Relevant bibliographies by topics / 6-azabicyclo[3.2.0]heptane

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  1. Journal articles
  2. Dissertations / Theses
  3. Book chapters

Academic literature on the topic '6-azabicyclo[3.2.0]heptane'

Author: Grafiati
Published: 4 June 2021
Last updated: 2 February 2022

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Journal articles on the topic "6-azabicyclo[3.2.0]heptane"

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Butcher, Ray J., Yousef M. Hijji, and Ellis Benjamin. "cis-3-Azabicyclo[3.2.0]heptane-2,4-dione." Acta Crystallographica Section E Structure Reports Online 62, no. 4 (March 8, 2006): o1266—o1268. http://dx.doi.org/10.1107/s1600536806006933.

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The title compound, C6H7NO2, was synthesized from cis-1,2-cyclobutanedicarboxylic anhydride by reaction with ammonium acetate under microwave conditions. The crystal structure of the compound shows that the cyclobutane ring is planar with angles ranging from 89.64 (12) to 90.37 (12)°. The cis-3-azabicyclo[3.2.0]heptane-2,4-dione molecules are linked into a chain formation through hydrogen N—H...O=C bonds. Parallel packing is seen between two cyclobutane rings related by inversion symmetry.
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Usman, Anwar, Ibrahim Abdul Razak, Hoong-Kun Fun, Suchada Chantrapromma, Bao-Guo Zhao, and Jian-Hua Xu. "1,5-Dichloro-3,6,6-triphenyl-3-azabicyclo[3.2.0]heptane-2,4-dione." Acta Crystallographica Section E Structure Reports Online 57, no. 8 (July 27, 2001): o792—o793. http://dx.doi.org/10.1107/s1600536801012673.

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Hijji, Yousef M., Ellis Benjamin, Earl Benjamin, Ray J. Butcher, and Jerry P. Jasinski. "3-(2,6-Dioxopiperidin-3-yl)-3-azabicyclo[3.2.0]heptane-2,4-dione." Acta Crystallographica Section E Structure Reports Online 65, no. 2 (January 28, 2009): o394—o395. http://dx.doi.org/10.1107/s1600536809002839.

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Saouane, Sofiane, Gernot Buth, and Francesca P. A. Fabbiani. "Crystal structure and packing energy calculations of (+)-6-aminopenicillanic acid." Acta Crystallographica Section C Crystal Structure Communications 69, no. 11 (October 24, 2013): 1238–42. http://dx.doi.org/10.1107/s0108270113025924.

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The X-ray single-crystal structure of (2S,5R,6R)-6-amino-3,3-dimethyl-7-oxo-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylic acid, commonly known as (+)-6-aminopenicillanic acid (C8H12N2O3S) and a precursor of a variety of semi-synthetic penicillins, has been determined from synchrotron data at 150 K. The structure represents an ordered zwitterion and the crystals are nonmerohedrally twinned. The crystal structure is composed of a three-dimensional network built by three charge-assisted hydrogen bonds between the ammonium and carboxylate groups. The complementary analysis of the crystal packing by thePIXELmethod brings to light the nature and ranking of the energetically most stabilizing intermolecular interaction energies. In accordance with the zwitterionic nature of the structure,PIXELlattice energy calculations confirm the predominance of the Coulombic term (−379.1 kJ mol−1) ahead of the polarization (−141.4 kJ mol−1), dispersion (−133.7 kJ mol−1) and repulsion (266.3 kJ mol−1) contributions.
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Reck, G., J. Ječný, K. Huml, and J. Symerský. "Structure of 6-azabicyclo[3.2.0]heptan-7-one." Acta Crystallographica Section C Crystal Structure Communications 46, no. 4 (April 15, 1990): 720–22. http://dx.doi.org/10.1107/s0108270189011832.

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Ji, Jianguo, William H. Bunnelle, Tao Li, Jennifer M. Pace, Michael R. Schrimpf, Kevin B. Sippy, David J. Anderson, and Michael D. Meyer. "Discovery of fused azetidines as novel selective α4β2 neuronal nicotinic receptor (NNR) agonists." Pure and Applied Chemistry 77, no. 12 (January 1, 2005): 2041–45. http://dx.doi.org/10.1351/pac200577122041.

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An efficient synthesis of (1R,5S)-6-(5-cyano-3-pyridinyl)-3,6-diaza-bicyclo[3.2.0]heptane A-366833, a novel potent selective neuronal nicotinic receptor (NNR) agonist, is described. The enantiomerically pure pharmacophore benzyl (1S,5S)-3,6-diaza-bicyclo[3.2.0]heptane-3-carbamate was successfully constructed from benzyl N-allyl-N-(2-hydroxyimino-ethyl)-carbamate through a convenient approach including an intramolecular [1,3]-dipolar cycloaddition, reductive ring-opening reaction, chiral resolution, and intramolecular cyclization. Subsequent N-arylation of the pharmacophore with 3-bromo-5-cyanopyridine and N-Cbz deprotection with trifluoroacetic acid furnished A-366833.
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Homon, Anton A., Oleksandr V. Hryshchuk, Serhii Trofymchuk, Oleg Michurin, Yuliya Kuchkovska, Dmytro S. Radchenko, and Oleksandr O. Grygorenko. "Synthesis of 3-Azabicyclo[3.2.0]heptane-Derived Building Blocks via [3+2] Cycloaddition." European Journal of Organic Chemistry 2018, no. 40 (October 1, 2018): 5596–604. http://dx.doi.org/10.1002/ejoc.201800972.

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Reinart-Okugbeni, Reet, Kerti Ausmees, Kadri Kriis, Franz Werner, Ago Rinken, and Tõnis Kanger. "Chemoenzymatic synthesis and evaluation of 3-azabicyclo[3.2.0]heptane derivatives as dopaminergic ligands." European Journal of Medicinal Chemistry 55 (September 2012): 255–61. http://dx.doi.org/10.1016/j.ejmech.2012.07.025.

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9

Glass, Timothy E., and Phyllis A. Leber. "The thermal rearrangement of 6-methyl-6-vinylbicyclo)[3.2.0]heptane." Tetrahedron Letters 31, no. 8 (January 1990): 1085–88. http://dx.doi.org/10.1016/s0040-4039(00)88732-8.

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Steiner, Gerd, Rainer Munschauer, Gerhard Klebe, and Lorenz Siggel. "Diastereoselective Synthesis of Exo-6-aryl-3-azabicyclo[3.2.0]heptane Derivatives by Intramolecular [2+2]Photocycloadditions of Diallylic Amines." HETEROCYCLES 40, no. 1 (1995): 319. http://dx.doi.org/10.3987/com-94-s34.

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Dissertations / Theses on the topic "6-azabicyclo[3.2.0]heptane"

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Hensienne, Raphaël. "Nouvelles classes d’iminosucres bicycliques : approche synthétique des squelettes 5-azaspiro[3.4]octane et 6-azabicyclo[3.2.0]heptane." Thesis, Strasbourg, 2016. http://www.theses.fr/2016STRAF049/document.

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Des études antérieures conduites par notre groupe ont permis d’identifier l’α-1-C-nonyl-1,5-didésoxy-1,5-imino-D-xylitol en tant que puissant inhibiteur de la β-glucocérébrosidase – enzyme impliquée dans la maladie de Gaucher. La conformation inhabituelle (chaise inversée) de ce composé nous a incités à étudier plus avant la relation entre conformation et activité biologique des iminosucres. L’objectif de ces travaux de thèse consistait ainsi en la synthèse d’analogues conformationnellement contraints d’iminosucres. Dans un premier temps, trois spiro-iminosucres basés sur un squelette 5-azaspiro[3.4]octane ont été obtenus via une séquence comportant trois étapes clés : formation du cyclobutane par cyclisation radicalaire, introduction de l’azote par C-H amination et formation de la pyrrolidine par métathèse. Dans un second temps, une séquence a été développée pour la synthèse stéréodivergente d’iminosucres bicycliques accolés basés sur un squelette 6-azabicyclo[3.2.0]heptane via l’enchaînement de deux étapes clés : formation de la structure azabicyclique par aldolisation de type Mukaiyama puis oxydation de la cétone résultante en énone
Previous studies performed by our group led to the identification of α-1-C-nonyl-1,5-dideoxy-1,5-imino-D-xylitol as a powerful inhibitor of β-glucocerebrosidase, the enzyme involved in Gaucher disease. This compound’s unusual (inverted chair) conformation prompted us to further study the relationship between iminosugars’ conformation and biological activity. The aim of this PhD work was thus the synthesis of conformationally restricted iminosugar analogues. Firstly, three spiro-iminosugars based on a 5-azaspiro[3.4]octane scaffold were synthesized through a sequence including three key steps: cyclobutane formation by way of radical cyclisation, nitrogen introduction by mean of C-H amination and pyrrolidine formation by way ofmetathesis. Secondly, we developed a sequence dedicated to the stereodivergent synthesis of fused bicyclic iminosugars based on a 6-azabicyclo[3.2.0]heptane scaffold through a succession of two key steps: azabicyclic scaffold formation by mean of Mukaiyama aldol reaction followed by ketone to enone oxidation
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Book chapters on the topic "6-azabicyclo[3.2.0]heptane"

1

Surman, M. D., and R. H. Hutchings. "From 2-Azabicyclo[3.2.0]heptane-3,4-diones." In Six-Membered Hetarenes with Two Unlike or More than Two Heteroatoms and Fully Unsaturated Larger-Ring Heterocycles, 1. Georg Thieme Verlag KG, 2004. http://dx.doi.org/10.1055/sos-sd-017-01190.

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"7-Oxa-2-thiabicyclo[3.2.0]hept-3-ene to 6-Oxa-2,4-diazabicyclo[3.2.0]heptane." In Substance Index, edited by Backes, Fröhlich, and Padeken. Stuttgart: Georg Thieme Verlag, 2000. http://dx.doi.org/10.1055/b-0035-114008.

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Surman, M. D., and R. H. Hutchings. "Base-Induced Rearrangement of 4-Tolyl 1,3,4,5-Tetraphenyl-6-azabicyclo[3.2.0]hept-3-ene-6-sulfonate." In Six-Membered Hetarenes with Two Unlike or More than Two Heteroatoms and Fully Unsaturated Larger-Ring Heterocycles, 1. Georg Thieme Verlag KG, 2004. http://dx.doi.org/10.1055/sos-sd-017-01186.

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Block, E. "Conversion of 2,3-Dihydrothiophenes into 6-Oxo-2-thiabicyclo[3.2.0]heptane-4-carboxylic Acids." In Ene-X Compounds (X=S, Se, Te, N, P), 1. Georg Thieme Verlag KG, 2007. http://dx.doi.org/10.1055/sos-sd-033-00267.

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