voor die hand liggend hoe belangrik vogbeskadiging en verharding met tyd, wat verwant is aan materiaaleienskappe, is. Die hoofdoelwit met hierdie studie is om die vooruitgang van BSM tegnologie te versnel deur dit moontlik te maak om gekose materiale te evalueer op grond van hulle invloed op duursaamheid en langtermyn-werkverrigting in alle toepassingsfases (naamlik mengontwerp, konstruksie en dienstoestand). Hierdie studie begin met ’n uitgebreide literatuuroorsig oor fundamentele begrippe van die karakterisering van interaksie van die bindstof en die minerale-aggregate. Inligting oor bitumen (skuimbitumen en bitumen emulsies) en eienskappe van minerale aggregate is bestudeer. Dit is gevolg deur ’n studie van die fundamentele begrip van die kolloïdale gedrag van skuim en emulsie, asook fisiochemiese en meganiese interaksie met minerale aggregate. Faktore wat die interaksie van BSM-materiale beïnvloed is geïdentifiseer. Die basiese teorie van termodinamika, hidrodinamika en elektrokinetika is daarna gebruik om stap vir stap die proses en formulering van adhesie-binding en kohesie in die BSMs, wat in hierdie studie aangebied word, te beskryf. Die kwantifisering van mengsel-duursaamheid in terme van vogbeskadiging is ontwikkel. Om hierdie doel te bereik, is die fisiese en meganiese proses van beskadiging deur vogindringing geïdentifiseer. Die gekontroleerde parameters is bepaal en ’n laboratoriumapparaat is ontwerp om hierdie parameters te kwantifiseer. Nuwe vogkondisioneringsprosedures is ontwikkel en in hierdie studie gedemonstreer. Van prosedures van voggeïnduseerde sensitiwiteitstoetsing (Engels: moisture induction simulation test (MIST)) was dit duidelik dat pulsering van waterdruk in BSM materiale die hidrodinamiese effek naboots wat in die veld bestaan as gevolg van dinamiese verkeerslaste. Verskillende mengselmatrikse wat tipies is van hergebruik, soos byvoorbeeld hoornfels-hersikleerde asfalt produk (Engels: recycled asphalt product (RAP)) en vergruisde granietklip, met skuimbitumen of bitumenemulsie gestabiliseer en met byvoeging van aktiewe vulmateriaal (sement of kalksteen), is ondersoek. Daar is bevind dat nuwe vogkondisioneringsprosedures (soos bepaal deur MIST apparaat en drie-assige toets) kan onderskei tussen BSM materiale wat weerstandig is teen vogbeskadiging en dié wat minder weerstandig (vatbaar) is. Die geldigheid van die MIST en monotone toetsresultate is bepaal deur gebruik van die APT apparaat wat ’n MMLS3 nat verkeerstoets is. Die resultate van beide toetse toon goeie korrelasie in die keuring van BM materiale in terme van vogvatbaarheid. In hierdie ondersoek is veldtemperatuurdata versamel en die toepaslike model om verouderende BM lae akkuraat te simuleer is geïdentifiseer en voorgelê vir verdere ondersoek en verifikasie. Daar is uit veldtemperatuurdata bevind dat temperatuurgradiënt op die betrokke terrein gewissel het met die dikte van die BSM, naamlik 10oC-17oC gedurende die winter en 17oC-47oC gedurende die somer. Begrip vir die invloed van temperatuuroordragkoëffisiënt en verdampingstempo is belangrik by die afleiding van vogbeskadiging en verharding met ouderdom en die korrekte keuse van BSM materiale.Verouderingsverhardinggedrag van BSMs is verwant aan die duursaamheidseienskappe en langtermynwerkverrigting van hierdie materiale. Die basiese karakteristieke wat met kort- en langtermyn verouderingsverharding geassosieer word, is in hierdie studie ondersoek. Die klem op die kort termyn is geplaas op die verouderingsverhardingsgedrag van die bindstof (skuimbitumen kolloïdes en bitumen-emulsiedruppels) voordat BSMs vervaardig word. In die lang termyn evaluasie het die studie ekstraksie en herwinning van bindstof uit brikette wat in die laboratorium gekompakteer is (van verskillende mengsels) en uit kerns verkry vanaf verskeie plaveiselgedeeltes na 8-10 jaar diens ingesluit. Die ondersoek het bevind dat die tydsverloop waarin bitumen in sirkulasie gehou is by verhoogde temperatuur (170oC-180oC) in die laboratorium-aanleg voordat BSMs vervaardig is, veral indien na 8 uur, bydra tot die veroudering van die bindstof. Die skuimproses op sigself verander nie die bitumeneienskappe nie. Daar word aanbeveel dat temperature tussen die grense 160oC-165oC gehandhaaf word vir produksie van skuimbitumen met sagter bitumen sonder dat die kwaliteit benadeel word en dat die sirkulasietyd nie 2 tot 3 ure behoort te oorskry nie. Die reologiese eienskappe van die herwinde bitumen vanuit laboratoriumbrikette en kerns van plaveisels toon dat ouderdomsverharding van skuimbitumen en bitumen-emulsie tydens die diensleeftyd plaasvind. Die veroudering is skynbaar ook afhanklik van verkeerseffekte, met belaste areas (in wielspoor of binne wielspoor) wat ’n hoër mate van veroudering toon as onbelaste areas (tussen wielspore). Die ekstraksie- en herwinningsproses op sigself was egter bevind as baie kompleks met uiters onseker resultate. Dit het gelei tot onsekere gedrag in terme van ouderdomsverharding van die BSM bindmiddel (skuim of emulsie). Alhoewel resultate toon dat die bindmiddels ouderdomsverharding ondergaan het, is die BSM werkverrigting nie duidelik uit die uitgebreide toetse wat in hierdie studie uitgevoer is nie. Die laaste deel van die studie bevat gevolgtrekkings en aanbevelings. Die studie lewer insig in die fundamentele duursaamheidseienskappe van die materiaal, wat bydra tot verbetering van die huidige prosedure van seleksie, saamstelling en formulering van die mengmatriks vir BSMs. Verder voorsien dit ’n metode wat in die praktyk gebruik kan word om met vertroue duursame mengsels met lang diensbaarheidsleeftye te vervaardig. ’n Nuwe oplossing en vooruitgang in die toepassing van BSMs is daargestel tot voordeel van alle partye betrokke by die ontwikkeling van herwinningstegnologie.
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Mikhailenko, Peter. "Valorization of by-products and products from agro-industry for the development of release and rejuvenating agents for bituminous materials." Thesis, Toulouse 3, 2015. http://www.theses.fr/2015TOU30094/document.

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La croissance de caution vis-à-vis l'utilisation des produits pétroliers dans la construction a nécessité le besoin de développement des alternatives. Le BTP, en particulaire pour le secteur routière, a un certain nombre des piste ou les produits pétrolières ont utilisés, par exemple le liant pour les enrobés comme les agents régénérant (pour recyclage des enrobés), mais aussi le produits qui sont utilisés sur le chantier comme les anti-adhérents (ARA) et les débituminants (BR). Alors, il y a une besoin de remplacer les produits d'origines pétrolières par les alternatives bio-sourcés. Ce présent ouvre est une partie d'un projet qui va développer une nouvelle filière dédiée à la production de nouvelles formulations pour le BTP à partir de la transformation des huiles végétales et des graisses animales. Ce thèse concerne les produits développés seront destinés au l'asphalte, et alors, deux types d'applications sont particulièrement visés : (i) des agents anti-adhérents et (ii) des agents régénérants. Un débituminant sera développé aussi. Les produits anti-adhérents ont pour fonction d'empêcher le bitume d'adhérer aux engins de travaux sans effet secondaire, théoriquement, sur la matrice liante.. L'objet du travail est de caractériser l'efficacité et l'innocuité des agents anti-adhérents développés dans le cadre du projet et de développer les méthodes expérimentales visant à les évaluer. Trois essais principaux ont été développés pour caractériser la performance et innocuité des anti-adhérents vis-à-vis des essais qui ont optimisé leur implémentation et paramètres. La performance des anti-adhérents a été caractérisé par l'essai de glissance des enrobés. L'innocuité des anti-adhérents ont été caractérisés par des essais de fendage sur les enrobés et par l'essai de la dégradation de bitume. L'essai de la dégradation de bitume a servi aussi comme une mesure de la performance de débituminant. Les essais sur les anti-adhérents commerciaux d'Etats-Unis et la France a trouvé que ils ont deux modes de fonctionnement : i) lixiviation du bitume et ii) en formation d'une interface entre le les enrobés et la surface métallique. Même comme les deux modes ont été trouvé dans des certains anti-adhérents, le mode interface ont été trouvé préférable, grâce à l'option de garder les mêmes applications du produit pour plusieurs cycles de usage. Ensuite, un produit - basé sur glycérol sourcé de l'agro-industrie - a été développé. Les débituminants commerciaux ont été essayé, aves les conclusions : i) les débituminants plus effectifs ont eu les plus grande % des esters et ii) que les esters chaines courtes (C7-10) d'hautes concentrations ont été trouvé les plus efficace. L'agent régénérant est destiné à régénérer le bitume vieilli issu des agrégats d'enrobés (RAP) en lui redonnant ses propriétés originelles et en assurant leur maintien dans le temps. Le travail sur les agents régénérants se compose de la caractérisation physico-chimique du vieillissement du bitume et du bitume vieilli avec l'agent. Plus précisément, le travail se serve des techniques de spectrométrie IRTF (avec imagerie) et thermogravimétrie. Dans ce contexte, une produit bio-sourcé a été évalué comme une régénérant. Pour la spectroscopie FTIR, une moyenne de polir le mastique a été développé pour rassuré la platitude des échantillons. La régénération du bitume a été observé avec la spectrométrie ITRF, donc quelques peaks (notamment les indices IC=O and IS=O) pendant 0-42 jours de vieillissement dans l'étuve (loin-durée). Il a été trouvé qu'une période de vieillissement de 14 jours à l'étuve était à peu près équivalente au bitume vieilli par un cycle de RTFOT + PAV en termes de rhéologie et de la pénétration. Le mastic (vieilli 14 jours) a ensuite été mélangé avec un agent de bio-source (à 7,5% en poids de mastic). Il a été constaté par imagerie FTIR que l'indicateur de l'oxydation IS=O a été réduit par l'incorporation de l'agent régénérant dans le bitume
The growing health and environmental concerns brought on by the use of petroleum based products in the asphalt construction industry have necessitated the development of alternatives. Infrastructure, especially that involving transportation has many uses for petroleum products including, as fuel, as well as in asphalt pavement construction - where petroleum products have traditionally constituted the binder for the mix as well as the rejuvenating agents (for asphalt recycling) - along with various agents used in the construction process including bitumen removers and asphalt release agents. Thus, there is a need to replace petroleum base agents with bio-sourced and biodegradable substitutes. The present work is part of a project to develop bio-sourced (recycled from agricultural waste) products for the construction industry. This work is dedicated to developing products relating to the asphalt industry. Two types of product applications were envisioned: i) an asphalt release agent (ARA) and ii) an asphalt rejuvenating agent. Additionally, a bitumen remover (BR) developed as part of the work on the ARA. ARAs prevent asphalt from adhering to tools and equipment used in asphalt production, without producing overly negative side effects with regards to the pavement. Three principal tests methods were developed and optimized for the performance and damage to asphalt of the ARAs. The asphalt slide test was developed to quantify the performance of the ARA by sliding hot asphalt mix down a plate with the ARA applied. The testing of the damage to asphalt from ARAs consisted of testing an asphalt cylinder - in contact with an ARA for seven days - in indirect-tensile strength (ITS). The bitumen degradation test consisted of submerging a bitumen sample in an agent over a certain time and weighing the bitumen that did not dissolve in the agent. This was followed by the observation of the bitumen-ARA chemical interaction by FTIR spectrometry. This test served as an assessment of ARA damage to bitumen as well as of the performance of BRs. The testing of the commercial ARAs from both the French and USA markets found that they had two primary modes of functioning: i) by softening the bitumen and ii) by forming an interface between the asphalt and the metal surface. While some agents had elements of both, it was found that interface agents are preferable, due to the ability to use a single ARA application for multiple occasions. With this completed, a water-based bio-sourced substrate ARA - based on glycerol derived from agricultural waste - was developed. The commercially available BRs were tested as well, finding that i) the most effective BRs had the highest ester concentration and ii) that highly concentrated short chained ester (C7-10) were very effective bitumen dissolvers. The goal of rejuvenating agents is to regenerate the old bitumen from recycled asphalt pavement (RAP) by restoring the original properties and ensuring the stability of these properties over time. This part consisted of the development of methods for bitumen and aging, as well as characterization of the chemical rejuvenation of bitumen by FTIR spectrometry (including imaging) and thermogravimetric analysis. A bio-sourced rejuvenating agent was evaluated as well. For the imaging, a mastic polishing method was developed in order to attain as samples as flat as possible for the analysis. The bitumen rejuvenation was observed using FTIR spectroscopy analysis. Several peaks (notably IC=O and IS=O) were observed for bitumen oven aged up to 42 days (long term). It was found that an oven aging period of 14 days was roughly equivalent to bitumen aged by a RTFOT+PAV cycle it terms of rheology and penetration. The mastic (aged for 14 days) was then combined with a bio-sourced agent (at 7.5%w of mastic). It was found by FTIR imaging that the oxidation indicator IS=O, was reduced by the incorporation of the rejuvenating agent
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3

Edwards, Ylva. "Influence of waxes on bitumen and asphalt concrete mixture performance." Doctoral thesis, KTH, Väg- och banteknik, 2005. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-553.

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This doctoral thesis consists of a literature review, presented in two papers, and another six papers describing experimental studies of the influence of different kinds of wax and polyphosporic acid on bitumen and asphalt concrete mixture properties. The literature review should give an extensive description of the field of knowledge concerning wax in bitumen. Effects of wax in crude oil, bitumen and asphalt concrete as well as test methods for studying these effects are described. Theories behind possible mechanisms are also discussed, and commercial wax as additive to bitumen for different purposes included. The experimental parts comprise laboratory studies involving totally five 160/220 penetration base bitumens from different sources, two isolated bitumen waxes, five commercial waxes and one polyphosphoric acid. Asphalt concrete slabs, containing base or modified bitumen were prepared and tested. Binder properties were evaluated using different types of laboratory equipment, such as dynamic shear rheometer (DSR), bending beam rheometer (BBR), differential scanning calorimeter (DSC), force ductilometer, as well as equipment for determining conventional parameters like penetration, softening point, viscosity, and Fraass breaking point. Fourier Transform Infrared (FTIR) spectroscopy and Thin Layer Chromatography (TLC-FID) were used for chemical characterization. The binders were aged by means of the rolling thin film oven test (RTFOT) and pressure ageing vessel (PAV) in combination. Asphalt concrete properties were evaluated at low temperatures using the tensile strain restrained specimen test (TSRST) and creep test at -25°C. Dynamic creep testing was performed at 40°C, as well as complex modulus tests between 0 and 20°C. Binder test results indicated that the magnitude and type of effect on bitumen rheology depend on the bitumen itself, type of crystallizing fraction in the bitumen and/or type and amount of additive used. Bitumen composition was found to be of decisive importance. Adding polyethylene wax or polyphosphoric acid, especially to a non-waxy 160/220 penetration grade bitumen, showed no or positive effects on the rheological behaviour at low temperatures (decrease in stiffness) as well as medium and high temperatures (increase in complex modulus and decrease in phase angle). However, the corresponding positive effects could not be shown in dynamic creep testing (at 40°C) of asphalt concrete mixtures containing these modified binders. Adding FT-paraffin decreased the physical hardening index for all bitumens. Also polyethylene wax and montan wax showed this effect for some bitumens. Slack wax showed a large increasing effect on physical hardening, and polyphosphoric acid none or a minor negative effect. No correlation between physical hardening index (PHI) and wax content by DSC was found in this study, involving both natural bitumen wax and commercial wax. Addition of the commercial waxes used showed no or marginally positive influence on bitumen ageing properties for the bitumens and test conditions used. Comparing asphalt mixture test results to the corresponding binder test results, the effects on asphalt mixtures from adding commercial wax or polyphosphoric acid were less evident. Significant binder physical hardening by BBR could not be confirmed by TSRST.
QC 20101006
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4

Hammoud, Oussama. "Étude de l’agressivité des pneumatiques sur les couches de roulement des structures routières." Electronic Thesis or Diss., Strasbourg, 2023. http://www.theses.fr/2023STRAD055.

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Le projet ANR BINARY vise à améliorer la compréhension et l'évaluation des mécanismes de détérioration des couches de roulement de chaussées sous trafic. Ce projet se concentre sur : i) l'arrachement des granulats d’enrobé bitumineux ; ii) la fissuration descendante ; iii) essayer de comprendre les contraintes et déformations impliquées ; iv) étudier l'influence des interfaces entre les couches d'enrobé ; et v) améliorer la prédiction de leur durée de vie.Avec le vieillissement du réseau routier, il est crucial d'avoir une meilleure connaissance des mécanismes de dégradation des couches de roulement. Les normes actuelles pour le dimensionnement des structures de chaussée couvrent l'adhérence, la texture et l'uniformité, mais ne définissent pas des critères mécaniques pour garantir la durabilité des couches subissant les charges du trafic.Cette thèse cherche à approfondir notre connaissance des matériaux bitumineux, notamment les couches de surface. Elle vise aussi à comprendre comment les conditions de charge, la température et la vitesse affectent ces matériaux, neufs et vieillis. Des tests expérimentaux ont été effectués et une modélisation combine les approches des éléments finis (FEM) et des éléments discrets (DEM) pour reproduire ces essais de laboratoire. Enfin, l'interaction pneu-chaussée fait l'objet d'une étude avec une nouvelle approche numérique pour offrir une simulation en conditions plus réalistes
The ANR BINARY project aims to enhance the understanding and assessment of the mechanisms causing deterioration in road pavement layers under traffic. This project focuses on i) the stripping of bituminous mix aggregates; ii) downward cracking; iii) attempting to comprehend the involved stresses and deformations; iv) studying the influence of interfaces between asphalt layers; and v) improving the prediction of their service life.With the aging of the road network, it is crucial to have a better understanding of the degradation mechanisms of pavement layers. Current standards for designing road structures cover adhesion, texture, and uniformity but do not define mechanical criteria to ensure the durability of layers subjected to traffic loads.This thesis seeks to deepen our knowledge of bituminous materials, especially surface layers. It also aims to understand how loading conditions, temperature, and speed affect these materials, both when new and aged. Experimental tests have been conducted, and a modeling approach combines finite element (FEM) and discrete element (DEM) methods to replicate these laboratory tests. Finally, tire-road interaction is studied with a novel numerical approach to provide a simulation under more realistic conditions
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5

Moloto, Percy Kgothatso. "Laboratory accelerated curing protocol for bitumen stabilized materials." Thesis, Stellenbosch : University of Stellenbosch, 2010. http://hdl.handle.net/10019.1/4187.

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Thesis (MScEng (Civil Engineering))--University of Stellenbosch, 2010.
ENGLISH ABSTRACT: The research conducted in this study forms part of the Phase II process of the Bitumen Stabilized Materials (BSMs) Guideline improvement initiative. The initiative aims to address areas of concern in the cold mix design procedures for BSMs. Current road rehabilitation using the bitumen stabilization process requires testing of representative specimens as means to evaluate pavement performance over time. In order to adequately acquire specimens representative of field conditions, it is necessary to condition the materials in a process called curing. Although curing procedures have been standard in many countries on different continents, the protocols are varied and an acceptable procedure is currently not available. In order to develop an acceptable curing protocol for BSMs, both field and laboratory environments were investigated. Considering that curing takes time in the field, production of representative samples intended for laboratory testing must undergo accelerated curing in the laboratory. Given the complexities involved in achieving close correlations between field and laboratory environments, the research strived to reconcile field and laboratory material behaviour. In particular, the main objective of the research was to unify the curing protocol for BSMs, with the standardization of the curing protocol being top priority. In this study, laboratory results have confirmed that the different natures of curing mechanisms inherent in a BSM-foam and BSM-emulsion contribute to irreconcilable material behaviour(s). Results have confirmed that curing of BSM-foam is largely a function of water repulsion, with the addition of active filler dominating material performance almost immediately. Unlike BSM-foam, curing of BSM-emulsion is both a function of the breaking of emulsion during the initial phase and the gradual release of moisture with time. In this instance, BSM-emulsion material performance resembled active filler influences past the breaking of the emulsion cycle. Consequently, given the observed differences regarding material behaviour(s), the unification of the curing protocol for BSMs has not been successful. In terms of accommodation of active filler in the final curing protocol for BSMs, findings in this research have revealed that active filler’s tendency to absorb moisture in the initial stages requires longer curing time to help extract the absorbed moisture during the curing process. Although the use of active filler has an impact on curing, its inclusion in a BSM does not justify its extension in the curing time as cementation is not one of the desired properties of these materials. BSMs are primarily desirable for their flexibility in pavement structures. For this reason, active filler was omitted in the final curing protocol due to reasons of simplifying the mix design process. In conclusion, different curing protocols were tested and developed to help produce reconcilable material behaviour in both the field and laboratory environments. Through the reconciliation of key material properties such as the resilient modulus, long term equilibrium moisture conditions and shear parameters, an acceptable standardized curing protocol for BSM-foam and BSMemulsion intended for application in industrial laboratories across South Africa was successfully developed.
AFRIKAANSE OPSOMMING: Die navorsing tydens hierdie studie gedoen, vorm deel van die Tweede fase van die Bitumen Gestabiliseerde Materiale Riglyne verbeteringsinisiatief. Die inisiatief het ten doel om areas van bekommernis in die kouemengsel-ontwerp-prosedures vir Bitumen Gestabiliseerde Materiale aan te spreek. Huidige padrehabilitasie wat gebruik maak van die Bitumen Gestabiliseerde Materiale proses, vereis toetsing van verteenwoordigende monsters om sodoende plaveiselgedrag oor ‘n tydperk te evalueer. Materiale moet deur die verouderingsproses gekondisioneer word, om sodoende monsters te verkry wat akkuraat verteenwoordigend van veldtoestande is. Alhoewel verouderingsprosesse in meeste lande - op verskillende kontinente - gestandariseerd is, is die protokol verskillend en ‘n aanvaarbare prosedure is nie tans beskikbaar nie. Beide veld- en laboratoriumomgewings is ondersoek, om sodoende ‘n aanvaarbare verouderings-protokol vir Bitumen Gestabiliseerde Materiale te ontwikkel. Wanneer in ag geneem word dat veroudering in die veld tydrowend is, moet vervaardiging van verteenwoordigende monsters vir laboratoriumgebruik versnelde veroudering in die laboratoruim ondergaan. Gegee die kompleksiteite betrokke om goeie korrelasie tussen velden laboratoriumomgewings te verkry, het die navorsing daarna gestreef om die veld- en laboratoriummateriaalgedrag te verenig. Die hoofdoel van die navorsing was om die verouderingsprotokol vir Bitumen Gestabiliseerde Materiale te verenig met die stardaardisering van die verouderingsprotokol as top prioriteit. In hierdie studie het laboratorium resultate bevestig dat die verskillende aard van voorbereidings- meganismes inherent in BSM-skuim en BSM-emulsie bydra tot onversoenbare materiaalgedrag. Resultate het bevestig dat voorbereiding van BSM-skuim ’n funksie van waterrepulsie het en met die byvoeging van aktiewe vullers dominieer dit die materiaalgedrag byna onmiddelik. Anders as BSM-skuim is die voorbereiding van BSM-emulsie beide ’n funksie vir die breek van emulsie tydens die begin fase en die geleidelike vrystelling van vog oor tyd. In hierdie geval het BSM-emulsie se materiaalgedrag die invloed van aktiewe vuller getoon nadat die emulsie gebreek het. Gevolglik, weens die waargenome verskille rakende materiaalgedrag is die vereniging van die voorbereidings- protokols vir BSMs nie suksesvol nie. In terme van inagneming van aktiewe vullers in die finale voorbereidingsprotokol vir BSM’s, is deur navorsing bevind dat aktiewe vullers neig se neiging om vog te absorbeer in die beginstadia dit benodig dus ‘n langer verouderingstyd vir die ontrekking van die geabsorbeerde vog. Hoewel die gebruik van aktiewe vullers ’n impak het op die voorbereiding, reverdig dit nie die verlenging van die verouderingstyd vir die insluiting daarvan in BSM nie, siende dat sementering nie een van die gewenste eienskappe van hierdie materiaal is nie. BSMs word hoofsaaklik verkies vir sy buigsaamheid in paveiselsturkture. Om die mengselontwerp prosesse te vereenvoudig, was aktiewe vullers dus weggelaat in die finale voorbereidingsprotokol. Ter afsluiting was verskeie voorbereidings protokolle getoets en ontwikkel om te help met die vervaardiging van versoenbare materaalgedrag in beide veld-en-laboratoriumomgewings. Deur die versoening van kern materiaal eienskappe soos die elastisiteitsmodulus, lang termynewewigvog kondisies en skuifparameters, is ’n aanvaarbare gestandariseerde voorbereidingsprotokol vir BSM-skuim en BSM-emulsie bedoel vir aanwending in industriele laboratoriums regoor Suid Afrika suksesvol ontwikkel.
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6

Nwando, Tiyon Achille. "Flexibility and performance properties of bitumen stabilised materials." Thesis, Stellenbosch : Stellenbosch University, 2014. http://hdl.handle.net/10019.1/86594.

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Thesis (MScEng)--Stellenbosch University, 2014.
ENGLISH ABSTRACT: This research investigates the flexibility and the performance properties of bitumen stabilised materials under the influence of mix variables. The laboratory testing consisted of two main phases. During the first phase (mix design), the strength and the flexibility of the mixes were assessed through ITS (Indirect Tensile Strength), UCS (Unconfined Compressive Strength), displacement at break, strain at break and fracture energy. The second phase consisted of a series of triaxial tests done to assess the performance properties (shear strength: cohesion and angle of internal friction; and stiffness: resilient modulus) of the mixes. The mineral aggregates used in this study were milled from different locations of the R35, near Bethal. This was a blend of granular material (dolerite, from various locations of the existing base and subbase layer of the R35) and Reclaimed Asphalt (RA) milled from the existing surfacing. During the mix design phase, two types of bituminous binders were used (bitumen emulsion and foamed bitumen) at bitumen content ranges of 2%, 2.4% and 2.8% each. Two types of active filler were used separately and in combination at a proportion of 1% and 2%. Finally, specimens were tested in wet and dry conditions for each mix combination. During the triaxial testing phase, only the optimum bitumen content of 2.4% was used, both for bitumen emulsion and foamed bitumen, with only cement as active filler in a proportion 1% and 2%. The specimens were tested at different ranges of densities and saturation levels. The flexibility of the mix was assessed through the fracture energy, the strain and the displacement at break parameters. An analysis of variance (ANOVA) was conducted on the data to assess the significance of experimental variables on this property. This property was found to be very sensitive to bitumen and cement content added to the mix. When assessing the combined effect and the significance of the variables on the flexibility of the mixes, it was found that fracture energy is mostly influenced by the cement content, followed by the bitumen content, then the type of treatment and finally the testing condition. However, the level of significance was not in the same order for the other two parameters (displacement and strain at break). It was also found that the combined effect of some independent variables (cement content + testing condition, type of treatment + cement content + bitumen content) had a significant effect on the fracture energy and the strain at break respectively. From the ITS and UCS tests, an increase in strength was noticed with the increase of cement content. On the other hand, the increase in bitumen content led to a decrease in strength of the material. The statistical analysis on the ITS and UCS values show that the independent variable with the most significant effect on the ITS is the cement content, followed by the testing conditions, then the bitumen content and finally the type of treatment. The combined effect of cement content + bitumen content was found to be significant both for ITS and UCS. In the second phase triaxial tests were performed in order to evaluate the performance properties of the mixes. It was found that the increase of the active filler content significantly improves the shear strength of the material. It was also found that at a fixed cement content, specimens tested at low density and/or high level of saturation show low shear strength. The Mr-θ model was used to model the resilient modulus of the mixes and the model coefficients used to evaluate the effect of experimental variables on the resilient modulus. It was found that the resilient modulus of the mixes increases as the bulk stress increases. This confirms the stress dependent behaviour of bitumen stabilised materials. The analysis show that increasing the percentage of active fillers content results in a significant increase in the resilient modulus values. An increase in relative density also resulted in an increase in the resilient modulus of the mixes, while the opposite effect was observed with the increased of the saturation level. Besides the engineering properties and the mechanical test parameters, other parameters such as the Tensile Strength Ratio (TSR) was calculated in order to evaluate the moisture sensitivity of the mixes. Weakening due to moisture was found to be more predominant in the mixes with less active filler. In addition, bitumen emulsion mixes were found to have a better resistance to moisture weakening effects compared to foamed bitumen. In addition, a comparison between the rapid curing and the accelerated curing was done. Higher ITS and UCS results were obtained for specimens cured using long term curing compared to specimens cured using the accelerated curing method. In conclusion, flexibility is an important property of bitumen road construction material (bitumen stabilised material include) however, it is not an easy property to measure. Although, displacement/strain at break and fracture energy from ITS and UCS were able to give us some indications on the main factors governing the flexibility of bitumen stabilised materials (the bitumen and active filler content), more accurate and adequate tests are required to evaluate the parameter.
AFRIKAANSE OPSOMMING: Die buigsaamheid en gedragseienskappe van bitumen gestabiliseerde materiale was getoets om sodoende die invloed van verskeie mengselveranderlikes te evalueer. Die ondersoek het uit twee fases bestaan. Tydens die eerste fase (mengfase) is die sterkte en buigsaamheid deur middel van indirekte treksterkte toetse (ITS), onbegrensde druksterkte toetse (UCS), verplasing – en vervorming by breekpunt sowel as breek-energie toetse gedoen en ondersoek. Die tweede fase het bestaan uit ʼn reeks drie-assige triaksiaal toetse. Triaksiaaltoetse is uitgevoer om die gedragseienskappe soos die skuifsterkte, kohesie, hoek van interne wrywing, styfheid en weerstand modulus te ondersoek. Die gemaalde mineraal-aggregaat wat in hierdie ondersoek gebruik is, was verkry op verskeie areas van die R35, geleë naby Bethal. Die materiaal is ʼn mengsel van granulêre materiaal (van die bestaande kroonlaag en stutlaag van die pad) en herwonne asfalt (RA). Tydens die mengontwerp fase is twee tipes bitumen gebruik naamlik bitumenemulsie en skuimbitumen in hoeveelhede van 2%, 2.4% en 2.8%. Twee tipes aktiewe vulstof (hoeveelhede van onderskeidelik 1% en 2%) was saam met elk van die verskeie bitumen-hoeveelhede gebruik. Proefstukke van elk van hierdie mengsel kombinasies is onder beide nat en droë kondisies getoets. Tydens die tweede fase, is slegs die optimum binder inhoud (2.4%) gebruik vir beide emulsie- en skuimbitumen, gekombineer met 1% en 2% aktiewe vulstof. Proefstukke was getoets by ʼn reeks van verskillende digthede en versadigingvlakke. Die buigsaamheid was ondersoek deur middel van breek-energie, vervorming en die verplasing by breekpunt. ʼn Analise van variasie (ANOVA) is uitgevoer op die toetsdata om sodoende die te evalueer of die veranderlikes beduidend is ten opsigte van buigsaamheid. Daar is gevind dat die buigsaamheideienskap sensitief is vir beide bitumen en sement inhoud. Met assessering van die gekombineerde effek en betekenis van die veranderlikes op die buigsaamheid van die mengsels, is daar gevind dat die hoogste beduidende veranderlike t.o.v breek-energie die sement inhoud is, gevolg deur die bitumeninhoud, tipe behandeling en laastens die toetskondisie. Die orde van belangrikheid verskil vir die ander twee parameters (verplasing en vervorming by breekpunt). Daar is ook gevind dat die gekombineerde effek van sommige veranderlikes (sement inhoud en toets kondisie, tipe behandeling en sement inhoud tesame met bitumen inhoud) ook beduidend was t.o.v breek-energie en vervorming by breekpunt. Vanuit die ITS en UCS toetse was daar ʼn toename in sterkte waargeneem soos die sementinhoud toeneem. Aan die anderkant, het ʼn toename in bitumeninhoud ‘n afname in sterkte veroorsaak. Die statistiese analise van ITS en UCS resultate, toon dat die grootste beduidende onafhanklike t.o.v ITS waardes ook die sement inhoud was, gevolg deur toets kondisies die grootste effek, bitumen inhoud en die tipe behandeling. Die gekombineerde effek van sementinhoud en bitumeninhoud, was betekenisvol vir beide ITS en UCS. Drie-assige triaksiaaltoetse was uitgevoer om die gedragseienskappe van die mengsels te evalueer. Daar is gevind dat die toename in sement inhoud, die skuif sterkte van die materiaal grootliks verbeter. By ʼn konstante sementinhoud, wys toetsresultate van proefstukke wat getoets is by lae digthede en hoë vlakke van versadiging, lae skuif sterkte. Die Mr – θ model was gebruik om die veerkragsmodulus van die mengsels te moduleer en die modelkoëffisiënte is gebruik om die effek van eksperimentele veranderlikes op die weerstand modulus te evalueer. Met toename in die omhullende spanning is ‘n toename in die veerkragsmodulus waargeneem, wat bevestig dat die gedrag van bitumen gestabiliseerde materiale spannings afhanklik is. ʼn Toename in die sement en relatiewe digtheid het ʼn merkwaardige toename in die veerkragsmodulus tot gevolg gehad, terwyl die teenoorgestelde waargeneem is met toename in versadigingsvlakke. Buiten die ingenieurseienskap en meganiese toetsfaktore, is ander faktore (soos die trekspanning verhouding) bereken om die vogsensitiwiteit van die mengsels te evalueer. Mengsels met laer sement inhoud het groter verswakking ervaar met blootstelling aan water. Bitumenemulsie proefstukke toon beter weerstand teen water as skuimbitumen. Vergelyking tussen versnelde en korttermyn nabehandelingsprosedure van proefstukke, toon hoër ITS en UCS waardes vir die versnelde nabehandelingsprosedure prosedure. Buigsaamheid is ‘n belangrike eienskap van bitumen in padkonstruksie materiale (insluitend bitumen gestabiliseerde materiale), maar word moeilik gemeet. Alhoewel verplasing/vervorming by breekpunt en breek energie, bepaal vanaf ITS en UCS, ‘n indikasie toon van die hooffaktore (binder en sement) wat buigsaamheid van bitumen gestabiliseerde materiaal beïnvloed, word meer akkurate toetse benodig om die eienskap te ondersoek.
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Campher, Lizemari. "Shrinkage and flexibilty behaviour of Bitumen Stabilised Materials." Thesis, Stellenbosch : Stellenbosch University, 2015. http://hdl.handle.net/10019.1/96991.

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Thesis (MSc)--Stellenbosch University, 2015.
ENGLISH ABSTRACT: The increasing awareness of climate change causes a growing interest in pavement rehabilitation. Pavement rehabilitation by in-situ stabilisation with bitumen reduces the extraction of natural aggregate resources while enhancing flexibility and durability properties, which lowers maintenance costs over the design-life of the pavement structure. Incorporating Bitumen Stabilised Materials (BSMs) into a pavement structure can therefore have economic and environmental benefits, but more research is needed to fully understand the behaviour and potential of these materials. Stabilising materials with bitumen provides useful properties to pavement layers. The “TG2 2nd Edition, Bitumen Stabilised Materials” was published by the Academy of South Africa in May 2009, which provides a good understanding of the usage of Bitumen Stabilised Materials (BSMs). However, the shrinkage and flexible behaviour of these materials are still not fully understood and therefore more research on these materials is needed. The aim of this project is thus to determine the shrinkage and flexible behaviour of BSMs to incorporate these behavioural types in the revised design method for flexible pavements in the SAPDM. In addition, the influence of several additives on the shrinkage and flexible behaviour of BSMs have been evaluated to get an improved understanding of these properties. The additives included cement (1% and 2% content) and both bitumen emulsion (0.9% and 2.4% content) and foamed bitumen (only 2.4% content). Two linear shrinkage testing methods have been designed to test the shrinkage potential of BSMs, including a beam testing method and a cylindrical testing method. Based on the usage of the shrinkage measurements the applicable method can be used to determine the shrinkage potential of a BSM. The flexibility is a more complex property and was tested using a simple monotonic beam test. The strain-at-break parameter obtained from this test provided an indication of the material flexibility. Slight differences in the trends were observed between beam and cylindrical shrinkage due to specimen geometry, exposed surface area and shrinkage testing direction. Beam specimens initially show swelling when bitumen is added to the mixture and shrinks thereafter. Cylindrical specimens on the other hand show initial shrinkage followed by a slight length increase, where after shrinkage continues. The additives had the same influence on the shrinkage for both the beam and cylindrical specimens. Although all shrinkage measurements were small, an increase in bitumen reduced shrinkage and an increase in cement increased shrinkage. Stabilisation with foamed bitumen rather than bitumen emulsion proved to show less shrinkage, but only in combination with 2% cement. The strain-at-break, dissipated energy and material stiffness calculated from the monotonic beam tests provided a good indication of the flexibility behaviour of BSMs. Higher bitumen content increased the flexibility potential and an increase in cement decreased the flexibility potential of BSMs. This project has provided good insight on both the shrinkage and flexibility behaviour of BSMs, which can be used in the revised copy of the SAPDM. Increased bitumen contents decreases the shrinkage potential and increases the flexibility of a BSM. Increased cement contents on the other hand, increases shrinkage and decreases flexibility of BSMs. The correct combination of cement and bitumen in a BSM can thus provide a material with the wanted flexibility while keeping the shrinkage to a minimum.
AFRIKAANSE OPSOMMING: Die toenemende bewustheid van klimaatsverandering veroorsaak toenemende belangstelling in die rehabilitasie van plaveisels. Plaveisel rehabilitasie deur in-veld stabilisasie met bitumen verminder die ontginning van natuurlike hulpbronne, terwyl die verbetering van buigsaamheid en duursaamheid eienskappe die onderhoudskoste verlaag oor die ontwerp-lewe van die plaveiselstruktuur. Die inkorporasie van Bitumen Gestabiliseerde Materiale (BGM) in 'n plaveisel struktuur kan dus omgewings en ekonomiese voordele inhou. Meer navorsing word wel benodig om die gedrag van hierdie materiale beter te verstaan. Die stabilisering van materiale met bitumen verskaf nuttige eienskappe aan 'n plaveisellaag. Die "TG2 2de Uitgawe, Bitumen Gestabiliseerde Materiale" is gepubliseer deur die Akademie van Suid-Afrika in Mei 2009 en verskaf 'n goeie begrip van Bitumen Gestabiliseerde Materiale (BGM). Die krimpings en buigsaamheid gedrag van die materiaal word wel nog nie ten volle verstaan nie en daarom word meer navorsing oor hierdie materiaal benodig. Die doel van hierdie projek is dus om die krimpings gedrag sowel as die buigsaamheid gedrag van 'n BGM te bepaal en sodoende die kennis te gebruik in die hersiende ontwerp metode vir buigsame plaveisels in die SAPDM. Die invloed van verskeie bymiddels op die krimpings en buigsaamheid gedrag van 'n BGM is ook geëvalueer om 'n beter begrip van hierdie eienskappe te verkry. Die bymiddels sluit sement in (1% en 2% inhoud) asook beide emulsie bitumen (0,9% en 2,4% inhoud) en skuim bitumen (slegs 2.4% inhoud). Twee lineêre krimpings toets metodes was ontwerp om die krimping potensiaal van BGM's te bepaal, wat 'n balk toets metode en 'n silindriese toets metode insluit. Die metode wat gebruik sal word om die krimping van 'n BGM te bepaal moet baseer word op die toepassing waarvoor die krimpings resultate gebruik gaan word. Die buigsaamheid is 'n meer komplekse eienskap en was getoets met behulp van 'n eenvoudige monotoniese balk toets. Die spanning-by-breekpunt waardes wat verkry was vanuit die balktoetse, het 'n goeie aanduiding van die buigsaamheid van die materiaal verskaf. Klein verskille in krimpingstendense tussen balk en silindriese proefstukke is opgemerk tydens die projek en is veroorsaak deur die geometrie van die proefstuk, die blotgestelde oppervlakte asook die rigting van kimp toetsing. Balk proefstukke toon aanvanklike swelling wanneer bitumen bygevoeg is, gevolg deur krimping. Silindriese proefstukke aan die ander kant toon aanvanklike krimping gevolg deur 'n effense toename in lengte, waarna krimping weer plaasvind. Die bymiddles het dieselfde invloed op die krimping van beide die balk en silindriese proefstukke. Alhoewel al die krimpingswaardes baie klein was, het 'n toename in bitumen 'n vermindering in krimping voortgebring en 'n toename in sement het 'n toename in krimping voortgebring. Stabilisasie met skuim bitumen in plaas van emulsie bitumen toon verlaagde krimping, maar slegs in kombinasie met 2% sement. Die spanning-by-breekpunt, verkose energie en materiaal styfheid wat bereken is vanaf die monotoniese balk toets resultate, het 'n goeie aanduiding van die buigsaamheid gedrag van BGM's verskaf. 'n Hoër bitumen inhoud verhoog die buigsaamheid potensiaal van BGM‟s terwyl 'n toename in sement die buigsaamheid potensiaal van BGM's verlaag. Hierdie projek bied goeie insigte vir beide die krimpings en buigsaamheid gedrag van BGM's, wat in die hersiende ontwerp metode van die SAPDM gebruik kan word. Verhoogde bitumen inhoud verminder die krimping potensiaal en verhoog die buigsaamheid van 'n BGM. Verhoogde sement inhoud aan die ander kant, verhoog krimping en verminder buigsaamheid van BGM's. Die korrekte kombinasie van sement en bitumen in 'n BGM kan dus 'n materiaal produseer met die gewenste buigsaamheidseienskappe en terselfde tyd die krimping tot 'n minimum beperk.
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8

Powell, Mark William. "An investigation of chemical factors influencing bitumen-mineral adhesion." Thesis, University of Hertfordshire, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.314732.

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Ali, Mahdi. "Study of the bitumen aging effects on the rheological properties and fatigue behavior." Master's thesis, Alma Mater Studiorum - Università di Bologna, 2018. http://amslaurea.unibo.it/16255/.

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A study of bitumen aging effects on the rheological properties and fatigue behavior is carried out on five polymer modified bitumen provided by an oil company. Dynamic Shear Rheometer (DSR), is used to perform advanced experimental investigation. It allows practicing frequency sweep tests, fatigue tests and time sweep tests. Polymer modified bitumen with different percentage of SBS with or without the presence of crumb rubber are tested before and after short and long aging processes. Master curves were generated based on frequency sweep tests data, they are studied, and a comparison was conducted between each bitumen before and after aging. In this thesis, the DSR is presented, as well as the testing procedure and the tested materials. A fatigue life analysis of the results, based on the use of two different criteria, the first criterion is classically used: it consists in defining the failure as a 50% loss of the initial stiffness. The other criteria based on dissipated energy data. This thesis provides results which show the effects of several factors on fatigue and healing response such as bitumen type, ageing, the presence of rubber and polymer modification.
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Mulusa, William Kapya. "Development of a simple trixial test for characterising bitumen stabilised materials." Stellenbosch : University of Stellenbosch, 2009. http://hdl.handle.net/10019.1/2848.

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Thesis (MScEng (Civil Engineering))--University of Stellenbosch, 2009.
The need for a more reliable testing procedure for the characterisation and Quality Assurance/ Control of Bitumen Stabilised Materials (BSMs), besides UCS and ITS testing, has long been recognised by the roads industry. In fact, at CAPSA 2004 and CAPSA 2007, discussions of improved test methods for granular materials, i.e. possible replacement tests for CBR procedures, were conducted in workshops. Triaxial testing for the evaluation of shear parameters is widely recognised as a reliable method of measuring these critical performance properties of granular and Bitumen Stabilised Materials (BSMs). However, the triaxial test in its current state as a research test has little chance of extensive use by practitioners and commercial laboratories, because of complexity, cost and time issues. Major adaptations to the research triaxial test are necessary, before this useful test can have a chance of being accepted by road practitioners. The main aim of this study is to investigate possibilities of developing a simple, affordable, reliable and robust test for characterizing granular and bitumen stabilized materials thus linking test outcome with in-situ performance. This is achieved through the innovative design and manufacture of a prototype triaxial cell capable of accommodating 150 mm diameter by 300 mm deep specimens. The cell is simpler than the research (geotechnical) triaxial cell and the operational protocols have been streamlined, thereby reducing the time and steps required in assembling specimens and testing them. In order to ensure the development of an appropriate triaxial cell for industry, a survey was conducted aimed at investigating currently available facilities, testing capacity and resources within civil engineering laboratories in South Africa. Findings of the survey (Appendix 4) have provided guidance with regard to the nature and sophistication of any new tests to be developed. The survey highlighted some of the limitations and lack of sophistication of the current loading frames used for CBR and UCS testing such as lack of electronic LVDTs, limited overhead space, limited loading capacity and others. Most laboratories would need to invest in new loading facilities to carry out triaxial tests. A review of the test procedure for monotonic triaxial test showed that two main factors contribute to the complexity of the research (geotechnical) triaxial cell namely, time taken to assemble the specimen accurately in the cell and secondly the inherent design of the cell which makes it water and/or air tight at relatively high pressures. The design of the Simple Triaxial Test, therefore, was aimed at overcoming the drawbacks of research triaxial test e.g. fitting a membrane to each specimen to be tested, through considerable simplification by means of a new structure design and procedure of assembly of specimen into the cell. The advantage of addressing these issues would be reduction in the number of steps required in the test procedure and therefore reduction in testing time. The design of the cell particularly was preceded by a conceptualization process that involved investigation of numerous options. Concepts such as the bottle, encapsulated-tube, bottle and sandwich concepts were considered and given reality checks. In addition, available triaxial procedures of a similar nature e.g. Texas Triaxial, were evaluated and analyzed. Ultimately, with some trials and innovation, a design was developed for a simple triaxial cell comprising a steel casing with a latex tube which is then introduced around the specimen sitting on a base plate. It is based on the ‘tube concept’ in which the specimen acts like a ‘rim’ and the cell acts like a ‘tyre’ providing confinement to the triaxial specimens for testing, within the tube. This approach eliminates the use of O-rings and membranes for the specimen and tie-rods for the triaxial cell, thus reducing testing time considerably. The overall dimensions of the cell are 244 mm diameter by 372 mm height (Appendix 5). The cell was manufactured at Stellenbosch University Civil Engineering workshop and preliminary tests were conducted under this study. Parallel tests were also conducted with the Research Triaxial Test setup at Stellenbosch University in order to determine if preliminary results obtained with the Simple Triaxial Test setup were comparable therefore providing a means of validating the data. Results of analysis of variance (ANOVA) show that variability between Simple Triaxial Test (STT) and Research Triaxial Test (RTT) results is less significant whilst that within samples of STT and RTT results is quite significant. Comparisons also show that good correlation were obtained from Reclaimed Asphalt Pavement (RAP) Hornfels + 3.3 % Emulsion + 0 % Cement mix and mixes with the G2 base course aggregate whilst completely different correlation was obtained from RAP + 3.3 % Emulsion + 1% Cement. It is evident however that the differences observed stem from material variability i.e. random variability to one degree or the other and not to the STT apparatus. It is recommended for future research that more STT versus RTT testing be done especially on a mix with known mechanical properties when compacted to a specified dry density, e.g. graded crushed stone (G1) compacted to 100% mod. AASHTO. In summary, a locally made, low cost, relatively durable triaxial cell with relatively easy and quick specimen assembly procedures has been developed. It is now possible to perform triaxial tests on 150 mm diameter by 300 mm high specimen relatively easily and quickly. However, the challenge of validating results obtained, as well as improving the manufacture process of its main component, the tube, still remains.
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Books on the topic "Aging of bitumen materials"

1

McNally, Tony. Polymer modified bitumen: Properties and characterisation. Oxford: Woodhead Publishing Ltd, 2011.

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M, Saleh. Detailed experimental investigation for foamed bitumen stabilisation. Wellington, N.Z: Transfund New Zealand, 2004.

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3

Daines, M. E. Assessment of 'Chem-Crete' as an additive for binders for wearing courses and roadbases. Crowthorne, Berkshire: Transport and Road Research Laboratory, 1985.

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Daines, M. E. Assessment of 'Chem-Crete' as an additive for binders for wearing courses and roadbases. Crowthorne, Berkshire: Transport and Road Research Laboratory, 1985.

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Daines, M. E. Assessment of 'Chem-Crete' as an additive for binders for wearing courses and roadbases. Crowthorne: Transport and Road Research Laboratory, 1985.

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Daines, M. E. Assessment of 'Chem-Crete' as an additive for binders for wearing courses and roadbases. Crowthorne, Berks: Transport and Road Research Laboratory, Highways and Structures Dept., Pavement Materials and Construction Division, 1985.

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7

Raw Materials Research and Development Council (Nigeria). Technical brief on mineral raw materials in Nigeria: Tar sand/bitumen. Abuja: Raw Materials Research and Development Council, Federal Ministry of Science and Technology, 2009.

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Briaud, J. L. Design and construction guidelines for downdrag on uncoated and bitumen-coated piles. Washington, D.C: National Academy Press, 1997.

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International SAMPE Symposium and Exhibition (41st 1996 Anaheim, Calif.). Materials and process challenges: Aging systems, affordability, alternative applications. Covina, Calif: Society for the Advancement of Material and Process Engineering, 1996.

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name, No. Dental materials in vivo: Aging and related phenomena. Chicago, IL: Quintessence Pub. Co., 2003.

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Book chapters on the topic "Aging of bitumen materials"

1

Salihov, Muhammet, and Evgeniy Veyukov. "Assessment of Thermal Aging of Bitumen-Mineral Materials in Various Ways." In Lecture Notes in Civil Engineering, 281–90. Cham: Springer International Publishing, 2022. http://dx.doi.org/10.1007/978-3-031-10853-2_26.

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Eberhardsteiner, Lukas, Josef Füssl, Bernhard Hofko, Florian Handle, Markus Hospodka, Ronald Blab, and Hinrich Grothe. "Micromechanical Description of Bitumen Aging Behavior." In RILEM Bookseries, 411–21. Dordrecht: Springer Netherlands, 2015. http://dx.doi.org/10.1007/978-94-017-7342-3_33.

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Jackson, Neil, and Ravindra K. Dhir. "Properties of Bitumen—Aggregate Mixes." In Civil Engineering Materials, 317–35. London: Macmillan Education UK, 1996. http://dx.doi.org/10.1007/978-1-349-13729-9_19.

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Jackson, Neil, and Ravindra K. Dhir. "Design of Bitumen—Aggregate Mixes." In Civil Engineering Materials, 336–47. London: Macmillan Education UK, 1996. http://dx.doi.org/10.1007/978-1-349-13729-9_20.

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Lyons, Arthur. "Bitumen and flat roofing materials." In Materials for Architects and Builders, 265–83. Sixth edition. | Abingdon, Oxon : Routledge, 2019.: Routledge, 2019. http://dx.doi.org/10.1201/9781351109550-6.

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Li, Ma, and Pan Yurong. "Aging Performance of Base and Modified Bitumen." In Lecture Notes in Civil Engineering, 33–38. Singapore: Springer Nature Singapore, 2022. http://dx.doi.org/10.1007/978-981-19-4293-8_4.

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Lombardi, Bernard. "Bitumen, Road Construction and Sustainable Development." In Organic Materials for Sustainable Construction, 389–406. Hoboken, NJ USA: John Wiley & Sons, Inc., 2013. http://dx.doi.org/10.1002/9781118616734.ch16.

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Ehrenstein, Gottfried W. "Aging and Stabilization." In Polymeric Materials, 229–40. München: Carl Hanser Verlag GmbH & Co. KG, 2001. http://dx.doi.org/10.3139/9783446434134.007.

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Maschauer, Daniel, Daniel Steiner, Johannes Mirwald, Bernhard Hofko, and Hinrich Grothe. "Viennese Aging Procedure – Behavior of Various Bitumen Provenances." In RILEM Bookseries, 62–67. Cham: Springer International Publishing, 2018. http://dx.doi.org/10.1007/978-3-030-00476-7_11.

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Marques, Severino P. C., and Guillermo J. Creus. "Materials with Aging." In Computational Viscoelasticity, 59–65. Berlin, Heidelberg: Springer Berlin Heidelberg, 2012. http://dx.doi.org/10.1007/978-3-642-25311-9_7.

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Conference papers on the topic "Aging of bitumen materials"

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Han, Jun, Shaopeng Wu, Zhiyi Huang, Dehong Zhou, and Fujian Li. "Research on Low Temperature Rheological Behavior of Aging Resistant Bitumen and Mixture." In Second International Conference on Sustainable Construction Materials: Design, Performance, and Application. Reston, VA: American Society of Civil Engineers, 2012. http://dx.doi.org/10.1061/9780784412671.0029.

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Samsudin, Mohamad Saifullah, Ahmad Kamil Arshad, Khairil Azman Masri, Mohd Khairul Afzan Mohd Lazi, Hasmawati Mat Hassan, and Ekarizan Shaffie. "The Influence of Colloidal Nanosilica on Microstructure of Asphalt Binder After Long-Term Aging." In World Sustainable Construction Conference Series 2022. Switzerland: Trans Tech Publications Ltd, 2023. http://dx.doi.org/10.4028/p-yo6318.

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The use of Atomic Force Microscopy (AFM) to observe the microstructure of asphalt binder promises a better insight compared to other microscopy techniques. In this study, AFM was used to investigate the effect of nanosilica concentration and aging conditions on the microstructure of asphalt binders. Asphalt binder penetration grade of 60/70 was modified with nanosilica (NS) by varying its concentration ranging from 1% to 5% (with the increment of 1%). Nanosilica modified binder (NSMB) were aged using a pressure aging vessel (PAV). The microstructure of the NSMB before and after aging were characterized using tapping mode of the atomic force microscopy (AFM). The effect of nanosilica (NS) addition and PAV ageing on the phase distribution, size of ‘bee’ structure and surface roughness of the asphalt binder were investigated. Based on this study, it was found that the addition of NS into asphalt binder tended to increase the distribution of the catana phase, as well as increasing the size of the bee structure and surface roughness of the AFM image. Besides that, the after long-term ageing was applied, the number of the bee structure and distribution of catana and peri phase also increased. It can be concluded that the addition of NS and aging increased the overall surface stiffness of the bitumen and has made the material surface more solid-like.
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Großegger, Daniel. "Microstructural aging of bitumen." In 6th Eurasphalt & Eurobitume Congress. Czech Technical University in Prague, 2016. http://dx.doi.org/10.14311/ee.2016.135.

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"Features of Aging of Road Bitumen." In Chemical technology and engineering. Lviv Polytechnic National University, 2021. http://dx.doi.org/10.23939/cte2021.01.087.

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Zhou, Xingye, Bo Su, and Xudong Wang. "Ultraviolet Aging Properties of Bitumen in Ultra-thin Asphalt Pavement." In 2017 2nd International Conference on Automation, Mechanical Control and Computational Engineering (AMCCE 2017). Paris, France: Atlantis Press, 2017. http://dx.doi.org/10.2991/amcce-17.2017.6.

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Donchenko, Myroslava, and O. Grynyshyn. "SPECIFICS OF AGING OF OXIDIZED OIL BITUMEN PRODUCED IN UKRAINE." In EDUCATION AND SCIENCE OF TODAY: INTERSECTORAL ISSUES AND DEVELOPMENT OF SCIENCES. European Scientific Platform, 2021. http://dx.doi.org/10.36074/logos-19.03.2021.v2.13.

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Pugin, K. G. "Change in Properties of Bitumen Used for Road Construction in Bitumineral Mixtures." In Modern Trends in Manufacturing Technologies and Equipment. Materials Research Forum LLC, 2022. http://dx.doi.org/10.21741/9781644901755-32.

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Abstract. Premature destruction of asphalt concrete can be caused by the aging of bitumen, which is associated with a change in the physical and chemical properties of bitumen. The article shows that in most cases, the improvement of the characteristics of asphalt concrete is achieved through the introduction of additives that affect the basic properties of the bituminous binder, such as penetration, softening temperature, viscosity. The influence of the chemical composition of the mineral filler on the rate of bitumen aging has been experimentally proved. The obtained research data show that the increase in the rate of aging of bitumen is influenced by the compounds of silicon and aluminum. On the other hand, metals such as iron and titanium contribute to the preservation of the initial plasticity of bitumen, and the accumulation of asphaltenes in the structure of the bitumen-mineral mixture slows down.
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Cannone Falchetto, Augusto, Alexander Alisov, Matthias Goeke, and Michael P. Wistuba. "Identification of structural changes in bitumen due to aging and fatigue." In 6th Eurasphalt & Eurobitume Congress. Czech Technical University in Prague, 2016. http://dx.doi.org/10.14311/ee.2016.196.

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Bhagat, N. T., H. P. Hadole, N. A. Hedaoo, and M. S. Ranadive. "Study of Flow Behavior and Aging Resistance of Pyro-Oil Modified Bitumen." In International Airfield and Highway Pavements Conference 2023. Reston, VA: American Society of Civil Engineers, 2023. http://dx.doi.org/10.1061/9780784484913.018.

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Malathi, R. "Performance Study on Partial Replacement of Bitumen using Waste Polypropylene Cement Bags for Pavement Construction." In Sustainable Materials and Smart Practices. Materials Research Forum LLC, 2022. http://dx.doi.org/10.21741/9781644901953-47.

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Abstract. Flexible pavement is most commonly used in the bituminous material mix. It consists of different binders such as asphalt or bitumen and other minerals are added and compacted and used together in the lower layer of the pavement. Bituminous pavement surface property changes due to varying weather conditions. In hot climatic conditions, the bitumen becomes soft and during cold conditions it becomes too stiff and brittle in nature. In this study, the main concept is to reuse the waste materials and to promote cost-effective solution and reduce environmental pollution. In this project, waste cement bags (polypropylene) are used to replace a portion of bitumen which is used in road construction. Effect of addition of additive materials on the strength of the pavement was evaluated. Previous studies state that polypropylene emits 60ppm less pollution than bitumen while burning. The used cement waste bag when mixed with bitumen improves the behaviour and mechanical properties as per standard specification. In this experimental work, cement bags are shredded into smaller fragments and heated to 90ºC for 30 minutes in a heating mantle till the plastic pieces turned into powder form. On heating, 5 gm of powder was obtained from 20 gm of the used cement bags. This powder was added subsequently to bitumen in 5%, 7%, 9% & 11% for partial replacement of bitumen. Finally, it is inferred that the optimum percentagewas 8.2% without the addition of binders or oxidizing agents, for better efficiency.
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Reports on the topic "Aging of bitumen materials"

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Moghtadernejad, Sara, Ehsan Barjasteh, Ren Nagata, and Haia Malabeh. Enhancement of Asphalt Performance by Graphene-Based Bitumen Nanocomposites. Mineta Transportation Institute, June 2021. http://dx.doi.org/10.31979/mti.2021.1918.

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As the State of California continues to grow, demand for enhanced infrastructure such as roadways and highways escalates. In view of the current average highway lifespan of 15–20 years, the improvement of asphalt binders leads to material sustainability by decreasing required maintenance and increasing the lifespan of roadways. In the present investigation, enhancement of asphalt binder properties was achieved by different methods of mixing varying compositions of graphene nanoparticles with an SBS polymer and asphalt binder. Additionally, experimental evaluation and comparison of the rheological and mechanical properties of each specimen is presented. Graphene nanoparticles have attracted great curiosity in the field of highway materials due to their incredible rigidity, even in small quantities. Addition of as little as 1.0%nanoparticles in combination with polymers in an asphalt binder is expected to increase the rigidity of the material while also maintaining the beneficial polymer characteristics. Evaluation of the effect of the mixing design established that the methods for application of graphene to the polymer-modified asphalt binder are critical in the improvement of a roadway, resulting in resistance to premature aging and strain from constant road operation.
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Gardea, Andrew D., Ryan Nishimoto, Nancy Y. C. Yang, Alfredo Martin Morales, Scott A. Whalen, Jeffrey M. Chames, and W. Miles Clift. Material compatibility and thermal aging of thermoelectric materials. Office of Scientific and Technical Information (OSTI), September 2009. http://dx.doi.org/10.2172/986608.

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Kubota, A., D. Reisman, and W. Wolfer. ASC Supercomputers Predict Effects of Aging on Materials. Office of Scientific and Technical Information (OSTI), August 2005. http://dx.doi.org/10.2172/878611.

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Battaile, Corbett Chandler, Brad Lee Boyce, Justin G. Brons, Stephen Martin Foiles, Khalid Mikhiel Hattar, Elizabeth A. Holm, Padilla, Henry A.,, John Anthony Sharon, and Gregory B. Thompson. Understanding and controlling low-temperature aging of nanocrystalline materials. Office of Scientific and Technical Information (OSTI), October 2013. http://dx.doi.org/10.2172/1096493.

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Archuleta, Kim M., and Rochelle Piatt. Materials compatibility and aging for flux and cleaner combinations. Office of Scientific and Technical Information (OSTI), January 2015. http://dx.doi.org/10.2172/1167670.

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Li, Meimei, K. Natesan, and Wei-Ying Chen. FY 2017 – Thermal Aging Effects on Advanced Structural Materials. Office of Scientific and Technical Information (OSTI), August 2017. http://dx.doi.org/10.2172/1409209.

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Gillen, K. T., and R. L. Clough. Predictive aging results for cable materials in nuclear power plants. Office of Scientific and Technical Information (OSTI), November 1990. http://dx.doi.org/10.2172/6189683.

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Fifield, Leonard S., Miguel Correa, and Andy Zwoster. Crystal River 3 Cable Materials for Thermal and Gamma Radiation Aging. Office of Scientific and Technical Information (OSTI), September 2017. http://dx.doi.org/10.2172/1400349.

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Dingreville, Remi Philippe Michel, Aaron Duun, and Laurent Capolungo. Predictive Modeling of Aging and Degradation of Materials in Extreme Environments. Office of Scientific and Technical Information (OSTI), October 2016. http://dx.doi.org/10.2172/1431187.

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Horwath, John, Zafer Turgut, and Richard Fingers. High Temperature Properties and Aging-Stress Related Changes of FeCo Materials. Fort Belvoir, VA: Defense Technical Information Center, July 2006. http://dx.doi.org/10.21236/ada460527.

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