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Thematische Bibliographien / Cyclometallates

Inhaltsverzeichnis

Zeitschriftenartikel
Dissertationen
Bücher
Buchteile
Konferenzberichte
Berichte der Organisationen

Auswahl der wissenschaftlichen Literatur zum Thema „Cyclometallates“

Autor: Grafiati

Veröffentlicht am 18. Mai 2024

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Zeitschriftenartikel zum Thema "Cyclometallates"

1

Tan, Gui Ping, Hong Bo Fan und Wai Yeung Wong. „Synthesis and Photophysical Properties of Charged Iridium(III) Cyclometallates Based on Hole-Transporting Carbazole Unit“. Applied Mechanics and Materials 633-634 (September 2014): 314–19. http://dx.doi.org/10.4028/www.scientific.net/amm.633-634.314.

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Four novel charged Ir (III) cyclometallates based on 9-phenylcarbazole unit have been developed. By attaching isoquinoline or 5-trifluoromethylpyridine group, the light-emitting properties of the resulting Ir (III) cyclometallates have been improved. Meanwhile, 1,10-phenanthroline or 4,4′-dimethyl-2,2′-bipyridine has been utilized to modify the thermal stability. The four Ir (III) cyclometallates emit yellow light with the highest photoluminescence quantum yields (ΦP) of 0.32 (C4), which is only less than that of the state-of-art complexfac-tris (2-phenylpyridine) iridium (III) [fac-Ir (ppy)3], which showsΦPof 0.40 under the same condition. This inspiring result reveals that the bulky character of CF3group enhances the performance of reported charged Ir (III) cyclometallates and makes them to be potential phosphors in OLED applications.

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2

Téllez, Juan, Albert Gallen, Joaquina Ferrer, Fernando J. Lahoz, Pilar García-Orduña, Antoni Riera, Xavier Verdaguer, Daniel Carmona und Arnald Grabulosa. „Half-sandwich complexes of Ir(iii), Rh(iii) and Ru(ii) with the MaxPhos ligand: metal centred chirality and cyclometallation“. Dalton Transactions 46, Nr. 45 (2017): 15865–74. http://dx.doi.org/10.1039/c7dt03327c.

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3

Tan, Guiping, Shuming Chen, Chi-Ho Siu, Adam Langlois, Yongfu Qiu, Hongbo Fan, Cheuk-Lam Ho et al. „Platinum(ii) cyclometallates featuring broad emission bands and their applications in color-tunable OLEDs and high color-rendering WOLEDs“. Journal of Materials Chemistry C 4, Nr. 25 (2016): 6016–26. http://dx.doi.org/10.1039/c6tc01594h.

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Two new phosphorescent platinum(ii) cyclometallates with flexible phenoxy moieties were prepared whose broad excimeric emissive states in the solid state allow the fabrication of high color-rendering two-emitter WOLEDs.

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4

Chakladar, Sukla, Parimal Paul und Kamalaksha Nag. „Organodipalladium(II) cyclometallates of the schiff base N,N′-diethyl-2,6-dialdiminobenzene“. Polyhedron 10, Nr. 13 (Januar 1991): 1513–19. http://dx.doi.org/10.1016/s0277-5387(00)86074-x.

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5

Barucki, Hubert, Simon J. Coles, James F. Costello und Michael B. Hursthouse. „Synthesis and structure of organoantimony (V) cyclometallates: transannular interactions and the barrier to cyclisation“. Journal of Organometallic Chemistry 622, Nr. 1-2 (März 2001): 265–73. http://dx.doi.org/10.1016/s0022-328x(00)00923-2.

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6

lal Pratihar, Jahar, Debprasad Patra und Surajit Chattopadhyay. „Syntheses, characterization, structure and redox properties of new Rh(III) cyclometallates incorporating azoimine ligands“. Journal of Organometallic Chemistry 690, Nr. 21-22 (November 2005): 4816–21. http://dx.doi.org/10.1016/j.jorganchem.2005.07.076.

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7

Nagaraju, Koppanathi, und Samudranil Pal. „Ruthenium(III) cyclometallates: Regioselective metallation of 1-pyrenyl in 1-pyrenaldehyde 4-R-benzoylhydrazones“. Journal of Organometallic Chemistry 737 (August 2013): 7–11. http://dx.doi.org/10.1016/j.jorganchem.2013.03.040.

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8

Babu, G. Narendra, und Samudranil Pal. „Mono- and dinuclear palladium(II) cyclometallates with 4-R-N'-(mesitylidene)benzohydrazides and mono- and diphosphines“. Journal of Organometallic Chemistry 805 (März 2016): 19–26. http://dx.doi.org/10.1016/j.jorganchem.2016.01.003.

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9

Narayan Biswas, Achintesh, Purak Das, Sandip Sengupta, Amitava Choudhury und Pinaki Bandyopadhyay. „C(naphthyl)–H bond activation by rhodium: isolation, characterization and TD-DFT study of the cyclometallates“. RSC Advances 1, Nr. 7 (2011): 1279. http://dx.doi.org/10.1039/c1ra00572c.

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10

Chattopadhyay, Surajit, Chittaranjan Sinha, Partha Basu und Animesh Chakravorty. „Chemistry of platinum(IV), platinum(II) and palladium(II) cyclometallates of benzylthio- or benzosulphinyl-substituted azobenzenes“. Journal of Organometallic Chemistry 414, Nr. 3 (August 1991): 421–31. http://dx.doi.org/10.1016/0022-328x(91)86340-v.

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Dissertationen zum Thema "Cyclometallates"

1

Chhetri, Satyadeep Singh. „C (Aryl) - H bond activation : isolation, characterization and reactivity of cyclometallates“. Thesis, University of North Bengal, 2012. http://hdl.handle.net/123456789/1471.

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Tan, Guiping. „Synthesis of new iridium (iii) and platinum (ii) cyclometallates and theiir application in high-efficiency organic light-emitting devices“. HKBU Institutional Repository, 2012. https://repository.hkbu.edu.hk/etd_ra/1418.

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Neogi, Debatra Narayan. „Cyclometallated compounds: synthesis, characterization and reactivity“. Thesis, University of North Bengal, 2005. http://hdl.handle.net/123456789/746.

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Slater, Jonathan. „Cyclometallated nitrogen heterocycles - metallomesogens“. Thesis, University of Warwick, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.269196.

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5

de, Geest Duncan J. „Synthesis and study of new cyclometallated complexes“. Thesis, University of Canterbury. Chemistry, 1998. http://hdl.handle.net/10092/8523.

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Twenty-nine heteroaromatic ligands, which are potentially capable of forming cyclometallated complexes, have been reacted with palladium and rhodium salts. In addition to a number of mono-cyclometallated complexes, two doubly cyclopalladated complexes have been prepared, as have a number of coordination complexes. Specifically, a number of phenoxy- and phenylthio-substituted pyridines and diazines, four of which could potentially be doubly cyclometallated, have been synthesised, and their coordination and cyclopalladation chemistry investigated. The previously reported reactions of 2-benzoylpyridine with rhodium trichloride trihydrate have been revisited, and are discussed in relation to the formation and characterisation of a novel cyclorhodated complex of the ligand. The syntheses-via homo-coupling reactions of aryl halide precursors - and cyclopalladations of two structural analogues of 2,2':4',4":2",2"'-quaterpyridine are also described. All of the soluble complexes and ligands have been fully characterised by ¹H and ¹³C NMR, using combinations of various one- and two-dimensional NMR techniques. The trends in the coordination induced shifts, observed for the NMR spectra of a series of cyclopalladated acetylacetonate complexes and the corresponding free ligands, are discussed, as are those for a related series of octahedral cyclorhodated complexes. Other methods, including IR spectroscopy, mass spectrometry and elemental analysis, have been used to characterise the prepared complexes. In addition, the characterisation of three cyclometallated complexes and four coordination complexes, by single crystal X-ray structure determination, is described.

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6

Singh, Shalini. „Luminescent cyclometallated Ir(III) complexes : synthesis, characterisation and applications“. Thesis, University of Leicester, 2011. http://hdl.handle.net/2381/9067.

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A range of luminescent Ir(III) complexes [Ir(C^N)2(X^Y)]n+ (n = 0, 1) containing different cyclometallated (C^N) and ancillary (X^Y) ligands has been synthesised. All new compounds were fully characterised by 1H and 13C NMR spectroscopy, mass spectrometry and elemental analyses and several compounds have been structurally characterised by X-ray crystallography. The photophysical and electrochemical properties of the complexes were also studied. Chapter one provides an introduction to luminescent transition metal complexes, in particular Ru(II) and Ir(III) complexes and gives an overview of the factors controlling the emission wavelengths of cyclometallated Ir(III) complexes and their applications, particularly as biological labels and probes. Chapter two discusses the synthesis and properties of [Ir(C^N)2(bipy)]+ and shows that substituents para to the metal on the cyclometallated phenyl have a significant effect on the emission wavelength. Chapter three describes complexes [Ir(C^N)2(X^Y)]n+ (n = 1, X^Y = pyridine imine; n = 0, X^Y = pyrrolylimine) and the effect of substituents on the redox properties and emission wavelength. Some of these complexes have been employed in live-cell imaging. In Chapter four the synthesis, characterisation and application of [Ir(C^N)2(phencat-OH)]+ complexes as molybdate sensors is discussed. Chapter five describes the synthesis of [Ir(C^N)2(X^Y)]n+ (n = 0, 1) containing a homochiral X^Y ligand i.e. (S)-soxH, (S)-pepH, (S)-phglyH, (+)-tfacH and (S)-ppea. The complexes are all formed as 1:1 mixtures of diastereomers with Δ or Λ chirality at the metal. Diastereomers containing the (S)-sox and (S)-pep ligands can often be separated via crystallisation or column chromatography. Treatment of a single diastereomer (ΛS or ΔS) with an appropriate acid removes the sox or pep ligand hence provides a route to complexes with only metal-centred chirality, for example Λ- and Δ-[Ir(ppz)2(bipy)]+.

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7

Crosby, Sarah H. „Cyclometallated complexes of platinum : C-H activation, oxidation and reduction“. Thesis, University of Warwick, 2011. http://wrap.warwick.ac.uk/55449/.

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Within this thesis, research related to the synthesis of Pt(II) and Pt(IV) cyclometallated complexes involving both aryl and alkyl C-H activation is discussed. The introduction reviews literature relevant to C-H activation, cyclometallation and reductive elimination, both historic and current. Four pyridine based pro-ligands, all with a 4-fluorophenyl substituent and a varying alkyl substituent, were synthesised in order to study both aryl and alkyl C-H activation. Initial reactions with K2PtCl4 led to the cyclometallation of the phenyl ring via a reversible aryl C-H activation, which then resulted in a variety of Pt(II) complexes by the addition of different co-ligands. Oxidation of these Pt(II) species gave Pt(IV) complexes, which subsequently underwent isomerisation to give the thermodynamic product. For the DMSO derivatives this was shown to occur via five coordinate complexes stabilised by agostic interactions with the alkyl chain and resulted in the first crystallographically characterised oxygen bound DMSO Pt(IV) complexes. Pt(II) and Pt(IV) sp2 cyclometallated complexes, each with an sp3 agostic interaction, were isolated and characterised when using the more sterically demanding tbutyl derivative of the pro-ligand. Subsequent alkyl C-H activation of the tbutyl group was observed via an intra-molecular transcyclometallation reaction to give complexes with an sp3 cyclometallation. From these species a series of complexes with a C(sp2)^N^C(sp3) tridentate ligand were also synthesised. It was also noted that a reversible rollover reaction of the Pt(II) agostic complex occurred in DMSO solvent by exchanging the C(sp2)^N cyclometallation for a C(sp2)^C(sp2) cyclometallation via decyclometallation, rotation about the central C-C bond and subsequent C-H activation. Reductive elimination of a chloride ligand with both sp2 and sp3 cyclometallated carbons occurred to give functionalised phenyl rings and tbutyl groups, respectively. Steric interactions were shown to play a major role in these reactions.

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8

Al-Duaij, Omar Khalid. „Synthesis and reactivity of cyclometallated complexes containing nitrogen donor ligands“. Thesis, University of Leicester, 2005. http://hdl.handle.net/2381/30095.

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This thesis describes the synthesis and reactivity of cyclometallated complexes containing nitrogen donor ligands.;Chapter One introduces the general chemistry of cyclometallated complexes containing C,N-bidentate ligands, then describes the mechanism of cyclometallated complexes. This is followed by an overview of the applications of cyclometallated complexes.;Chapter Two provides an introduction to hemilability and reviews the synthesis of cyclopalladated complexes containing C,N,X tridentate ligands (X= N, S, O). The synthesis of new cyclopalladated imines containing oxygen-functionalised tethers is described. Coordination of the oxygen is shown to depend on i) the nature of the oxygen donor, ether, alcohol or phenol. ii) the length of the linker. iii) whether the complexes are neutral or cationic.;Chapter Three establishes the scope of acetate-assisted C-H activation for the synthesis of arene ruthenium and Cp*M (M = Ir, Rh) half-sandwich cyclometallated complexes with nitrogen-donor ligands viz. imine, amine, oxadoline and pyridine and with P(OPh)3. The method can activate sp2 C-H bonds of phenyl, pyrrole and thiophene, and one example of an sp3 C-H bond. The method also allows N-H activation of a pyrrole-imine. Preliminary investigations of the mechanism are also described.;Chapter Four reports the reactivity of the cyclometallated half-sandwich complexes (synthesised in chapter three). Alkenes and CO provide simple substitution products. Alkynes are shown to insert regioselectivity into the M-C bond. In some cases subsequent C-C or C-N bond formation occurs to form carbocyclic or heterocyclic products. With PhC-CH, insertion of two molecules can occur to give novel products. Throughout the thesis X-ray crystallography has been used to verify or identify some of the products (>40 structures).

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9

Zaarour, Moussa. „Luminescent and NLO active tris- and bis-cyclometallated iridium complexes“. Rennes 1, 2012. http://www.theses.fr/2012REN1S110.

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New series of substituted Ir(ppy)3 derivatives incorporating various vinyl-aryl systems with electron-donating groups on their pyridyl rings or donor/acceptor groups on their phenyl rings were synthesized using the so-called technique “chemistry on the complex”. These complexes are luminescent with emission wavelength that is tuned by introducing stronger donating groups or extending the π-system. These complexes present strong NLO properties controlled by the charge transfer transitions (ILCT and MLCT) induced by donor-acceptor interaction within the complex. We have developed the first example of palladium-catalyzed direct arylation of metallated thiophenes. The arylated derivatives of tris-cyclometallated Ir(thpy)3 and thienyl containing bis-cyclometalated complexes were prepared. The latter were arylated at their thienyl ring located either on the cyclometallated ligand of Ir(thpy)2(acac) and Ir(tbth)2(acac) or on the ancillary ligand of Ir(ppy)2(tta). The resulting complexes present interesting luminescence properties originating from LC 3(π-π*) for complexes with thienyl ring on their C^N ligands while Ir(ppy)2(tta) derivatives emit from excited state based on the ancillary ligand. Preliminary results of the synthesis of iridium platinum tetrametallated complexes Ir-Pt3 were reported. A complex having Ir(ppy)3 core and three (N^N^C)Pt-acetylide fragments was prepared. At room temperature, it shows an emission originating from the platinum fragments. Attempts were made to prepare a more rigid Ir-Pt3 complex based on Ir(thpy)3 core and three (N^N^C)Pt fragments. The complex was successfully prepared; however, its purification was not finished
Une nouvelle série de complexes de type Ir(ppy)3 fonctionnalisés par divers vinyle-aryles substitués, soient par des groupements électro-donneurs sur la noyau pyridyle, soient par des groupements donneurs ou accepteurs sur la noyau phényle, ont été synthétisés en utilisant la technique dite de “chimie sur le complexe”. Ces complexes sont luminescents avec une longueur d'onde qui peut être déplacée en introduisant un groupement fortement donneur ou bien en allongeant le système π. Ils présentent de fortes activités en optique non linéaire quadratique qui sont contrôlées par les transitions de transfert de charge (ILCT et MLCT). Nous avons développé le premier exemple d'arylation directe de thiophènes métallés catalysée par le palladium. Les dérivés arylés des complexes Ir(thpy)3 et bis-cyclométallés ont été synthétisés. Les complexes bis-cyclométallés sont arylés au niveau du cycle thiényle situé sur le ligand cyclométallés de Ir(thpy)2(acac) et Ir(tbth)2(acac), ou sur le ligand ancillaire de Ir(ppy)2(tta). Les complexes qui en résultent sont luminescents provenant d’un état excité émissif LC 3(π-π*) pour les complexes avec le thiényle sur les ligands C^N, tandis que les dérivés Ir(ppy)2(tta) émettent à partir de l'état excité centré sur les ligands ancillaires. Les résultats préliminaires sur la synthèse de complexes tétramétallés Ir-Pt3 sont également décrits. Un complexe ayant un cœur Ir(ppy)3 et trois fragments (N^N^C)Pt-acétylure liés a ainsi été préparé. Ce complexe montre une émission provenant des entités platine. Les premiers essais concernant la synthèse d’un complexe plus rigide basé sur un cœur Ir(thpy)3 et trois fragments (N^N^C)Pt sont également décrits

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Contaldi, Simone <1982&gt. „Synthesis and Structures of palladium(II) and platinum(II) complexes containing cyclometallated 2-thienylpyridines“. Doctoral thesis, Alma Mater Studiorum - Università di Bologna, 2010. http://amsdottorato.unibo.it/2727/1/contaldi_simone_tesi.pdf.

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Bücher zum Thema "Cyclometallates"

1

Beers, Olaf Cornelis Petrus. The coordination and activation of (cyclometallated) monoazadienes in mono- and heteronuclear metal carbonyl complexes. [Amsterdam]: Universiteit van Amsterdam, 1992.

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Buchteile zum Thema "Cyclometallates"

1

Jastrzebski, Johann T. B. H., Gerard Van Koten, M. F. Lappert, P. C. Blake und D. R. Hankey. „Cyclometallated Organolithium Compounds“. In Inorganic Syntheses, 150–55. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132579.ch27.

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2

Maestri, Mauro, Vincenzo Balzani, Christine Deuschel-Cornioley und Alex Von Zelewsky. „Photochemistry and Luminescence of Cyclometallated Complexes“. In Advances in Photochemistry, 1–68. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470133484.ch1.

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3

Pardasani, R. T., und P. Pardasani. „Magnetic properties of ruthenium(III) cyclometallated complex with Schiff-base ligand“. In Magnetic Properties of Paramagnetic Compounds, 579–80. Berlin, Heidelberg: Springer Berlin Heidelberg, 2017. http://dx.doi.org/10.1007/978-3-662-54231-6_313.

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Housecroft, Catherine E., und Edwin C. Constable. „Development of Cyclometallated Iridium(III) Complexes for Light-Emitting Electrochemical Cells“. In Light-Emitting Electrochemical Cells, 167–202. Cham: Springer International Publishing, 2017. http://dx.doi.org/10.1007/978-3-319-58613-7_7.

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5

Bennett, M. A., J. L. Latten, L. J. Ayers und D. L. Thorn. „An Iridium(III) Complex Containing Cyclometallated Triphenylphosphine Formed by Isomerization of an Iridium(I) Triphenylphosphine Complex“. In Inorganic Syntheses, 200–203. Hoboken, NJ, USA: John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470132579.ch35.

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6

Henderson, William. „The Chemistry of Cyclometallated Gold(III) Complexes with C,N-Donor Ligands“. In Advances in Organometallic Chemistry, 207–65. Elsevier, 2006. http://dx.doi.org/10.1016/s0065-3055(05)54005-x.

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Spencer, John, und Michel Pfeffer. „State of the art in selective hetero-and carbocyclic syntheses mediated by cyclometallated complexes“. In Advances in Metal-Organic Chemistry, 103–44. Elsevier, 1998. http://dx.doi.org/10.1016/s1045-0688(98)80005-1.

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Konferenzberichte zum Thema "Cyclometallates"

1

Rúa-Sueiro, Marcos, Paula Munin-Cruz, Francisco Reigosa, José M. Vila, M. Teresa Pereira und Juan M. Ortigueira. „Synthesis of mono- and dinuclear cyclometallated compounds with palladium and platinum“. In The 24th International Electronic Conference on Synthetic Organic Chemistry. Basel, Switzerland: MDPI, 2020. http://dx.doi.org/10.3390/ecsoc-24-08299.

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Fillaut, Jean-Luc, Pierre-Henri Lanoe, Veronique Guerchais, Hubert Le Bozec und J. A. Gareth Williams. „Engineering of cyclometallated platinum(II) complexes incorporating acetylide ligands for chemosensing“. In 2009 3rd ICTON Mediterranean Winter Conference (ICTON-MW 2009). IEEE, 2009. http://dx.doi.org/10.1109/ictonmw.2009.5385644.

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Rúa Sueiro, Marcos, Paula Munin-Cruz, Juan M. Ortigueira und José M. Vila. „X-Ray diffraction study of fluorine-functionalized thiosemicarbazones and cyclometallated compounds.“ In The 3rd International Online Conference on Crystals. Basel, Switzerland: MDPI, 2022. http://dx.doi.org/10.3390/iocc_2022-12140.

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Rúa Sueiro, Marcos, Paula Munin-Cruz, Juan M. Ortigueira und José M. Vila. „X-Ray diffraction study of fluorine-functionalized thiosemicarbazones and cyclometallated compounds.“ In The 3rd International Online Conference on Crystals. Basel, Switzerland: MDPI, 2022. http://dx.doi.org/10.3390/iocc_2022-12140.

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Rúa-Sueiro, Marcos, Paula Munín-Cruz, Sara Bermúdez-Fernández und José M. Vila. „Palladium Cyclometallated Compounds: Evaluation of Their Catalytic Activity in Cross-Coupling Reactions“. In ECCS 2021. Basel Switzerland: MDPI, 2022. http://dx.doi.org/10.3390/eccs2021-11034.

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Berichte der Organisationen zum Thema "Cyclometallates"

1

Watts, R. J. Cyclometallated and cyclometalsilylated complexes of transition elements as photoredox sensitizers. Office of Scientific and Technical Information (OSTI), Januar 1992. http://dx.doi.org/10.2172/6923703.

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Watts, R. J. Cyclometallated and cyclometalsilylated complexes of transition elements as photoredox sensitizers. Office of Scientific and Technical Information (OSTI), Januar 1992. http://dx.doi.org/10.2172/5396788.

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Watts, R. J. Cyclometallated and cyclometalsilylated complexes of transition elements as photoredox sensitizers. Progress report, October 1, 1991--November 31, 1992. Office of Scientific and Technical Information (OSTI), Mai 1992. http://dx.doi.org/10.2172/10138113.

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Watts, R. J. Cyclometallated and cyclometalsilylated complexes of transition elements as photoredox sensitizers. Final report, January 1, 1988--September 30, 1996. Office of Scientific and Technical Information (OSTI), Dezember 1996. http://dx.doi.org/10.2172/656625.

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Watts, R. J. Cyclometallated and cyclometalsilylated complexes of transition elements as photoredox sensitizers. Progress report for the period December 1, 1991--September 30, 1992. Office of Scientific and Technical Information (OSTI), Dezember 1992. http://dx.doi.org/10.2172/10116518.

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