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Journal articles on the topic 'Acetamide'

Author: Grafiati

Published: 4 June 2021

Last updated: 6 September 2023

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1

Nagarsha, K. M., T. M. Sharanakumar, D. Ramesh, N. Y. Praveen Kumar, M. N. Kumarswamy, D. R. Ramesh, and K. P. Latha. "NOVEL SYNTHESIS, CHARACTERIZATION AND ANTIMICROBIAL ACTIVITY OF N-(5BROMO-2-(5-PHENYL1,3,4-OXADIAZOL-2-YL)NAPHTHA[2,1-B]FURAN-1- YL)ACETAMIDE AND N-(5-NITRO-2-(5-PHENYL-1,3,4- OXADIAZOL-2-YL)NAPHTHA[2,1-BFURAN-1-YL]ACETAMIDE AND THEIR DERIVATIVES." RASAYAN Journal of Chemistry 16, no. 01 (2023): 167–75. http://dx.doi.org/10.31788/rjc.2023.1618088.

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The novel derivatives of naphtho-furan such N-(5bromo-2-(5-phenyl-1,3,4-oxadiazol-2-yl)naphtha[2,1-b]furan-1- yl)acetamide (8), N-(5-bromo-2-(hydrazinecarbonyl)naphtha[2,1-b]furan-1-yl]acetamide (7), ethyl-1-acetamido-5- bromonaphtho[2,1-b]furan-2-carboxylate (6), N-(5-nitro-2-(5-phenyl-1,3,4-oxadiazol-2-yl)naphtha[2,1-bfuran-1- yl]acetamide (5),N-(2-(hydrazinecarbonyl)-5-nitronaphtho[2,1-b]furan-1-yl)acetamide (4), ethyl-1-acetamido-5- nitrpnaphtho[2,1-b]furan-2-carboxylate (3), are prepared by ethyl-1-acetamidonaphtho[2,1-b]furan-2-carboxyate and ethyl 1-aminonaphtho[2,1-b]furan-2-carboxylate. All newly synthesized compounds were confirmed by Mass, NMR, and FTIR spectroscopic techniques. Those compounds were used for antimicrobial activity it exhibits good antibacterial and anti-functional activity.

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2

Qiu, Guanyinsheng, Yuewen Li, Lele Ma, and Hongwei Zhou. "KBr/K2S2O8-mediated dibromohydration of N-(2-alkynylaryl)acetamide." Organic Chemistry Frontiers 4, no. 6 (2017): 1069–73. http://dx.doi.org/10.1039/c6qo00840b.

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3

Girel, Sergey, Vadim Schütz, Laurent Bigler, Peter Dörmann, and Margot Schulz. "Bioactive Nitrosylated and Nitrated N-(2-hydroxyphenyl)acetamides and Derived Oligomers: An Alternative Pathway to 2-Amidophenol-Derived Phytotoxic Metabolites." Molecules 27, no. 15 (July 26, 2022): 4786. http://dx.doi.org/10.3390/molecules27154786.

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Incubation of Aminobacter aminovorans, Paenibacillus polymyxa, and Arthrobacter MPI764 with the microbial 2-benzoxazolinone (BOA)-degradation-product 2-acetamido-phenol, produced from 2-aminophenol, led to the recently identified N-(2-hydroxy-5-nitrophenyl) acetamide, to the hitherto unknown N-(2-hydroxy-5-nitrosophenyl)acetamide, and to N-(2-hydroxy-3-nitrophenyl)acetamide. As an alternative to the formation of phenoxazinone derived from aminophenol, dimers- and trimers-transformation products have been found. Identification of the compounds was carried out by LC/HRMS and MS/MS and, for the new structure N-(2-hydroxy-5-nitrosophenyl)acetamide, additionally by 1D- and 2D-NMR. Incubation of microorganisms, such as the soil bacteria Pseudomonas laurentiana, Arthrobacter MPI763, the yeast Papiliotrema baii and Pantoea ananatis, and the plants Brassica oleracea var. gongylodes L. (kohlrabi) and Arabidopsis thaliana Col-0, with N-(2-hydroxy-5-nitrophenyl) acetamide, led to its glucoside derivative as a prominent detoxification product; in the case of Pantoea ananatis, this was together with the corresponding glucoside succinic acid ester. In contrast, Actinomucor elegans consortium synthesized 2-acetamido-4-nitrophenyl sulfate. 1 mM bioactive N-(2-hydroxy-5-nitrophenyl) acetamide elicits alterations in the Arabidopsis thaliana expression profile of several genes. The most responsive upregulated gene was pathogen-inducible terpene synthase TPS04. The bioactivity of the compound is rapidly annihilated by glucosylation.

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4

Gowda, Basavalinganadoddy Thimme, Jozef Kožíšek, Ingrid Svoboda, and Hartmut Fuess. "Effect of Meta-Substitution on Solid State Geometry of N-(Aryl)-2,2,2-trichloro-acetamides, 3-XC6H4NH-CO-CCl3 and 3,5-X2C6H3NH-CO-CCl3 (X = Cl, CH3)." Zeitschrift für Naturforschung A 62, no. 1-2 (February 1, 2007): 91–100. http://dx.doi.org/10.1515/zna-2007-1-213.

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The crystal structures of N-(meta-substituted phenyl)-2,2,2-trichloro-acetamides such as N- (3-methylphenyl)-2,2,2-trichloro-acetamide, 3-CH3C6H4NH-CO-CCl3 (3MPTCA); N-(3-chlorophenyl)- 2,2,2-trichloro-acetamide, 3-ClC6H4NH-CO-CCl3 (3CPTCA); N-(3,5-dimethylphenyl)- 2,2,2-trichloro-acetamide, 3,5-(CH3)2C6H3NH-CO-CCl3 (35DMPTCA) and N-(3,5-dichlorophenyl)- 2,2,2-trichloro-acetamide, 3,5-Cl2C6H3NH-CO-CCl3 (35DCPTCA) have been determined at room temperature. The crystal system, space group, formula units and lattice constants (Å ) of the new structures are: 3MPTCA: orthorhombic, Pbca, Z = 8, a = 12.3199(11), b = 8.9719(8), c = 20.2058(15); 3CPTCA: orthorhombic, Fdd2, Z =16, a=19.285(4), b=40.765(8), c=5.5920(11); 35DMPTCA: triclinic, P1̄, Z = 2, a = 8.994(4), b = 9.9890(10), c = 14.760(5), α = 79.56(2)°, β = 73.32(3)°, γ = 86.47(2)°; and 35DCPTCA: orthorhombic, Pbca, Z = 8, a = 22.485(5), b=10.738(2), c=10.028(3). The compound 35DMPTCA has two molecules in its asymmetric unit, similar to o-NO2-, m-NO2- and p-CH3-substituted phenyl-trichloro-acetamides, while 3MPTCA, 3CPTCA and 35DCPTCA have one molecule each in their asymmetric units. The analysis of data indicates that the substitution of a strong electron withdrawing group such as a nitro group into PTCA at ortho or meta positions has a significant effect on the crystal parameters.

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5

Alagarsamy, Veerachamy, Viswas Raja Solomon, Mohaideen Thasthagir Sulthana, Meduri Satyasai Vijay, and Bandi Narendhar. "Design and synthesis of quinazolinyl acetamides for their analgesic and anti-inflammatory activities." Zeitschrift für Naturforschung B 70, no. 8 (August 1, 2015): 597–604. http://dx.doi.org/10.1515/znb-2015-0035.

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AbstractA variety of novel 2-(substituted)-N-(4-oxo-2-phenylquinazolin-3(3H)-yl)acetamides were synthesized by the reaction of 2-chloro-N-(4-oxo-2-phenylquinazolin-3(3H)-yl)acetamide with various amines. The starting material, 2-chloro-N-(4-oxo-2-phenylquinazolin-3(3H)-yl)acetamide, was synthesized from anthranilic acid by the multistep process. The title compounds were investigated for analgesic, anti-inflammatory, and ulcerogenic index activities. Among those, the compound 2-(ethylamino)-N-(4-oxo-2-phenylquinazolin-3(3H)-yl)acetamide (V9) showed most potent analgesic and anti-inflammatory activities of the series and it is moderately more potent compared to the reference standard diclofenac sodium. Interestingly, the test compounds showed only mild ulcerogenic potential compared to aspirin.

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6

Chen, Xuanhua, Rongwei Guo, and Zhongyuan Zhou. "N-[3-Acetamido-1,3-bis(4-ethylphenyl)butenyl]acetamide." Acta Crystallographica Section E Structure Reports Online 58, no. 6 (May 24, 2002): o671—o672. http://dx.doi.org/10.1107/s1600536802008607.

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7

Eagle, Cassandra T., Nkongho Atem-Tambe, Kenneth K. Kpogo, Jennie Tan, and Fredricka Quarshie. "(3-Methylbenzonitrile-κN)tetrakis(μ-N-phenylacetamidato)-κ4N:O;κ4O:N-dirhodium(II)(Rh—Rh)." Acta Crystallographica Section E Structure Reports Online 69, no. 12 (November 6, 2013): m639. http://dx.doi.org/10.1107/s1600536813029838.

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In the title compound, [Rh2(C8H8NO)4(C8H7N)], the four acetamidate ligands bridging the dirhodium core are arranged in a 2,2-transmanner. One RhIIatom is five-coordinate, in a distorted pyramidal geometry, while the other is six-coordinate, with a disorted octahedral geometry. For the six-coordinate RhIIatom, the axial nitrile ligand shows a non-linear Rh–nitrile coordination with an Rh—N—C bond angle of 166.4 (4)° and a nitrile N—C bond length of 1.138 (6) Å. Each unique RhIIatom is coordinated by atranspair of N atoms and atranspair of O atoms from the four acetamide ligands. The Neq—Rh—Rh—Oeqtorsion angles on the acetamide bridge varies between 12.55 (11) and 14.04 (8)°. In the crystal, the 3-methylbenzonitrile ring shows a π–π interaction with an inversion-related equivalent [interplanar spacing = 3.360 (6) Å]. A phenyl ring on one of the acetamide ligands also has a face-to-face π–π interaction with an inversion-related equivalent [interplanar spacing = 3.416 (5) Å].

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8

Que, Chuqiang, Peipei Huang, Zhanhui Yang, Ning Chen, and Jiaxi Xu. "Intramolecular Carbene C-H Insertion Reactions of 2-Diazo-2-sulfamoylacetamides." Molecules 24, no. 14 (July 19, 2019): 2628. http://dx.doi.org/10.3390/molecules24142628.

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The intramolecular C-H insertions of carbenes derived from 2-diazo-2-sulfamoylacetamides were studied. 2-Diazo-2-sulfamoylacetamides were first prepared from chloroacetyl chloride and secondary amines through acylation followed by sequential treatments with sodium sulfite, phosphorus oxychloride, secondary amines, and 4-nitrobenzenesulfonyl azide. The results indicate that: (1) 2-diazo-N,N-dimethyl-2-(N,N-diphenylsulfamoyl)acetamide can take the formal aromatic 1,5-C-H insertion in its N-phenylsulfonamide moiety to afford the corresponding 1,3-dihydrobenzo[c]isothiazole-3-carboxamide 2,2-dioxide derivative; (2) no aliphatic C-H insertions occur for 2-diazo-2-(N,N-dialkylsulfamoyl)acetamides; and (3) for 2-diazo-N-phenyl-2-(N-phenylsulfamoyl)acetamides, the formal aromatic 1,5-C-H insertion in the N-phenylacetamide moiety is favorable to afford the corresponding 3-sulfamoylindolin-2-one derivatives as sole or major products. The intramolecular competitive aromatic 1,5-C-H insertion reactions of 2-diazo-2-sulfamoylacetamides with aryl groups on both amide and sulfonamide groups reveal that the N-aryl substituents on acetamide are more active than those on sulfonamide. The chemoselectivity is controlled by electronic effect of the aryl group.

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9

Gowda, Basavalinganadoddy Thimme, Helmut Paulus, and Jozef Kožíšek. "Effect of Substitution on the Molecular Geometry of N-(2/3/4-Substituted-phenyl)-2,2-dichloro-acetamides, 2/3/4-XC6H4NH-CO-CHCl2 (X = CH3 or Cl)." Zeitschrift für Naturforschung A 61, no. 12 (December 1, 2006): 675–82. http://dx.doi.org/10.1515/zna-2006-1210.

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2MPDCAThe effect of ring substitution on the molecular geometry of amides of the type 2/3/4-XC6H4NHCO- CHCl2 (X = CH3 or Cl) has been studied by determining the crystal structures of the compounds N-(2-methylphenyl)-2,2-dichloro-acetamide, 2-CH3C6H4NH-CO-CHCl2 (); N-(3-methylphenyl)- 2,2-dichloro-acetamide, 3-CH3C6H4NH-CO-CHCl2 (3MPDCA) and N-(3-chlorophenyl)- 2,2-dichloro-acetamide, 3-ClC6H4NH-CO-CHCl2 (3CPDCA). The results are analyzed along with our earlier crystal structures of the amides N-(phenyl)-2,2-dichloro-acetamide, C6H5NH-COCHCl2 (PDCA); N-chloro-N-(phenyl)-2,2-dichloro-acetamide, C6H5NCl-CO-CHCl2 (NCPDCA); N-(4-methylphenyl)-2,2-dichloro-acetamide, 4-CH3C6H4NH-CO-CHCl2 (4MPDCA); N-(2-chlorophenyl)- 2,2-dichloro-acetamide, 2-ClC6H4NH-CO-CHCl2 (2CPDCA); N-(4-chlorophenyl)-2,2-dichloro- acetamide, 4-ClC6H4NH-CO-CHCl2 (4CPDCA). The results have also been compared and correlated with the crystal structure data of trichloro-acetamide analogues of the type 2/3/4- XC6H4NH-CO-CCl3 (X = CH3 or Cl): N-(phenyl)-2,2,2-trichloro-acetamide, N-(2-methylphenyl)- 2,2,2-trichloro-acetamide, N-(3-methylphenyl)-2,2,2-trichloro-acetamide, N-(4-methylphenyl)- 2,2,2-trichloro-acetamide, N-(2-chlorophenyl)-2,2,2-trichloro-acetamide, N-(3-chlorophenyl)-2,2,2- trichloro-acetamide, N-(4-chlorophenyl)-2,2,2-trichloro-acetamide, N-chloro-N-(phenyl)-2,2,2-trichloro- acetamide and N-(phenyl)-acetamide. The crystal system, space group, formula units and lattice constants in Å of the new structures are: 2MPDCA: monoclinic, P21/n, Z = 4, a = 4.7059(5), b = 11.600(1), c = 18.918(2), β = 94.702(9)° ; 3MPDCA: orthorhombic, P212121, Z = 4, a = 4.759(1), b = 10.543(3), c = 20.205(5); 3CPDCA: orthorhombic, Pnma, Z = 4, a = 9.935(1), b = 6.997(1), c = 14.140(2). 2MPDCA, 3MPDCA and 3CPDCA show a molecule each in their asymmetric units, in agreement with the observed 35Cl NQR spectra of the compounds

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10

Nagarsha, K. M., T. M. Sharanakumar, D. Ramesh, M. N. Kumarswamy, and K. P. Latha. "SYNTHESIS, CHARACTERIZATION, AND ANTIBACTERIAL ACTIVITIES OF NAPHTHO[2,1-b]FURAN DERIVATIVES." RASAYAN Journal of Chemistry 15, no. 04 (2022): 2477–84. http://dx.doi.org/10.31788/rjc.2022.1548052.

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The naphthofuran and its derivatives are important biological compounds so we have focused on the synthesis of naphthofuran derivatives. The synthesized compounds of ethyl 1-(acetylamino)-5-nitronaphtho[2,1-b]furan-2- carboxylate (3), and N-[2-(hydrazinylcarbonyl)-5-nitronaphtho[2,1-b]furan-1-yl]acetamide (4) used for the synthesis of N-(2-{[(2Z)-2-benzylidenehydrazinyl]carbonyl}-5-nitronaphtho[2,1-b]furan-1-yl)acetamide compounds of four derivatives 5 (a-d) and 1-acetamido-5-nitro-N-(5-oxo-2-phenylthiazolidin-3-yl)naphtha[2,1-b]furan-2-carboxamide compounds of four derivatives 6 (a-d). The prepared compounds were confirmed by FTIR NMR, and mass methods. The prepared naphthofuran derivatives used for the antibacterial activity versus both Gram(+ve) and Gram(-ve) bacteria show excellent results. Therefore the synthesized compounds are used for further antibacterial studies in the medical field.

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11

Liu, L. K., F. T. Luo, and L. C. Hsieh. "Acetamide hydrochloride." Acta Crystallographica Section C Crystal Structure Communications 50, no. 8 (August 15, 1994): 1333–35. http://dx.doi.org/10.1107/s0108270194001952.

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12

Kerridge, D. H. "The chemistry of molten acetamide and acetamide complexes." Chemical Society Reviews 17 (1988): 181. http://dx.doi.org/10.1039/cs9881700181.

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13

Gowda, Basavalinganadoddy Thimme, Helmut Paulus, Ingrid Svoboda, and Hartmut Fuess. "Structural Studies on N-(Phenyl)-2,2,2-trimethyl-acetamide, N-(2,4,6-Trimethylphenyl)-2,2,2-trimethyl-acetamide and N-(2,4,6-Trimethylphenyl)-2,2,2-trichloro-acetamide, 2,4,6-X3C6H2NH-CO-CY3 (X = H or CH3; Y = CH3 or Cl)." Zeitschrift für Naturforschung A 62, no. 5-6 (June 1, 2007): 331–37. http://dx.doi.org/10.1515/zna-2007-5-615.

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To study the effect of side chain and ring substitutions on the solid state geometry of amides of the general formulae C6H5NH-CO-CX3 and 2,4,6-X3C6H2NH-CO-CH3−yXy (X = CH3 or Cl and y = 0,1,2, 3), crystal structures of N-(phenyl)-2,2,2-trimethyl-acetamide, C6- H5NH-CO-C(CH3)3 (PTMA); N-(2,4,6-trimethylphenyl)-2,2,2-trimethyl-acetamide, 2,4,6-(CH3)3- C6H2NH-CO-C(CH3)3 (TMPTMA) and N-(2,4,6-trimethylphenyl)-2,2,2-trichloro-acetamide, 2,4, 6-(CH3)3C6H2NH-CO-CCl3 (TMPTCA) have been determined. The data are analyzed along with those of N-(phenyl)-acetamide, C6H5NH-CO-CH3; N-(phenyl)-2,2,2-trichloro-acetamide, C6- H5NH-CO-CCl3; N-(2,4,6-trimethylphenyl)-acetamide, 2,4,6-(CH3)3C6H2NH-CO-CH3; N-(2,4,6- trimethylphenyl)-2-chloro-acetamide, 2,4,6-(CH3)3C6H2NH-CO-CH2Cl; N-(2,4,6-trimethylphenyl)- 2,2-dichloro-acetamide, 2,4,6-(CH3)3C6H2NH-CO-CHCl2; N-(2,4,6-trimethylphenyl)-2-methyl- acetamide, 2,4,6-(CH3)3C6H2NH-CO-CH2CH3; N-(2,4,6-trimethylphenyl)-2,2-dimethyl-acetamide, 2,4,6-(CH3)3C6H2NH-CO-CH(CH3)2; N-(2,4,6-trichlorophenyl)-acetamide, 2,4,6-Cl3C6H2- NH-CO-CH3; N-(2,4,6-trichlorophenyl)-2-chloro-acetamide, 2,4,6-Cl3C6H2NH-CO-CH2Cl; N-(2, 4,6-trichlorophenyl)-2,2-dichloro-acetamide, 2,4,6-Cl3C6H2NH-CO-CHCl2 and N-(2,4,6-trichlorophenyl)- 2,2,2-trichloro-acetamide, 2,4,6-Cl3C6H2NH-CO-CCl3. The crystallographic system, space group, formula units and lattice constants in Å are: PTMA: orthorhombic, Pca21, Z = 4, a = 9.969(3), b = 10.642(3), c = 10.172(3); TMPTMA: tetragonal, P41212, Z = 8, a = 12.708(3), b = 12.708(3), c = 17.354(4); TMPTCA: monoclinic, P21/n, Z = 8, a = 12.255(4), b = 17.904(6), c = 12.619(4), β = 95.23(2)◦. PTMA and TMPTMA have 1 molecule each in their asymmetric units, but TMPTMA shows disorder. TMPTCA has 2 molecules in its asymmetric unit. The comparison of the bond parameters reveals that there are significant changes in the structural parameters with ring and side chain substitutions.

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14

Sawant, Ramesh, and Deepali Kawade. "Synthesis and biological evaluation of some novel 2-phenyl benzimidazole-1-acetamide derivatives as potential anthelmintic agents." Acta Pharmaceutica 61, no. 3 (September 1, 2011): 353–61. http://dx.doi.org/10.2478/v10007-011-0029-z.

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Synthesis and biological evaluation of some novel 2-phenyl benzimidazole-1-acetamide derivatives as potential anthelmintic agentsThe present study describes synthesis of a series of 2-phenyl benzimidazole-1-acetamide derivatives and their evaluation for anthelmintic activity using Indian adult earthworms,Pheretima posthuma.The structure of the title compounds was elucidated by elemental analysis and spectral data. The compounds 4-({[2-(4-nitrophenyl)-1H-benzimidazol-1-yl]acetyl}amino) benzoic acid (3a),N-ethyl-2-[2-(4-nitrophenyl)-1H-benzimidazol-1-yl] acetamide (3c),N-benzyl-2-[2-(4-nitrophenyl)-1H-benzimidazol-1-yl] acetamide (3d),N-(4-hydroxyphenyl)-2-[2-(4-nitrophenyl)-1H-benzimidazol-1-yl] acetamide (3f), 2-[2-(4-nitrophenyl)-1H-benzimidazol-1-yl]-N-phenyl acetamide (3h), 2-[2-(4-chlorophenyl)-1H-benzimidazol-1-yl]-N'-phenylacetohydrazide (3k), 2-[2-(4-chlorophenyl)-1H-benzimidazol-1-yl]-N-(4-nitrophenyl) acetamide (3n) and 2-[2-(4-chlorophenyl)-1H-benzimidazol-1-yl]-N-phenyl acetamide (3q) were found better to paralyze worms whereasN-ethyl-2-[2-(4-nitrophenyl)-1H-benzimidazol-1-yl] acetamide (3c), N-(4-nitrophenyl)-2-[2-(4-nitrophenyl)-1H-benzimidazol-1-yl] acetamide (3e), 4-({[2-(4-chlorophenyl)-1H-benzimidazol-1-yl] acetyl}amino) benzoic acid (3j), 2-[2-(4-chlorophenyl)-1H-benzimidazol-1-yl]-N-ethyl acetamide (31) and 2-[2-(4-chlorophenyl)-1H-benzimidazol-1-yl]-N-phenyl acetamide (3q) were better to cause death of worms compared to the anthelmintic drug albendazole.

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15

Dziadek, Jaroslaw, Stacey A. Rutherford, Murty V. Madiraju, Mark A. L. Atkinson, and Malini Rajagopalan. "Conditional expression of Mycobacterium smegmatis ftsZ, an essential cell division gene." Microbiology 149, no. 6 (June 1, 2003): 1593–603. http://dx.doi.org/10.1099/mic.0.26023-0.

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To understand the role of Mycobacterium smegmatis ftsZ (ftsZsmeg ) in the cell division process, the ftsZ gene was characterized at the genetic level. This study shows that ftsZsmeg is an essential gene in that it can only be disrupted in a merodiploid background carrying another functional copy. Expression of ftsZsmeg in M. smegmatis from a constitutively active mycobacterial promoter resulted in lethality whereas that from a chemically inducible acetamidase (ami) promoter led to FtsZ accumulation, filamentation and cell lysis. To further understand the roles of ftsZ in cell division a conditionally complementing ftsZsmeg mutant strain was constructed in which ftsZ expression is controlled by acetamide. Growth in the presence of 0·2 % acetamide increased FtsZ levels approximately 1·4-fold, but did not decrease viability or change cell length. Withdrawal of acetamide reduced FtsZ levels, decreased viability, increased cell length and eventually lysed the cells. Finally, it is shown that ftsZsmeg function in M. smegmatis can be replaced with the Mycobacterium tuberculosis counterpart, indicating that heterologous FtsZ tb can independently initiate the formation of Z-rings and catalyse the septation process. It is concluded that optimal levels of M. smegmatis FtsZ are required to sustain cell division and that the cell division initiation mechanisms are similar in mycobacteria.

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16

Olszewska, E., S. Pikus, and B. Tarasiuk. "New powder diffraction data of some derivatives of N-alkyl (aryl)-2,4-dichlorophenoxyacetamide—New potential pesticides." Powder Diffraction 23, no. 4 (December 2008): 338–49. http://dx.doi.org/10.1154/1.3009636.

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Four new derivatives of N-aryl-2,4-dichlorophenoxyacetamide, 2-(2,4-dichlorophenoxy)-N-(4-fluorophenyl)acetamide, N-(4-bromophenyl)-2-(2,4-dichlorophenoxy)acetamide, N-[4-chloro-3-(trifluoromethyl)phenyl]-2-(2,4-dichlorophenoxy)acetamide, and N-(3-chloro-4-fluorophenyl)-2-(2,4-dichlorophenoxy)acetamide, and two of N-alkyl-2,4-dichlorophenoxyacetamide, N-dodecyl-2,4-dichlorophenoxy-acetamide and 2-(2,4-dichlorophenoxy)-N-hexadecylacetamide, have been characterized by X-ray powder diffraction. These organic compounds are potential pesticides. Experimental 2θ peaks positions, relative peak intensities, values of d and Miller indices, and unit cell parameters are presented.

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17

Nikolić, Ružica, and Gordana Ristić. "Activity of acetamide in acetamide-calcium nitrate melt solutions." Journal of Solution Chemistry 23, no. 7 (July 1994): 787–94. http://dx.doi.org/10.1007/bf00972673.

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18

Ma, Cha, Long Li, Hu Lu, Xu Bo Yuan, and Gang Wang. "Study on the Effect of Humic Acid Acetamide on the Rheological Properties of Diesel Oil-Based Drilling Fluids." Applied Mechanics and Materials 620 (August 2014): 449–52. http://dx.doi.org/10.4028/www.scientific.net/amm.620.449.

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A new kind of humic acid acetamide compoud was synthesized by chemical modification of humic acid with octadecylamine, and the effect of humic acid acetamide on the rheological properties of oil-based drilling fluids was investigated. The results indicated that the humic acid acetamide had excellent dispersing property, and good capacity of depressing fluid loss. Moreover, the humic acid acetamide had better property of depressing fluid loss than oxidated asphalt. As a result, this humic acid acetamide is an excellent fluid loss agent for diesel oil-based drilling fluids, and is an good alternative to oxidated asphalt.

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19

Olszewska, E., B. Tarasiuk, and S. Pikus. "New powder diffraction data of some derivatives of N-(hydroxyalkyl)-4-chlorophenoxyacetamide—Potential pesticides." Powder Diffraction 24, no. 4 (December 2009): 327–36. http://dx.doi.org/10.1154/1.3257637.

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Five new derivatives of N-(ω-hydroxyalkyl)-4-chlorophenoxyacetamide [namely, 2-(4-chlorophenoxy)-N-(2-hydroxyethyl) acetamide, 2-(4-chlorophenoxy)-N-(3-hydroxypropyl) acetamide, 2-(4-chlorophenoxy)-N-[1-(hydroxymethyl) propyl] acetamide, 2-(4-chlorophenoxy)-N-(2-hydroxy-1,1-dimethylethyl) acetamide, and 2-(4-chlorophenoxy)-N-{2-[(2-hydroxyethyl) amino] ethyl} acetamide] and one 2-(4-chlorophenoxy) acetohydrazide have been characterized by X-ray powder diffraction. These organic compounds are potential pesticides. New diffraction data including experimental and calculated 2θ peaks positions, values of d, experimental relative peak intensities, and Miller indices as well as unit-cell parameters are reported.

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Linh, Bùi Thị Thùy, Nguyễn Tiến Công, and Huỳnh Thị Xuân Trang. "SYNTHESIS AND STRUCTURE OF SOME CHALCONES CONTAINING ACETAMIDE GROUP." Tạp chí Khoa học 17, no. 9 (September 30, 2020): 1536. http://dx.doi.org/10.54607/hcmue.js.17.9.2789(2020).

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Hai chalcone là (E)-3-(2-hydroxyphenyl)-1-phenylprop-2-en-1-one (3a) và (E)-3-(4-hydroxyphenyl)-1-phenylprop-2-en-1-one (3b) đã được tổng hợp tương ứng từ phản ứng của acetophenone với 2-hydroxybenzaldehyde hoặc 4-hydroxybenzaldehyde. Phản ứng Williamson giữa (3a) hoặc (3b) với các N-aryl-2-chloroacetamide khác nhau đã tạo thành 8 hợp chất (E)-N-(4-aryl)-2-(2/4-(3-oxo-3-phenylprop-1-en-1-yl)phenoxy)acetamide; 7 trong số đó là chất mới: (E)-N-(4-bromophenyl)-2-(2-(3-oxo-3-phenylprop-1-en-1-yl)phenoxy)acetamide (5a), (E)-N-(4-chlorophenyl)-2-(2-(3-oxo-3-phenylprop-1-en-1-yl)phenoxy)acetamide (5b), (E)-N-(4-methoxyphenyl)-2-(2-(3-oxo-3-phenylprop-1-en-1-yl)phenoxy)acetamide (5c), (E)-2-(2-(3-oxo-3-phenylprop-1-en-1-yl)phenoxy)-N-(p-tolyl)acetamide (5d), (E)-N-(4-bromophenyl)-2-(4-(3-oxo-3-phenylprop-1-en-1-yl)phenoxy)acetamide (5e), (E)-N-(4-chlorophenyl)-2-(4-(3-oxo-3-phenylprop-1-en-1-yl)phenoxy)acetamide (5f), (E)-N-(4-methoxyphenyl)-2-(4-(3-oxo-3-phenylprop-1-en-1-yl)phenoxy)acetamide (5g), (E)-2-(4-(3-oxo-3-phenylprop-1-en-1-yl)phenoxy)-N-(p-tolyl)acetamide (5h). Cấu trúc của các hợp chất đã được xác nhận qua các phổ IR, 1H-NMR, 13C-NMR và phổ HR-MS.

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21

Olszewska, E., B. Tarasiuk, and S. Pikus. "New powder diffraction data of some N-derivatives of 4-chloro-3,5-dimethylphenoxyacetamide-potential pesticides." Powder Diffraction 26, no. 4 (December 2011): 337–45. http://dx.doi.org/10.1154/1.3652921.

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N-derivatives of 4-chloro-3,5-dimethylphenoxyacetamide—2-(4-chloro-3,5-dimethylphenoxy)-N-(4-fluorophenyl)acetamide, 2-(4-chloro-3,5-dimethylphenoxy)-N-(3-chloro-4-fluorophenyl) acetamide, 2-(4-chloro-3,5-dimethylphenoxy)-N-[4-chloro-3-(trifluoromethyl)phenyl] acetamide, 2-(4-chloro-3,5-dimethylphenoxy)-N-[3-chloro-4-methylphenyl]acetamide, 2-(4-chloro-3,5-dimethylphenoxy)-N-(2,4,6-tribromophenyl) acetamide, 2-(4-chloro-3,5-dimethylphenoxy)-N-pyridin-2-ylacetamide, 1-[(4-chloro-3,5-dimethylphenoxy)acetyl]-4-methylpiperazine, and 1-benzyl-4-[(4-chloro-3,5-dimethylphenoxy)acetyl]piperazine—have been characterized by X-ray powder diffraction. These organic compounds are potential pesticides. Experimental 2θ peak positions, relative peak intensities, values of d and Miller indices, and unit-cell parameters are presented.

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22

Gowda, B. Thimme, Sabine Foro, and Hartmut Fuess. "2-Chloro-N-(4-chlorophenyl)acetamide." Acta Crystallographica Section E Structure Reports Online 63, no. 11 (October 31, 2007): o4488. http://dx.doi.org/10.1107/s1600536807053093.

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The structure of the title compound, C8H7Cl2NO, resembles those of N-(4-chlorophenyl)acetamide, N-2-chloro-(4-methylphenyl)acetamide, N-2-chloro-(4-nitrophenyl)acetamide and other related amides, with similar bond parameters. Molecules are linked into chains through N—H...O hydrogen bonding.

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23

Gowda, B. Thimme, Sabine Foro, P. G. Nirmala, and Hartmut Fuess. "N-(Phenylsulfonyl)acetamide." Acta Crystallographica Section E Structure Reports Online 66, no. 6 (May 8, 2010): o1284. http://dx.doi.org/10.1107/s1600536810015849.

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24

Pei, Wen, Li Sun, Yueshui Shao, and Dongwei Li. "2-(Benzhydrylsulfinyl)acetamide." Acta Crystallographica Section E Structure Reports Online 60, no. 3 (February 14, 2004): o372—o373. http://dx.doi.org/10.1107/s1600536804001382.

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25

Castellani, F., G. Berchiesi, and V. Bartocci. "Acetamide-ammonium sulfamate." Journal of Thermal Analysis 36, no. 3 (May 1990): 1071–76. http://dx.doi.org/10.1007/bf01904644.

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26

Jiang, Jikang, Haixia Ye, Jingfei Zhou, Chenlu Wang, Zheng Shen, and Yalei Zhang. "Research and Mechanism of Two-step Preparation of Acetamide from Microalgae under Hydrothermal Conditions." E3S Web of Conferences 194 (2020): 02006. http://dx.doi.org/10.1051/e3sconf/202019402006.

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A two-step synthesis of acetamide under hydrothermal condition from microalgae, is presented. results showed that the best yield of acetamide and selectivity of acetic acid were 9.5 % and 60.1 % at 320 ℃ for 8 min with a NH3 supply of 30. Algae such as spirulina, cyanobacteria and autotrophic chlorella could also acquire acetamide, and lactic acid was found to be an important intermediate during the exploration of reaction pathways. These results demonstrated that it is possible to develop a process for conversion of microalgae biomass into acetamide.

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27

Narayana, Badiadka, Hemmige S. Yathirajan, Ravindranath Rathore, and Christopher Glidewell. "Crystal structures of two C,N-disubstituted acetamides: 2-(4-chlorophenyl)-N-(2-iodophenyl)acetamide and 2-(4-chlorophenyl)-N-(pyrazin-2-yl)acetamide." Acta Crystallographica Section E Crystallographic Communications 72, no. 9 (August 9, 2016): 1270–75. http://dx.doi.org/10.1107/s2056989016012512.

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In the crystal of 2-(4-chlorophenyl)-N-(2-iodophenyl)acetamide, C14H11ClINO, molecules are linked by a combination of N—H...O and C—H...O hydrogen bonds to form aC(4)C(4)[R21(7)] chain of rings and chains of this type are linked by a combination of C—Cl...π(arene) and C—I...π(arene) interactions to form deeply puckered twofold interwoven sheets. In the crystal of 2-(4-chlorophenyl)-N-(pyrazin-2-yl)acetamide, C12H10ClN3O, molecules are linked into complex sheets by N—H...N, C—H...N and C—H...O hydrogen bonds, and by C—H...π(arene) interactions.

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28

Yu, Jia, Xuan Chen, Xiaoliang Ma, Qingfei Song, Yukun Zhao, and Jiahao Cao. "Influence of Nanoparticles and Graphite Foam on the Supercooling of Acetamide." Journal of Nanomaterials 2014 (2014): 1–10. http://dx.doi.org/10.1155/2014/313674.

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Acetamide is a promising phase change materials (PCMs) for thermal storage,but the large supercooling during the freezing process has limited its application. In this study, we prepared acetamide-SiO2composites by adding nano-SiO2into acetamide. This modified PCM was then impregnated into the porous graphite foam forming acetamide-SiO2-graphite foam form-stable composites. These composites were subjected to melting-solidification cycles 50 times; the time-temperature curves were tracked and recorded during these cycles. The time-temperature curves showed that, for the acetamide containing 2 wt. % SiO2, the supercooling phenomenon was eliminated and the material’s performance was stable for 50 cycles. The solidification temperature of the acetamide-SiO2-graphite foam samples was 65°C and the melting temperature was lowered to 65°C. The samples exhibited almost no supercooling and the presence of SiO2had no significant effect on the melting-solidification temperature. The microscopic supercooling of the acetamide-SiO2composite was measured using differential scanning calorimetry (DSC). The results indicated that when the content of SiO2was 1 wt. to 2 wt. %, the supercooling could be reduced to less than 10°C and heat was sufficiently released during solidification. Finally, a set of algorithms was derived using MATLAB software for simulating the crystallization of samples based on the classical nucleation theory. The results of the simulation agreed with the experiment results.

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29

Wang, Hong, Dong Yuan Jin, Zhi Qiang Yang, Yong Hong Gao, Jian Wei Tao, and Li Hua Li. "Synthesis of Phenoxy Amide Derivatives." Advanced Materials Research 396-398 (November 2011): 2318–21. http://dx.doi.org/10.4028/www.scientific.net/amr.396-398.2318.

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Several kinds of new derivatives of N-substituted-4-(p-chlorophenoxy)acetamide and N-substituted-2,4-dichlorophenoxy acetamide were synthesized with methyl chloroacetate. The influence of solvent on the chlorination occurred in the benzene ring of phenoxy acetamide additives has been investigated by using sulfonyl chloride as chlorination agent. Result shows that the higher polarity of solvent is beneficial to the chlorination.

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30

Zikmundová, M., K. Drandarov, L. Bigler, M. Hesse, and C. Werner. "Biotransformation of 2-Benzoxazolinone and 2-Hydroxy-1,4-Benzoxazin-3-one by Endophytic Fungi Isolated from Aphelandra tetragona." Applied and Environmental Microbiology 68, no. 10 (October 2002): 4863–70. http://dx.doi.org/10.1128/aem.68.10.4863-4870.2002.

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ABSTRACT The biotransformation of the phytoanticipins 2-benzoxazolinone (BOA) and 2-hydroxy-1,4-benzoxazin-3-one (HBOA) by four endophytic fungi isolated from Aphelandra tetragona was studied. Using high-performance liquid chromatography-mass spectrometry, several new products of acylation, oxidation, reduction, hydrolysis, and nitration were identified. Fusarium sambucinum detoxified BOA and HBOA to N-(2-hydroxyphenyl)malonamic acid. Plectosporium tabacinum, Gliocladium cibotii, and Chaetosphaeria sp. transformed HBOA to 2-hydroxy-N-(2-hydroxyphenyl)acetamide, N-(2-hydroxyphenyl)acetamide, N-(2-hydroxy-5-nitrophenyl)acetamide, N-(2-hydroxy-3-nitrophenyl)acetamide, 2-amino-3H-phenoxazin-3-one, 2-acetylamino-3H-phenoxazin-3-one, and 2-(N-hydroxy)acetylamino-3H-phenoxazin-3-one. BOA was not degraded by these three fungal isolates. Using 2-hydroxy-N-(2-hydroxyphenyl)[13C2]acetamide, it was shown that the metabolic pathway for HBOA and BOA degradation leads to o-aminophenol as a key intermediate.

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31

El Kayal, Wassim, Hanna Severina, Vadim Tsyvunin, Sergiy Zalevskyi, Sergiy Shtrygol’, Sergiy Vlasov, Olga Golovchenko, Sergiy Kovalenko, and Victoriya Georgiyants. "Synthesis and anticonvulsant activity evaluation of n-[(2,4-dichlorophenyl)methyl]-2-(2,4-dioxo-1h-quinazolin-3-yl)acetamide novel 1-benzylsubstituted derivatives." ScienceRise: Pharmaceutical Science, no. 1(35) (February 28, 2022): 58–69. http://dx.doi.org/10.15587/2519-4852.2022.253554.

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The aim. Synthesis of 1-benzylsubstituted derivatives of N-[(2,4-dichlorophenyl)methyl]-2-(2,4-dioxo-1h-quinazolin-3-yl)acetamide, and determination of affinity to GABAergic biotargets with the following anticonvulsant activity estimation using PTZ-induced seizures model in mice. Materials and methods. Standard organic synthesis methods were used; the structure of the synthesized compounds was proved by elemental analysis, 1H and 13C NMR spectroscopy, and LC/MS method; composition of the synthesized compounds – by elemental analysis, their individuality – by TLC and LC/MS methods. AutoDockTools-1.5.6, as well as AutoDock Vina software, was used to perform molecular docking. Anticonvulsant activity was studied using pentylenetetrazole-induced seizures in mice. Results. A targeted N-[(2,4-dichlorophenyl)methyl]-2-(1-(R-benzyl)-2,4-dioxo-quinazolin-3-yl)acetamides were obtained by alkylation of N-[(2,4-dichlorophenyl)methyl]-2-(2,4-dioxo-1H-quinazolin-3-yl)acetamide by corresponding 1-chloromethylbenzene in dimethylformamide environment with excess of potassium carbonate at a temperature 70-80 ˚С. Prediction of activity of 1-benzyl derivatives in the pentylenetetrazole-induced seizures in an in vivo experiment was carried out according to the obtained results of docking studies – affinity calculation for GABA receptor and GABA enzyme active sites, as well as analysis of conformational placement in them. In relation to the binding energy, the studied ligands were inferior to the reference drugs: GABA receptor positive allosteric modulators – benzamidine and diazepam, and GABA inhibitor – vigabatrin. The synthesized substances did not show anticonvulsant activity: only 2 compounds have shown a tendency to their activity manifestation according to the criterion of integral protective indicator – reduction of mortality by 17 % compared to control, as well as prolonging the time death of the animals. Comparison with the preliminary obtained results of the activity of the promising anticonvulsant N-[(2,4-dichlorophenyl)methyl] -2-(2,4-dioxo-1H-quinazolin-3-yl) acetamide N-[(2,4-dichlorophenyl)methyl]-2-(2,4-dioxo-1H-quinazolin-3-yl)acetamide made possible to prove the pharmacophore role of the cyclic amide fragment in anticonvulsant activity manifestation. Conclusion. The synthesis of N-[(2,4-dichlorophenyl)methyl]-2-(1-(R-benzyl)-2,4-dioxo-quinazolin-3-yl)acetamides, which have not still described in the literature, was carried out, as well as the structure of the mentioned compounds was proved. Unfortunately, the substances did not show anticonvulsant activity on the model of pentylenetetrazole-induced seizures. However, the obtained results allowed establishing the key role of the NHCO cyclic fragment on anticonvulsant activity. A positive correlation between the results of in vivo studies and in silico calculations was found – the model of pentylenetetrazole-induced seizures and docking into the active sites of PAMs GABAА receptor and enzyme inhibitor GABAАТ, which allows to recommend the given docking methodology as a tool to streamline and optimize the screening on the mentioned model

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32

Sharma, Manu, Harikrishnan K, Umesh Kumar Gaur, and Ashok K. Ganguli. "Synthesis of mesoporous SiO₂–CeO₂ hybrid nanostructures with high catalytic activity for transamidation reaction." RSC Advances 13, no. 19 (2023): 13134–41. http://dx.doi.org/10.1039/d3ra01552a.

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33

Kong, Youqing, Bin Ye, Lei Yang, Xiangnong Liu, and Cai Gao. "Comparative Molecular Dynamics Study On Interaction Of Acetamide And Glycerol With Phospholipid Bilayer." Cryoletters 43, no. 1 (January 1, 2022): 42–49. http://dx.doi.org/10.54680/fr22110110412.

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BACKGROUND: The exact mechanisms that acetamide and glycerol interact with cell membrane remains a matter of debate. OBJECTIVE: To investigate the microscopic interactions of acetamide and glycerol with phospholipid bilayers at various temperatures. MATERIALS AND METHODS: Molecular dynamics simulations of a hydrated dipalmitoyl-phosphatidylcholine (DPPC) bilayer in the presence of glycerol and acetamide were performed. The system contains 128 lipids and about 700 cryoprotectant molecules, and simulations extended to 15 ns. RESULT: When compared to glycerol, acetamide shows a stronger affinity with water rather than the lipid bilayer. CONCLUSION: The knowledge of the mixing dynamics of present system helps to develop better cryoprotective formulas and to propose more optimal cooling/warming protocols.

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34

Nakamura, Kenji, Yuji Ishii, Shinji Takasu, Takehiko Nohmi, Makoto Shibutani, and Kumiko Ogawa. "Lack of In Vivo Mutagenicity of Acetamide in a 13-Week Comprehensive Toxicity Study Using F344 gpt Delta Rats." Toxicological Sciences 177, no. 2 (September 21, 2020): 431–40. http://dx.doi.org/10.1093/toxsci/kfaa126.

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Abstract Acetamide, a food contaminant, has been shown to induce hepatocellular tumors in rats. However, the mode of action underlying acetamide-induced hepatocarcinogenesis remains unclear. In the current study, we aimed to examine the possible involvement of in vivo mutagenicity in hepatocarcinogenesis of acetamide and evaluate its toxicological profile using a comprehensive medium-term toxicity study in gpt delta rats. Six-week-old male F344 gpt delta rats were given a basal diet containing 0%, 0.625%, 1.25%, or 2.5% acetamide for 13 weeks. In general toxicologic assessment, hepatotoxic parameters in serum, such as aspartate aminotransferase and alanine aminotransferase were significantly changed at the 1.25% group and higher. Histopathological examination of the liver revealed that various changes related to hepatic injury were observed at the 1.25% group and higher. Interestingly, Feulgen-positive cytoplasmic inclusion was frequently observed in hepatocytes in these groups. In the hematopoietic system, red blood cell parameters in plasma, such as mean corpuscular volume and mean corpuscular hemoglobin were significantly changed at the 1.25% group and higher, and decrease of erythroblast in the spleen was observed histopathologically in the 2.5% group. Thus, the no-observed-adverse-effect level of acetamide in this study was 0.625% (equivalent to 394 mg/kg body weight/day). In vivo mutation assays showed that acetamide induced no changes in gpt and red/gam gene mutant frequencies, even at the carcinogenic target site. In contrast, Ki67-positive hepatocytes were increased significantly at carcinogenic doses. Therefore, these results suggested that cell proliferation activity, but not mutagenicity, played crucial roles in acetamide-induced hepatocarcinogenesis in rats.

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35

Gowda, B. Thimme, Jozef Kožíšek, Miroslav Tokarčík, and Hartmut Fuess. "N-(2-Methylphenyl)acetamide." Acta Crystallographica Section E Structure Reports Online 63, no. 4 (March 30, 2007): o1977—o1978. http://dx.doi.org/10.1107/s1600536807012998.

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36

Gowda, B. Thimme, Sabine Foro, and Hartmut Fuess. "N-(3,5-Dichlorophenyl)acetamide." Acta Crystallographica Section E Structure Reports Online 63, no. 5 (April 13, 2007): o2341—o2342. http://dx.doi.org/10.1107/s1600536807015280.

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37

Gowda, B. Thimme, Sabine Foro, Hiromitsu Terao, and Hartmut Fuess. "N-(2,3-Dimethylphenyl)acetamide." Acta Crystallographica Section E Structure Reports Online 65, no. 5 (April 8, 2009): o964. http://dx.doi.org/10.1107/s1600536809011891.

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38

Zhang, Min, Ran-Zhe Lu, Lu-Na Han, Wen-Bin Wei, and Hai-Bo Wang. "N-(4-Isopropoxyphenyl)acetamide." Acta Crystallographica Section E Structure Reports Online 65, no. 5 (April 10, 2009): o1017. http://dx.doi.org/10.1107/s1600536809012665.

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39

Gowda, B. Thimme, Sabine Foro, Hiromitsu Terao, and Hartmut Fuess. "N-(3-Bromophenyl)acetamide." Acta Crystallographica Section E Structure Reports Online 65, no. 5 (April 18, 2009): o1039. http://dx.doi.org/10.1107/s1600536809013294.

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40

Gowda, B. Thimme, Ingrid Svoboda, and Hartmut Fuess. "N-(2-Chlorophenyl)acetamide." Acta Crystallographica Section E Structure Reports Online 63, no. 7 (June 20, 2007): o3267. http://dx.doi.org/10.1107/s1600536807028991.

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41

Gowda, B. Thimme, Ingrid Svoboda, and Hartmut Fuess. "N-(2,4-Dichlorophenyl)acetamide." Acta Crystallographica Section E Structure Reports Online 63, no. 7 (June 27, 2007): o3308. http://dx.doi.org/10.1107/s1600536807030292.

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42

Gowda, B. Thimme, Sabine Foro, and Hartmut Fuess. "N-(2,5-Dichlorophenyl)acetamide." Acta Crystallographica Section E Structure Reports Online 63, no. 9 (August 8, 2007): o3709. http://dx.doi.org/10.1107/s1600536807037178.

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43

Wang, Bo, Yun Chai, Peizhen Tao, and Mingliang Liu. "N-(4-Hydroxyphenethyl)acetamide." Acta Crystallographica Section E Structure Reports Online 65, no. 8 (July 8, 2009): o1789. http://dx.doi.org/10.1107/s1600536809025409.

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44

Shakuntala, K., Sabine Foro, and B. Thimme Gowda. "N-(2-Chlorophenylsulfonyl)acetamide." Acta Crystallographica Section E Structure Reports Online 67, no. 5 (April 13, 2011): o1097. http://dx.doi.org/10.1107/s1600536811012785.

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45

Shakuntala, K., Sabine Foro, and B. Thimme Gowda. "N-(2-Methylphenylsulfonyl)acetamide." Acta Crystallographica Section E Structure Reports Online 67, no. 5 (April 22, 2011): o1188. http://dx.doi.org/10.1107/s1600536811014218.

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46

Ronaldson, Vicki, John M. D. Storey, and William T. A. Harrison. "N-(2-Bromophenyl)acetamide." Acta Crystallographica Section E Structure Reports Online 61, no. 10 (September 7, 2005): o3156—o3158. http://dx.doi.org/10.1107/s1600536805027492.

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47

Hansen, Lars Kr, German L. Perlovich, and Annette Bauer-Brandl. "N-(3-Hydroxyphenyl)acetamide." Acta Crystallographica Section E Structure Reports Online 62, no. 9 (August 2, 2006): o3627—o3628. http://dx.doi.org/10.1107/s1600536806025785.

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48

Mizoguchi, J. I., M. Takayuki, and S. Kashino. "N-(1-Adamantyl)acetamide." Acta Crystallographica Section C Crystal Structure Communications 53, no. 11 (November 15, 1997): IUC9700024. http://dx.doi.org/10.1107/s0108270197099319.

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49

Asiri, Abdullah M., Hassan M. Faidallah, Tariq R. Sobahi, Seik Weng Ng, and Edward R. T. Tiekink. "N-(4-Sulfamoylphenyl)acetamide." Acta Crystallographica Section E Structure Reports Online 68, no. 4 (March 24, 2012): o1155. http://dx.doi.org/10.1107/s1600536812011701.

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In the title compound, C8H10N2O3S, the dihedral angle between the acetamide group and the benzene ring is 15.59 (12)° and the amino group is close to being perpendicular to the benzene ring [N—S—Car—Car(ar = aromatic) torsion angle = 109.4 (2)°]. In the crystal, molecules are linked into supramolecular tubes parallel to [001] by amine–amide N—H...O interactions and these are connected into the three-dimensional architecture by amide–sulfonamide N—H...O hydrogen bonds. The crystal studied was a racemic twin.

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50

Slater, Heather L., Hanna Rozynski, Guy Crundwell, and Neil M. Glagovich. "N-(2-Acetylphenyl)acetamide." Acta Crystallographica Section E Structure Reports Online 62, no. 5 (April 21, 2006): o1957—o1958. http://dx.doi.org/10.1107/s1600536806013560.

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The title compound, C10H11NO2, was synthesized from 2′-aminoacetophenone in acetic anhydride. In the molecular structure, an intramolecular N—H...O hydrogen bond [H...O = 1.893 (18) Å] appears to affect the overall planar conformation of the molecule.

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